CN107964826A - A kind of preparation method of antirust waterproof and oilproof paper - Google Patents
A kind of preparation method of antirust waterproof and oilproof paper Download PDFInfo
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- CN107964826A CN107964826A CN201711131641.0A CN201711131641A CN107964826A CN 107964826 A CN107964826 A CN 107964826A CN 201711131641 A CN201711131641 A CN 201711131641A CN 107964826 A CN107964826 A CN 107964826A
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Classifications
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- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/10—Coatings without pigments
- D21H19/14—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/10—Coatings without pigments
- D21H19/14—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
- D21H19/20—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12 comprising macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D21H19/22—Polyalkenes, e.g. polystyrene
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/16—Sizing or water-repelling agents
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/18—Reinforcing agents
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H25/00—After-treatment of paper not provided for in groups D21H17/00 - D21H23/00
- D21H25/04—Physical treatment, e.g. heating, irradiating
- D21H25/06—Physical treatment, e.g. heating, irradiating of impregnated or coated paper
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
- D21H27/10—Packing paper
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Paper (AREA)
Abstract
The present invention provides a kind of preparation method of antirust waterproof and oilproof paper, comprise the following steps:(1)Stearic acid, ammonium hydroxide and distilled water are mixed, are heated to 65 75 DEG C of stirrings;(2)Room temperature is down to, adds sodium alginate, Arabic gum, caprolactam and glycerine stirring;(3)Polytetrafluoroethylene (PTFE), chitosan, sodium nitrite, triethylene tetramine, carbamide, benzyl salicylate and ethanol are added, is put into sonic oscillation instrument and carries out sonic oscillation;(4)Vacuum outgas removes bubble, is equably coated on it on wrapping paper using spreading rod;(5)Be put into electric heating constant-temperature blowing drying box it is dry after be placed on and carry out rewetting when 24 26 is small in climatic chamber and handle to obtain the final product.A kind of preparation method of antirust waterproof and oilproof paper of the present invention, prepared paper have good rust-proof effect, and waterproof oil-proof result is good, while also has extraordinary mechanical property.
Description
Technical field
The present invention relates to a kind of preparation method of antirust waterproof and oilproof paper.
Background technology
In history, due to being limited be subject to raw material and technology, paper was once a kind of invaluable material, later with
The continuous development of modern paper technology, the price of paper becomes more and more lower, it is just gradually widely used as packaging material.
Paper has the advantages of other packaging materials are incomparable as packaging material:Raw material sources extensively, cost economy, be easy to cut,
Technique is simple, light weight, is readily transported, has good printing performance, nontoxic and recoverable etc..On the other hand,
There are many geneogenous defects in original paper and cardboard without special processing:As surface gloss and flatness be not high and waterproof
Grease proofness difference etc., and with the raising of scientific and technological level, functional requirement for paper is also higher and higher, and plain paper is remote
It can not far meet these requirements.Therefore, research and development feature paper becomes irresistible trend.
The content of the invention
Technical problems to be solved:It is made the object of the present invention is to provide a kind of preparation method of antirust waterproof and oilproof paper
Standby paper has good rust-proof effect, and waterproof oil-proof result is good, while also has extraordinary mechanical property.
Technical solution:A kind of preparation method of antirust waterproof and oilproof paper, comprises the following steps:
(1)2-5g stearic acid, 1-2ml ammonium hydroxide and 50-100ml distilled water are mixed, it is small to be heated to 65-75 DEG C of stirring 2.5-3
When;(2)Room temperature is down to, adds 1-3g sodium alginates, 1-2g Arabic gums, 1-2g caprolactams and 5-8ml glycerine, is being turned
Stirred 30-50 minutes under fast 400-600r/min;
(3)Add 1-2g polytetrafluoroethylene (PTFE), 1-2g chitosans, 0.2-0.3g sodium nitrites, 0.1-0.3g triethylene tetramines,
0.1-0.2g carbamides, 0.2-0.5g benzyl salicylates and 5-10ml ethanol, are put into sonic oscillation instrument and are in ultrasonic power
Sonic oscillation is carried out under 300-400W 20-40 minutes;
(4)Vacuum outgas removes bubble, is equably coated on it on wrapping paper using spreading rod;
(5)Be put into electric heating constant-temperature blowing drying box it is 30-50 minutes dry after be placed on when 24-26 is small in climatic chamber into
Row rewetting is handled to obtain the final product.
Further, the preparation method of a kind of antirust waterproof and oilproof paper, the step(1)In be heated to 70
DEG C, when mixing time is 2.75 small.
Further, the preparation method of a kind of antirust waterproof and oilproof paper, the step(2)Middle rotating speed is
500r/min, mixing time are 40 minutes.
Further, the preparation method of a kind of antirust waterproof and oilproof paper, the step(3)Middle chitosan takes off
Acetyl degree is 90%, ultrasonic power 350W, and duration of oscillation is 25-35 minutes.
Further, the preparation method of a kind of antirust waterproof and oilproof paper, the step(4)Middle coating weight is
1.5-1.8g/m2。
Further, the preparation method of a kind of antirust waterproof and oilproof paper, the step(5)Middle temperature is 20-
25 DEG C, relative humidity 50%.
Beneficial effect:The antirust waterproof and oilproof paper of the present invention has good rust-proof effect, will wrap up one layer of paper of the present invention
Iron plate hang indoors 15 days after measure its rate of corrosion, minimum is only 3.733 × 10-4%, moisture-vapor transmission minimum 0.78
×10-11g·cm/(Pa·s·cm2), for oil resistant fat grade up to 7 grades, waterproof oil-proof result is good, while paper of the present invention also has
Extraordinary mechanical property, folding strength is up to 483 times, and tear index and tensile index highest are respectively up to 22.8mNm2/ g and
91.9N·m/g。
Embodiment
Embodiment 1
A kind of preparation method of antirust waterproof and oilproof paper, comprises the following steps:
(1)By 2g stearic acid, 1ml ammonium hydroxide and 50ml distilled water mix, be heated to 65 DEG C stirring 2.5 it is small when;
(2)Room temperature is down to, 1g sodium alginates, 1g Arabic gums, 1g caprolactams and 5ml glycerine are added, in rotating speed 400r/
Stirred 30 minutes under min;
(3)Add 1g polytetrafluoroethylene (PTFE), 1g chitosans, 0.2g sodium nitrites, 0.1g triethylene tetramines, 0.1g carbamides, 0.2g
Benzyl salicylate and 5ml ethanol, are put into sonic oscillation instrument and carry out sonic oscillation 20 minutes in the case where ultrasonic power is 300W;
(4)Vacuum outgas removes bubble, is equably coated on it on wrapping paper using spreading rod, coating weight 1.5g/m2;
(5)It is put into be placed on when 24 is small in climatic chamber after drying 30 minutes in electric heating constant-temperature blowing drying box and carries out rewetting
Handle to obtain the final product.
Embodiment 2
A kind of preparation method of antirust waterproof and oilproof paper, comprises the following steps:
(1)By 3g stearic acid, 1.5ml ammonium hydroxide and 60ml distilled water mix, be heated to 70 DEG C stirring 2.5 it is small when;
(2)Room temperature is down to, 1.5g sodium alginates, 1.5g Arabic gums, 1.5g caprolactams and 6ml glycerine are added, in rotating speed
Stirred 35 minutes under 450r/min;
(3)Add 1.5g polytetrafluoroethylene (PTFE), 1.5g chitosans, 0.25g sodium nitrites, 0.2g triethylene tetramines, 0.15g phosphinylidynes
Amine, 0.3g benzyl salicylates and 6ml ethanol, are put into sonic oscillation instrument the progress sonic oscillation 25 in the case where ultrasonic power is 350W and divide
Clock;
(4)Vacuum outgas removes bubble, is equably coated on it on wrapping paper using spreading rod, coating weight 1.6g/m2;
(5)It is put into be placed on when 24.5 is small in climatic chamber after drying 35 minutes in electric heating constant-temperature blowing drying box and is returned
Wet process to obtain the final product.
Embodiment 3
A kind of preparation method of antirust waterproof and oilproof paper, comprises the following steps:
(1)By 3.5g stearic acid, 1.5ml ammonium hydroxide and 75ml distilled water mix, be heated to 70 DEG C stirring 2.75 it is small when;
(2)Room temperature is down to, 2g sodium alginates, 1.5g Arabic gums, 1.5g caprolactams and 6.5ml glycerine are added, in rotating speed
Stirred 40 minutes under 500r/min;
(3)Add 1.5g polytetrafluoroethylene (PTFE), 1.5g chitosans, 0.25g sodium nitrites, 0.2g triethylene tetramines, 0.15g phosphinylidynes
Amine, 0.35g benzyl salicylates and 7.5ml ethanol, are put into sonic oscillation instrument and carry out sonic oscillation in the case where ultrasonic power is 350W
30 minutes;
(4)Vacuum outgas removes bubble, is equably coated on it on wrapping paper using spreading rod, coating weight 1.6g/m2;
(5)It is put into electric heating constant-temperature blowing drying box dry be placed on after forty minutes when 25 is small in climatic chamber and carries out rewetting
Handle to obtain the final product.
Embodiment 4
A kind of preparation method of antirust waterproof and oilproof paper, comprises the following steps:
(1)By 4g stearic acid, 1.5ml ammonium hydroxide and 90ml distilled water mix, be heated to 70 DEG C stirring 3 it is small when;
(2)Room temperature is down to, 2.5g sodium alginates, 1.5g Arabic gums, 1.5g caprolactams and 7ml glycerine are added, in rotating speed
Stirred 45 minutes under 550r/min;
(3)Add 1.5g polytetrafluoroethylene (PTFE), 1.5g chitosans, 0.25g sodium nitrites, 0.25g triethylene tetramines, 0.15g phosphinylidynes
Amine, 0.4g benzyl salicylates and 9ml ethanol, are put into sonic oscillation instrument the progress sonic oscillation 35 in the case where ultrasonic power is 350W and divide
Clock;
(4)Vacuum outgas removes bubble, is equably coated on it on wrapping paper using spreading rod, coating weight 1.7g/m2;
(5)It is put into be placed on when 25.5 is small in climatic chamber after drying 45 minutes in electric heating constant-temperature blowing drying box and is returned
Wet process to obtain the final product.
Embodiment 5
A kind of preparation method of antirust waterproof and oilproof paper, comprises the following steps:
(1)By 5g stearic acid, 2ml ammonium hydroxide and 100ml distilled water mix, be heated to 75 DEG C stirring 3 it is small when;
(2)Room temperature is down to, 3g sodium alginates, 2g Arabic gums, 2g caprolactams and 8ml glycerine are added, in rotating speed 600r/
Stirred 50 minutes under min;
(3)Add 2g polytetrafluoroethylene (PTFE), 2g chitosans, 0.3g sodium nitrites, 0.3g triethylene tetramines, 0.2g carbamides, 0.5g
Benzyl salicylate and 10ml ethanol, are put into sonic oscillation instrument and carry out sonic oscillation 40 minutes in the case where ultrasonic power is 400W;
(4)Vacuum outgas removes bubble, is equably coated on it on wrapping paper using spreading rod, coating weight 1.8g/m2;
(5)It is put into be placed on when 26 is small in climatic chamber after drying 50 minutes in electric heating constant-temperature blowing drying box and carries out rewetting
Handle to obtain the final product.
Comparative example 1
A kind of preparation method of antirust waterproof and oilproof paper, comprises the following steps:
(1)By 2g stearic acid, 1ml ammonium hydroxide and 50ml distilled water mix, be heated to 65 DEG C stirring 2.5 it is small when;
(2)Room temperature is down to, 1g caprolactams and 5ml glycerine is added, is stirred 30 minutes under rotating speed 400r/min;
(3)Add 1g polytetrafluoroethylene (PTFE), 1g chitosans, 0.2g sodium nitrites, 0.1g triethylene tetramines, 0.1g carbamides, 0.2g
Benzyl salicylate and 5ml ethanol, are put into sonic oscillation instrument and carry out sonic oscillation 20 minutes in the case where ultrasonic power is 300W;
(4)Vacuum outgas removes bubble, is equably coated on it on wrapping paper using spreading rod, coating weight 1.5g/m2;
(5)It is put into be placed on when 24 is small in climatic chamber after drying 30 minutes in electric heating constant-temperature blowing drying box and carries out rewetting
Handle to obtain the final product.
Comparative example 2
A kind of preparation method of antirust waterproof and oilproof paper, comprises the following steps:
(1)By 2g stearic acid, 1ml ammonium hydroxide and 50ml distilled water mix, be heated to 65 DEG C stirring 2.5 it is small when;
(2)Room temperature is down to, 1g sodium alginates, 1g Arabic gums, 1g caprolactams and 5ml glycerine are added, in rotating speed 400r/
Stirred 30 minutes under min;
(3)1g polytetrafluoroethylene (PTFE), 0.2g sodium nitrites, 0.1g triethylene tetramines, 0.1g carbamides and 5ml ethanol are added, is put into
In sonic oscillation instrument sonic oscillation is carried out in the case where ultrasonic power is 300W 20 minutes;
(4)Vacuum outgas removes bubble, is equably coated on it on wrapping paper using spreading rod, coating weight 1.5g/m2;
(5)It is put into be placed on when 24 is small in climatic chamber after drying 30 minutes in electric heating constant-temperature blowing drying box and carries out rewetting
Handle to obtain the final product.
Iron plate rate of corrosion is measured using indoor hanging test, and the iron plate for wrapping up one layer of paper of the present invention is hung 15 days indoors
After measure.
The assay method of moisture-vapor transmission is:The anhydrous calcium chloride of a tall regular weighing bottle, built-in 3g or so are taken, is cut
The lower pattern slightly larger than bottleneck is drawn, covers on bottleneck, edge is sealed with gummed paper, bottle is placed in relative humidity as 65%(34% it is dense
Sulfuric acid)Constant humidity drier in, weighed once every 2-4h to bottle with assay balance to determine the water absorption of anhydrous calcium chloride,
And it is accurate to 0.0001g.
Oil resistant fat grade assay method is using oil-drop experiment (559 pm-96 of Oil Kit Test-TAPPI T):Will
Height of the grease from 2.54cm
Degree is dropped onto on paper product to be measured, is gently wiped with clean cotton balls after 15 s.Oil droplet, which is penetrated into inside paper, can make its change
Secretly, represent that oil-resistant characteristic is not reaching to the grade that this oil droplet represents, do not produce and permeate this phenomenon, and number it is highest that
No.1, that is, represent the kit rating of tested paper product.Every group of sample does 5 experiments, does not differ 0.5 grade therebetween, is averaged conduct
The kit rating of the paper product.
The measure of folding strength uses standard GB/T 457-2002.
The measure of tear index uses standard GB/T 455-2002.
The measure of tensile index uses standard GB/T 12914-2008.
The partial properties index of the antirust waterproof and oilproof paper of the present invention see the table below 1, it will be seen that it has well
Rust-proof effect, its rate of corrosion is measured after the iron plate for wrapping up one layer of paper of the present invention is hung 15 days indoors, minimum only 3.733 ×
10-4%, moisture-vapor transmission minimum 0.78 × 10-11g·cm/(Pa·s·cm2), oil resistant fat grade up to 7 grades, prevent by waterproof
Oily effect is good, while paper of the present invention also has extraordinary mechanical property, and up to 483 times, tear index and anti-tensile refer to folding strength
Number highest is respectively up to 22.8mNm2/ g and 91.9Nm/g.
The partial properties index of the antirust waterproof and oilproof paper of the present invention of table 1
Claims (6)
- A kind of 1. preparation method of antirust waterproof and oilproof paper, it is characterised in that:Comprise the following steps:(1)2-5g stearic acid, 1-2ml ammonium hydroxide and 50-100ml distilled water are mixed, it is small to be heated to 65-75 DEG C of stirring 2.5-3 When;(2)Room temperature is down to, adds 1-3g sodium alginates, 1-2g Arabic gums, 1-2g caprolactams and 5-8ml glycerine, is being turned Stirred 30-50 minutes under fast 400-600r/min;(3)Add 1-2g polytetrafluoroethylene (PTFE), 1-2g chitosans, 0.2-0.3g sodium nitrites, 0.1-0.3g triethylene tetramines, 0.1-0.2g carbamides, 0.2-0.5g benzyl salicylates and 5-10ml ethanol, are put into sonic oscillation instrument and are in ultrasonic power Sonic oscillation is carried out under 300-400W 20-40 minutes;(4)Vacuum outgas removes bubble, is equably coated on it on wrapping paper using spreading rod;(5)Be put into electric heating constant-temperature blowing drying box it is 30-50 minutes dry after be placed on when 24-26 is small in climatic chamber into Row rewetting is handled to obtain the final product.
- A kind of 2. preparation method of antirust waterproof and oilproof paper according to claim 1, it is characterised in that:The step(1) In be heated to 70 DEG C, mixing time for 2.75 it is small when.
- A kind of 3. preparation method of antirust waterproof and oilproof paper according to claim 1, it is characterised in that:The step(2) Middle rotating speed is 500r/min, and mixing time is 40 minutes.
- A kind of 4. preparation method of antirust waterproof and oilproof paper according to claim 1, it is characterised in that:The step(3) The deacetylation of middle chitosan is 90%, ultrasonic power 350W, and duration of oscillation is 25-35 minutes.
- A kind of 5. preparation method of antirust waterproof and oilproof paper according to claim 1, it is characterised in that:The step(4) Middle coating weight is 1.5-1.8g/m2。
- A kind of 6. preparation method of antirust waterproof and oilproof paper according to claim 1, it is characterised in that:The step(5) Middle temperature is 20-25 DEG C, relative humidity 50%.
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Cited By (1)
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CN111411363A (en) * | 2019-01-04 | 2020-07-14 | 艾克索防腐研究有限公司 | Compositions and methods for pretreating substrates for subsequent fixation of vapor phase corrosion inhibitors |
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JP2003328292A (en) * | 2002-04-30 | 2003-11-19 | Yasuo Sakai | Paper material for food container and method for producing the paper material |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN111411363A (en) * | 2019-01-04 | 2020-07-14 | 艾克索防腐研究有限公司 | Compositions and methods for pretreating substrates for subsequent fixation of vapor phase corrosion inhibitors |
US11827806B2 (en) | 2019-01-04 | 2023-11-28 | Excor Korrosionsforschung Gmbh | Compositions and methods for pretreating substrates for the subsequent fixing of vapor phase corrosion inhibitors |
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