CN108079079A - A kind of Chinese yew formula of medicated bath and preparation method thereof - Google Patents
A kind of Chinese yew formula of medicated bath and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of Chinese yew formula of medicated bath and preparation method thereof, formula includes folium artemisiae argyi, safflower, rhizome of chuanxiong, monkshood, radix cyathulae, cassia bark, the root of Chinese clematis, asarum and taxus chinensis essential oil powder, preparation method includes the preparation method of taxus chinensis essential oil powder and the preparation method of Chinese yew medical bathing powder, and the preparation method of taxus chinensis essential oil powder includes pretreatment, extraction of essential oil and absorption again.The Chinese yew medical bathing powder that preparation method using the present invention is prepared is safe and non-toxic, so that beneficiating ingredient dissolution rate is high using the volatility of essential oil, it can boost metabolism, it promotes blood circulation, improve sleep, its principle is that the drug ingedient in essential oil distributes and warms stimulation and can be transmitted to central nervous system by thigmoreceptor and skin receptor, makes the excitement of maincenter and inhibits orderly.With relaxing tendons and activating collaterals, dehumidifying of warding off the cold, it is promoting blood circulation and removing blood stasis the effect of, to rheumatism, rheumatoid, pain of neck, shoulder, waist and leg, there is prevention and adjustment effect well.
Description
Technical field
The present invention relates to Chinese yew applied technical fields more particularly to a kind of Chinese yew formula of medicated bath and preparation method thereof.
Background technology
Chinese yew is a kind of evergreen needle arbor or shrub, is that have passed through the ancient seeds that the 4th glacier carries over,
Have the history of 2,500,000 years on earth, contain anticancer component taxol in bark, branches and leaves and tree root, be public in the world
The natural rare plants for anticancer recognized.Chinese yew likes dark and damp environment, the weather of warm and moist, has a drought-enduring cold-resistant, disease and insect resistance, compared with
Strong rudiment ability, it is slow-growing, the features such as long lifespan, but also with high value of exploiting and utilizing.But Chinese yew exists
It is slow-growing under natural conditions, ever-increasing market demand can not be met, under the driving of tremendous economic interests, natural resources
It is subject to artificial serious destruction, resource scarcity at present by artificial growth Chinese yew, meets the market demand of Chinese yew.
Branches and leaves of yew, bitter, in extract containing magical cancer-resisting substance taxol outside, also containing abundant plant ferment
Element, plant fiber, growth hormone, protein, fat and a variety of amino acid, the medicinal ingredient of Taxus leaf is higher than Chinese yew
Other positions are not only contained abundant anticarcinogen-taxol, are also contained there are many water-soluble flavone in Taxus leaf, including
Active extremely strong, biological utilisation is worth high preceding blue and white element in human body, also has catechin and a variety of unrighted acids, also
Rich in chlorophyll, multivitamin.
Chinese dipping is with a history of thousands of years in China, and according to records since the Zhou Dynasty, just popular fragrant soup bath, that is, use Chinese medicine
The liquid medicine that eupatorium is decocted is bathed, and fragrant is strong fragrant, have relieving summer-heat clearing damp, inducing resuscitation feel well brain the effect of.The traditional Chinese medical science 5,000 is contained in dipping
Year clinical crystallization, has passed through the combination of medicine and hot water, the magical work(of " getting instant result " can be played in the of short duration time
Effect.Have Chinese yew medical bathing powder on the market at present, be to do the leaf of Chinese yew or root or fruit or bark by simple process
Dry crush is made, due to containing a small amount of Water-soluble toxic substance, such as taxine in branches and leaves of yew, if be not pocessed,
It is used directly to bath, noxious material can be dissolved in water, and infiltrates into human body, and long-time service can bring injury to human body；In addition,
Benefit materials in Chinese yew discharge less in water, it is impossible to reach the effect of preferable.
The content of the invention
In view of this, the object of the present invention is to provide a kind of Chinese yew formula of medicated bath and preparation method thereof, using the preparation
The Chinese yew medical bathing powder that method is prepared is safe and non-toxic, so that beneficiating ingredient dissolution rate is high using the volatility of essential oil, can
Boost metabolism, promote blood circulation, improve sleep, have relaxing tendons and activating collaterals, ward off the cold dehumidifying, it is promoting blood circulation and removing blood stasis the effect of, to wind
Wet, rheumatoid, pain of neck, shoulder, waist and leg have prevention and adjustment effect well.
The present invention solves above-mentioned technical problem by following technological means：
A kind of Chinese yew formula of medicated bath, which is characterized in that include the raw material of following parts by weight：
22~30 parts of taxus chinensis essential oil powder, 10~18 parts of folium artemisiae argyi, 16~23 parts of safflower
6~12 portions of rhizome of chuanxiong, 5~15 portions of monkshood, 5~15 parts of radix cyathulae
3~8 parts of cassia bark, 4~10 parts of the root of Chinese clematis, 2~6 parts of asarum.
Further, the taxus chinensis essential oil powder is the nano particle for being adsorbed with taxus chinensis essential oil, the taxus chinensis essential oil with
The mass ratio of nano particle is 2：8.
Further, the nano particle is mesoporous silicon oxide, the one or two of nano bamboo powdered carbon.
The invention also discloses a kind of preparation methods of Chinese yew medical bathing powder, include the following steps：
Normal disease-free folium artemisiae argyi, safflower, rhizome of chuanxiong, monkshood, radix cyathulae, cassia bark, the root of Chinese clematis, asarum is won to clean cut respectively
Duan Hou, it is dry to water content below 6%, weigh mixing according to components by weight percent, be crushed to grain size and be less than 60 μm, add red bean
China fir essential oil powder is protected from light uniformly mixed, is fitted into envelope in food filter bag with 3g/ bags of specification, after low temperature sterilization disinfection, is packed into bag
It is sealed in pack.
Further, described crush uses air blast ultramicro powder broken.
Further, the preparation method of the taxus chinensis essential oil powder is as follows：
Step 1, pretreatment：The above disease-free branches and leaves of yew of life in 10 years is won, segment is cut into after cleaning, is put into vinegar
12h~20h is impregnated in acid solution, is pulled out after being put into and impregnating 15h~for 24 hours in distilled water, pulls out with distillation water wash 10min, does
It is dry to water content be less than 8%, ultramicro grinding to grain size be less than 80 μm, obtain Chinese yew powder；
Step 2, extraction of essential oil：Chinese yew powder in step 1 is fitted into extraction kettle and carries out supercritical CO2Extraction,
Using absolute ethyl alcohol as entrainer, 40 DEG C~50 DEG C of extraction temperature is set, extracting pressure is 22MPa~23MPa, and extraction time is
1.6h~2.8h, separation temperature are 40 DEG C~50 DEG C, and separating pressure is 6MPa~7MPa, collects volatile oil, obtain Chinese yew essence
Oil；
Step 3, absorption：20g~30g taxus chinensis essential oils are added in the distilled water of every 100mL, add 2g~6g points
Powder and nano particle, ultrasound 35min~50min under 35 DEG C~42 DEG C temperature conditionss, then the glucan of 1.2 times of volumes is added dropwise
Quaternary ammonium salt aqueous solution is centrifuged after ultrasonic 6min~9min, collects sediment, sediment is washed, be dried under reduced pressure after to get
To taxus chinensis essential oil powder.
Further, the concentration of the acetum in the step 1 is 0.1mol/L, and the temperature that acetum impregnates is 26
DEG C~33 DEG C.
Further, the CO in the step 22Flow velocity is 16L/h~22L/h, and extraction is fast with 2.00mL/min after starting
The logical absolute ethyl alcohol of degree.
Further, the dispersant in step 3 is one kind in glyceryl monostearate, vinyl bis-stearamides.
Further, the concentration of the glucan quaternary ammonium salt aqueous solution in step 3 is 0.6g/mL.
Folium artemisiae argyi, safflower, rhizome of chuanxiong, monkshood, radix cyathulae, cassia bark, the root of Chinese clematis, thin has been used in the Chinese yew medical bathing powder of the present invention
Pungent and Chinese yew raw material, wherein, folium artemisiae argyi, warming channel for arresting bleeding, eliminating cold to stop pain, external application removing dampness to stop itchin.Safflower, property pungent-warm and nontoxic, work
Blood promoting menstruation, stasis eliminatings analgesic.Rhizome of chuanxiong, pungent-warm perfume (or spice) is dry, walks without keeping, can go it is scattered, uplink up to top push up；Enter blood system again, downlink can
Up to the sea of blood.Promoting blood circulation effect is extensive, suitable for the various illnesss of congestion blood block；Wind-expelling pain-stopping has sensible qi and blood effect.Monkshood,
Dispelling wind and eliminating dampness, antalgic.Have a pain for wind-cold-dampness arthralgia, arthralgia, trusted subordinate's crymodynia, cold hernia.Radix cyathulae, dispelling stasis of blood and stimulating the menstrual flow,
It is easing joint movement, inducing diuresis for treating strangurtia.Cassia bark, property heat, acrid-sweet flavor, gas are fragrant, nontoxic, have warm stomach dispelling cold, activate blood and relax tendons, coronary circulation-promoting pain-relieving
With the function of antidiarrheal.The root of Chinese clematis has effects that wind-damp dispelling, diuresis, analgesia, degrading the channel, the bone that disappears stalk.Asarum has wind-dispelling, dissipates
Cold, row water, the effect of having one's ideas straightened out, and with air-cooled headache is controlled, nasosinusitis, dentalgia, phlegm and retained fluid cough is inverse, arthralgia pain due to rheumatism etc..
After the branches and leaves of yew that the present invention will pick cleans up, impregnated to remove alkaline Toxic with acetum
Matter, then with distilled water immersion for removing Water-soluble toxic substance, so as to ensure that the security of Chinese yew medical bathing powder.Essential oil
Matter is unstable, readily volatilized to scatter and disappear, and the present invention is using mesoporous silicon oxide and the characterization of adsorption of nano bamboo powdered carbon, in dispersant
Essential oil absorption is scattered in mesoporous silicon oxide and nano bamboo powdered carbon under effect, efficiently solves that essential oil is unstable, period of effectiveness
The problems such as short so that essential oil can more be stablized, and have slow release effect, while utilize the volatile sporadic of essential oil, when bathing
It puts it into hot water, drug dissolution is high, and the beneficiating ingredient of Chinese yew can be enable effectively to discharge, and has preferable treat
Effect.
The Chinese yew medical bathing powder of the present invention is safe and non-toxic, can boost metabolism, promote blood circulation, and improves sleep,
Its principle be the drug ingedient in essential oil distribute and warm stimulation can be by thigmoreceptor and skin receptor, in being transmitted to
Pivot nervous system makes the excitement of maincenter and inhibits orderly.With relaxing tendons and activating collaterals, dehumidifying of warding off the cold, it is promoting blood circulation and removing blood stasis the effect of, to wind
Wet, rheumatoid, pain of neck, shoulder, waist and leg have prevention and adjustment effect well.
Specific embodiment
Below with reference to specific embodiment, the present invention is described in detail：
Embodiment one
The preparation of taxus chinensis essential oil powder：The above complete disease-free branches and leaves of yew of life in 10 years is won, is first cleaned with clear water
After surface impurity, then after being cleaned with acid detergent, 10min is eluted with clear water, then with after distilled water hydro-peening 10min, is cut into small
Section is put into the 0.1mol/L acetums that temperature is 33 DEG C and impregnates 12h, pulls out and is put into distilled water under room temperature after immersion 15h,
It pulls out with water wash 10min is distilled, drying to water content is less than 8%, and ultramicro grinding to grain size is less than 80 μm, obtains Chinese yew
Powder；Chinese yew powder is fitted into extraction kettle and carries out supercritical CO2Extraction using absolute ethyl alcohol as entrainer, sets CO2Flow velocity
For 16L/h, extraction with 2.00mL/min speed leads to absolute ethyl alcohol after starting, wherein, 50 DEG C of extraction temperature, extracting pressure is
22MPa~23MPa, extraction time 1.6h, separation temperature are 40 DEG C, and separating pressure is 6MPa~7MPa, collects volatile oil,
Obtain taxus chinensis essential oil；In the distilled water of every 100mL add in 20g taxus chinensis essential oils, add 2g glyceryl monostearates and
80g mesoporous silicon oxides, the ultrasound 35min under 35 DEG C of temperature conditionss, then be added dropwise 1.2 times of volumes concentration be 0.6g/mL Portugal
Glycan quaternary ammonium salt aqueous solution is centrifuged after ultrasonic 6min, collects sediment, sediment is washed, be dried under reduced pressure after to get to
Taxus chinensis essential oil powder.
The preparation of Chinese yew medical bathing powder：Include the formula material of following components by weight percent, 10 parts of folium artemisiae argyi, 16 parts of safflower, rhizome of chuanxiong
22 parts of 12 parts, 5 parts of monkshood, 10 parts of radix cyathulae, 5 parts of cassia bark, 4 parts of the root of Chinese clematis, 6 parts of asarum and taxus chinensis essential oil powder.It wins normal
Disease-free folium artemisiae argyi, safflower, rhizome of chuanxiong, monkshood, radix cyathulae, cassia bark, the root of Chinese clematis, asarum, first clean surface blot with clear water, then use
Distilled water hydro-peening, after being cut into segment, it is dry to water content below 6%, by weight component weigh respectively folium artemisiae argyi, safflower, rhizome of chuanxiong,
Monkshood, radix cyathulae, cassia bark, the root of Chinese clematis, asarum are crushed to grain size less than 60 μm, add taxus chinensis essential oil powder and are protected from light mixing
It is even, envelope in food filter bag is fitted into 3g/ bags of specification, Low Temperature Plasma Sterilizers progress can be used in low temperature sterilization disinfection
Sterilization is fitted into packaging bag and seals.
Embodiment two
The preparation of taxus chinensis essential oil powder：The above complete disease-free branches and leaves of yew of life in 10 years is won, is first cleaned with clear water
After surface impurity, then after being cleaned with acid detergent, 10min is eluted with clear water, then with after distilled water hydro-peening 10min, is cut into small
Section, it is to impregnate 20h in 26 DEG C of 0.1mol/L acetums to be put into temperature, is pulled out after being put into and being impregnated for 24 hours under room temperature in distilled water,
It pulls out with water wash 10min is distilled, drying to water content is less than 8%, and ultramicro grinding to grain size is less than 80 μm, obtains Chinese yew
Powder；Chinese yew powder is fitted into extraction kettle and carries out supercritical CO2Extraction using absolute ethyl alcohol as entrainer, sets CO2Flow velocity
For 22L/h, extraction with 2.00mL/min speed leads to absolute ethyl alcohol after starting, wherein, 40 DEG C of extraction temperature, extracting pressure is
22MPa~23MPa, extraction time 2.8h, separation temperature are 50 DEG C, and separating pressure is 6MPa~7MPa, collects volatile oil,
Obtain taxus chinensis essential oil；In the distilled water of every 100mL add in 30g taxus chinensis essential oils, add 6g glyceryl monostearates and
120g nano bamboo powdered carbons, the ultrasound 50min under 42 DEG C of temperature conditionss, then be added dropwise 1.2 times of volumes concentration be 0.6g/mL Portugal
Glycan quaternary ammonium salt aqueous solution is centrifuged after ultrasonic 9min, collects sediment, sediment is washed, be dried under reduced pressure after to get to
Taxus chinensis essential oil powder.
The preparation of Chinese yew medical bathing powder：Include the formula material of following components by weight percent, 18 parts of folium artemisiae argyi, 23 parts of safflower, rhizome of chuanxiong
26 parts of 6 parts, 10 parts of monkshood, 5 parts of radix cyathulae, 8 parts of cassia bark, 6 parts of the root of Chinese clematis, 2 parts of asarum and taxus chinensis essential oil powder.Win normal nothing
The folium artemisiae argyi of disease, safflower, rhizome of chuanxiong, monkshood, radix cyathulae, cassia bark, the root of Chinese clematis, asarum first clean surface blot with clear water, then with steaming
Distilled water hydro-peening, after being cut into segment, drying is to water content below 6%, and component weighs folium artemisiae argyi, safflower, rhizome of chuanxiong, river respectively by weight
Crow, radix cyathulae, cassia bark, the root of Chinese clematis, asarum are crushed to grain size less than 60 μm, add taxus chinensis essential oil powder be protected from light it is uniformly mixed,
Envelope in food filter bag is fitted into 3g/ bags of specification, low temperature sterilization disinfection can be used Low Temperature Plasma Sterilizers and sterilize
Disinfection, is fitted into packaging bag and seals.
Embodiment three
The preparation of taxus chinensis essential oil powder：The above complete disease-free branches and leaves of yew of life in 10 years is won, is first cleaned with clear water
After surface impurity, then after being cleaned with acid detergent, 10min is eluted with clear water, then with after distilled water hydro-peening 10min, is cut into small
Section is put into the 0.1mol/L acetums that temperature is 30 DEG C and impregnates 15h, pulls out and is put into distilled water under room temperature after immersion 20h,
It pulls out with water wash 10min is distilled, drying to water content is less than 8%, and ultramicro grinding to grain size is less than 80 μm, obtains Chinese yew
Powder；Chinese yew powder is fitted into extraction kettle and carries out supercritical CO2Extraction using absolute ethyl alcohol as entrainer, sets CO2Flow velocity
For 18L/h, extraction with 2.00mL/min speed leads to absolute ethyl alcohol after starting, wherein, 45 DEG C of extraction temperature, extracting pressure is
22MPa~23MPa, extraction time 2.5h, separation temperature are 45 DEG C, and separating pressure is 6MPa~7MPa, collects volatile oil,
Obtain taxus chinensis essential oil；25g taxus chinensis essential oils are added in the distilled water of every 100mL, add 4g vinyl bis-stearamides
With 100g mesoporous silicon oxides and the mixture of nano bamboo powdered carbon, the ultrasound 40min under 38 DEG C of temperature conditionss, then it is added dropwise 1.2 times
The concentration of volume is the glucan quaternary ammonium salt aqueous solution of 0.6g/mL, is centrifuged after ultrasonic 8min, collects sediment, sediment
It is washed, be dried under reduced pressure after to get to taxus chinensis essential oil powder.
The preparation of Chinese yew medical bathing powder：Include the formula material of following components by weight percent, 15 parts of folium artemisiae argyi, 20 parts of safflower, rhizome of chuanxiong
30 parts of 10 parts, 6 parts of monkshood, 15 parts of radix cyathulae, 3 parts of cassia bark, 5 parts of the root of Chinese clematis, 4 parts of asarum and taxus chinensis essential oil powder.It wins normal
Disease-free folium artemisiae argyi, safflower, rhizome of chuanxiong, monkshood, radix cyathulae, cassia bark, the root of Chinese clematis, asarum, first clean surface blot with clear water, then use
Distilled water hydro-peening, after being cut into segment, it is dry to water content below 6%, by weight component weigh respectively folium artemisiae argyi, safflower, rhizome of chuanxiong,
Monkshood, radix cyathulae, cassia bark, the root of Chinese clematis, asarum are crushed to grain size less than 60 μm, add taxus chinensis essential oil powder and are protected from light mixing
It is even, envelope in food filter bag is fitted into 3g/ bags of specification, Low Temperature Plasma Sterilizers progress can be used in low temperature sterilization disinfection
Sterilization is fitted into packaging bag and seals.
Example IV
The preparation of taxus chinensis essential oil powder：The above complete disease-free branches and leaves of yew of life in 10 years is won, is first cleaned with clear water
After surface impurity, then after being cleaned with acid detergent, 10min is eluted with clear water, then with after distilled water hydro-peening 10min, is cut into small
Section is put into the 0.1mol/L acetums that temperature is 28 DEG C and impregnates 18h, pulls out and is put into distilled water under room temperature after immersion 22h,
It pulls out with water wash 10min is distilled, drying to water content is less than 8%, and ultramicro grinding to grain size is less than 80 μm, obtains Chinese yew
Powder；Chinese yew powder is fitted into extraction kettle and carries out supercritical CO2Extraction using absolute ethyl alcohol as entrainer, sets CO2Flow velocity
For 20L/h, extraction with 2.00mL/min speed leads to absolute ethyl alcohol after starting, wherein, 48 DEG C of extraction temperature, extracting pressure is
22MPa~23MPa, extraction time 2.0h, separation temperature are 44 DEG C, and separating pressure is 6MPa~7MPa, collects volatile oil,
Obtain taxus chinensis essential oil；22g taxus chinensis essential oils are added in the distilled water of every 100mL, add 5g vinyl bis-stearamides
With 88g mesoporous silicon oxides, the ultrasound 45min under 40 DEG C of temperature conditionss, then the concentration of 1.2 times of volumes is added dropwise as 0.6g/mL's
Glucan quaternary ammonium salt aqueous solution is centrifuged after ultrasonic 7min, collects sediment, sediment is washed, be dried under reduced pressure after to get
To taxus chinensis essential oil powder.
The preparation of Chinese yew medical bathing powder：Include the formula material of following components by weight percent, 16 parts of folium artemisiae argyi, 18 parts of safflower, rhizome of chuanxiong
25 parts of 8 parts, 15 parts of monkshood, 8 parts of radix cyathulae, 6 parts of cassia bark, 6 parts of the root of Chinese clematis, 5 parts of asarum and taxus chinensis essential oil powder.Win normal nothing
The folium artemisiae argyi of disease, safflower, rhizome of chuanxiong, monkshood, radix cyathulae, cassia bark, the root of Chinese clematis, asarum first clean surface blot with clear water, then with steaming
Distilled water hydro-peening, after being cut into segment, drying is to water content below 6%, and component weighs folium artemisiae argyi, safflower, rhizome of chuanxiong, river respectively by weight
Crow, radix cyathulae, cassia bark, the root of Chinese clematis, asarum are crushed to grain size less than 60 μm, add taxus chinensis essential oil powder be protected from light it is uniformly mixed,
Envelope in food filter bag is fitted into 3g/ bags of specification, low temperature sterilization disinfection can be used Low Temperature Plasma Sterilizers and sterilize
Disinfection, is fitted into packaging bag and seals.
After the branches and leaves of yew that the present invention will pick cleans up, impregnated to remove alkaline Toxic with acetum
Matter, then with distilled water immersion for removing Water-soluble toxic substance, so as to ensure that the security of Chinese yew medical bathing powder.Essential oil
Matter is unstable, readily volatilized to scatter and disappear, and the present invention is using mesoporous silicon oxide and the characterization of adsorption of nano bamboo powdered carbon, in dispersant
Essential oil absorption is scattered in mesoporous silicon oxide and nano bamboo powdered carbon under effect, efficiently solves that essential oil is unstable, period of effectiveness
The problems such as short so that essential oil can more be stablized, and have slow release effect, while utilize the volatile sporadic of essential oil, when bathing
It puts it into hot water, drug dissolution is high, and the beneficiating ingredient of Chinese yew can be enable effectively to discharge, and has preferable treat
Effect.
The Chinese yew medical bathing powder of the present invention is safe and non-toxic, can boost metabolism, promote blood circulation, and improves sleep,
Its principle be the drug ingedient in essential oil distribute and warm stimulation can be by thigmoreceptor and skin receptor, in being transmitted to
Pivot nervous system makes the excitement of maincenter and inhibits orderly.With relaxing tendons and activating collaterals, dehumidifying of warding off the cold, it is promoting blood circulation and removing blood stasis the effect of, to wind
Wet, rheumatoid, pain of neck, shoulder, waist and leg have prevention and adjustment effect well.
The above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although with reference to preferred embodiment to this hair
It is bright to be described in detail, it will be understood by those of ordinary skill in the art that, it can modify to technical scheme
Or equivalent substitution, without departing from the objective and scope of technical solution of the present invention, the claim in the present invention should all be covered
Among scope.The present invention be not described in detail technology, shape, construction part be known technology.
Claims (10)
1. a kind of Chinese yew formula of medicated bath, which is characterized in that include the raw material of following parts by weight：
22~30 parts of taxus chinensis essential oil powder, 10~18 parts of folium artemisiae argyi, 16~23 parts of safflower
6~12 portions of rhizome of chuanxiong, 5~15 portions of monkshood, 5~15 parts of radix cyathulae
3~8 parts of cassia bark, 4~10 parts of the root of Chinese clematis, 2~6 parts of asarum.
2. a kind of Chinese yew formula of medicated bath according to claim 1, which is characterized in that the taxus chinensis essential oil powder is absorption
There is a nano particle of taxus chinensis essential oil, the mass ratio of the taxus chinensis essential oil and nano particle is 2：8.
3. a kind of Chinese yew formula of medicated bath according to claim 2, which is characterized in that the nano particle is mesoporous dioxy
The one or two of SiClx, nano bamboo powdered carbon.
4. according to a kind of preparation method of any Chinese yew medical bathing powder of claims 1 to 3, which is characterized in that the system
Preparation Method includes the following steps：
It wins normal disease-free folium artemisiae argyi, safflower, rhizome of chuanxiong, monkshood, radix cyathulae, cassia bark, the root of Chinese clematis, asarum and cleans segment respectively
Afterwards, dry to water content below 6%, weigh mixing according to components by weight percent, be crushed to grain size and be less than 60 μm, add Chinese yew
Essential oil powder is protected from light uniformly mixed, is fitted into envelope in food filter bag with 3g/ bags of specification, after low temperature sterilization disinfection, is packed into packaging
It is sealed in bag.
5. the preparation method of a kind of Chinese yew medical bathing powder according to claim 4, which is characterized in that described to crush using gas
Streaming ultramicro grinding.
A kind of 6. preparation method of Chinese yew medical bathing powder according to claim 5, which is characterized in that the taxus chinensis essential oil
The preparation method of powder is as follows：
Step 1, pretreatment：The above disease-free branches and leaves of yew of life in 10 years is won, segment is cut into after cleaning, it is molten to be put into acetic acid
12h~20h is impregnated in liquid, is pulled out after being put into and impregnating 15h~for 24 hours in distilled water, is pulled out with distillation water wash 10min, it is dry extremely
Water content is less than 8%, and ultramicro grinding to grain size is less than 80 μm, obtains Chinese yew powder；
Step 2, extraction of essential oil：Chinese yew powder in step 1 is fitted into extraction kettle and carries out supercritical CO2Extraction, with anhydrous
Ethyl alcohol is entrainer, set 40 DEG C~50 DEG C of extraction temperature, extracting pressure be 22MPa~23MPa, extraction time for 1.6h~
2.8h, separation temperature are 40 DEG C~50 DEG C, and separating pressure is 6MPa~7MPa, collects volatile oil, obtains taxus chinensis essential oil；
Step 3, absorption：20g~30g taxus chinensis essential oils are added in the distilled water of every 100mL, add 2g~6g dispersants
And nano particle, ultrasound 35min~50min under 35 DEG C~42 DEG C temperature conditionss, then the glucan quaternary ammonium of 1.2 times of volumes is added dropwise
Saline solution is centrifuged after ultrasonic 6min~9min, collects sediment, sediment is washed, be dried under reduced pressure after to get to red
Beans China fir essential oil powder.
7. the preparation method of a kind of Chinese yew medical bathing powder according to claim 6, which is characterized in that in the step 1
The concentration of acetum is 0.1mol/L, and the temperature that acetum impregnates is 26 DEG C~33 DEG C.
8. a kind of preparation method of Chinese yew medical bathing powder according to claim 6, it is characterised in that：In the step 2
CO2Flow velocity is 16L/h~22L/h, extracts and leads to absolute ethyl alcohol after starting with 2.00mL/min speed.
9. a kind of preparation method of Chinese yew medical bathing powder according to claim 6, it is characterised in that：In the step 3
Dispersant is glyceryl monostearate, one kind in vinyl bis-stearamides.
10. a kind of preparation method of Chinese yew medical bathing powder according to claim 6, it is characterised in that：In the step 3
Glucan quaternary ammonium salt aqueous solution concentration be 0.6g/mL.
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| CN114984092A (en) * | 2022-07-18 | 2022-09-02 | 江西喜果生物科技有限公司 | Chinese medicinal composition health preserving bath bag based on taxus chinensis raw materials and preparation method thereof |
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Application publication date: 20180529 |