CN108078827B - Alopecia-stopping and hair-growing shampoo and preparation method thereof - Google Patents
Alopecia-stopping and hair-growing shampoo and preparation method thereof Download PDFInfo
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- CN108078827B CN108078827B CN201810014117.3A CN201810014117A CN108078827B CN 108078827 B CN108078827 B CN 108078827B CN 201810014117 A CN201810014117 A CN 201810014117A CN 108078827 B CN108078827 B CN 108078827B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The invention provides a hair loss stopping and hair growth promoting shampoo and a preparation method thereof, the hair loss stopping and hair growth promoting shampoo comprises conventional shampoo and fulvic acid; the conventional shampoo comprises the following components in parts by weight: 0.1-0.5 part of essence, 400-500 parts of deionized water and 100-200 parts of surfactant; the shampoo is added with the fulvic acid, has the effect of treating both symptoms and root causes of alopecia, and has a quicker response than the shampoo containing common traditional Chinese medicine components.
Description
Technical Field
The field relates to the field of washing and caring products, in particular to a hair loss stopping and hair growth promoting shampoo and a preparation method thereof.
Background
Alopecia is a common phenomenon, and is especially common in middle-aged men, people suffering from alopecia increase along with the acceleration of social life rhythm, and the alopecia is also common in many women and teenagers due to the fact that the people are younger and have the effect of eliminating dampness. The common alopecia is mainly caused by the following reasons, namely, nervous alopecia, and alopecia increase frequently occurs when the mental stress is too large. Under the action of mental pressure, the human pilus muscle contracts, the hair stands upright, the vegetative nerve or central nerve is disordered, the hair follicle papilla is changed and is malnourished, so that the hair growth function is inhibited, and the hair enters the resting stage to cause alopecia. Endocrine alopecia, namely hair growth is influenced by various endocrine hormones, so that alopecia is caused frequently when endocrine abnormality occurs; nutritional alopecia, namely the external appearance of physical conditions, the change of hair quality and hair color caused by the malnutrition and the abnormal metabolism of the organism, and even the diffuse alopecia caused by serious malnutrition.
Chinese patent No. 201310372654.2 discloses a preparation method of ginger shampoo, which comprises adding gingerol component into shampoo, and has effects of cleaning hair, removing dandruff, preventing alopecia, promoting blood circulation of head, strengthening hairy root, and protecting hair. However, the ginger hair growth is not suitable for all people, the ginger mainly plays a role in stimulating local skin vasodilatation and hyperemia in the hair growth for treating alopecia, so that the local blood supply is increased, the nutrition of hair follicles is improved, the hair growth is promoted, and the ginger mainly has a better effect in treating seborrheic alopecia. However, ginger belongs to a traditional Chinese medicine component, has slow effect and can achieve good effect only by long-term continuous use.
Disclosure of Invention
In order to solve the technical problems, the invention provides the hair loss stopping and hair growth promoting shampoo and the preparation method thereof, and the addition of fulvic acid plays a role in treating both symptoms and root causes of alopecia, and has a quicker response than the shampoo with common traditional Chinese medicine components.
The technical scheme adopted by the invention for solving the technical problems is as follows:
the first technical scheme is as follows:
a shampoo for preventing alopecia and promoting hair growth comprises conventional shampoo and fulvic acid; the conventional shampoo
Comprises the following components in parts by weight: 0.1-0.5 part of essence, 400-500 parts of deionized water and 100-200 parts of surfactant.
As a further improvement of the invention, the fulvic acid is mineral source fulvic acid extracted from minerals such as lignite, weathered coal, peat and the like; the content is 0.1 to 1 part by weight.
The fulvic acid accounts for 0.1-1 part by weight.
As a further improvement of the invention, the traditional Chinese medicine composition also comprises traditional Chinese medicine extracts.
As a further improvement of the invention, the traditional Chinese medicine extract comprises the following components in parts by weight: 0.2 to 1
The traditional Chinese medicine composition comprises cacumen biotae tincture, 0.1-1 part of ginger extract and 0.2-1 part of mulberry leaf extract.
As a further improvement of the present invention, the surfactant is an amino acid surfactant.
As a further improvement of the invention, the surfactant is sodium cocoanut oil amino acid salt.
The mulberry leaf extract is prepared by a water extraction method, and the specific preparation steps are as follows:
a) carrying out ultrasonic strengthening treatment;
b) stirring with hot water and extracting;
c) filtering, repeatedly extracting the residue with hot water under stirring for 1-2 times, centrifuging to remove impurities to obtain supernatant;
d) concentrating the supernatant with film until the content of soluble solid reaches 50%, and sealing for storage. (see Chinese patent, a mulberry leaf extract, and a preparation method and application thereof, patent No. 200710027588. X)
The ginger extract is prepared by an ethanol extraction method, and the specific steps are shown in Chinese national patent-a high-efficiency extract
A method for preparing rhizoma Zingiberis recens extract with the assistance of circulation pulse ultrasonic wave is disclosed in patent No. 201410129624.3.
The second technical scheme is as follows:
the preparation method of the shampoo for preventing alopecia and promoting hair growth is characterized by comprising the following steps:
(1) mixing the cacumen biotae tincture, the ginger extract and the mulberry leaf extract, and stirring by using a temperature control stirrer at the stirring speed of 200-; the temperature control stirrer is a planetary stirrer of Tai Jie brand, and the model is TXJ-0.5;
(2) adding deionized water during stirring, setting the temperature of the stirrer at 50 ℃, and heating the mixed solution;
(3) uniformly stirring, adding fulvic acid, and keeping the temperature at 50-60 ℃;
(4) adding essence and a surfactant, dissolving and stirring, starting an ultrasonic oscillator, and keeping the temperature at 50-60 ℃;
(5) taking the mixed solution out to a container, and cooling to room temperature;
(6) and (5) disinfecting and sterilizing.
The invention has the following technical effects:
the composition is added with the fulvic acid, and the fulvic acid contains carboxyl and phenolic hydroxyl, so that the composition has natural weak acidity, can improve scalp environment and balance the pH value of scalp; fulvic acid is a hydrophilic colloid, has strong water absorption capacity, can prevent scalp moisture evaporation, keep water and oil balance and reduce sebum secretion, thereby optimizing the growth environment of hair and playing a role in preventing alopecia; the benzo-alpha pyrone in the fulvic acid has the anti-inflammatory effect and can inhibit the growth and reproduction of fungi inside and outside the scalp, so that alopecia can be fundamentally and effectively prevented and hair can be grown, and meanwhile, the addition of the fulvic acid can effectively improve the growth environment of hair roots, improve the quality of scalp cells, has the efficacy of removing dandruff and relieving itching, and further prevents the generation of alopecia; fulvic acid contains a plurality of oxygen-containing functional groups which are active groups, and the active groups can activate subcutaneous hair follicle tissues, accelerate the metabolism of the subcutaneous hair follicle tissues and promote the hair proliferation;
the invention also adds traditional Chinese medicine extracts, namely the oriental arborvitae tincture, the ginger extract and the mulberry leaf extract, and the gingerol component in the ginger extract, not only can clean hair, remove dandruff and prevent alopecia, but also can promote blood circulation of head, strengthen hairy roots and protect the roots and the hair; the mulberry leaves contain active ingredients such as alkaloid, phytosterol and the like, have a nourishing effect on the scalp, and can help the hair to better absorb nutrition, so that the effects of hair strengthening and hair nourishing are achieved; the cacumen biotae tincture has good effects of stopping bleeding and removing damp-heat, has very obvious effects of regulating blood circulation and removing blood heat, and the root of alopecia is caused by kidney deficiency and body dysfunction, and can be used for fundamentally fixing hair and growing hair by adding the cacumen biotae tincture; meanwhile, the fulvic acid is a colloid, has positive and negative charges, can absorb anions and cations, can preserve nutrients in the traditional Chinese medicine extract through a complexing reaction, and forms a protective film rich in nutrients and water on the surface of the scalp, so that on one hand, the loss of water and nutrients is prevented, on the other hand, the nutrients and water can be continuously and slowly released to the scalp to continuously nourish the scalp, and thus, the effects of preventing alopecia and growing hair are achieved; the invention has simple process, safety and reliability, no toxic or side effect and can achieve the purpose of preventing alopecia and growing hair for a long time.
Detailed Description
The technical solution of the present invention will be described in further detail with reference to examples.
A hair loss stopping and hair growth promoting shampoo is prepared by the following steps: mixing the cacumen Platycladi tincture, rhizoma Zingiberis recens extract and folium Mori extract, and stirring with a temperature-controlled stirrer at a rotation speed of 300 r/min; the temperature control stirrer is a planetary stirrer of Tai Jie brand, and the model is TXJ-0.5; slowly adding deionized water in the stirring process, setting the temperature of the stirrer to be 50 ℃, and heating the mixed solution; uniformly stirring, adding fulvic acid, and keeping the temperature at 50-60 ℃; adding essence and coconut oil amino acid sodium salt, dissolving and stirring, starting an ultrasonic oscillator, and keeping the temperature at 50-60 ℃; taking the mixed solution out to a container, and cooling to room temperature; and (5) disinfecting and sterilizing. The weight of each component of examples 1 to 4 and comparative examples 1 to 4 is shown in Table 1.
TABLE 1 ingredient ratio table
The quality of the shampoos described in examples 1-4 and comparative examples 1-4 was tested, and the hygiene indexes thereof are shown in table 2; the sensory physical and chemical indexes are shown in Table 3.
TABLE 2 sanitation index
TABLE 3 sensory, physicochemical indices
As can be seen from tables 2 and 3, the hygiene indexes and physicochemical sensory indexes of the shampoos described in examples 1 to 4 and comparative examples 1 to 4 all meet the industry standards, and the inspection methods thereof are conventional inspection methods specified in the industry, which are common knowledge that a person skilled in the art should know, and are not described herein again.
The shampoo disclosed by the invention is subjected to an in-vitro anti-hair loss test, and the test method comprises the following steps:
270 volunteers are selected to participate in the test, the age distribution is 25-45 years old, the volunteers are divided into 9 groups, each group is uniformly distributed according to the age and the gender, no other diseases which can influence the observation result exist in the volunteers, the test time is 45 days, and other hair washing and protecting products are not used in the test period; the test time is 9 months and 1 day to 10.14 days, and 9 groups of volunteers respectively try out examples 1 to 4 and comparative examples 1 to 4 and a commercially available common shampoo; the frequency of shampooing of volunteers was once every two days, the shampooing time was 7-9 am, the volunteers combed hair three times a day, in the morning, in the evening, and the number of hair loss was collected, and the total number of hair loss was recorded, and the whole number was taken after the average value was found, and after the test for 45 days, the statistical data was recorded in table 4.
TABLE 4 statistical Table of total number of missing hairs
As can be seen from Table 4, the shampoo provided by the invention has a remarkable anti-hair loss effect, the anti-hair loss effect is positively correlated with the content of fulvic acid within the specified addition range of fulvic acid, and the anti-hair loss effect is better than that of common commercial shampoos.
The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.
Claims (5)
1. A shampoo for preventing alopecia and promoting hair growth comprises conventional shampoo, and is characterized by also comprising fulvic acid; the conventional shampoo comprises the following components in parts by weight: 0.1-0.5 part of essence, 400-500 parts of deionized water, 100-200 parts of surfactant and traditional Chinese medicine extract; wherein the traditional Chinese medicine extract comprises the following components in parts by weight: 0.2-1 part of cacumen biotae tincture, 0.1-1 part of ginger extract and 0.2-1 part of mulberry leaf extract.
2. The shampoo for preventing alopecia and promoting hair growth as claimed in claim 1, wherein the fulvic acid is mineral fulvic acid, and the content of the fulvic acid is 0.1-1 part by weight.
3. The shampoo for stopping hair loss and promoting hair growth as claimed in claim 2, wherein the surfactant is an amino acid surfactant.
4. The shampoo for stopping hair loss and promoting hair growth as claimed in claim 3, wherein the surfactant is sodium cocoanut oil amino acid salt.
5. The preparation method of the shampoo for stopping hair loss and promoting hair growth as claimed in claim 4, which comprises the following steps:
(1) mixing the cacumen biotae tincture, the ginger extract and the mulberry leaf extract, and stirring by using a temperature control stirrer at the stirring speed of 200-;
(2) adding deionized water in the stirring process, and setting the temperature of the stirrer to be 50 ℃;
(3) uniformly stirring, adding fulvic acid, and keeping the temperature at 50-60 ℃;
(4) adding essence and a surfactant, dissolving and stirring, starting an ultrasonic oscillator, and keeping the temperature at 50-60 ℃;
(5) taking the mixed solution out to a container, and cooling to room temperature;
(6) and (5) disinfecting and sterilizing.
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CN110917073A (en) * | 2019-12-19 | 2020-03-27 | 陕西科技大学 | Fulvic acid moisturizing and anti-dandruff shampoo and preparation method thereof |
KR102255269B1 (en) * | 2020-03-24 | 2021-05-24 | 이태옥 | Method for manufacturing scalp care soap |
Citations (3)
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CN1568929A (en) * | 2003-07-16 | 2005-01-26 | 刘南凯 | Cosmetics containing humic acid and application of humic acid in cosmetics |
CN102871885A (en) * | 2012-10-18 | 2013-01-16 | 昆明理工大学 | Pilatory and application of pilatory |
CN104069042A (en) * | 2014-07-23 | 2014-10-01 | 李雪萍 | Biochemical fulvic acid (BFA) cosmetic preparation |
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US20070212434A1 (en) * | 2006-03-07 | 2007-09-13 | Day Kenneth S | Compositions and methods for human use containing fulvic acid |
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CN1568929A (en) * | 2003-07-16 | 2005-01-26 | 刘南凯 | Cosmetics containing humic acid and application of humic acid in cosmetics |
CN102871885A (en) * | 2012-10-18 | 2013-01-16 | 昆明理工大学 | Pilatory and application of pilatory |
CN104069042A (en) * | 2014-07-23 | 2014-10-01 | 李雪萍 | Biochemical fulvic acid (BFA) cosmetic preparation |
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