CN108148509A - A kind of preparation method of leather polishing new material - Google Patents
A kind of preparation method of leather polishing new material Download PDFInfo
- Publication number
- CN108148509A CN108148509A CN201711141011.1A CN201711141011A CN108148509A CN 108148509 A CN108148509 A CN 108148509A CN 201711141011 A CN201711141011 A CN 201711141011A CN 108148509 A CN108148509 A CN 108148509A
- Authority
- CN
- China
- Prior art keywords
- new material
- ethyl alcohol
- preparation
- leather polishing
- leather
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/06—Other polishing compositions
- C09G1/14—Other polishing compositions based on non-waxy substances
- C09G1/16—Other polishing compositions based on non-waxy substances on natural or synthetic resins
-
- C—CHEMISTRY; METALLURGY
- C14—SKINS; HIDES; PELTS; LEATHER
- C14C—CHEMICAL TREATMENT OF HIDES, SKINS OR LEATHER, e.g. TANNING, IMPREGNATING, FINISHING; APPARATUS THEREFOR; COMPOSITIONS FOR TANNING
- C14C11/00—Surface finishing of leather
- C14C11/003—Surface finishing of leather using macromolecular compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Treatment And Processing Of Natural Fur Or Leather (AREA)
Abstract
The present invention relates to a kind of preparation methods of leather polishing new material.By weight, ethyl alcohol is added in a kettle, dimethyl polysiloxane, acetylacetone,2,4-pentanedione enol trimethyl silicane alkyl ester, perfluoro polyether oil, allyloxy t-butyldimethyl silane, poly(ethylene glycol) phenyl ether acrylate, bis- (cyclohexyl sulfydryl) titaniums of tetrachloro, heating, stirring is to get to leather polishing new material.
Description
Technical field
The present invention relates to a kind of brightener, especially a kind of preparation method of leather polishing new material.
Background technology
It comes as the improvement of people's living standards, leather and fur products has also been popularized in people's lives, money can be used as
Packet, waistband, clothes, accessories, footwear packet, the every field of packaging；The function of leather gloss agent is to enable leather products with more soft
It is soft, submissive, the characteristic of gloss, and on the basis of the original gas permeability of leather is kept enhance leather products water-resistance, prevent
Viscosity and solvent resistance；Make the appearance of leather products, feel, surface property gets a promotion.
CN105419646A discloses a kind of leather gloss agent, composed of the following components：Dispersions of polyurethanes 30-40%,
Cosolvent 10-20%, organic silicon modified by polyether oxygen alkane 0.2-0.8%, silicone oil 1-5%, polyglycol ether 1-5%, polyvinylether 2-8%,
Remaining is deionized water；The cosolvent is N- methyl-pyrrolidons and isopropanol.
CN104893589A discloses a kind of leather gloss agent, is prepared from the following raw materials in parts by weight：Beeswax 4-8
Part, 5-10 parts of cetostearyl alcohol, 3-6 parts of moisturizer, 5-7 parts of lanolin, 4-7 parts of castor oil ethylene oxide, 2-6 parts of snake oil, silicon
It is 4-7 parts oily, NP-4PK2-6 parts of phenolic ether phosphate kalium salt, 10-25 parts of ethyl acetate, 4-6 parts of cerosin, 3-7 parts of dimethicone,
6-10 parts of Brazil wax, 2-4 parts of acetone, 1.5-3.5 parts of fatty alcohol polyoxyethylene ether.
Existing organosilicon leather gloss agent has the shortcomings that attachment is not strong, poor solvent resistance mostly, causes leather products
Easily surface water resistance, bright degree decline after use.
Invention content
In view of the deficiencies of the prior art, the present invention provides a kind of preparation method of leather polishing new material, including as follows
Step：
By weight, ethyl alcohol is added in a kettle, dimethyl polysiloxane, acetylacetone,2,4-pentanedione enol trimethyl silicane alkyl ester, entirely
Perfluoroalkyl polyether oil, allyloxy-tert-butyl dimethylsilane, poly(ethylene glycol) phenyl ether acrylate, bis- (the cyclohexyl mercaptos of tetrachloro
Base) titanium, 70-80 DEG C is warming up to, with the rotating speed of 100-300rpm stirring 4-8h to get to leather polishing new material.
The dimethyl polysiloxane, quality dosage are the 5-10% of ethyl alcohol.
The acetylacetone,2,4-pentanedione enol trimethyl silicane alkyl ester, quality dosage are the 1-3% of ethyl alcohol.
The perfluoro polyether oil, quality dosage are the 0.5-1.5% of ethyl alcohol.
The allyloxy-tert-butyl dimethylsilane, quality dosage are the 0.1-0.5% of ethyl alcohol.
The poly(ethylene glycol) phenyl ether acrylate, quality dosage are the 0.1-0.5% of ethyl alcohol.
Bis- (cyclohexyl sulfydryl) titaniums of the tetrachloro, quality dosage are the 0.1-0.5% of ethyl alcohol.
The ethyl alcohol, dimethyl polysiloxane, acetylacetone,2,4-pentanedione enol trimethyl silicane alkyl ester, perfluoro polyether oil, allyl oxygen
Base-tert-butyl dimethylsilane, poly(ethylene glycol) phenyl ether acrylate, bis- (cyclohexyl sulfydryl) titaniums of tetrachloro are commercially available production
Product.
Beneficial effects of the present invention：
The leather gloss agent composition that the present invention is produced, each component are easily uniformly dispersed, and make leather and fur products light water resistant effect
Well, uniformly；Film forming, adhesion are good, can ensure to enable leather and fur products waterproof, bright function for a long time.
Specific embodiment
Embodiment 1
In a kettle, ethyl alcohol 100Kg, dimethyl polysiloxane 7.5Kg, acetylacetone,2,4-pentanedione enol trimethyl silicane alkyl ester 2Kg are added in,
Perfluoro polyether oil 1Kg, allyloxy-tert-butyl dimethylsilane 0.3Kg, poly(ethylene glycol) phenyl ether acrylate 0.3Kg,
Bis- (cyclohexyl sulfydryl) the titanium 0.3Kg of tetrachloro, are warming up to 75 DEG C, with the rotating speed of 200rpm stirring 6h to get to leather polishing green wood
Material.
Embodiment 2
In a kettle, ethyl alcohol 100Kg, dimethyl polysiloxane 5Kg, acetylacetone,2,4-pentanedione enol trimethyl silicane alkyl ester 1Kg are added in, entirely
Perfluoroalkyl polyether oil 0.5Kg, allyloxy-tert-butyl dimethylsilane 0.1Kg, poly(ethylene glycol) phenyl ether acrylate 0.1Kg,
Bis- (cyclohexyl sulfydryl) the titanium 0.1Kg of tetrachloro, are warming up to 70 DEG C, with the rotating speed of 100rpm stirring 4h to get to leather polishing green wood
Material.
Embodiment 3
In a kettle, ethyl alcohol 100Kg, dimethyl polysiloxane 10Kg, acetylacetone,2,4-pentanedione enol trimethyl silicane alkyl ester 3Kg are added in,
Perfluoro polyether oil 1.5Kg, allyloxy-tert-butyl dimethylsilane 0.5Kg, poly(ethylene glycol) phenyl ether acrylate
0.5Kg, bis- (cyclohexyl sulfydryl) the titanium 0.5Kg of tetrachloro, is warming up to 80 DEG C, with the rotating speed of 300rpm stirring 8h to get to leather light
Bright new material.
Comparative example 1
Perfluoro polyether oil is added without, other conditions are the same as embodiment 1.
Comparative example 2
Poly(ethylene glycol) phenyl ether acrylate is added without, other conditions are the same as embodiment 1.
Comparative example 3
Bis- (cyclohexyl sulfydryl) titaniums of tetrachloro are added without, other conditions are the same as embodiment 1.
Embodiment 4
By the product produced of embodiment 1-3 and comparative example 1-3, the method that reference standard GB/T9754-1988 is provided,
The measure of 60 ° of angle finish is carried out, is shown in Table 1.
Table 1:60 ° of angle finish of leather gloss agent that different process is produced.
Claims (7)
1. a kind of preparation method of leather polishing new material, it is characterised in that include the following steps：
By weight, ethyl alcohol is added in a kettle, dimethyl polysiloxane, acetylacetone,2,4-pentanedione enol trimethyl silicane alkyl ester, entirely
Perfluoroalkyl polyether oil, allyloxy-tert-butyl dimethylsilane, poly(ethylene glycol) phenyl ether acrylate, bis- (the cyclohexyl mercaptos of tetrachloro
Base) titanium, 70-80 DEG C is warming up to, with the rotating speed of 100-300rpm stirring 4-8h to get to leather polishing new material.
2. a kind of preparation method of leather polishing new material according to claim 1, it is characterised in that：The dimethyl
Polysiloxanes, quality dosage are the 5-10% of ethyl alcohol.
3. a kind of preparation method of leather polishing new material according to claim 1, it is characterised in that：The levulinic
Ketonenol trimethyl silicane alkyl ester, quality dosage are the 1-3% of ethyl alcohol.
4. a kind of preparation method of leather polishing new material according to claim 1, it is characterised in that：The perfluor gathers
Ether oil, quality dosage are the 0.5-1.5% of ethyl alcohol.
5. a kind of preparation method of leather polishing new material according to claim 1, it is characterised in that：The allyl oxygen
Base-tert-butyl dimethylsilane, quality dosage are the 0.1-0.5% of ethyl alcohol.
6. a kind of preparation method of leather polishing new material according to claim 1, it is characterised in that：Poly- (the second
Glycol) phenyl ether acrylate, quality dosage is the 0.1-0.5% of ethyl alcohol.
7. a kind of preparation method of leather polishing new material according to claim 1, it is characterised in that：The tetrachloro is double
(cyclohexyl sulfydryl) titanium, quality dosage are the 0.1-0.5% of ethyl alcohol.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711141011.1A CN108148509A (en) | 2017-11-17 | 2017-11-17 | A kind of preparation method of leather polishing new material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711141011.1A CN108148509A (en) | 2017-11-17 | 2017-11-17 | A kind of preparation method of leather polishing new material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108148509A true CN108148509A (en) | 2018-06-12 |
Family
ID=62468942
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711141011.1A Pending CN108148509A (en) | 2017-11-17 | 2017-11-17 | A kind of preparation method of leather polishing new material |
Country Status (1)
| Country | Link |
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| CN (1) | CN108148509A (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102660197A (en) * | 2012-04-20 | 2012-09-12 | 上海皇宇科技发展有限公司 | Leather brightening agent and leather brightening wet wiper |
| CN102796461A (en) * | 2012-09-10 | 2012-11-28 | 李长河 | Diversified cleaning agent and preparation method thereof |
| CN103666290A (en) * | 2013-11-27 | 2014-03-26 | 南通市通州区川姜镇盛世王朝家用纺织品设计工作室 | Leather cleaner |
| CN104194651A (en) * | 2014-08-20 | 2014-12-10 | 刘骏 | Method for manufacturing leather brightening agent |
| CN105256578A (en) * | 2015-11-09 | 2016-01-20 | 广州大学 | Waterborne three-proofing leather finishing agent and using method thereof |
| CN106085246A (en) * | 2016-06-19 | 2016-11-09 | 王金明 | A kind of leather gloss agent compositions containing polyethers |
-
2017
- 2017-11-17 CN CN201711141011.1A patent/CN108148509A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102660197A (en) * | 2012-04-20 | 2012-09-12 | 上海皇宇科技发展有限公司 | Leather brightening agent and leather brightening wet wiper |
| CN102796461A (en) * | 2012-09-10 | 2012-11-28 | 李长河 | Diversified cleaning agent and preparation method thereof |
| CN103666290A (en) * | 2013-11-27 | 2014-03-26 | 南通市通州区川姜镇盛世王朝家用纺织品设计工作室 | Leather cleaner |
| CN104194651A (en) * | 2014-08-20 | 2014-12-10 | 刘骏 | Method for manufacturing leather brightening agent |
| CN105256578A (en) * | 2015-11-09 | 2016-01-20 | 广州大学 | Waterborne three-proofing leather finishing agent and using method thereof |
| CN106085246A (en) * | 2016-06-19 | 2016-11-09 | 王金明 | A kind of leather gloss agent compositions containing polyethers |
Non-Patent Citations (1)
| Title |
|---|
| 李正军: "皮革工业用有机硅化合物综述", 《中国皮革》 * |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180612 |