CN108084879A - Atactic polypropylene (APP) modified bituminous material and preparation method thereof, the waterproof roll of coating of insulation - Google Patents
Atactic polypropylene (APP) modified bituminous material and preparation method thereof, the waterproof roll of coating of insulation Download PDFInfo
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- CN108084879A CN108084879A CN201711309987.5A CN201711309987A CN108084879A CN 108084879 A CN108084879 A CN 108084879A CN 201711309987 A CN201711309987 A CN 201711309987A CN 108084879 A CN108084879 A CN 108084879A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D195/00—Coating compositions based on bituminous materials, e.g. asphalt, tar, pitch
-
- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04B—GENERAL BUILDING CONSTRUCTIONS; WALLS, e.g. PARTITIONS; ROOFS; FLOORS; CEILINGS; INSULATION OR OTHER PROTECTION OF BUILDINGS
- E04B1/00—Constructions in general; Structures which are not restricted either to walls, e.g. partitions, or floors or ceilings or roofs
- E04B1/62—Insulation or other protection; Elements or use of specified material therefor
- E04B1/66—Sealings
- E04B1/665—Sheets or foils impervious to water and water vapor
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2207/00—Properties characterising the ingredient of the composition
- C08L2207/10—Peculiar tacticity
- C08L2207/14—Amorphous or atactic polypropylene
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- Engineering & Computer Science (AREA)
- Architecture (AREA)
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Electromagnetism (AREA)
- Civil Engineering (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
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Abstract
The present invention relates to architectural waterproof material fields, more particularly to atactic polypropylene (APP) modified bituminous material and preparation method thereof, the waterproof roll of coating of insulation；A kind of atactic polypropylene (APP) modified bituminous material of coating of insulation, which is characterized in that composition of raw materials by percentage to the quality, including following components：35~60 parts of bitumen, 2~15 parts of softening agent, 0.1~5 part of graphene aerogel, 3~15 parts of thermoplastic, 3~12 parts of rubber, 15~40 parts of filler；The beneficial effects of the present invention are：It is described coat material and the waterproof roll have heat preservation and heat-proof quality, in the case where not influencing modified asphalt waterproof coiled material water resistance, impart modified asphalt waterproof coiled material incubation and thermal insulation function, widened the application range of architectural waterproof material.
Description
Technical field
The present invention relates to building heat preservation field of waterproof materials, more particularly to insulation it is atactic polypropylene (APP) modified bituminous coat material and
Its preparation method, waterproof roll.
Background technology
Atactic polypropylene (APP) modified bituminous waterproof sheet material has excellent high temperature resistance, suitable for all kinds of buildings waterproofs, moisture-proof work
Journey is particularly suitable for high temperature or has the building waterproof in strong solar radiation area, and the structure of modified asphalt waterproof coiled material is general
It is for reinforcement with polyester blank, glass fiber blank, fiberglass reinforcing polyester tire etc., positioned at coiled material centre position, is coated in reinforcement both sides
Modified pitch is coated material, is coated material overlying isolated material in modified pitch.
Graphene aerogel is current most light solid material known in the world, inside have many holes, be flooded with sky
Gas, elasticity and oil absorption make us pleasantly surprised, and preparation method is simple, and the bigger serface and cavernous structure of graphene aerogel cause
It is with excellent thermal and insulating performance, and graphene aerogel is more suitable for current Green Development as environmentally friendly material
Trend.
With the development of building, waterproof and heat insulation function become the basic demand that roofing and wall is built, traditional construction
Mode is to set waterproof layer and insulating layer respectively on roofing and wall, and so from material to construction, either waterproof is still kept the temperature,
All fight separately, functional independence it is single, shortage is made overall plans, and shortcoming has three：First, between waterproof material and thermal insulation material mutually
Benefit property is poor, and waterproof thermal-insulated performance reduces, second is that waterproof layer loses heat insulation function immediately once there is leakage insulating layer, third, point
It constructs twice, cost costly, increases incubation and thermal insulation function newly on the Plastomer asphalt waterproof coiled material with excellent waterproof effect,
And itself waterproof effect and performance are not influenced, the coiled material for integrating insulation and water-proof function is made, is one
Kind economically viable method.
Graphene aerogel and pitch are mixed one kind material of coating to be applied on asphalt felt, a kind of collection heat preservation is made
Heat-insulated and water-proof function meets the demand of this field in the coiled material of one.
The content of the invention
It is an object of the invention to provide a kind of atactic polypropylene (APP) modified bituminous material and preparation method thereof, the waterproofs of coating of insulation
Coiled material, the atactic polypropylene (APP) modified bituminous material of coating of the insulation, waterproof roll have both excellent heat preservation and water resistance, Neng Gouti
Low temperature flexibility, heat-resisting quantity and the cohesive force of high-ductility modified asphalt waterproof roll, and it is made to show more excellent waterproof
Performance.
To achieve these goals, the technical scheme is that：
One of the objects of the present invention is to provide a kind of atactic polypropylene (APP) modified bituminous material of coating of insulation, it is by naturally dripping
Green grass or young crops, softening agent, graphene aerogel, thermoplastic, rubber and filler are prepared, and each raw material is according to the mass fraction：
35~60 parts of bitumen
2~15 parts of softening agent
0.1~5 part of graphene aerogel
3~15 parts of thermoplastic
3~12 parts of rubber
15~40 parts of filler.
The bitumen is rock asphalt and/or lake asphalt.
The softening agent includes at least one of base oil, readymade oil or naphthenic oil.
The thermoplastic is Atactic Polypropelene and/or polyolefin polymers.
The rubber includes at least one of rubber SBS, rubber SBR or rubber SBRS.
The filler is one kind in talcum powder, powdered whiting or mountain flour.
A kind of preparation method of the above-mentioned atactic polypropylene (APP) modified bituminous material of coating of insulation, comprises the following steps：
A, each raw material is according to the mass fraction：35~60 parts of bitumen, 2~15 parts of softening agent, graphene aerogel 0.1
~5 parts, 3~15 parts of thermoplastic, 3~12 parts of rubber, 15~40 parts of filler, choose pitch, softening agent, graphene airsetting
Glue, thermoplastic, rubber and filler, it is spare；
B, bitumen and softening oil are added separately to reaction kettle and are heated to 170~180 DEG C, start shear agitation
Machine under the rotating speed of 300~800rpm, is slowly added to graphene aerogel, and when persistently stirring 1~1.5 is small, holding temperature is
170~180 DEG C；
C, reaction kettle is transferred to after resulting material being carried out decentralized processing by colloid mill, then heats to 180~190 DEG C,
Add in thermoplastic, be stirred to react under the rotating speed of 300~500rpm 0.5~1 it is small when；
D, after treating thermoplastic molten, it is 180 DEG C~200 DEG C to keep temperature, rubber is added in, in 300~500rpm
Rotating speed under be stirred to react 2~3 it is small when；
E, mixing speed is reduced to 200~300rpm, adds in filler, it is 180 DEG C~200 DEG C to keep temperature, continues to stir
Mix 0.5~1 it is small when, draw material, insulation atactic polypropylene (APP) modified bituminous material of coating be made.
Another object of the present invention is provides a kind of insulation atactic polypropylene (APP) modified bituminous waterproof sheet material, including above-mentioned guarantor
The heat-insulated atactic polypropylene (APP) modified bituminous material of coating of temperature.
The insulation atactic polypropylene (APP) modified bituminous waterproof sheet material, including from top to bottom set the first separation layer, first
Coat the bed of material, enhancement layer, second coat the bed of material, the second separation layer, wherein, the first lid bed of material is by above-mentioned insulation plasticity
Modified asphalt material of coating is made, and described second bed of material of coating is made of the atactic polypropylene (APP) modified bituminous material of coating of above-mentioned insulation.
Beneficial effects of the present invention：
1st, by atactic polypropylene (APP) modified bituminous middle addition graphene aerogel, utilizing the insulation of graphene aerogel special
Property increases atactic polypropylene (APP) modified bituminous function of heat insulation, prepare with excellent water resistance and thermal and insulating performance in
The atactic polypropylene (APP) modified bituminous material of coating of insulation of the waterproof roll of one.
2nd, thermoplastic belongs to high-molecular compound, and chance ultraviolet light is degradable, when graphene aerogel is in stirring and glue
Body mill peptizaiton under with network structure stabilization in pitch when, uniformly mixed with thermoplastic, graphene aerogel it is big
Specific surface area and cavernous structure can also play thermoplastic better ultraviolet protection, can effectively avoid ultraviolet light to thermoplastic
The degradation of property plastics, so as to significantly improve the anti-ultraviolet ageing ability of thermoplast-modified pitch.
3rd, graphene aerogel has the function of good heat preservation and sound insulation, and utilizes its high adsorption and elastomeric spy
Point can absorb the small-molecule substance in pitch, and can assign the better tensile strength of pitch and resilience, and it is not
Water suction does not interfere with the originally outstanding water resistance of pitch, has positive interaction with pitch, and graphene aerogel disperses
Property is good, can uniformly and stably be dispersed in modified pitch system, without settling.
Specific embodiment
The present invention is specifically described below by embodiment, it is necessary to which indicated herein is that following embodiment is simply used
It is further detailed in the present invention, it is impossible to be interpreted as limiting the scope of the invention, which is skilled in technique
Personnel still fall within protection scope of the present invention according to some nonessential modifications and adaptations that foregoing invention content is made.
A kind of atactic polypropylene (APP) modified bituminous material of coating of insulation, it include bitumen, softening agent, graphene aerogel,
Thermoplastic, rubber and filler, each raw material are according to the mass fraction：
35~60 parts of bitumen
2~15 parts of softening agent
0.1~5 part of graphene aerogel
3~15 parts of thermoplastic
3~12 parts of rubber
15~40 parts of filler.
The bitumen is rock asphalt and/or lake asphalt.
The softening agent includes at least one of base oil, readymade oil or naphthenic oil.
The thermoplastic is Atactic Polypropelene and/or polyolefin polymers.
The rubber includes at least one of rubber SBS, rubber SBR or rubber SBRS.
The filler is one kind in talcum powder, powdered whiting or mountain flour.
Insulation atactic polypropylene (APP) modified bituminous waterproof sheet material obtained by following examples of the present invention is by as follows
Specification is made：
Model：PYG (fiberglass reinforcing polyester felt tire) II type
Width：1000mm
Thickness：5mm
Embodiment 1
50 parts (mass parts, similarly hereinafter) natural lake asphalt and 8 parts of base oils are compounded and are heated to 175 DEG C, starts and cuts
Mixer is cut, under the rotating speed of 500rpm, is slowly added to 2 parts of graphene aerogels, it is 170~180 DEG C to keep temperature, is persistently stirred
Mix 1.5 it is small when, be transferred to reaction kettle after resulting material is carried out decentralized processing by colloid mill, then heat to 185 DEG C, add in 9
Part Atactic Polypropelene, it is 180~190 DEG C to keep temperature, be stirred to react under the rotating speed of 400rpm 1 it is small when, then heat to
190 DEG C, 7 parts of s-B-Ss are added in, it is 180~190 DEG C to keep temperature, is stirred under the rotating speed of 400rpm anti-
Answer 2.5 it is small when, mixing speed is reduced to 200rpm, adds in 34 parts of talcum powder, it is 180~190 DEG C to keep temperature, continues to stir
1 it is small when, obtain the atactic polypropylene (APP) modified bituminous material of coating of insulation.
A kind of insulation atactic polypropylene (APP) modified bituminous waterproof sheet material, including the above-mentioned atactic polypropylene (APP) modified bituminous painting of insulation
Lid material.
Embodiment 2
50 parts (mass parts, similarly hereinafter) natural lake asphalt and 8 parts of base oils are compounded and are heated to 175 DEG C, starts and cuts
Mixer is cut, under the rotating speed of 500rpm, is slowly added to 3 parts of graphene aerogels, it is 170~180 DEG C to keep temperature, is persistently stirred
Mix 1 it is small when, be transferred to reaction kettle after resulting material is carried out decentralized processing by colloid mill, then heat to 185 DEG C, add in 9 parts
Atactic Polypropelene, keep temperature be 180~190 DEG C, be stirred to react under the rotating speed of 500rpm 0.5 it is small when, then heat to
190 DEG C, 7 parts of s-B-Ss are added in, it is 180~190 DEG C to keep temperature, is stirred under the rotating speed of 500rpm anti-
Answer 2 it is small when, mixing speed is reduced to 300rpm, adds in 35 parts of talcum powder, it is 180~190 DEG C to keep temperature, continues to stir
0.5 it is small when, obtain the atactic polypropylene (APP) modified bituminous material of coating of insulation.
A kind of insulation atactic polypropylene (APP) modified bituminous waterproof sheet material, including the above-mentioned atactic polypropylene (APP) modified bituminous painting of insulation
Lid material.
Embodiment 3
55.5 parts (mass parts, similarly hereinafter) natural lake asphalt and 13 parts of base oils are compounded and are heated to 175 DEG C, is started
Shear mixer under the rotating speed of 800rpm, is slowly added to 0.5 part of graphene aerogel, and it is 170~180 DEG C to keep temperature, is held
When continuous stirring 1.5 is small, reaction kettle is transferred to after resulting material is carried out decentralized processing by colloid mill, 185 DEG C is then heated to, adds
Enter 5 parts of Atactic Polypropelenes, it is 180~190 DEG C to keep temperature, by mixing speed be reduced to 500rpm and be stirred to react 1 it is small when,
190 DEG C are then heated to, adds in 4 parts of s-B-Ss, it is 180~190 DEG C to keep temperature, in turning for 500rpm
Be stirred to react under speed 3 it is small when, mixing speed is reduced to 300rpm, adds in 22 parts of talcum powder, it is 180~190 DEG C to keep temperature,
Continue stirring 0.5 it is small when, obtain the atactic polypropylene (APP) modified bituminous material of coating of insulation.
A kind of insulation atactic polypropylene (APP) modified bituminous waterproof sheet material, including the above-mentioned atactic polypropylene (APP) modified bituminous painting of insulation
Lid material.
Embodiment 4
38 parts (mass parts, similarly hereinafter) natural lake asphalt and 4 parts of base oils are compounded and are heated to 175 DEG C, starts and cuts
Mixer is cut, under the rotating speed of 300rpm, is slowly added to 4 parts of graphene aerogels, it is 170~180 DEG C to keep temperature, is persistently stirred
Mix 1.5 it is small when, be transferred to reaction kettle after resulting material is carried out decentralized processing by colloid mill, then heat to 185 DEG C, add in 13
Part Atactic Polypropelene, it is 180~190 DEG C to keep temperature, be stirred to react under the rotating speed of 300rpm 0.5 it is small when, then heat up
To 190 DEG C, 10 parts of s-B-Ss are added in, it is 180~190 DEG C to keep temperature, is stirred under the rotating speed of 300rpm
Mix reaction 2 it is small when, mixing speed is reduced to 200rpm, adds in 31 parts of talcum powder, it is 180~190 DEG C to keep temperature, continues to stir
Mix 1 it is small when, obtain the atactic polypropylene (APP) modified bituminous material of coating of insulation.
A kind of insulation atactic polypropylene (APP) modified bituminous waterproof sheet material, including the above-mentioned atactic polypropylene (APP) modified bituminous painting of insulation
Lid material.
Insulation atactic polypropylene (APP) modified bituminous waterproof sheet material properties obtained by 1 embodiment of table：
Claims (8)
1. the atactic polypropylene (APP) modified bituminous material of coating of a kind of insulation, which is characterized in that it includes bitumen, softening agent, graphite
Alkene aeroge, thermoplastic, rubber and filler, each raw material are according to the mass fraction：
35~60 parts of bitumen
2~15 parts of softening agent
0.1~5 part of graphene aerogel
3~15 parts of thermoplastic
3~12 parts of rubber
15~40 parts of filler.
A kind of 2. atactic polypropylene (APP) modified bituminous material of coating of insulation according to claim 1, which is characterized in that the natural drip
Green grass or young crops includes rock asphalt and/or lake asphalt.
A kind of 3. atactic polypropylene (APP) modified bituminous material of coating of insulation according to claim 1, which is characterized in that the softening agent
Including at least one of base oil, readymade oil or naphthenic oil.
A kind of 4. atactic polypropylene (APP) modified bituminous material of coating of insulation according to claim 1, which is characterized in that the thermoplasticity
Plastics are Atactic Polypropelene and/or polyolefin polymers.
A kind of 5. atactic polypropylene (APP) modified bituminous material of coating of insulation according to claim 1, which is characterized in that the rubber bag
Include at least one of rubber SBS, rubber SBR or rubber SBRS.
A kind of 6. atactic polypropylene (APP) modified bituminous material of coating of insulation according to claim 1, which is characterized in that the filler bag
Include one kind in talcum powder, powdered whiting or mountain flour.
7. a kind of preparation method of the atactic polypropylene (APP) modified bituminous material of coating of the insulation according to claim 1~6 any one,
It is characterised in that it includes following steps：
A, each raw material is according to the mass fraction：35~60 parts of bitumen, 2~15 parts of softening agent, graphene aerogel 0.1~5
Part, 3~15 parts of thermoplastic, 3~12 parts of rubber, 15~40 parts of filler choose pitch, softening agent, graphene aerogel, heat
Thermoplastic plastic, rubber and filler, it is spare；
B, bitumen and softening oil are added separately to reaction kettle and are heated to 170~180 DEG C, start shear mixer,
Under the rotating speed of 300~800rpm, be slowly added to graphene aerogel, persistently stir 1~1.5 it is small when, keep temperature for 170~
180℃；
C, reaction kettle is transferred to after resulting material being carried out decentralized processing by colloid mill, then heats to 180~190 DEG C, is added in
Thermoplastic, be stirred to react under the rotating speed of 300~500rpm 0.5~1 it is small when；
D, after treating thermoplastic molten, it is 180 DEG C~200 DEG C to keep temperature, adds in rubber, in turning for 300~500rpm
Be stirred to react under speed 2~3 it is small when；
E, mixing speed is reduced to 200~300rpm, adds in filler, it is 180 DEG C~200 DEG C to keep temperature, continues stirring 0.5
~1 it is small when, draw material, insulation atactic polypropylene (APP) modified bituminous material of coating be made.
8. according to the atactic polypropylene (APP) modified bituminous insulation made of material of coating of insulation described in claim 1~6 any one
Atactic polypropylene (APP) modified bituminous waterproof sheet material.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711309987.5A CN108084879A (en) | 2017-12-11 | 2017-12-11 | Atactic polypropylene (APP) modified bituminous material and preparation method thereof, the waterproof roll of coating of insulation |
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|---|---|---|---|
| CN201711309987.5A CN108084879A (en) | 2017-12-11 | 2017-12-11 | Atactic polypropylene (APP) modified bituminous material and preparation method thereof, the waterproof roll of coating of insulation |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110951266A (en) * | 2019-10-23 | 2020-04-03 | 长安大学 | High-performance modified asphalt and preparation method thereof |
| CN115975532A (en) * | 2023-03-03 | 2023-04-18 | 湖南百米体育产业有限公司 | Heat-preservation and heat-insulation rubber coiled material and production process thereof |
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| CN115975532A (en) * | 2023-03-03 | 2023-04-18 | 湖南百米体育产业有限公司 | Heat-preservation and heat-insulation rubber coiled material and production process thereof |
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Inventor after: Luo Xiaobin Inventor after: Du Yong Inventor before: Du Yong |
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Application publication date: 20180529 |
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