CN108048639B - A method of improving graphitizable steel plate stamping and forming performance - Google Patents

A method of improving graphitizable steel plate stamping and forming performance Download PDF

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Publication number
CN108048639B
CN108048639B CN201711315901.XA CN201711315901A CN108048639B CN 108048639 B CN108048639 B CN 108048639B CN 201711315901 A CN201711315901 A CN 201711315901A CN 108048639 B CN108048639 B CN 108048639B
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China
Prior art keywords
steel plate
graphitization
ferrite
stamping
rolling
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CN201711315901.XA
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Chinese (zh)
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CN108048639A (en
Inventor
张永军
张鹏程
王九花
于文杰
韩静涛
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University of Science and Technology Beijing USTB
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University of Science and Technology Beijing USTB
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    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/02Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips
    • C21D8/04Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips to produce plates or strips for deep-drawing
    • C21D8/0421Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips to produce plates or strips for deep-drawing characterised by the working steps
    • C21D8/0431Warm rolling
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/02Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips
    • C21D8/04Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips to produce plates or strips for deep-drawing
    • C21D8/0447Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips to produce plates or strips for deep-drawing characterised by the heat treatment
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/02Ferrous alloys, e.g. steel alloys containing silicon
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/04Ferrous alloys, e.g. steel alloys containing manganese
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D2211/00Microstructure comprising significant phases
    • C21D2211/005Ferrite
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D2211/00Microstructure comprising significant phases
    • C21D2211/006Graphite

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Heat Treatment Of Steel (AREA)
  • Heat Treatment Of Sheet Steel (AREA)

Abstract

A method of graphitizable steel plate stamping and forming performance is improved, steel material processing technique field is belonged to.It is characterized in that carrying out the warm deformation of Dynamic Recrystallization of Ferrite to the graphitization steel plate after graphitization processing using warm deformation technology, the stamping formabilily of graphitization steel plate is improved by controlling refinement and the homogenization of ferrite dynamic crystal grain.Specific method is that the graphitization steel plate Jing Guo graphitization processing is heated to 550~710 DEG C, and the flat rolling that drafts is 8~15% is carried out after samming, is air-cooled to room temperature after rolling.The graphitization steel plate handled using this method, ferrite crystal grain are fined and uniformly, and stamping formabilily is good, yield tensile ratio≤0.56, strain hardening exponent >=0.25, in-plane anisotropy≤0.15.

Description

A method of improving graphitizable steel plate stamping and forming performance
Technical field
The present invention relates to a kind of methods for improving graphitizable steel plate stamping and forming performance, belong to steel material processing technology neck Domain.
Background technique
The preparation flow of graphitization steel plate mainly includes the techniques mistakes such as steel-making, casting, hot rolling or cold rolling, graphitization processing Journey.Wherein, steel plate shows higher stamping formabilily after graphitization processing, has lower yield tensile ratio, can soften To the level as mild steel.
Steel plate through graphitization processing, tissue are mainly made of ferrite+graphite.However, due to graphitization processing mistake The time that journey needs is longer, and the ferritic structure often led in steel plate is coarse, and uneven, and such tissue characteristic is difficult Make steel plate that there is good stamping formabilily.
Therefore, coarse to solve ferrite crystal grain present in existing graphitization processing method, and non-uniform problem, this Invention is proposed using warm deformation technology, and the temperature of Dynamic Recrystallization of Ferrite is carried out to the graphitization steel plate after graphitization processing Roll, with realize ferrite crystal grain refinement, homogenization, for it is subsequent it is stamping good Preparedness Directorate is provided, further to mention Its high stamping formabilily.
Summary of the invention
Graphitization steel plate after graphitization processing, stamping formabilily with higher.Due to graphitization processing process In easily cause ferrite crystal grain coarse, and it is uneven.Therefore, in order to solve this problem, the present invention is based on warm deformations can make iron Ferritic recrystallization, to make fetrite grain refinement and homogenization, propose one kind can further improve graphitization steel plate strike out The method of shape performance.
The present invention is realized by following technical measures:
A method of improving graphitizable steel plate stamping and forming performance, it is characterised in that warm deformation technology is utilized, to graphite Change treated graphitization steel plate carry out Dynamic Recrystallization of Ferrite warm deformation, with realize ferrite crystal grain refinement and uniformly Change.Specific method is that the graphitization steel plate Jing Guo graphitization processing is heated to 550~710 DEG C, and drafts is carried out after samming For 8~15% flat rolling, room temperature is air-cooled to after rolling.The graphitization processing, refers to and in temperature is to graphitization steel plate 8~16 hours isothermals are carried out within the scope of 600 DEG C~Ac1, and cool to a heat treatment process of room temperature with the furnace.This method is main Being to C content is 0.30~1.20%, Si content is 0.60~1.60%, Mn content is 0.20~0.50%, P content≤ 0.015%, S content≤0.015%, the graphitization steel plate that remaining content is Fe carry out.
Beneficial effects of the present invention:
The graphitization steel plate handled using this method, it can be subsequent punching that ferrite crystal grain, which is fined and homogenizes, Pressing formation provides good Preparedness Directorate, hence it is evident that improves the stamping formabilily of graphitization steel plate, yield tensile ratio≤0.56, strain Hardenability value >=0.25, in-plane anisotropy≤0.15.
Specific embodiment
After now the embodiment of the present invention is specifically described in.
Technical solution of the present invention is described further with reference to embodiments.Embodiment is merely to illustrate the present invention, Rather than limit the present invention in any way.
Embodiment 1
The present embodiment selection C content is 0.86%, Si content is 0.98%, Mn content is 0.36%, P content is 0.008%, the graphitization steel plate for the 2.3mm thickness that S content is 0.015%, remaining content is Fe, through 680 DEG C, 10 hours etc. Temperature, after being furnace-cooled to the graphitization processing of room temperature, tissue is mainly made of ferrite and graphite, but ferrite crystal grain is coarse, and Unevenly.The steel plate is packed into heating furnace at room temperature, is come out of the stove after being graphitized steel plate and being heated to 630 DEG C of sammings, is started Warm-rolling, drafts 0.3mm, i.e., 13% are carried out on flat roll mill to it;Finishing temperature is not less than 550 DEG C;It is air-cooled to after rolling Room temperature.
Metallographic Analysis and mechanical test are carried out to the graphitization steel plate Jing Guo above-mentioned processing, the results show that its institutional framework In observe ferrite crystal grain it is uniform, radial dimension is mostly the yield tensile ratio σ in 15~18 μ mssbFor 0.52, strain hardening exponentIt is 0.28, in-plane anisotropy △ r is 0.13.
Embodiment 2
The present embodiment selection C content is 1.16%, Si content is 1.38%, Mn content is 0.42%, P content is 0.009%, the graphitization steel plate for the 3.3mm thickness that S content is 0.008%, remaining content is Fe, through 700 DEG C, 12 hours isothermals, After being furnace-cooled to the graphitization processing of room temperature, tissue is mainly made of ferrite and graphite, and same ferrite crystal grain is coarse, and not Uniformly.The steel plate is packed into heating furnace at room temperature, is come out of the stove after being graphitized steel plate and being heated to 660 DEG C of sammings, is started flat Warm-rolling, drafts 0.3mm, i.e., 9.1% are carried out on roller mill to it;Finishing temperature is not less than 550 DEG C;Room is air-cooled to after rolling Temperature.
Metallographic Analysis and mechanical test are carried out to the graphitization steel plate Jing Guo above-mentioned processing, the results show that its institutional framework In observe ferrite crystal grain it is uniform, radial dimension is mostly the yield tensile ratio σ in 19~21 μ mssbFor 0.55, strain hardening exponentIt is 0.26, in-plane anisotropy △ r is 0.15.
By embodiment as it can be seen that before graphitizable steel plate stamping and forming, warm-rolling deformation is carried out to it, it can be ensured that steel plate tool There is a good stamping formabilily, i.e. warm-rolling deformation stamping can provide good Preparedness Directorate to be rear.

Claims (1)

1. a kind of method for improving graphitizable steel plate stamping and forming performance, it is characterised in that warm deformation technology is utilized, to graphitization Treated graphitization steel plate carry out Dynamic Recrystallization of Ferrite warm deformation, with realize ferrite crystal grain refinement and uniformly Change;
The graphitization processing refers to that graphitization steel plate be to carry out 8~16 hours etc. within the scope of 600 DEG C~Ac1 in temperature Temperature, and cool to a heat treatment process of room temperature with the furnace;
The main chemical compositions and its mass percentage content of the graphitization steel plate are as follows: C:0.86~1.20%;Si:0.60~ 1.60%;Mn:0.20~0.42%;P≤0.015%;S :≤0.015%;Remaining content is Fe;
Specific method is that the graphitization steel plate Jing Guo graphitization processing is heated to 550~710 DEG C, and drafts is carried out after samming For 8~15% flat rolling, room temperature is air-cooled to after rolling;
Yield tensile ratio≤0.56 of steel plate, strain hardening exponent >=0.25, in-plane anisotropy≤0.15 are graphitized after warm deformation.
CN201711315901.XA 2017-12-12 2017-12-12 A method of improving graphitizable steel plate stamping and forming performance Active CN108048639B (en)

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CN108048639B true CN108048639B (en) 2019-07-12

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CN111189701B (en) * 2020-01-08 2021-09-17 吉林大学 Method for measuring large-strain compression hardening curve of metal hyperbolic sample
CN111471844B (en) * 2020-04-02 2021-03-05 北京科技大学 Treatment method for realizing superplasticity of graphitized steel

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CN101899555B (en) * 2010-08-04 2011-12-14 武汉钢铁(集团)公司 Production method of graphitized free-machining steel
KR101657790B1 (en) * 2014-12-09 2016-09-20 주식회사 포스코 Steel material for graphitization and graphite steel with excellent machinability and cold forging characteristic
CN106048179B (en) * 2016-07-15 2017-09-15 北京科技大学 A kind of preparation method of graphitization hot rolled steel plate
CN106917044B (en) * 2017-03-03 2019-02-26 北京科技大学 A kind of stamping preparation method with graphitization cold rolling high carbon steel sheet

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