CN107988799A - A kind of preparation process of the water proof fire retardant polyamide fabric of anti-infrared monitoring - Google Patents
A kind of preparation process of the water proof fire retardant polyamide fabric of anti-infrared monitoring Download PDFInfo
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- CN107988799A CN107988799A CN201711474253.2A CN201711474253A CN107988799A CN 107988799 A CN107988799 A CN 107988799A CN 201711474253 A CN201711474253 A CN 201711474253A CN 107988799 A CN107988799 A CN 107988799A
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- fire retardant
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- fabric
- water proof
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- 239000004744 fabric Substances 0.000 title claims abstract description 57
- 239000003063 flame retardant Substances 0.000 title claims abstract description 49
- 239000004952 Polyamide Substances 0.000 title claims abstract description 25
- 229920002647 polyamide Polymers 0.000 title claims abstract description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 238000012544 monitoring process Methods 0.000 title claims abstract description 17
- 239000011248 coating agent Substances 0.000 claims abstract description 37
- 238000000576 coating method Methods 0.000 claims abstract description 37
- 238000004026 adhesive bonding Methods 0.000 claims abstract description 29
- 239000003292 glue Substances 0.000 claims abstract description 21
- 238000000034 method Methods 0.000 claims abstract description 15
- 239000000463 material Substances 0.000 claims abstract description 10
- 230000008569 process Effects 0.000 claims abstract description 10
- 238000004513 sizing Methods 0.000 claims abstract description 9
- 238000001704 evaporation Methods 0.000 claims abstract description 8
- 238000010981 drying operation Methods 0.000 claims abstract description 6
- 239000002562 thickening agent Substances 0.000 claims abstract description 6
- 239000003431 cross linking reagent Substances 0.000 claims abstract description 5
- 238000010422 painting Methods 0.000 claims abstract description 5
- 239000011347 resin Substances 0.000 claims abstract description 5
- 229920005989 resin Polymers 0.000 claims abstract description 5
- 239000000344 soap Substances 0.000 claims abstract description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 36
- 239000007788 liquid Substances 0.000 claims description 30
- 239000003795 chemical substances by application Substances 0.000 claims description 27
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 22
- 239000000975 dye Substances 0.000 claims description 16
- 238000004078 waterproofing Methods 0.000 claims description 15
- 235000011121 sodium hydroxide Nutrition 0.000 claims description 12
- 238000001035 drying Methods 0.000 claims description 10
- 238000007654 immersion Methods 0.000 claims description 9
- 238000007639 printing Methods 0.000 claims description 9
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims description 8
- 238000009991 scouring Methods 0.000 claims description 8
- 239000000654 additive Substances 0.000 claims description 7
- 230000000996 additive effect Effects 0.000 claims description 7
- 238000009990 desizing Methods 0.000 claims description 7
- SJEYSFABYSGQBG-UHFFFAOYSA-M Patent blue Chemical compound [Na+].C1=CC(N(CC)CC)=CC=C1C(C=1C(=CC(=CC=1)S([O-])(=O)=O)S([O-])(=O)=O)=C1C=CC(=[N+](CC)CC)C=C1 SJEYSFABYSGQBG-UHFFFAOYSA-M 0.000 claims description 6
- 239000000980 acid dye Substances 0.000 claims description 6
- 239000002738 chelating agent Substances 0.000 claims description 6
- 239000003112 inhibitor Substances 0.000 claims description 6
- 238000013508 migration Methods 0.000 claims description 6
- 230000005012 migration Effects 0.000 claims description 6
- 235000019353 potassium silicate Nutrition 0.000 claims description 6
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 6
- 239000012752 auxiliary agent Substances 0.000 claims description 5
- 229910001629 magnesium chloride Inorganic materials 0.000 claims description 4
- 238000002386 leaching Methods 0.000 claims description 3
- 238000007790 scraping Methods 0.000 claims description 3
- 241000208340 Araliaceae Species 0.000 claims description 2
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 claims description 2
- 235000003140 Panax quinquefolius Nutrition 0.000 claims description 2
- 235000008434 ginseng Nutrition 0.000 claims description 2
- 238000010025 steaming Methods 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 12
- 229920002994 synthetic fiber Polymers 0.000 abstract description 5
- 238000004043 dyeing Methods 0.000 abstract description 4
- 239000004758 synthetic textile Substances 0.000 abstract description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 8
- 238000003490 calendering Methods 0.000 description 8
- 238000012545 processing Methods 0.000 description 8
- 238000005457 optimization Methods 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 4
- 239000000835 fiber Substances 0.000 description 4
- 239000000853 adhesive Substances 0.000 description 3
- 230000001070 adhesive effect Effects 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000004753 textile Substances 0.000 description 3
- XADCESSVHJOZHK-UHFFFAOYSA-N Meperidine Chemical compound C=1C=CC=CC=1C1(C(=O)OCC)CCN(C)CC1 XADCESSVHJOZHK-UHFFFAOYSA-N 0.000 description 2
- 230000002706 hydrostatic effect Effects 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000012209 synthetic fiber Substances 0.000 description 2
- 241000876833 Emberizinae Species 0.000 description 1
- 208000015220 Febrile disease Diseases 0.000 description 1
- 229920000297 Rayon Polymers 0.000 description 1
- DHKHKXVYLBGOIT-UHFFFAOYSA-N acetaldehyde Diethyl Acetal Natural products CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 description 1
- 125000002777 acetyl group Chemical class [H]C([H])([H])C(*)=O 0.000 description 1
- 229920006231 aramid fiber Polymers 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 210000000981 epithelium Anatomy 0.000 description 1
- 230000009970 fire resistant effect Effects 0.000 description 1
- 238000004079 fireproofing Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 230000000505 pernicious effect Effects 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 239000002861 polymer material Substances 0.000 description 1
- 239000011527 polyurethane coating Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000000979 retarding effect Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 150000003457 sulfones Chemical class 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 230000007306 turnover Effects 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/564—Polyureas, polyurethanes or other polymers having ureide or urethane links; Precondensation products forming them
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
- D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
- D06M11/155—Halides of elements of Groups 2 or 12 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/38—Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with hydrogen peroxide or peroxides of metals; with persulfuric, permanganic, pernitric, percarbonic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/39—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using acid dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/06—Material containing basic nitrogen containing amide groups using acid dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/34—Polyamides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/10—Repellency against liquids
- D06M2200/12—Hydrophobic properties
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/30—Flame or heat resistance, fire retardancy properties
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a kind of preparation process of the water proof fire retardant polyamide fabric of anti-infrared monitoring, solves the problems, such as to can not find in the prior art well for the fire-retardant dyeing and finishing mode of the synthetic fabrics such as Fypro.(1) fabric of the invention carries out turning over cloth, cold pad--batch, kiering, sizing, dye bottom and stamp；(2) dried after the completion of stamp；Then baked under conditions of temperature is 160 DEG C, speed is 50m/min；Evaporated again under conditions of speed is 15~18m/min, temperature is 101~103 DEG C；Drying operation is carried out after evaporating again；(3) soap, then carry out fixation treatment；(4) finished product is made after carrying out reverse side gluing, the process of reverse side gluing tentering is：Gluing operation is carried out using coating blade, glue uses fire retardant glue TF 680B, and also added with coating yellow G 24, painting material basket G 31, the black G 51 of coating, smooth resin TF 399, crosslinking agent TF 694B, thickener DM 5299 in fire retardant glue TF 680B.The present invention has the advantages that intensity is high, water proof fire retardant effect is good.
Description
Technical field
The present invention relates to weaving manufacturing field, and in particular to a kind of water proof fire retardant polyamide fabric of anti-infrared monitoring
Preparation process.
Background technology
Synthetic fibers and its fabric, such as carpet, curtain, bunting, are the necessitys of people's daily life.However, by
There is inflammability in them, often bring on a disaster to us.US and European is to automotive trim, aircraft interior fittings, household textile
The stringent heat-insulating, fire-preventing requirement of the proposition such as product, extraordinary industrial and protective clothing, military uniform.From the point of view of long-range trend, fire-retardant demand is day
Often one of primary demand in life.
The domestic fire-retardant dyeing and finishing mode to fabric is mainly from the aspect of two：First, fire resistance fibre is selected, such as aramid fiber, virtue
Sulfone synthetic fibre, ceramic fibre, fire resistant viscose acetal fibre institute knitted fabric.Arranged second, rolling fire retardant after using to reach fire-retardant mesh
's.But the inflaming retarding fabric of both types has the shortcomings that bigger, first, cost is higher, color control is difficult, second, to ring
Border pollution level and risk are bigger；And for the fire-retardant dye of the synthetic fabrics such as Regenerated Polyester Fibres, Fypro
Perfect square formula, the country can not find good solution always.
The content of the invention
The technical problems to be solved by the invention are：It can not find in the prior art well for the synthesis such as Fypro
The problem of fire-retardant dyeing and finishing mode of fabric, is, and it is an object of the present invention to provide a kind of water proof fire retardant polyamide of anti-infrared monitoring
The preparation process of fabric, can be effectively applicable to waterproof, the flame retardant treatment of polyamide fabric, and the fabric after processing
Waterproof, flame retardant effect it is good, while also there is high intensity, high durable, resistance to hydrostatic pressure and other effects.
The present invention is achieved through the following technical solutions：
A kind of preparation process of the water proof fire retardant polyamide fabric of anti-infrared monitoring, including：
(1) fabric carries out turning over cloth, cold pad--batch, kiering, sizing, dye bottom and stamp；
(2) dried after the completion of stamp；Then baked under conditions of temperature is 160 DEG C, speed is 50m/min；Again
Evaporated under conditions of speed is 15~18m/min, temperature is 101~103 DEG C；Drying operation is carried out after evaporating again；
(3) soap, then carry out fixation treatment；
(4) finished product is made after carrying out reverse side gluing, the process of reverse side gluing tentering is：Gluing behaviour is carried out using coating blade
To make, glue uses fire retardant glue TF-680B, and also added with 0.15~0.25% coating yellow G-24,0.08 in fire retardant glue TF-680B
~0.12% painting material basket G-31, the black G-51 of 0.1~0.15% coating, 1.5~2.5% smooth resin TF-399,1.5~
2.5% crosslinking agent TF-694B, 2.0~3.0% thickener DM-5299.
Coating technology technique is a kind of important means in fabric post-treatment, it is by coating another material, and imparting is knitted
The more functions of thing and style.Flame retardant coating arrangement is the product of higher-end in top finish, is hindered accordingly except assigning fabric
Fire outside performance, can also impart to the function of fabric waterproof, anti-rain.
In the prior art, the mode of flame retardant coating has very much, but the characteristic due to polyamide fabric in itself, such as absorbs water
Property it is poor, self lubricity is preferable and friction coefficient is low, thus thereon set waterproof coating when easily there is the problem of adhesive force is not high,
The Collator Mode of flame retardant coating of the prior art is caused to be not applied for polyamide fabric.
The present invention has invented a kind of Collator Mode that can be suitably used for polyamide fabric flame retardant coating after research, i.e.,
Using water-based polyurethane coating medium, fire proofing is coated in coating adhesive.The present invention is set by the optimization of process conditions
Put, the present invention is had little to no effect in process of production without the generation of pernicious gas to environment.Meanwhile the present invention passes through
Added in fire retardant glue TF-680B coating yellow G-24, apply material basket G-31, the black G-51 of coating, etc. after the compounding of auxiliary agent, can effectively with
The dyestuff of polyamide fabric cooperates, and achievees the purpose that adhesion-tight degree preferably and stretching Tear strength, together
When can effectively control influence of the glue-line to dyestuff infrared reflection rate, and then reach after effectively being adjusted by color control it is infrared
The purpose of line, meets the anti-infrared detection requirement of fabric；Also, fabulous fire-retardant, waterproof effect can also be obtained, effect is very aobvious
Write.
Further, for the processing suitable for polyamide fabric, make the comprehensive performance in later stage more preferable, the step
(1) fabric is padded using the caustic soda of 40g/L and the hydrogen peroxide of 8g/L during cold pad--batch in, pad rear clot bank up 12h with
On.
Further, in the step (1) during kiering using five leaching five roll by the way of, then carry out decatize；The auxiliary agent of immersion liquid
Including desizing scouring agent, chelating agent, caustic soda, hydrogen peroxide, waterglass, the wherein concentration of desizing scouring agent is 3~5g/L, chelating agent
Concentration be 1~3g/L, the concentration of caustic soda is 8~12g/L, and the concentration of hydrogen peroxide is 4~6g/L, the concentration of waterglass for 4~
6g/L；The speed of decatize is 35~45 ms/min, the time is 50~70min, temperature is 90~110 DEG C；Pad the band liquid after immersion liquid
Rate is 70~90%.
Further, the speed in the step (1) during sizing using 85~95m/min, under the conditions of 180~200 DEG C into
OK, expanding breadth is maintained at 156cm, and cropping breadth reaches 154cm, and the speed difference of overfeeding is 11m/min.
Further, dye liquor is made using acid dyes and migration inhibitor during dye bottom in the step (1), migration inhibitor
Additive amount is 8~12g/L, and the fabric after sizing is sequentially carried out to pad dye liquor, preliminary drying, drying operation, pads the band after dye liquor
Liquid rate is 50~70%, and preliminary drying temperature is 100~120 DEG C, and drying temperature is 120~140 DEG C.
Further, in the step (1) during stamp, the concentrator mixed using printing gum and acid dyes is handled,
It is 1.5Kpa that the viscosity of concentrator, which controls the scraping edge pressure on 20dPas, printing machine, and speed is 40 ms/min.
Further, the condition of drying is in the step (2)：Speed is 40 ms/min, temperature is 110~120 DEG C.
By the setting of the above process, processing early period effectively can be carried out to polyamide fabric, the later stage is rolled waterproof whole
The operation for managing liquid and reverse side gluing provides preferable ground foundation, increases the attachment stability of later stage water-proof finish liquid and glue, effect is more
Add significantly.
In order to reach optimal waterproof effect, water-proof finish liquid is rolled before reverse side gluing is carried out in the step (4), is prevented
Water dressing liquid includes the waterproofing agent DM-3680K that mass ratio is 1: 2: 1: 1, waterproofing agent DM-3665, waterproofing agent DM-1000, waterproof
Agent DTM648-2；The magnesium chloride that additive amount is 4~6g/L is further included in the water-proof finish liquid.
The present invention first carries out water-proofing treatment, then thinly applies one layer of epithelium glue in envers, encloses between fiber
Gap, prevent the infiltration of rainwater, so as to achieve the purpose that anti-rain, effect is more notable.It is also, whole by above-mentioned waterproof
The optimization of liquid and coating technique is managed, is not only only capable of being greatly enhanced the performance of waterproof, and fabric and skin can also be effectively increased
Adhesion-tight degree between film glue, improves durable performance.
Preferably, the viscosity in the step (4) during gluing is 110~130cps, and temperature is 175~180 DEG C, and speed is
40~50 ms/min.In the step (4) during gluing, the parameter of the coating blade of more than 1000D thicker open meshes is：Scraper
Thickness 2mm, knife are away from 6mm, depression distance 2mm, tension pressure 0.4Kpa, 40 ms/min of speed；The coating blade of other close weaves
Parameter be：Blade thickness 1mm, knife are away from 4mm, depression distance 4mm, tension pressure 0.45Kpa, 50 ms/min of speed.Other are close
Fabric refers to the close weave of below 1000D.
By the optimization of above-mentioned processing step, not only it is only capable of that effectively glue is attached on polyamide fabric, moreover it is possible to have
Effect improves the flatness after gluing, makes the fabric face after gluing more smooth, bright and clean, comfort level higher.
Product of the present invention has the function of stealthy anti-infrared, fire-retardant, waterproof, anti-rain etc., is to be related to polymer material science
High-tech product.Product quality of the present invention meets military camouflage facing material standard and the European Union that the country such as Great Britain and America, Europe provides
Oeko-Tex100 standards, ISO series standards.This item purpose develops the innovation ability that will further improve enterprise, strengthens enterprise
Core competitiveness；Structural adjustment and our province textile industry technology to textile printing and dyeing enterprises product will play a role in promoting；
It is more advantageous to the manufacturing technology level of lifting China's military hardware.
In the present invention in addition to particularly pointing out, all percentage is mass percent.
Compared with prior art, the present invention have the following advantages and advantages：
1st, fabric of the invention have the function of anti-infrared, fire-retardant, anti-rain also have at the same time high intensity, height it is durable,
The characteristics of resistance to hydrostatic pressure, waterproof, greatly improve the protective and comfort of synthetic fiber fabric；
2nd, the present invention effectively improves the stability of fabrics flame resistance effect and the uniformity of coating, and solves coating cloth cover
The problem of roughness, make coat side brighter and cleaner, feel is more comfortable.
Embodiment
For the object, technical solutions and advantages of the present invention are more clearly understood, with reference to embodiment, the present invention is made
Further to describe in detail, exemplary embodiment of the invention and its explanation are only used for explaining the present invention, are not intended as to this
The restriction of invention.
Embodiment 1
A kind of preparation process of the water proof fire retardant polyamide fabric of anti-infrared monitoring, its specific preparation process bag
Include：Fabric → turn over cloth → cold pad--batch → kiering → sizing → dye bottom → stamp → bakes → evaporating → and soap, and → fixation treatment → is anti-
Water tentering → calendering → reverse side gluing tentering → calendering → inspection → finished product.
Wherein, the parameter setting in each step is as follows：
During cold pad--batch processing, fabric is padded using the caustic soda of 40g/L and the hydrogen peroxide of 8g/L, pads rear clot heap
Put 12 it is small when, which is more than 1000D thicker open meshes.
During kiering, immersion liquid is first carried out, then carries out decatize.Wherein, immersion liquid mode is rolled for five leachings five, liquid carrying rate 80%,
Rinsing machine tension force is arranged to 4Mpa；The auxiliary agent of immersion liquid includes desizing scouring agent YZ-1118, chelating agent, caustic soda, hydrogen peroxide, water glass
Glass, the wherein concentration of desizing scouring agent are 4g/L, and the concentration of chelating agent is 2g/L, and the concentration of caustic soda is 10g/L, hydrogen peroxide it is dense
Spend for 5g/L, the concentration of waterglass is 5g/L.During decatize, speed is 40 ms/min, and steaming time is 60 minutes, and steam temperature is
100℃。
During sizing, using 90 ms/min of speed, carried out at 190 DEG C, expanding breadth is maintained at 156 centimetres, cropping breadth
Reach 154 centimetres, the speed difference of overfeeding is 11 ms/min.
, it is necessary to first pad dye liquor when contaminating bottom, then preliminary drying again, is finally dried.Wherein, dye liquor include acid dyes and
The additive amount of migration inhibitor CY-K, wherein migration inhibitor are 10g/L.Liquid carrying rate is 60% after contaminating bottom, first passes through 110 DEG C pre-
Dry, then dried under conditions of 130 DEG C.
During stamp, the concentrator mixed using printing gum and acid dyes is handled, and wherein printing gum uses thickener
HR-4, it is 1.5Kpa that the viscosity of concentrator, which controls the scraping edge pressure on 20dPas, printing machine, and speed is 40 ms/min.Stamp
Drying operation is carried out after slurry processing under 40 ms/min of speed, drying temperature is 100 DEG C.
When baking, speed is 50 ms/min, and baking temperature is 160 DEG C.
When evaporating, speed is 15~18 ms/min, and temperature is 101~103 DEG C when evaporating；Again at 110~120 DEG C after evaporating
Under the conditions of dry.
When soaping, soaped using soaping agent PR-102, the additive amount of soaping agent PR-102 is 3.0g/L, the temperature soaped
Spend for 60~70 DEG C, speed is 50 ms/min.
Fixation treatment, carries out fixation, dosage 1.5g/L, color fixing temperature are 75 DEG C, fixation using color fixing agent ZetesalNR
Time is 30min.
Waterproof tenter process is：Water-proof finish liquid is padded, then dries tentering.The proportioning of wherein water-proof finish liquid is：Matter
Measure waterproofing agent DM-3680K, waterproofing agent DM-3665, waterproofing agent DM-1000, the waterproofing agent DTM648-2 than being 1: 2: 1: 1, waterproof
Agent DM-3680K, waterproofing agent DM-3665 and waterproofing agent DM-1000 originate from dolantin chemical industry, and waterproofing agent DTM648-2 originates from Jia Ni
This, is also added with magnesium chloride, the additive amount of magnesium chloride is 5g/L in water-proof finish liquid；The water-proof finish liquid will by pH neutralizers
PH is adjusted to 6.8, which includes NaOH or/and HCl.Dry tentering when speed be 50 ms/min, dry tentering when
Temperature is 175~180 DEG C.
Calendering is carried out after the processing of waterproof tentering, calendering conditions are：180 DEG C, pressure 8.5KPa of temperature, 30 ms/min of speed.
Reverse side gluing tentering is carried out after calendering, the process of reverse side gluing tentering is：Gluing operation is carried out using coating blade,
Glue use Zhejiang development of evil in febrile disease group fire retardant glue TF-680B, and in fire retardant glue TF-680B also added with 0.2% coating yellow G-24,
0.1% painting material basket G-31, the black G-51 of 0.12% coating, 2% smooth resin TF-399,2% crosslinking agent TF-694B,
The thickener DM-5299 of 2.5% dolantin chemical industry.
Viscosity during gluing is 120cps, and temperature is 175~180 DEG C, and speed is 40~50 ms/min.The ginseng of coating blade
Number is：Blade thickness 2mm, knife are away from 6mm, depression distance 2mm, tension pressure 0.4Kpa, 40 ms/min of speed.
Finally, then carry out a calendaring operation finished product is made, calendering conditions are：180 DEG C, pressure 8.5KPa of temperature, speed
30 ms/min.
Embodiment 2
Difference lies in without evaporating operation in step (2) in the present embodiment, and walk the present embodiment with embodiment 1
Suddenly the material added in (4) in fire retardant glue TF-680B varies in weight, and specific setting is as follows：
The process of reverse side gluing tentering is：Gluing operation is carried out using coating blade, glue uses fire retardant glue TF-680B, and
Also added with 0.3% coating yellow G-24,0.05% painting material basket G-31, the black G- of 0.2% coating in fire retardant glue TF-680B
51st, 3% smooth resin TF-399,3% crosslinking agent TF-694B, 1% thickener DM-5299.
Embodiment 3
Difference lies in the operating parameter of scraper is different in step (4) in the present embodiment, tool with embodiment 1 for the present embodiment
Body sets as follows：
Viscosity in the present embodiment during gluing is 140cps, and temperature is 130~140 DEG C, more than 1000D thicker open meshes
The parameter of coating blade be：Blade thickness 2mm, knife away from 6mm, depression distance 2mm, tension pressure 0.6Kpa, 30 meters of speed/
Point；The parameter of the coating blade of other close weaves is：Blade thickness 1mm, knife are away from 4mm, depression distance 4mm, tension pressure
40 ms/min of 0.7Kpa, speed.
Embodiment 4
Difference lies in the parameter in the present embodiment in step (1)~(3) is different, specifically sets with embodiment 1 for the present embodiment
Put as follows：The auxiliary agent of immersion liquid uses desizing scouring agent, caustic soda, hydrogen peroxide during kiering, and the wherein concentration of desizing scouring agent is 5g/L,
The concentration of caustic soda is 20g/L, and the concentration of hydrogen peroxide is 12g/L；The speed of decatize is 50 ms/min, time 60min, temperature are
70℃；The liquid carrying rate after immersion liquid is padded for 60%；Rinsing machine tension force is 4MPa.
Embodiment 5
Difference lies in do not have waterproof tenter process, solid to the present embodiment in the present embodiment in step (4) with embodiment 1
Reverse side gluing tentering is directly carried out after color processing, finished product is made after finally carrying out calendering.
The finished product of above-described embodiment is detected, testing result is as shown in table 1,
Table 1
Adhesive strength in above-mentioned table 1 is to promote the size of the separated power of flame-retardant layer and fabric itself.
Optimization of the invention by composition in coating technique and technique, while flame retardant effect can be effectively improved, moreover it is possible to have
Effect improves adhesion-tight degree, and can also be effectively increased stretching and Tear strength.Meanwhile water-proof finish liquid and coating technique
Optimization, be not only only capable of being greatly enhanced waterproof, fire-retardant performance, moreover it is possible to the flatness after gluing is effectively improved, after making gluing
Fabric face it is more smooth, bright and clean, make comfort level more preferable.
Above-described embodiment, has carried out the purpose of the present invention, technical solution and beneficial effect further
Describe in detail, it should be understood that the foregoing is merely the embodiment of the present invention, be not intended to limit the present invention
Protection domain, within the spirit and principles of the invention, any modification, equivalent substitution, improvement and etc. done, should all include
Within protection scope of the present invention.
Claims (10)
- A kind of 1. preparation process of the water proof fire retardant polyamide fabric of anti-infrared monitoring, it is characterised in that including：(1) fabric carries out turning over cloth, cold pad--batch, kiering, sizing, dye bottom and stamp；(2) dried after the completion of stamp；Then baked under conditions of temperature is 160 DEG C, speed is 50m/min；Again in car Speed is 15~18m/min, temperature is evaporated under conditions of being 101~103 DEG C；Drying operation is carried out after evaporating again；(3) soap, then carry out fixation treatment；(4) finished product is made after carrying out reverse side gluing, the process of reverse side gluing tentering is：Gluing operation is carried out using coating blade, Glue uses fire retardant glue TF-680B, and in fire retardant glue TF-680B also added with 0.15~0.25% coating yellow G-24,0.08~ 0.12% painting material basket G-31, the black G-51 of 0.1~0.15% coating, 1.5~2.5% smooth resin TF-399,1.5~ 2.5% crosslinking agent TF-694B, 2.0~3.0% thickener DM-5299.
- 2. a kind of preparation process of the water proof fire retardant polyamide fabric of anti-infrared monitoring according to claim 1, its It is characterized in that, fabric is padded using the caustic soda of 40g/L and the hydrogen peroxide of 8g/L during cold pad--batch in the step (1), soaks Roll rear clot and bank up more than 12h.
- 3. a kind of preparation process of the water proof fire retardant polyamide fabric of anti-infrared monitoring according to claim 1, its It is characterized in that, decatize is then carried out by the way of five leachings five are rolled during kiering in the step (1)；The auxiliary agent of immersion liquid includes moving back Scouring agent, chelating agent, caustic soda, hydrogen peroxide, waterglass are starched, the wherein concentration of desizing scouring agent is 3~5g/L, the concentration of chelating agent For 1~3g/L, the concentration of caustic soda is 8~12g/L, and the concentration of hydrogen peroxide is 4~6g/L, and the concentration of waterglass is 4~6g/L；Vapour The speed of steaming is 35~45 ms/min, the time is 50~70min, temperature is 90~110 DEG C；The liquid carrying rate after immersion liquid is padded for 70 ~90%.
- 4. a kind of preparation process of the water proof fire retardant polyamide fabric of anti-infrared monitoring according to claim 1, its It is characterized in that, the speed in the step (1) during sizing using 85~95m/min, carries out, expanding under the conditions of 180~200 DEG C Breadth is maintained at 156cm, and cropping breadth reaches 154cm, and the speed difference of overfeeding is 11m/min.
- 5. a kind of preparation process of the water proof fire retardant polyamide fabric of anti-infrared monitoring according to claim 1, its It is characterized in that, in the step (1) during dye bottom, dye liquor, the additive amount of migration inhibitor is made using acid dyes and migration inhibitor For 8~12g/L, the fabric after sizing is sequentially carried out to pad dye liquor, preliminary drying, drying operation, padding the liquid carrying rate after dye liquor is 50~70%, preliminary drying temperature is 100~120 DEG C, and drying temperature is 120~140 DEG C.
- 6. a kind of preparation process of the water proof fire retardant polyamide fabric of anti-infrared monitoring according to claim 1, its It is characterized in that, in the step (1) during stamp, the concentrator mixed using printing gum and acid dyes is handled, printing paste It is 1.5Kpa that the viscosity of material, which controls the scraping edge pressure on 20dPas, printing machine, and speed is 40 ms/min.
- 7. a kind of preparation process of the water proof fire retardant polyamide fabric of anti-infrared monitoring according to claim 1, its It is characterized in that, the condition of drying is in the step (2)：Speed is 40 ms/min, temperature is 110~120 DEG C.
- 8. a kind of preparation process of the water proof fire retardant polyamide fabric of anti-infrared monitoring according to claim 1, its It is characterized in that, rolls water-proof finish liquid in the step (4) before reverse side gluing is carried out, it is 1 that water-proof finish liquid, which includes mass ratio: 2: 1: 1 waterproofing agent DM-3680K, waterproofing agent DM-3665, waterproofing agent DM-1000 and waterproofing agent DTM648-2；The water-proof finish The magnesium chloride that additive amount is 4~6g/L is further included in liquid.
- 9. a kind of preparation process of the water proof fire retardant polyamide fabric of anti-infrared monitoring according to claim 1, its It is characterized in that, the viscosity in the step (4) during gluing is 110~130cps, and temperature is 175~180 DEG C, and speed is 40~50 M/min.
- 10. a kind of preparation process of the water proof fire retardant polyamide fabric of anti-infrared monitoring according to claim 9, its It is characterized in that, in the step (4) during gluing, the parameter of the coating blade of more than 1000D thicker open meshes is：Blade thickness 2mm, knife are away from 6mm, depression distance 2mm, tension pressure 0.4Kpa, 40 ms/min of speed；The ginseng of the coating blade of other close weaves Number is：Blade thickness 1mm, knife are away from 4mm, depression distance 4mm, tension pressure 0.45Kpa, 50 ms/min of speed.
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| CN108729220A (en) * | 2018-06-19 | 2018-11-02 | 南通全技纺织涂层有限公司 | Preparation method with floride-free waterproof, the fabric of waterborne flame retardant |
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| CN108729220A (en) * | 2018-06-19 | 2018-11-02 | 南通全技纺织涂层有限公司 | Preparation method with floride-free waterproof, the fabric of waterborne flame retardant |
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| CN110747666A (en) * | 2019-11-15 | 2020-02-04 | 四川鑫敬业化纤织带有限公司 | Nylon 56 flame-retardant infrared-resistant camouflage ribbon |
| CN112095349A (en) * | 2020-09-18 | 2020-12-18 | 苏州红旭新材料科技有限公司 | Method for manufacturing cloth of far infrared resistant tent outer net |
| CN112111980A (en) * | 2020-09-18 | 2020-12-22 | 苏州红旭新材料科技有限公司 | Manufacturing method of far infrared ray-proof flame-retardant fabric |
| CN112411195A (en) * | 2020-10-22 | 2021-02-26 | 浙江依莱特纺织有限公司 | Waterproof treatment method for grey cloth |
| CN112411195B (en) * | 2020-10-22 | 2023-12-26 | 浙江依莱特纺织有限公司 | Waterproof treatment method for grey cloth |
| CN112609450A (en) * | 2020-12-03 | 2021-04-06 | 绵阳佳禧印染有限责任公司 | Nylon 66 anti-infrared fabric and preparation method thereof |
| CN112609460A (en) * | 2020-12-04 | 2021-04-06 | 绵阳佳联印染有限责任公司 | Manufacturing process of high-strength wear-resistant waterproof fabric |
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