CN108030709A - A kind of facial ointment and preparation method thereof - Google Patents
A kind of facial ointment and preparation method thereof Download PDFInfo
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- CN108030709A CN108030709A CN201711347967.7A CN201711347967A CN108030709A CN 108030709 A CN108030709 A CN 108030709A CN 201711347967 A CN201711347967 A CN 201711347967A CN 108030709 A CN108030709 A CN 108030709A
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- ointment
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/895—Polysiloxanes containing silicon bound to unsaturated aliphatic groups, e.g. vinyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
The present invention provides a kind of facial ointment and preparation method thereof, the facial ointment includes by mass percentage：Silicon polymer 30.0 50.0%, emulsifying agent 1.0 5.0%, grease 20.0 40.0% and wax 5.0 10.0%, surplus is deionized water, and facial ointment of the invention contains silicon polymer, improves the lightness of product and salubrious degree so that product easily absorbs；Silicon polymer is rationally compounded with emulsifying agent, improves the stability of product.
Description
Technical field
The invention belongs to cosmetic field, is related to a kind of facial ointment and preparation method thereof, more particularly to a kind of siliceous poly-
Facial ointment of compound and preparation method thereof.
Background technology
In recent years, the formula of skin-protection product is gradually diversified, and the gradual Focus of performance, meets different type, not the same year
Age, the consumer demand of different levels.Ointment type skin care item are a kind of oil being made of grease, wax class, essence and preservative
Property product, it is not soluble in water, there is lubrication, skin softening, moisturizing, because it is convenient for carrying, using is subject to consumer's at any time
Favor.However, the shortcomings that ointment type product is that skin sense is greasy, absorbability is poor, and effect is single, is mainly used in lip treatment at present
Product.
106890113 A of CN disclose a kind of transparent skin-care lipstick, and the lipstick includes with the following group by weight percentage
Point：12.0% ceresine, 18.0% beeswax, 6.0% microwax, 20.0% albolene, 10.0% cocoa butter,
15.0% white oil, 5.0% olive oil, 10.0% isopropyl myristate, 2.0% lanolin fatty acid, 2.0% poly- second two
Alcohol wool acid esters and suitable essence.But lipstick quality is thick and heavy, and it cannot be used for nursing face skin.
106361667 A of CN disclose a kind of snake oil ointment, and the snake oil ointment includes the raw material of following parts by weight：Snake oil
1-5 parts of 10-20 parts, hyaluronic acid or its sodium salt and 1-10 parts of vegetables and fruits, have smoothing wrinkle, cracking resistance, moisturizing, nourishes rough skin, raising
The functions such as elasticity of skin, but quality is thick and heavy, glutinous soapy feeling is strong, skin sense is poor.
Therefore it provides a kind of salubrious moisturizing, the facial ointment for moistening brilliant white, desalinating wrinkle, have in daily cosmetics field
There are important meaning and vast market prospect.
The content of the invention
For overcome the deficiencies in the prior art, the present invention provides a kind of facial ointment and preparation method thereof, the skin care oil
Cream is rich in silicon polymer, silicon polymer and emulsifying agent mating reaction, is a product for having concurrently and nourishing with salubrious skin-care effect.
For this purpose, the present invention uses following technical scheme：
In a first aspect, the present invention provides a kind of facial ointment, the facial ointment includes by mass percentage：
In the present invention, silicon polymer is added with facial ointment, improves the lightness of product and salubrious degree so that production
Product easily absorb, while silicon polymer is rationally compounded with emulsifying agent, synergistic effect, improve the height temperature stability of facial ointment.
Preferably, mass percent of the silicon polymer in the facial ointment is 30.0-50.0%, such as can be with
30%, 31%, 32%, 33%, 34%, 35%, 36%, 37%, 38%, 39%, 40%, 41%, 42%, 43%, 44%,
45%th, 46%, 47%, 48%, 49% or 50%, it is preferably 40.0-50.0%, more preferably 50.0%.
Preferably, mass percent of the emulsifying agent in the facial ointment is 1.0-5.0%, such as can be
1%th, 2%, 3%, 4% or 5%, it is preferably 2.0-4.0%, more preferably 2.0%.
Preferably, mass percent of the grease in the facial ointment is 20.0-40.0%, such as can be
20%th, 21%, 22%, 23%, 24%, 25%, 26%, 27%, 28%, 29%, 30%, 31%, 32%, 33%, 34%,
35%th, 36%, 37%, 38%, 39% or 40%, it is preferably 25.0-30.0%, more preferably 30.0%.
Preferably, mass percent of the wax in the facial ointment is 5.0-10.0%, such as can be 5%,
6%th, 7%, 8%, 9% or 10%, it is preferably 8.0-10.0%, more preferably 10.0%.
Preferably, the silicon polymer for Dimethicone/Vinyl Dimethicone cross-linked polymer,
C30-45 alkyl cetearyls Dimethicone Crosspolymer, cetearyl dimethyl silicone polymer/vinyl
Dimethicone Crosspolymer, dimethyl silicone polymer/phenyl vinyl dimethione cross-linked polymer or second
In alkenyl dimethyl silicone polymer/lauryl dimethicone cross-linked polymer any one or at least two group
Close.
Preferably, the emulsifying agent is cetyl PEG/PPG-10/1 dimethyl silicone polymers, the poly- diformazans of lauryl PEG-9
Base silica ethyl dimethyl silicone polymer, PEG-10 Polydimethylsiloxane or cetyl polyethylene/polypropylene glycol -10/1 are poly-
In dimethyl siloxane any one or at least two combination.
Preferably, the grease is carbonic acid dioctyl ester, isononyl isononanoate, arachic acid monooctyl ester, isopropyl isostearate
Or in hydroxy stearic acid ethylhexyl, ring five dimethyl silicone polymer, dimethyl silicone polymer or the poly- trimethicone of methyl
Any one or at least two combination.
Preferably, the wax be paraffin, microwax, beeswax, tribehenin essence, in ceresine or Tissuemat E any one or
At least two combination.
Preferably, the facial ointment further includes mineral matter powder.
Preferably, mass percent of the mineral matter powder in the facial ointment is 1.0-5.0%, such as can be
1%th, 2%, 3%, 4% or 5%, it is preferably 5.0%.
Preferably, the mineral matter powder is any one in titanium dioxide, mica, silica or zinc oxide or at least two
Combination.
Preferably, the facial ointment includes by mass percentage：
Preferably, the facial ointment includes by mass percentage：
Preferably, the facial ointment includes by mass percentage：
Second aspect, the present invention provides a kind of method for preparing facial ointment as described in relation to the first aspect, including it is following
Step：
(1) silicon polymer, emulsifying agent, grease and mineral matter powder are stirred evenly according to formula rate, obtains mixed liquor；
(2) wax and deionized water are added according to formula rate into the mixed liquor described in step (1), dissolved by heating, stirring
Uniformly；
(3) facial ointment is made in filling cooling after cooling down.
Preferably, the temperature of step (2) described heating is 80-90 DEG C, for example, can be 80 DEG C, 81 DEG C, 82 DEG C, 83 DEG C,
84 DEG C, 85 DEG C, 86 DEG C, 87 DEG C, 88 DEG C, 89 DEG C or 90 DEG C, be preferably 84-86 DEG C.
Preferably, the temperature of step (3) described cooling is 60-70 DEG C, for example, can be 60 DEG C, 61 DEG C, 62 DEG C, 63 DEG C,
64 DEG C, 65 DEG C, 66 DEG C, 67 DEG C, 68 DEG C, 69 DEG C or 70 DEG C, be preferably 65-70 DEG C.
As optimal technical scheme, the present invention provides a kind of method for preparing facial ointment as described in relation to the first aspect,
Comprise the following steps：
(1) silicon polymer, emulsifying agent, grease and mineral matter powder are stirred evenly according to formula rate, obtains mixed liquor；
(2) wax and deionized water are added according to formula rate into the mixed liquor described in step (1), are heated to 80-90 DEG C,
Dissolving stirs evenly；
(3) it is cooled to 60-70 DEG C of filling cooling and the facial ointment is made.
Compared with prior art, the present invention has the advantages that：
(1) facial ointment of the invention is added with silicon polymer, improves the lightness of product and salubrious degree so that product
Easily absorb, and there is certain skin lightening；
(2) silicon polymer in facial ointment is rationally compounded with emulsifying agent, has the function that substantially stabilized ointment；
(3) to be placed three months in facial ointment high temperature and low temperature environment prepared by the present invention, stability is good, homogeneous,
Oil separation and crystal precipitation phenomenon do not occur.
Brief description of the drawings
Fig. 1 is the feeling evaluation comparison diagram of facial ointment.
Embodiment
The technological means and its effect taken for the present invention is further explained, with reference to embodiments with attached drawing to this hair
It is bright to be further described.It is understood that the specific embodiments described herein are used only for explaining the present invention, rather than
Limitation of the invention.
In the examples where no specific technique or condition is specified, according to the described technology of document in the art or condition,
Or carried out according to product description.Reagents or instruments used without specified manufacturer, be can be by regular channel commercially available from
The conventional products of acquisition.
Embodiment 1
The formula of facial ointment is shown in Table 1.
Table 1
Preparation method is as follows：
(1) by C30-45 alkyl cetearyls Dimethicone Crosspolymer, dimethyl silicone polymer/ethene
Base Dimethicone Crosspolymer, cetyl PEG/PPG-10/1 dimethyl silicone polymers, five polydimethylsiloxanes of ring
Alkane, carbonic acid dioctyl ester, isopropyl isostearate, titanium dioxide and mica are stirred evenly according to formula rate, obtain mixed liquor；
(2) paraffin, microwax and deionized water, heating are added according to formula rate into the mixed liquor described in step (1)
To 85 DEG C, dissolving stirs evenly；
(3) 65 DEG C of filling coolings are cooled to the facial ointment is made.
Embodiment 2
The formula of facial ointment is shown in Table 2.
Table 2
Preparation method is as follows：
(1) by C30-45 alkyl cetearyls Dimethicone Crosspolymer, cetyl PEG/PPG-10/1
Dimethyl silicone polymer, ring five dimethyl silicone polymer, carbonic acid dioctyl ester, isononyl isononanoate, titanium dioxide and silica according to
Formula rate stirs evenly, and obtains mixed liquor；
(2) beeswax, microwax and deionized water, heating are added according to formula rate into the mixed liquor described in step (1)
To 84 DEG C, dissolving stirs evenly；
(3) 65 DEG C of filling coolings are cooled to the facial ointment is made.
Embodiment 3
The formula of facial ointment is shown in Table 3.
Table 3
Preparation method is as follows：
(1) by cetearyl Dimethicone/Vinyl Dimethicone cross-linked polymer, lauryl
PEG-9 Polydimethylsiloxyethyl Dimethicone, ring five dimethyl silicone polymer, isopropyl isostearate, titanium dioxide
Titanium and zinc oxide are stirred evenly according to formula rate, obtain mixed liquor；
(2) Tissuemat E, microwax and deionized water are added according to formula rate into the mixed liquor described in step (1),
86 DEG C are heated to, dissolving stirs evenly；
(3) 65 DEG C of filling coolings are cooled to the facial ointment is made.
Embodiment 4
The formula of facial ointment is shown in Table 4.
Table 4
Preparation method is as follows：
(1) by dimethyl silicone polymer/phenyl vinyl dimethione cross-linked polymer, PEG-10 poly dimethyl silicon
Oxygen alkane, dimethyl silicone polymer, arachic acid monooctyl ester and titanium dioxide are stirred evenly according to formula rate, obtain mixed liquor；
(2) tribehenin essence and deionized water are added according to formula rate into the mixed liquor described in step (1), is heated to 80
DEG C, dissolving stirs evenly；
(3) 60 DEG C of filling coolings are cooled to the facial ointment is made.
Embodiment 5
The formula of facial ointment is shown in Table 5.
Table 5
Preparation method is as follows：
(1) by vinyldimethicone/lauryl dimethicone cross-linked polymer, the poly- second two of cetyl
Alcohol/the dimethyl silicone polymer of polypropylene glycol -10/1, the poly- trimethicone of methyl, hydroxy stearic acid ethylhexyl and titanium dioxide
Titanium is stirred evenly according to formula rate, obtains mixed liquor；
(2) ceresine and deionized water are added according to formula rate into the mixed liquor described in step (1), are heated to 90 DEG C,
Dissolving stirs evenly；
(3) 70 DEG C of filling coolings are cooled to the facial ointment is made.
Comparative example 1
Compared with Example 1, except not containing silicon polymer, mass percent of the deionized water in facial ointment is
53.0%, other preparation methods are same as Example 1.
Comparative example 2
Compared with Example 1, except not containing cetyl PEG/PPG-10/1 dimethyl silicone polymers, deionized water is being protected
Mass percent in skin ointment is 5.0%, other preparation methods are same as Example 1.
Comparative example 3
Compared with Example 1, C30-45 alkyl cetearyl Dimethicone Crosspolymer is in facial ointment
In mass percent be 30.0%, Dimethicone/Vinyl Dimethicone cross-linked polymer is in skin care oil
Mass percent in cream is 30.0%, and mass percent of the wax in facial ointment is 1.0%, without mineral matter powder, other
Preparation method is same as Example 1.
Comparative example 4
Compared with Example 1, C30-45 alkyl cetearyl Dimethicone Crosspolymer is in facial ointment
In mass percent be 10.0%, Dimethicone/Vinyl Dimethicone cross-linked polymer is in skin care oil
Mass percent in cream is 10.0%, and mass percent of the deionized water in facial ointment is 33.0%, other preparation sides
Method is same as Example 1.
High/low temperature stability experiment
By the facial ointment good seal of embodiment and comparative example, it is placed in constant-temperature enclosed drying box, puts at different temperatures
Put three months, observe the stability of facial ointment, the results are shown in Table 6.
Table 6
It can be seen from the above that the facial ointment of embodiment 1-5 is cooperated using silicon polymer and emulsifying agent, rationally compounding, makes
Standby facial ointment has excellent height temperature stability；The facial ointment of comparative example 1 does not contain silicon polymer, comparative example 2
Facial ointment does not contain emulsifying agent, it is impossible to plays synergistic effect and stablizes ointment, the stability of ointment is poor, under high and low temperature environment
Water oil separation can occur, coarse and crystal separates out；The mass percent of the silicon polymer of the facial ointment of comparative example 3-4 does not conform to
Reason, stability are poor.
Sensory evaluation is tested
In order to evaluate the using effect of facial ointment of the present invention, using the facial ointment of embodiment and comparative example as test specimens
Product, choose 10 subjects and carry out skin sense evaluation test.
In constant temperature freestanding environment, relative humidity is 50 ± 5%, and after 1 hour of resting, subject uses embodiment and right
The facial ointment of ratio, feels to score according to during use, and scoring uses ten point system, and 1 point worst for effect, 10 points
For best results.It the results are shown in Table 7 and Fig. 1.
Table 7
It can be seen from the above that the use feeling of the facial ointment of embodiment is significantly better than that the facial ointment of comparative example, special table
Four salubrious property, lightness, absorbability and skin lightening result aspects now.The facial ointment non-greasy of the present invention, absorb soon, has
Certain the effect of covering microgroove, bright skin.
In conclusion the facial ointment of the present invention contains silicon polymer, the lightness of product and salubrious degree are improved so that
Product easily absorbs；Silicon polymer is rationally compounded with emulsifying agent, improves the stability of product, homogeneous, and oily separation does not occur
With crystal precipitation phenomenon.
Applicant states that the present invention illustrates the method detailed of the present invention, but not office of the invention by above-described embodiment
It is limited to above-mentioned method detailed, that is, does not mean that the present invention has to rely on above-mentioned method detailed and could implement.Technical field
Technical staff it will be clearly understood that any improvement in the present invention, equivalence replacement and auxiliary element to each raw material of product of the present invention
Addition, selection of concrete mode etc., all fall within protection scope of the present invention and the open scope.
Claims (10)
1. a kind of facial ointment, it is characterised in that the facial ointment includes by mass percentage：
2. facial ointment according to claim 1, it is characterised in that the silicon polymer is dimethyl silicone polymer/second
Alkenyl Dimethicone Crosspolymer, C30-45 alkyl cetearyls Dimethicone Crosspolymer, whale
Wax Stearyl dimethicone/vinyl dimethicone cross polymer, dimethyl silicone polymer/phenylethylene
Base dimethione cross-linked polymer or vinyldimethicone/lauryl dimethicone cross-linked polymer
In any one or at least two combination；
Preferably, the emulsifying agent is cetyl PEG/PPG-10/1 dimethyl silicone polymers, lauryl PEG-9 poly dimethyl silicon
- 10/1 poly- diformazan of oxygen ethyl dimethyl silicone polymer, PEG-10 Polydimethylsiloxane or cetyl polyethylene/polypropylene glycol
In radical siloxane any one or at least two combination；
Preferably, the grease is carbonic acid dioctyl ester, isononyl isononanoate, arachic acid monooctyl ester, isopropyl isostearate, hydroxyl
It is any in ethylhexyl stearate, ring five dimethyl silicone polymer, dimethyl silicone polymer or the poly- trimethicone of methyl
It is a kind of or at least two combination；
Preferably, the wax be paraffin, microwax, beeswax, tribehenin essence, in ceresine or Tissuemat E any one or at least
Two kinds of combination.
3. facial ointment according to claim 1 or 2, it is characterised in that the facial ointment further includes mineral matter powder；
Preferably, mass percent of the mineral matter powder in the facial ointment is 1.0-5.0%；
Preferably, the mineral matter powder is any one in titanium dioxide, mica, silica or zinc oxide or at least two group
Close.
4. according to claim 1-3 any one of them facial ointments, it is characterised in that the facial ointment is by mass percentage
Including：
5. according to claim 1-4 any one of them facial ointments, it is characterised in that the facial ointment is by mass percentage
Including：
6. according to claim 1-5 any one of them facial ointments, it is characterised in that the facial ointment is by mass percentage
Including：
7. a kind of prepare such as the method for claim 1-6 any one of them facial ointments, it is characterised in that including following step
Suddenly：
(1) silicon polymer, emulsifying agent, grease and mineral matter powder are stirred evenly according to formula rate, obtains mixed liquor；
(2) wax and deionized water are added according to formula rate into the mixed liquor described in step (1), dissolves by heating, stir evenly；
(3) facial ointment is made in filling cooling after cooling down.
8. the method according to the description of claim 7 is characterized in that the temperature of step (2) described heating is 80-90 DEG C, preferably
For 84-86 DEG C.
9. the method according to claim 7 or 8, it is characterised in that the temperature of step (3) described cooling is 60-70 DEG C, excellent
Elect 65-70 DEG C as.
10. according to claim 7-9 any one of them methods, it is characterised in that comprise the following steps：
(1) silicon polymer, emulsifying agent, grease and mineral matter powder are stirred evenly according to formula rate, obtains mixed liquor；
(2) wax and deionized water are added according to formula rate into the mixed liquor described in step (1), is heated to 80-90 DEG C, dissolving
Stir evenly；
(3) it is cooled to 60-70 DEG C of filling cooling and the facial ointment is made.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108904328A (en) * | 2018-08-14 | 2018-11-30 | 广州芊植本草化妆品有限公司 | A kind of preparation method of magnet facial mask |
| CN111388356A (en) * | 2020-04-02 | 2020-07-10 | 上海中翊日化有限公司 | Massage ointment and preparation method thereof |
| CN113318009A (en) * | 2021-05-17 | 2021-08-31 | 科丝美诗(中国)化妆品有限公司 | Oil-dispersed mousse paste composition and preparation method thereof |
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| CN102973436A (en) * | 2012-12-19 | 2013-03-20 | 珀莱雅化妆品股份有限公司 | Making-up cosmetics composition with elastic touch |
| CN103655234A (en) * | 2013-10-12 | 2014-03-26 | 广州环亚化妆品科技有限公司 | Moisture type CC cream composition and preparation method thereof |
| CN104940044A (en) * | 2015-06-30 | 2015-09-30 | 广州环亚化妆品科技有限公司 | Foundation cream with stable wire-drawing effect and preparation method of foundation cream |
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| CN102186456A (en) * | 2008-10-14 | 2011-09-14 | 宝洁公司 | Resilient personal care composition comprising polyalkyl ether containing siloxane elastomers |
| CN102973436A (en) * | 2012-12-19 | 2013-03-20 | 珀莱雅化妆品股份有限公司 | Making-up cosmetics composition with elastic touch |
| CN103655234A (en) * | 2013-10-12 | 2014-03-26 | 广州环亚化妆品科技有限公司 | Moisture type CC cream composition and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108904328A (en) * | 2018-08-14 | 2018-11-30 | 广州芊植本草化妆品有限公司 | A kind of preparation method of magnet facial mask |
| CN111388356A (en) * | 2020-04-02 | 2020-07-10 | 上海中翊日化有限公司 | Massage ointment and preparation method thereof |
| CN111388356B (en) * | 2020-04-02 | 2022-06-14 | 上海中翊日化有限公司 | Massage ointment and preparation method thereof |
| CN113318009A (en) * | 2021-05-17 | 2021-08-31 | 科丝美诗(中国)化妆品有限公司 | Oil-dispersed mousse paste composition and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN108030709B (en) | 2021-05-04 |
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Address after: Guangzhou Science City in Guangdong province 510000 Ke Lin Lu Guangzhou high tech Industrial Development Zone No. 15 Patentee after: Guangzhou Huanya cosmetics technology Co.,Ltd. Address before: Guangzhou Science City in Guangdong province 510000 Ke Lin Lu Guangzhou high tech Industrial Development Zone No. 15 Patentee before: GUANGZHOU HUANYA COSMETICS TECHNOLOGY Co.,Ltd. |