CN108175463A - Microsurgery sewing system - Google Patents

Microsurgery sewing system Download PDF

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Publication number
CN108175463A
CN108175463A CN201810063459.4A CN201810063459A CN108175463A CN 108175463 A CN108175463 A CN 108175463A CN 201810063459 A CN201810063459 A CN 201810063459A CN 108175463 A CN108175463 A CN 108175463A
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CN
China
Prior art keywords
light source
microsurgery
needle
sewing
fluorescent powder
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810063459.4A
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Chinese (zh)
Inventor
唐举玉
石臻
朱文欣
刘慧�
史越
潘丁
刘睿
马彬彬
金瑞琦
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Xiangya Hospital of Central South University
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Xiangya Hospital of Central South University
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Filing date
Publication date
Application filed by Xiangya Hospital of Central South University filed Critical Xiangya Hospital of Central South University
Priority to CN201810063459.4A priority Critical patent/CN108175463A/en
Publication of CN108175463A publication Critical patent/CN108175463A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61BDIAGNOSIS; SURGERY; IDENTIFICATION
    • A61B17/00Surgical instruments, devices or methods, e.g. tourniquets
    • A61B17/04Surgical instruments, devices or methods, e.g. tourniquets for suturing wounds; Holders or packages for needles or suture materials
    • A61B17/06Needles ; Sutures; Needle-suture combinations; Holders or packages for needles or suture materials
    • A61B17/06066Needles, e.g. needle tip configurations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L31/00Materials for other surgical articles, e.g. stents, stent-grafts, shunts, surgical drapes, guide wires, materials for adhesion prevention, occluding devices, surgical gloves, tissue fixation devices
    • A61L31/08Materials for coatings
    • A61L31/082Inorganic materials
    • A61L31/088Other specific inorganic materials not covered by A61L31/084 or A61L31/086
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L31/00Materials for other surgical articles, e.g. stents, stent-grafts, shunts, surgical drapes, guide wires, materials for adhesion prevention, occluding devices, surgical gloves, tissue fixation devices
    • A61L31/14Materials characterised by their function or physical properties, e.g. injectable or lubricating compositions, shape-memory materials, surface modified materials
    • GPHYSICS
    • G02OPTICS
    • G02BOPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B21/00Microscopes
    • GPHYSICS
    • G02OPTICS
    • G02BOPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B21/00Microscopes
    • G02B21/0004Microscopes specially adapted for specific applications
    • G02B21/0012Surgical microscopes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61BDIAGNOSIS; SURGERY; IDENTIFICATION
    • A61B17/00Surgical instruments, devices or methods, e.g. tourniquets
    • A61B2017/00831Material properties

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  • Health & Medical Sciences (AREA)
  • Surgery (AREA)
  • General Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Heart & Thoracic Surgery (AREA)
  • Epidemiology (AREA)
  • Vascular Medicine (AREA)
  • Optics & Photonics (AREA)
  • General Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Engineering & Computer Science (AREA)
  • Biomedical Technology (AREA)
  • Medical Informatics (AREA)
  • Molecular Biology (AREA)
  • Surgical Instruments (AREA)

Abstract

The invention discloses a kind of microsurgery sewing systems, including microscope and sewing needle, the sewing needle is equipped with fluorescent powder sedimentary, the fluorescence excitation light source for the fluorescent powder sedimentary to be excited to shine is installed on the microscope, the illumination of the fluorescence excitation light source at least covers operation stitching region.The present invention, which has, can make sewing needle generation be clear to light, convenient for finding, so that the advantages of improving operation safety and efficiency.

Description

Microsurgery sewing system
Technical field
The present invention relates to field of medical appliances, and in particular to a kind of microsurgery sewing system.
Background technology
Micro anastomosis is often 8-0 to 11-0 models with suture specification in microsurgery operation, needle it is a diameter of 0.05mm to 0.14mm, chord length are 3 to 5mm, and arc length is 3.8mm to 6.4mm, and suture diameter is 0.015 to 0.045mm, length For 10-15cm.So tiny micro suture needlework, it is high-visible under field of microscope, it must be anti-in comparison under the naked eyes visual field It is just distinguishable under the larger solid background of difference.Under microscope magnifying state, conventional operating distance be 20-25cm, herein away from It is difficult to look for due to easily being covered by complicated surgical wound surface background from the microsurgery needlework to fall into operation visual area.
For medical worker when micro- amplification system progress micro suture is performed the operation in application, micro- amplification factor is usually on 10 times of left sides The right side also needs to be amplified to 40 times sometimes, and the field number for amplifying visual area is usually 9.5mm-20mm(0.95-2cm).Due to micro- The length of suture is usually 10-15cm, is far longer than field number, in practical operation, inevitably micro- seam Close the situation that needle leaves microscopic field.Simultaneously as it by medical worker's skilled operation degree, art area hoc scenario to be stapled, shows The influence of the factors such as microoperation instrument quality and support staff's skilled operation degree, microsurgery carry out in be difficult to avoid that meeting There is the phenomenon that " flying needle ", " bouncing pilotage " and " broken needle ".In this case, micro- suture needle, which can be unpredictably detached from, micro- holds needle Device, usual micro- suture needle can leave field of microscope, and not patient is pre-designed the orientation for placing suture needle.
In some cases, it has knotted fixed microsutures for suture tail portion, medical worker can pass through drawing Suture quickly finds suture needle.But due to the sharp keen needle of weak part, in addition micro- suture needle that the connecting portion of micro- needlework is stress Head is easily pierced into neighbouring tissue and causes resistance, and the diameter of microsutures is tiny, improperly firmly is easily allowed to be broken, leads to needle Line detaches, and the microsurgery surface of a wound is complicated, and nervus vasculairs are densely distributed, and this measure is it is possible that the tissue damage of bigger can be caused.
Therefore, deviate from the micro- visual area of micro- suture needle disengaging, especially suture tail portion with needle, the situation of " broken needle "; The situation in micro- visual area is remained secured to suture needle abjection but tail portion, in order to avoid external force drawing suture causes needlework to detach or seam Thread breakage, it is mobile restricted because microscopic field of view diameter is excessively narrow, it is impossible to be used in find micro- suture needle, need patient's naked eyes in complexity Surgical wound surface background under find micro- needlework.And requirement and working distance of microscope of the aseptic condition to sighting distance performed the operation will It asks and is more the increase in the difficulty that naked eyes seek needle.In surgical procedure, in order to find the micro- suture needle of " missing ", when can waste a large amount of Between, being delayed blood vessel and dialyneury process leads to tissue ischemia time lengthening, causes the failure entirely performed the operation;Extend patient's anesthesia Time can cause the raising of incidence of complications to even result in patient and life danger occurs.
In addition, if micro- suture needle is not found, since it is very tiny, it is difficult to be sent out by conventional B ultrasound, x-ray and CT examination It is existing.Since micro- suture needle is metal object, it can cause patient that cannot carry out magnetic resonance examination and high-intensity magnetic field ring cannot be entered Border.Micro- suture needle remains in patient body, can cause very big hidden danger to the health of patient.Suture needle is residual as non-implantable foreign matter It stays in and easily causes tissue infection in local organization, influence patient's post-operative recovery;If suture is needled into nerve or tendon, then can draw It plays patient's post-surgical sites pain, lead to the feeling for being difficult to alleviate and dyskinesia;If suture needle is pierced into thin vessels, postoperative blood can be caused Obstacle is transported, local thrombus formation is caused to lead to local organization ischemic or extravasated blood or even necrosis;If suture needle is pierced into big or middle arteriovenous, Sewing needle is easily poured big internal blood vessel by rapid blood flow, and sharp syringe needle can damage big blood vessel, cause artery dissection, The formation of the fatal diseases such as aneurysm;Suture needle reaches whole body vessel branch everywhere with the circulatory system, can lead to heart valve, big The damage of vein valve etc., causes lateral thrombus to be formed, and thrombus breaks loose can cause whole body important organ embolism threat to life.
Meanwhile for microsurgery beginner, when practicing micromanipulation due to holding needle, inserting needle, the gimmick for going out needle It is unskilled, it holds needle and overexerts, holds the reasons such as pin position mistake, needle angle, inserting needle positional fault, cause " flying needle ", " jump The probability of needle " and " broken needle " greatly increases, and beginner usually requires to waste a large amount of time and looks for needle or select new needle, causes not having Necessary time and the wasting of resources.
There are multiple and different producer's production microsurgery swaged needles both at home and abroad at present, wherein domestic microsurgery suture Needle it is cheap, although compared with foreign vendor still have a certain distance, material, finish, hardness and sharp keen degree The requirement of microsurgery can be met.However, being foreign countries or domestic microinstrument and microsurgical instrument manufacturer, all neglect It is tiny depending on micro- needlework, quick naked eyes is needed to find this actual conditions of suture needle and want in disengaging microscope visual area It asks.Meanwhile in the relevant corollary equipment of micromanipulation and instrument, in the deisgn product of domestic and international microinstrument producer, do not have Have and optimized for the situation that naked eyes is needed to find micro- suture needle, also lack the solution to the above situation.
Invention content
The technical problem to be solved by the present invention is to overcome the deficiencies in the prior art, and providing one kind can be such that sewing needle generates easily Light is seen, convenient for finding, so that improving operation safety and the microsurgery sewing system of efficiency.
In order to solve the above technical problems, the present invention uses following technical scheme:
A kind of microsurgery sewing system, including microscope and sewing needle, the sewing needle is equipped with fluorescent powder sedimentary, The fluorescence excitation light source for the fluorescent powder sedimentary to be excited to shine, the fluorescence excitation light source are installed on the microscope Illumination at least cover operation stitching region.
As a further improvement of the above technical scheme:
The fluorescent powder sedimentary is set as Ca- α-Sialon:Eu2+Yellow fluorescent powder, the fluorescence excitation light source generation wavelength For 460 nanometers of blue light.
The fluorescent powder sedimentary is coated on the outer surface of the sewing needle, and is covered at the 1/4 of sewing needle rear end.
The fluorescent powder deposit thickness is 10~20 microns.
The fluorescence excitation light source is installed on the microscopical motion arm.
The fluorescence excitation light source includes point light source and magnet, and the point light source is fixed on described by the magnet adsorption On motion arm.
The microscope is equipped with the first light source switch for opening and closing the point light source.
The fluorescence excitation light source includes array light source and connector, and the connector side is equipped with pillar, the connection Part is rotatable to be sleeved on the motion arm, and the detachable set of array light source is fixed on the pillar of the connector.
The array light source is equipped with to be switched for opening and closing the second light source of the array light source, built in the array light source Rechargeable battery.
Compared with prior art, the advantage of the invention is that:
Microsurgery sewing system of the present invention, including being equipped with the sewing needle of fluorescent powder sedimentary and being installed with fluorescent exciting The microscope in source, in surgical procedure, if micro-needle is fallen, you can generated using fluorescence excitation light source excitated fluorescent powder sedimentary Fluorescent effect, the color for generating light is the more sensitive color of naked eyes, doctor can be allowed to find sewing needle as soon as possible, avoid sewing needle It leaves, improves operation safety, saved operating time, improve procedure efficiency.
Description of the drawings
Fig. 1 is the structure diagram of microsurgery sewing system sewing needle of the present invention.
Fig. 2 is 1 microscopical structure diagram of microsurgery sewing system embodiment of the present invention.
Fig. 3 is the structure diagram of 2 fluorescence excitation light source of microsurgery sewing system embodiment of the present invention.
Fig. 4 is the structure diagram of 2 connector of microsurgery sewing system embodiment of the present invention.
Each label represents in figure:
1st, sewing needle;11st, fluorescent powder sedimentary;2nd, microscope;21st, fluorescence excitation light source;211st, point light source;2111st, the first light Source switch;212nd, array light source;2121st, second light source switchs;213rd, magnet;214th, connector;2141st, pillar;22nd, it operates Arm.
Specific embodiment
The present invention is described in further details below with reference to Figure of description and specific embodiment.
Embodiment 1:
As depicted in figs. 1 and 2, the first embodiment of microsurgery sewing system of the present invention, including microscope 2 and suture Needle 1, sewing needle 1 are equipped with fluorescent powder sedimentary 11, be installed on microscope 2 shine for excitated fluorescent powder sedimentary 11 it is glimmering Phot-luminescence source 21, the illumination of fluorescence excitation light source 21 at least cover operation stitching region.In the structure, including carrying fluorescent powder The sewing needle 1 of sedimentary 12 and the microscope 2 for being installed with fluorescence excitation light source 21, and the illumination covering hand of fluorescence excitation light source 21 Art seam area, in surgical procedure, if sewing needle 1 is fallen, you can fluorescence excitation light source 21 is made to emit light irradiation sewing needle 1 Fluorescent powder sedimentary 11 come excitated fluorescent powder sedimentary 11 generate fluorescent effect, fluorescent effect generate light color for naked eyes compared with Sensitive color and easily as it can be seen that doctor can be allowed to be found as soon as possible with the sewing needle 1 for being clear to light, avoids sewing needle 1 from being retained in trouble In person's body, operation safety is improved, has saved operating time, improves procedure efficiency.
In the present embodiment, fluorescent powder sedimentary 11 is set as Ca- α-Sialon:Eu2+Yellow fluorescent powder, fluorescence excitation light source 21 generation wavelengths are 460 nanometers of blue light.In the structure, 21 generation wavelength of fluorescence excitation light source is 460 nanometers of blue Light, this blue light can excite Ca- α-Sialon:Eu2+Yellow fluorescent powder emission peak wavelength is Huang-orange of 570-610 nm Light fluorescent effect, this wavelength are that Huang-orange light of 570-610 nm is the very sensitive color of naked eyes, are very easy to find, can be with It allows doctor is easier to find this sensitive light, and finds sewing needle 1, further improve the efficiency for finding sewing needle 1.
In the present embodiment, fluorescent powder sedimentary 11 is coated on the outer surface of sewing needle 1, and is covered in 1 rear end of sewing needle At 1/4.In the structure, fluorescent powder sedimentary 11 is coated on the outer surface of the sewing needle 1, is more advantageous to fluorescence excitation light source 21 Emit the irradiation of light, when fluorescent powder sedimentary 11 emits the irradiation of light by fluorescence excitation light source 21, the fluorescence in outer surface Powder sedimentary 11 can quickly generate fluorescent effect, since the fluorescent effect reaction of the fluorescent powder sedimentary 11 of sewing needle 1 is fast Speed, so doctor sees that the sewing needle 1 with fluorescent effect is also fast, so as to further improve the speed for finding sewing needle 1; Fluorescent powder sedimentary 11 covers the rear end 1/4 of sewing needle 1, when operation, does not interfere with the surgical procedure of doctor.
In the present embodiment, 11 thickness of fluorescent powder sedimentary is 10~20 microns.In the structure, 11 thickness of fluorescent powder sedimentary It it is 10~20 microns, the thickness of fluorescent powder sedimentary 11 within this range, is made in the light emitted excitation of fluorescence excitation light source 21 Under, more preferably fluorescent effect can be generated.
In the present embodiment, fluorescence excitation light source 21 is installed on the motion arm 22 of microscope 2.In the structure, fluorescence excitation Light source 21 is installed on the motion arm 22 of microscope 2, and suture when needing, is opened in the operation stitching region in transmitting light irradiation front 1 fluorescence excitation light source 21 of needle, fluorescence excitation light source 21 emit the operation stitching region in light irradiation front, the seam in operation stitching region It closes needle 1 and generates fluorescent effect, send out the fluorescent powder sedimentary 11 of sewing needle 1 and be clear to light, this 21 installation position of fluorescence excitation light source It is appropriate to put, and can be irradiated to the operation stitching region in front, and does not influence surgical procedure, and can also be irradiated to sewing needle 1 in time Fluorescent powder sedimentary 11.
In the present embodiment, fluorescence excitation light source 21 includes point light source 211 and magnet 213, and point light source 211 passes through magnet 213 It is absorbed and fixed on motion arm 22.In the structure, point light source 211 is absorbed and fixed at by magnet 213 on motion arm 22 so that point Light source 211 dismounts very convenient, during installation, directly fills magnet 213 and adsorbs on motion arm 22, then point light source 211 is adsorbed Magnet 213, it is very convenient, when equally changeing, firmly point light source 211 is taken from magnet 213, same to point light sources 211 also easily take from magnet 213, then hand-held light source 211 irradiates any region, when sewing needle 1 falls on operation stitching area When other than domain, hand-holdable light source 211 is irradiated to this region and finds sewing needle 1, and point light source 211 also can be by adjusting magnet 213 adjust the direction of illumination of point light source 211 in 22 position of motion arm, so that point light source 211 emits luminous energy covering operation stitching Region.
In the present embodiment, microscope 2 is equipped with the first light source switch 2111 for opening and closing point light source 211.In the structure, The first light source switch 2111 of point light source 211 is for opening and closing point light source 211, and when needed, connection first light source switch 2111 is opened Opening point light source 211 makes it emit light, when not needed, disconnects first light source switch 2111 and closes point light source 211, save electric energy, Extend the service life of point light source 211.
Embodiment 2:
It is shown as shown in Figure 1, Figure 3 and Figure 4, second of embodiment of microsurgery sewing system of the present invention, the sewing system with Embodiment 1 is essentially identical, differs only in:In the present embodiment, fluorescence excitation light source 21 includes array light source 212 and connector 214,214 side of connector is equipped with pillar 2141, and connector 214 is rotatable to be sleeved on motion arm 22, and array light source 212 can Detachable set is fixed on the pillar 2141 of connector 214.In the structure, array light source 212 passes through three on array light source 212 Slack adjuster(2123)Detachable set is fixed on the pillar 2141 of connector 214, three slack adjusters(2123)Pass through array 212 outer periphery of light source is placed in array light source 212, tightens slack adjuster(2123), slack adjuster(2123)Bottom end squeeze The periphery of pillar 2141 makes connector 214 be anchored on the pillar 2141 of connector 214, meanwhile, back-out slack adjuster(2123), Slack adjuster(2123)Periphery of the bottom end far from pillar 2141, connector 214 can be from the pillar 2141 of connector 214 at this time It takes out free end;Connector 214 is rotatable to be sleeved on motion arm 22 so that is fixed on the pillar 2141 of connector 214 Array light source 212 axial direction and motion arm 22 it is axial into an angle of 90 degrees degree(According to the pillar 2141 of connector 214 not Tongfang To can also be into other angles)And connector 214 can encircling operation arm 22 rotate unspecified angle grasped to adjust connector 214 Make position on arm 22, array light source 212 is adjusted with respect to motion arm 22 so as to drive the rotation of 212 encircling operation arm 22 of array light source Position so that adjustment array light source 212 emits the direction of illumination of light, and the bulb 2122 of array light source 212 is in array light The end face circumference array arrangement of the separate motion arm 22 in source 212, makes its irradiation area bigger.
In the present embodiment, array light source 212 is equipped with the second light source switch 2121 for opening and closing array light source 212, battle array 212 built-in rechargeable battery of row light source.In the structure, the second light source switch 2121 of array light source 212 is used to open and close array light Source 212, when needed, 2121 unlatching array light source 212 of second light source switch is connected in connection makes it emit light, when not needed, It disconnects second light source switch 2121 and closes array light source 212, save electric energy, extend the service life of array light source 212;Array light 212 built-in rechargeable battery of source can be that array light source 212 provides electricity, shine for it.
Although the present invention is disclosed as above with preferred embodiment, it is not limited to the present invention.It is any to be familiar with ability The technical staff in domain, in the case where not departing from technical solution of the present invention range, all using the technology contents pair of the disclosure above Technical solution of the present invention makes many possible changes and modifications or is revised as the equivalent embodiment of equivalent variations.Therefore, it is every Without departing from the content of technical solution of the present invention, according to the present invention technical spirit any simple modification made to the above embodiment, Equivalent variations and modification should all be fallen in the range of technical solution of the present invention protection.

Claims (9)

1. a kind of microsurgery sewing system, including microscope(2)And sewing needle(1), it is characterised in that:The sewing needle (1)It is equipped with fluorescent powder sedimentary(11), the microscope(2)On be installed with to excite the fluorescent powder sedimentary(11)Hair The fluorescence excitation light source of light(21), the fluorescence excitation light source(21)Illumination at least cover operation stitching region.
2. microsurgery sewing system according to claim 1, it is characterised in that:The fluorescent powder sedimentary(11) It is set as Ca- α-Sialon:Eu2+Yellow fluorescent powder, the fluorescence excitation light source(21)Generation wavelength is 460 nanometers of blue Light.
3. microsurgery sewing system according to claim 2, it is characterised in that:The fluorescent powder sedimentary(11) Coated on the sewing needle(1)Outer surface, and be covered in sewing needle(1)At the 1/4 of rear end.
4. microsurgery sewing system according to claim 3, it is characterised in that:The fluorescent powder sedimentary(11) Thickness is 10 ~ 20 microns.
5. microsurgery sewing system according to any one of claim 1 to 4, it is characterised in that:The fluorescence Excitation light source(21)It is installed on the microscope(2)Motion arm(22)On.
6. microsurgery sewing system according to claim 5, it is characterised in that:The fluorescence excitation light source(21) Including point light source(211)And magnet(213), the point light source(211)Pass through the magnet(213)It is absorbed and fixed at the operation Arm(22)On.
7. microsurgery sewing system according to claim 6, it is characterised in that:The microscope(2)It is equipped with For opening and closing the point light source(211)First light source switch(2111).
8. microsurgery sewing system according to claim 5, it is characterised in that:The fluorescence excitation light source(21) Including array light source(212)And connector(214), the connector(214)Side is equipped with pillar(2141), the connector (214)It is rotatable to be sleeved on the motion arm(22)On, the array light source(212)Detachable set is fixed in the connector (214)Pillar(2141)On.
9. microsurgery sewing system according to claim 8, it is characterised in that:The array light source(212)On Equipped with for opening and closing the array light source(212)Second light source switch(2121), the array light source(212)It is built-in chargeable Battery.
CN201810063459.4A 2018-01-23 2018-01-23 Microsurgery sewing system Pending CN108175463A (en)

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CN203217161U (en) * 2013-04-04 2013-09-25 *** Novel microscope used for hand and foot microsurgery
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US20090317002A1 (en) * 2008-06-23 2009-12-24 John Richard Dein Intra-operative system for identifying and tracking surgical sharp objects, instruments, and sponges
CN201664343U (en) * 2008-11-11 2010-12-08 深圳市莫廷影像技术有限公司 Operating microscope system with angiographic function
CN202015212U (en) * 2011-02-12 2011-10-26 高宏 Magnetic fluorescent surgical suture needle
CN203217161U (en) * 2013-04-04 2013-09-25 *** Novel microscope used for hand and foot microsurgery
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王德刘等: "Ca-α-SiAlON:Eu~(2+)荧光发光材料的合成与发光性能", 稀有金属材料与工程, vol. 37, no. 04, 15 April 2008 (2008-04-15), pages 713 - 716 *

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