CN108004787A - A kind of fleece fabrics antipilling finishing agent and preparation method thereof - Google Patents
A kind of fleece fabrics antipilling finishing agent and preparation method thereof Download PDFInfo
- Publication number
- CN108004787A CN108004787A CN201711237081.7A CN201711237081A CN108004787A CN 108004787 A CN108004787 A CN 108004787A CN 201711237081 A CN201711237081 A CN 201711237081A CN 108004787 A CN108004787 A CN 108004787A
- Authority
- CN
- China
- Prior art keywords
- finishing agent
- fleece fabrics
- pilling
- hyaluronic acid
- chitosan
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
- D06M23/12—Processes in which the treating agent is incorporated in microcapsules
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
- D06M11/70—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with oxides of phosphorus; with hypophosphorous, phosphorous or phosphoric acids or their salts
- D06M11/71—Salts of phosphoric acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
- D06M16/003—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic with enzymes or microorganisms
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
- D06M2101/12—Keratin fibres or silk
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/35—Abrasion, pilling or fibrillation resistance
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Microbiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of fleece fabrics antipilling finishing agent and preparation method thereof, the finishing agent is spherical in shape or elliposoidal, average grain diameter are 6~20 μm, and the mass ratio of its core and wall material is 1:0.3~1.2；The core is made of protease and sodium dihydrogen phosphate, and wall material is made of chitosan and hyaluronic acid.Finishing agent of the present invention can assign fleece fabrics surface anti-pilling property, and can guarantee that its original comfortable, thermal property is stablized；Finishing agent of the present invention is easy to use, and stability is good.
Description
Technical field
The invention belongs to textile technology field, is related to a kind of functional treatment compound of fabric, is specially a kind of cashmere
Fabric antipilling finishing agent and preparation method thereof.
Background technology
Knitted fabric is various in style, such as all kinds of looped fabrics, sweater, woollen sweater etc., especially woollen sweater are worn in actual
And washing process in, due to being constantly subject to either large or small friction so that the fiber of knitted surfaces exposes the surface of fabric,
There is young pilose antler in fabric face, and these young pilose antlers can form many spherical granules by tied up in knots mutually in the course of time, be commonly called as
Ball, these protrude the ball top in fabric exterior, have serious influence to the beautiful and hygienic of knitted fabric.
In the prior art, the finishing technique of the shrinkproof anti-pilling of Chinese patent CN1410624A cashmere products, the technique exist
Former technique soaks, washes contracting, cleaning and dehydration, stoving process interprocedual adds shrinkproof anti-pilling, cleans, improves soft finish
Technique.The formula of its shrinkproof anti-pilling is sodium dihydrogen phosphate, bleeding agent, softening agent, crosslinking agent, shrinkproof anti-pilling agent and water.Institute
Stating the cashmere product that technique arranges acquisition has the function of anti-pilling, but it is used and its auxiliary agent is easy to cause cashmere
Surface is hardened, so as to influence the comfort and warmth retention property of dress.
The content of the invention
Present invention solves the technical problem that：The defects of in order to overcome the prior art, obtain a kind of imparting fleece fabrics surface
The function of anti pilling, and ensure original soft and thermal property the finishing agent of cashmere, the present invention provides a kind of fleece fabrics
Antipilling finishing agent and preparation method thereof.
Technical solution：A kind of fleece fabrics anti-pilling finishing agent, the finishing agent is spherical in shape or elliposoidal, average grain diameter are
6~20 μm, the mass ratio of its core and wall material is 1:0.3~1.2；The core is made of protease and sodium dihydrogen phosphate, wall
Material is made of chitosan and hyaluronic acid.
Preferably, the core is by protease and sodium dihydrogen phosphate by weight 3~8:2~3 compositions.
Preferably, the wall material is by chitosan and hyaluronic acid by weight 1~2:2~3 compositions.
A kind of preparation method of fleece fabrics anti-pilling finishing agent, comprises the steps of：
(1) hyaluronic acid is dissolved in deionized water, is configured to the hyaluronic acid solution that mass concentration is 2.5~7%；
(2) chitosan is dissolved in glacial acetic acid solution, is configured to the chitosan-acetic acid solution that mass fraction is 2~5%, so
Add emulsifying agent, protease and sodium dihydrogen phosphate afterwards, magnetic agitation is to being uniformly dispersed to obtain lotion；
(3) lotion that step (2) obtains is added drop-wise in the hyaluronic acid solution of step (1) acquisition, it is 7.5 to adjust pH value
~8.8,25~40min is reacted, dispersant is added, is uniformly mixing to obtain multiple curdled milk liquid；
(4) the multiple curdled milk liquid that step (3) obtains is placed in ice-water bath and is cooled to 0~4 DEG C, add curing agent, cure 10
PH value 6.8~7.5 is adjusted after~35min, then is moved into 45~55 DEG C of tepidariums and is cured 1.5~4h and obtain fleece fabrics and prevented
Ball arranges lotion, and anti-pilling finishing lotion is centrifuged, takes precipitation, and precipitation is filtered, is dried to obtain fleece fabrics anti-pilling finishing
Agent.
Preferably, the emulsifying agent is Tween-80 or OP-80.
Preferably, the dispersant is polyvinylpyrrolidone or polyvinyl alcohol.
Preferably, the curing agent is glutaraldehyde, dialdehyde starch or glutamine transaminage.
Beneficial effect：(1) finishing agent of the present invention can assign fleece fabrics surface anti-pilling property, and can guarantee that it
Original comfortable, thermal property is stablized；(2) finishing agent of the present invention is easy to use, and stability is good.
Embodiment
Embodiment 1
A kind of fleece fabrics anti-pilling finishing agent, the finishing agent is spherical in shape or elliposoidal, average grain diameter are 6 μm, its core
Material and the mass ratio of wall material are 1:0.3；The core is made of protease and sodium dihydrogen phosphate, and wall material is by chitosan and hyalomitome
Acid composition.
The core is by protease and sodium dihydrogen phosphate by weight 3:2 compositions.
The wall material is by chitosan and hyaluronic acid by weight 1:2 compositions.
A kind of preparation method of fleece fabrics anti-pilling finishing agent, comprises the steps of：
(1) hyaluronic acid is dissolved in deionized water, is configured to the hyaluronic acid solution that mass concentration is 2.5%；
(2) chitosan is dissolved in glacial acetic acid solution, is configured to the chitosan-acetic acid solution that mass fraction is 2%, then
Add emulsifying agent, protease and sodium dihydrogen phosphate, magnetic agitation is to being uniformly dispersed to obtain lotion；
(3) lotion that step (2) obtains is added drop-wise in the hyaluronic acid solution of step (1) acquisition, adjusting pH value is
7.5,25min is reacted, dispersant is added, is uniformly mixing to obtain multiple curdled milk liquid；
(4) the multiple curdled milk liquid that step (3) obtains is placed in ice-water bath and is cooled to 0 DEG C, add curing agent, cure 10min
PH value 6.8 is adjusted afterwards, then is moved into curing 1.5h in 45 DEG C of tepidariums and obtained fleece fabrics anti-pilling finishing lotion, anti-pilling is whole
Lotion centrifugation is managed, takes precipitation, precipitation is filtered, is dried to obtain fleece fabrics anti-pilling finishing agent.
The emulsifying agent is Tween-80.
The dispersant is polyvinylpyrrolidone.
The curing agent is glutaraldehyde.
Embodiment 2
A kind of fleece fabrics anti-pilling finishing agent, the finishing agent is spherical in shape or elliposoidal, average grain diameter are 14 μm, its core
Material and the mass ratio of wall material are 1:0.8；The core is made of protease and sodium dihydrogen phosphate, and wall material is by chitosan and hyalomitome
Acid composition.
The core is by protease and sodium dihydrogen phosphate by weight 5:3 compositions.
The wall material is by chitosan and hyaluronic acid by weight 1:3 compositions.
A kind of preparation method of fleece fabrics anti-pilling finishing agent, comprises the steps of：
(1) hyaluronic acid is dissolved in deionized water, is configured to the hyaluronic acid solution that mass concentration is 5%；
(2) chitosan is dissolved in glacial acetic acid solution, is configured to the chitosan-acetic acid solution that mass fraction is 3.5%, so
Add emulsifying agent, protease and sodium dihydrogen phosphate afterwards, magnetic agitation is to being uniformly dispersed to obtain lotion；
(3) lotion that step (2) obtains is added drop-wise in the hyaluronic acid solution of step (1) acquisition, adjusting pH value is
8.2,32min is reacted, dispersant is added, is uniformly mixing to obtain multiple curdled milk liquid；
(4) the multiple curdled milk liquid that step (3) obtains is placed in ice-water bath and is cooled to 2 DEG C, add curing agent, cure 20min
PH value 7.2 is adjusted afterwards, then is moved into curing 2.5h in 50 DEG C of tepidariums and obtained fleece fabrics anti-pilling finishing lotion, anti-pilling is whole
Lotion centrifugation is managed, takes precipitation, precipitation is filtered, is dried to obtain fleece fabrics anti-pilling finishing agent.
The emulsifying agent is OP-80.
The dispersant is polyvinyl alcohol.
The curing agent is dialdehyde starch.
Embodiment 3
A kind of fleece fabrics anti-pilling finishing agent, the finishing agent is spherical in shape or elliposoidal, average grain diameter are 20 μm, its core
Material and the mass ratio of wall material are 1:1.2；The core is made of protease and sodium dihydrogen phosphate, and wall material is by chitosan and hyalomitome
Acid composition.
The core is by protease and sodium dihydrogen phosphate by weight 8:3 compositions.
The wall material is by chitosan and hyaluronic acid by weight 2:3 compositions.
A kind of preparation method of fleece fabrics anti-pilling finishing agent, comprises the steps of：
(1) hyaluronic acid is dissolved in deionized water, is configured to the hyaluronic acid solution that mass concentration is 7%；
(2) chitosan is dissolved in glacial acetic acid solution, is configured to the chitosan-acetic acid solution that mass fraction is 5%, then
Add emulsifying agent, protease and sodium dihydrogen phosphate, magnetic agitation is to being uniformly dispersed to obtain lotion；
(3) lotion that step (2) obtains is added drop-wise in the hyaluronic acid solution of step (1) acquisition, adjusting pH value is
8.8,40min is reacted, dispersant is added, is uniformly mixing to obtain multiple curdled milk liquid；
(4) the multiple curdled milk liquid that step (3) obtains is placed in ice-water bath and is cooled to 4 DEG C, add curing agent, cure 35min
PH value 7.5 is adjusted afterwards, then moves into curing 4h in 55 DEG C of tepidariums and obtains fleece fabrics anti-pilling finishing lotion, by anti-pilling finishing
Lotion centrifuges, and takes precipitation, and precipitation is filtered, is dried to obtain fleece fabrics anti-pilling finishing agent.
The emulsifying agent is OP-80.
The dispersant is polyvinyl alcohol.
The curing agent is glutamine transaminage.
The fleece fabrics anti-pilling finishing agent that embodiment 1~3 prepares is tested for the property, as a result such as following table institute
Show：
| Anti pilling grade/level | Feel | |
| Embodiment 1 | 4 | It is excellent |
| Embodiment 2 | 5 | It is excellent |
| Embodiment 3 | 4 | It is excellent |
Claims (7)
1. a kind of fleece fabrics anti-pilling finishing agent, it is characterised in that the finishing agent is spherical in shape or elliposoidal, average grain diameter are
6~20 μm, the mass ratio of its core and wall material is 1:0.3~1.2；The core is made of protease and sodium dihydrogen phosphate, wall
Material is made of chitosan and hyaluronic acid.
2. a kind of fleece fabrics anti-pilling finishing agent according to claim 1, it is characterised in that the core is by protease
With sodium dihydrogen phosphate by weight 3~8:2~3 compositions.
3. a kind of fleece fabrics anti-pilling finishing agent according to claim 1, it is characterised in that the wall material is by chitosan
With hyaluronic acid by weight 1~2:2~3 compositions.
4. any a kind of preparation method of fleece fabrics anti-pilling finishing agent of claims 1 to 3, it is characterised in that include
Following steps：
(1) hyaluronic acid is dissolved in deionized water, is configured to the hyaluronic acid solution that mass concentration is 2.5~7%；
(2) chitosan is dissolved in glacial acetic acid solution, is configured to the chitosan-acetic acid solution that mass fraction is 2~5%, Ran Houjia
Enter emulsifying agent, protease and sodium dihydrogen phosphate, magnetic agitation is to being uniformly dispersed to obtain lotion；
(3) lotion that step (2) obtains is added drop-wise in the hyaluronic acid solution of step (1) acquisition, adjust pH value for 7.5~
8.8,25~40min is reacted, dispersant is added, is uniformly mixing to obtain multiple curdled milk liquid；
(4) the multiple curdled milk liquid that step (3) obtains is placed in ice-water bath and is cooled to 0~4 DEG C, add curing agent, cure 10~
PH value 6.8~7.5 is adjusted after 35min, then is moved into 45~55 DEG C of tepidariums and is cured 1.5~4h to obtain fleece fabrics anti-pilling whole
Lotion is managed, anti-pilling finishing lotion is centrifuged, takes precipitation, precipitation is filtered, is dried to obtain fleece fabrics anti-pilling finishing agent.
A kind of 5. preparation method of fleece fabrics anti-pilling finishing agent according to claim 4, it is characterised in that the breast
Agent is Tween-80 or OP-80.
6. the preparation method of a kind of fleece fabrics anti-pilling finishing agent according to claim 4, it is characterised in that described point
Powder is polyvinylpyrrolidone or polyvinyl alcohol.
7. the preparation method of a kind of fleece fabrics anti-pilling finishing agent according to claim 4, it is characterised in that described solid
Agent is glutaraldehyde, dialdehyde starch or glutamine transaminage.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711237081.7A CN108004787A (en) | 2017-11-30 | 2017-11-30 | A kind of fleece fabrics antipilling finishing agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711237081.7A CN108004787A (en) | 2017-11-30 | 2017-11-30 | A kind of fleece fabrics antipilling finishing agent and preparation method thereof |
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| Publication Number | Publication Date |
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| CN108004787A true CN108004787A (en) | 2018-05-08 |
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| CN201711237081.7A Pending CN108004787A (en) | 2017-11-30 | 2017-11-30 | A kind of fleece fabrics antipilling finishing agent and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109440467A (en) * | 2018-10-11 | 2019-03-08 | 苏州市职业大学 | A kind of finishing agent and preparation method thereof and application method preventing embroidery fluffing |
| CN115305620A (en) * | 2022-08-12 | 2022-11-08 | 江苏天章医用卫生新材料股份有限公司 | High-water-absorption cotton gauze and preparation method and application thereof |
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Cited By (3)
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|---|---|---|---|---|
| CN109440467A (en) * | 2018-10-11 | 2019-03-08 | 苏州市职业大学 | A kind of finishing agent and preparation method thereof and application method preventing embroidery fluffing |
| CN109440467B (en) * | 2018-10-11 | 2021-05-04 | 苏州市职业大学 | Finishing agent for preventing embroidery from fluffing and preparation method and using method thereof |
| CN115305620A (en) * | 2022-08-12 | 2022-11-08 | 江苏天章医用卫生新材料股份有限公司 | High-water-absorption cotton gauze and preparation method and application thereof |
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