CN108048508B - 一种利用魔芋制备低聚甘露糖的方法 - Google Patents
一种利用魔芋制备低聚甘露糖的方法 Download PDFInfo
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- CN108048508B CN108048508B CN201810094246.8A CN201810094246A CN108048508B CN 108048508 B CN108048508 B CN 108048508B CN 201810094246 A CN201810094246 A CN 201810094246A CN 108048508 B CN108048508 B CN 108048508B
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- 229920002752 Konjac Polymers 0.000 title claims abstract description 93
- 235000010485 konjac Nutrition 0.000 title claims abstract description 90
- 238000000034 method Methods 0.000 title claims abstract description 30
- WQZGKKKJIJFFOK-QTVWNMPRSA-N D-mannopyranose Chemical compound OC[C@H]1OC(O)[C@@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-QTVWNMPRSA-N 0.000 title claims abstract description 29
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 54
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 43
- 239000007788 liquid Substances 0.000 claims abstract description 35
- 239000002994 raw material Substances 0.000 claims abstract description 31
- 241001312219 Amorphophallus konjac Species 0.000 claims abstract description 28
- 235000001206 Amorphophallus rivieri Nutrition 0.000 claims abstract description 28
- 238000001694 spray drying Methods 0.000 claims abstract description 28
- 108090000790 Enzymes Proteins 0.000 claims abstract description 21
- 102000004190 Enzymes Human genes 0.000 claims abstract description 21
- 229940088598 enzyme Drugs 0.000 claims abstract description 21
- 238000004537 pulping Methods 0.000 claims abstract description 21
- 229940059442 hemicellulase Drugs 0.000 claims abstract description 19
- 108010002430 hemicellulase Proteins 0.000 claims abstract description 19
- 239000002002 slurry Substances 0.000 claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 238000002360 preparation method Methods 0.000 claims abstract description 15
- 238000002156 mixing Methods 0.000 claims abstract description 11
- 238000003756 stirring Methods 0.000 claims abstract description 11
- 230000002255 enzymatic effect Effects 0.000 claims abstract description 10
- 239000000413 hydrolysate Substances 0.000 claims abstract description 10
- 230000009849 deactivation Effects 0.000 claims abstract description 7
- 230000007062 hydrolysis Effects 0.000 claims abstract description 7
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 7
- 230000001105 regulatory effect Effects 0.000 claims description 26
- 238000001556 precipitation Methods 0.000 claims description 17
- 230000008569 process Effects 0.000 claims description 11
- HRZFUMHJMZEROT-UHFFFAOYSA-L sodium disulfite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])(=O)=O HRZFUMHJMZEROT-UHFFFAOYSA-L 0.000 claims description 11
- 229940001584 sodium metabisulfite Drugs 0.000 claims description 11
- 235000010262 sodium metabisulphite Nutrition 0.000 claims description 11
- 238000004140 cleaning Methods 0.000 claims description 9
- 238000005520 cutting process Methods 0.000 claims description 9
- 238000005119 centrifugation Methods 0.000 claims description 2
- 230000008961 swelling Effects 0.000 abstract description 5
- 238000001035 drying Methods 0.000 abstract description 3
- 238000005265 energy consumption Methods 0.000 abstract description 3
- 238000000227 grinding Methods 0.000 abstract description 3
- 230000008901 benefit Effects 0.000 abstract description 2
- 238000001879 gelation Methods 0.000 abstract description 2
- 230000001376 precipitating effect Effects 0.000 abstract 1
- 239000000252 konjac Substances 0.000 description 25
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 18
- 230000000694 effects Effects 0.000 description 8
- 230000003301 hydrolyzing effect Effects 0.000 description 7
- 230000000415 inactivating effect Effects 0.000 description 7
- 238000006116 polymerization reaction Methods 0.000 description 7
- 238000012545 processing Methods 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 5
- 239000000047 product Substances 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 3
- 241000186660 Lactobacillus Species 0.000 description 2
- 229920000057 Mannan Polymers 0.000 description 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 229940039696 lactobacillus Drugs 0.000 description 2
- 150000003272 mannan oligosaccharides Chemical class 0.000 description 2
- -1 mannose trisaccharide Chemical class 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- LUEWUZLMQUOBSB-FSKGGBMCSA-N (2s,3s,4s,5s,6r)-2-[(2r,3s,4r,5r,6s)-6-[(2r,3s,4r,5s,6s)-4,5-dihydroxy-2-(hydroxymethyl)-6-[(2r,4r,5s,6r)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-4,5-dihydroxy-2-(hydroxymethyl)oxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound O[C@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@@H](O[C@@H]2[C@H](O[C@@H](OC3[C@H](O[C@@H](O)[C@@H](O)[C@H]3O)CO)[C@@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O LUEWUZLMQUOBSB-FSKGGBMCSA-N 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 241000186000 Bifidobacterium Species 0.000 description 1
- 241000193468 Clostridium perfringens Species 0.000 description 1
- 241000588914 Enterobacter Species 0.000 description 1
- 241000194033 Enterococcus Species 0.000 description 1
- 229920002581 Glucomannan Polymers 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 229920002488 Hemicellulose Polymers 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 235000013527 bean curd Nutrition 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000431 effect on proliferation Effects 0.000 description 1
- 238000012869 ethanol precipitation Methods 0.000 description 1
- 239000000834 fixative Substances 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- 210000001035 gastrointestinal tract Anatomy 0.000 description 1
- 229940046240 glucomannan Drugs 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 229920001542 oligosaccharide Polymers 0.000 description 1
- 150000002482 oligosaccharides Chemical class 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 235000013406 prebiotics Nutrition 0.000 description 1
- 239000006041 probiotic Substances 0.000 description 1
- 235000018291 probiotics Nutrition 0.000 description 1
- 230000035755 proliferation Effects 0.000 description 1
- 239000008213 purified water Substances 0.000 description 1
- 230000002040 relaxant effect Effects 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/14—Preparation of compounds containing saccharide radicals produced by the action of a carbohydrase (EC 3.2.x), e.g. by alpha-amylase, e.g. by cellulase, hemicellulase
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/04—Polysaccharides, i.e. compounds containing more than five saccharide radicals attached to each other by glycosidic bonds
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/12—Disaccharides
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P2203/00—Fermentation products obtained from optionally pretreated or hydrolyzed cellulosic or lignocellulosic material as the carbon source
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Biotechnology (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Preparation Of Fruits And Vegetables (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
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CN114831246B (zh) * | 2022-04-08 | 2023-04-28 | 江南大学 | 一种黄珠芽魔芋碱诱导凝胶防褐变的方法 |
Citations (7)
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CN102187986A (zh) * | 2010-03-03 | 2011-09-21 | 陕西理工学院 | 低硫魔芋粉快速加工方法 |
CN103349244A (zh) * | 2013-07-02 | 2013-10-16 | 陕西理工学院 | 一种魔芋精粉无硫或低硫湿法加工方法 |
CN103382493A (zh) * | 2012-05-03 | 2013-11-06 | 桂林微邦生物技术有限公司 | 一种快速生产高纯度低聚甘露糖的方法 |
CN104561187A (zh) * | 2013-10-22 | 2015-04-29 | 李金成 | 一种面点食品辅料的低聚甘露糖配制方法及应用 |
CN105063128A (zh) * | 2015-07-16 | 2015-11-18 | 江南大学 | 一种调节肠道菌群的低分子量魔芋低聚糖的制备方法 |
CN105166765A (zh) * | 2015-07-22 | 2015-12-23 | 江南大学 | 一种甘露寡糖合生元肠溶微胶囊的制备方法 |
CN106306731A (zh) * | 2015-06-16 | 2017-01-11 | 陕西理工学院 | 一种魔芋精粉无硫湿法综合加工方法 |
-
2018
- 2018-01-31 CN CN201810094246.8A patent/CN108048508B/zh active Active
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102187986A (zh) * | 2010-03-03 | 2011-09-21 | 陕西理工学院 | 低硫魔芋粉快速加工方法 |
CN103382493A (zh) * | 2012-05-03 | 2013-11-06 | 桂林微邦生物技术有限公司 | 一种快速生产高纯度低聚甘露糖的方法 |
CN103349244A (zh) * | 2013-07-02 | 2013-10-16 | 陕西理工学院 | 一种魔芋精粉无硫或低硫湿法加工方法 |
CN104561187A (zh) * | 2013-10-22 | 2015-04-29 | 李金成 | 一种面点食品辅料的低聚甘露糖配制方法及应用 |
CN106306731A (zh) * | 2015-06-16 | 2017-01-11 | 陕西理工学院 | 一种魔芋精粉无硫湿法综合加工方法 |
CN105063128A (zh) * | 2015-07-16 | 2015-11-18 | 江南大学 | 一种调节肠道菌群的低分子量魔芋低聚糖的制备方法 |
CN105166765A (zh) * | 2015-07-22 | 2015-12-23 | 江南大学 | 一种甘露寡糖合生元肠溶微胶囊的制备方法 |
Non-Patent Citations (3)
Title |
---|
纤维素酶制备魔芋葡甘低聚糖;张迎庆;《吉首大学学报(自然科学版)》;20030930;第24卷(第3期);全文 * |
酸酶结合法水解魔芋葡甘露聚糖工艺研究;陶兴无;《武汉工业学院学报》;20050930;第24卷(第3期);摘要,第1页左栏第1段-第4页右栏第1段 * |
魔芋低聚糖生产制备工艺优化研究;党娅;《食品工业科技》;20151231(第8期);摘要,第251页左栏第1段-第255页右栏第4段 * |
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