CN107938346A - 丝绸织物抗静电整理剂 - Google Patents

丝绸织物抗静电整理剂 Download PDF

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CN107938346A
CN107938346A CN201711243125.7A CN201711243125A CN107938346A CN 107938346 A CN107938346 A CN 107938346A CN 201711243125 A CN201711243125 A CN 201711243125A CN 107938346 A CN107938346 A CN 107938346A
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silk
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郭新华
张会良
叶萍
韩建钢
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Thai Fashion Apparel (suzhou) Co Ltd
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Abstract

本发明公开了丝绸织物抗静电整理剂。该静电整理剂包括以下按重量份数计的组分：壳聚糖2‑8份、改性丝蛋白12‑24份、聚氧乙烯多胺25‑42份、异丙醇钛1‑8份、银杏叶提取物25‑38份、椰油酰单乙醇胺8‑18份、聚乙二醇3‑8份、对苯二甲酸二甲酯24‑38份、十六烷基一甲基二乙羟基溴化铵1‑8份、丙烯酸乙酯18‑25份、油酸钠1‑5份。本发明丝绸织物抗静电整理剂通过添加丝蛋白，并对丝蛋白改性处理后结合其他组分制备得到的，该整理剂抗静电效果好，且干燥环境中抗静电效果持久。另外组分中银杏叶提取物和壳聚糖的协同作用，更提高了整理剂的抗菌抗老化的效果，提高了丝绸织物在太阳暴晒下的抗静电抗老化能力。

Description

丝绸织物抗静电整理剂
技术领域
本发明涉及织物整理领域，具体涉及一种丝绸织物抗静电整理剂。
背景技术
随着时代的发展，人们生活水平的不断提高，健康与时尚是人们追求的一种消费方式，现有的普通面料已经不能满足人们的需求。在众多的面料中，丝绸面料是我国面料上的一块瑰宝，因其轻盈、薄透等特点，深受人们的喜爱，但丝绸面料一直存在静电问题，干燥环境下，容易摩擦产生静电，吸附灰尘，影响衣着美观，如何使得丝绸面料抗静电能力强，抗静电时间久，且恶劣环境中仍然保证高的抗静电能力是我们继续解决的技术问题。
银杏叶中含有较多量的黄酮类物质，黄酮类化合物是一类存在于自然界的，具有2-苯基色原酮结构的化合物。它们的分子中有1个酮式羰基，第1位上的氧原子具有碱性，能与强酸成盐，其羟基衍生物为黄色，故又称黄碱素或黄酮。黄酮类化合物的分类主要有二氢黄酮醇类与二氢黄酮、二氢异黄酮与异黄酮、黄酮类黄酮醇类、花色素类和黄烷醇类等。黄酮类化合物具有诸多生物学活性，如具有明显抗氧化性；能抑制大肠杆菌和金黄色葡萄球菌等致病细菌，同时具有抗肺癌、乳腺癌和结肠癌等功效。
发明内容
针对现有技术的不足，本发明的目的在于提供一种丝绸织物抗静电整理剂，该整理剂处理后丝绸抗静电效果好，太阳下暴晒也不易变黄。
为解决现有技术问题，本发明采取的技术方案为：
丝绸织物抗静电整理剂，包括以下按重量份数计的组分：壳聚糖2-8份、改性丝蛋白12-24份、聚氧乙烯多胺25-42份、异丙醇钛1-8份、银杏叶提取物25-38份、椰油酰单乙醇胺8-18份、聚乙二醇3-8份、对苯二甲酸二甲酯24-38份、十六烷基一甲基二乙羟基溴化铵1-8份、丙烯酸乙酯18-25份、油酸钠1-5份。
作为改进的是，上述丝绸织物抗静电整理剂，包括以下按重量份数计的组分：壳聚糖6份、改性丝蛋白20份、聚氧乙烯多胺32份、异丙醇钛6份、银杏叶提取物30份、椰油酰单乙醇12份、聚乙二醇4份、对苯二甲酸二甲酯32份、十六烷基一甲基二乙羟基溴化铵4份、丙烯酸乙酯20份、油酸钠3份。
作为改进的是，所述壳聚糖的分子量为1500-2000。
作为改进的是，所述改性丝蛋白的制备方法，包括以下步骤：步骤1，将废蚕丝去除杂质，脱胶处理后捞出，自然晾干，清水洗涤2-5次至无滑腻感；步骤2，将洁净处理后的蚕丝置于醋酸锌溶液中，微波溶解10-20min后，移入旋转蒸发仪中浓缩至含水率20-30％的丝素溶液；步骤3，向丝素溶液中加入泡沫铝和马来酸接枝剂，搅拌均匀得到改性丝蛋白。
进一步改进的是，步骤1中脱胶处理所用的溶液为5-8g/L的碳酸氢钠溶，且碳酸氢钠的加入量为废蚕丝的1.5-5倍。
作进一步改进的是，步骤2中醋酸锌溶液的密度为1-2g/L。
进一步改进的是，步骤2中浓缩所用的温度为40-60℃。
进一步改进的是，步骤3中泡沫铝的加入量为废蚕丝干重的0.2-0.8倍，马来酸接枝剂的加入量为废蚕丝干重的0.01-0.05倍。
与现有技术相比，本发明丝绸织物抗静电整理剂通过添加丝蛋白，并对丝蛋白改性处理后结合其他组分制备得到的，该整理剂抗静电效果好，且干燥环境中抗静电效果持久。另外组分中银杏叶提取物和壳聚糖的协同作用，更是提高了整理剂的抗菌抗老化的效果，提高了丝绸织物在太阳暴晒下的抗静电抗老化能力。
具体实施方式
下面通过具体实施例对本发明作进一步详细介绍。
实施例1
丝绸织物抗静电整理剂，包括以下按重量份数计的组分：壳聚糖2份、改性丝蛋白12份、聚氧乙烯多胺25份、异丙醇钛1份、银杏叶提取物25份、椰油酰单乙醇胺8份、聚乙二醇3份、对苯二甲酸二甲酯24份、十六烷基一甲基二乙羟基溴化铵1份、丙烯酸乙酯18份、油酸钠1份。
所述壳聚糖的分子量为1500。
所述改性丝蛋白的制备方法，包括以下步骤：步骤1，将废蚕丝去除杂质，脱胶处理后捞出，自然晾干，清水洗涤2次至无滑腻感，脱胶处理所用的溶液为5-8g/L的碳酸氢钠溶，且碳酸氢钠的加入量为废蚕丝的1.5倍；步骤2，将洁净处理后的蚕丝置于浓度1g/L醋酸锌溶液中，微波溶解10-20min后，移入旋转蒸发仪中40℃浓缩至含水率20％的丝素溶液；步骤3，向丝素溶液中加入泡沫铝和马来酸接枝剂，搅拌均匀得到改性丝蛋白，其中，泡沫铝的加入量为废蚕丝干重的0.2倍，马来酸接枝剂的加入量为废蚕丝干重的0.01倍。
实施例2
丝绸织物抗静电整理剂，包括以下按重量份数计的组分：壳聚糖6份、改性丝蛋白20份、聚氧乙烯多胺32份、异丙醇钛6份、银杏叶提取物30份、椰油酰单乙醇12份、聚乙二醇4份、对苯二甲酸二甲酯32份、十六烷基一甲基二乙羟基溴化铵4份、丙烯酸乙酯20份、油酸钠3份。
所述壳聚糖的分子量为1800。
所述改性丝蛋白的制备方法，包括以下步骤：步骤1，将废蚕丝去除杂质，脱胶处理后捞出，自然晾干，清水洗涤4次至无滑腻感，脱胶处理所用的溶液为6g/L的碳酸氢钠溶，且碳酸氢钠的加入量为废蚕丝的3.2倍；步骤2，将洁净处理后的蚕丝置于1.2g/L醋酸锌溶液中，微波溶解115min后，移入旋转蒸发仪中50℃浓缩至含水率25％的丝素溶液；步骤3，向丝素溶液中加入泡沫铝和马来酸接枝剂，搅拌均匀得到改性丝蛋白，其中泡沫铝的加入量为废蚕丝干重的0.6倍，马来酸接枝剂的加入量为废蚕丝干重的0.03倍。
实施例3
丝绸织物抗静电整理剂，包括以下按重量份数计的组分：壳聚糖2-8份、改性丝蛋白12-24份、聚氧乙烯多胺25-42份、异丙醇钛1-8份、银杏叶提取物25-38份、椰油酰单乙醇胺8-18份、聚乙二醇3-8份、对苯二甲酸二甲酯24-38份、十六烷基一甲基二乙羟基溴化铵1-8份、丙烯酸乙酯18-25份、油酸钠1-5份。
所述壳聚糖的分子量为2000。
所述改性丝蛋白的制备方法，包括以下步骤：步骤1，将废蚕丝去除杂质，脱胶处理后捞出，自然晾干，清水洗涤5次至无滑腻感，脱胶处理所用的溶液为8g/L的碳酸氢钠溶，且碳酸氢钠的加入量为废蚕丝的5倍；步骤2，将洁净处理后的蚕丝置于2g/L醋酸锌溶液中，微波溶解20min后，移入旋转蒸发仪中60℃浓缩至含水率30％的丝素溶液；步骤3，向丝素溶液中加入泡沫铝和马来酸接枝剂，搅拌均匀得到改性丝蛋白，其中，泡沫铝的加入量为废蚕丝干重的0.8倍，马来酸接枝剂的加入量为废蚕丝干重的0.05倍。
对比例1
除丝蛋白不改性处理外，其余同实施例2。
对比例2
除不含银杏叶提取物外，其余同实施例2。
对比例3
除不含壳聚糖外，其余同实施例2。
用实施例1-3和对比例1-3的抗静电整理剂处理丝绸织物后，测定丝绸织物的抗静电、抗老化等相关效果，结果如下表所示。其中，处理前丝绸的最大静电压为800V，比电阻0.85×1015Ω/cm。
从上述结果可以看出，本发明丝绸织物抗静电整理剂处理后的丝绸抗静电和抗菌效果明显。太阳暴晒后，抗静电能力并未受到较大影响，高温环境下可抗老化能力强。
另外，本发明不限于上述实施方式，只要在不超出本发明的范围内，可以采取各种方式实施本发明。

Claims (8)

1.丝绸织物抗静电整理剂，其特征在于，包括以下按重量份数计的组分：壳聚糖2-8份、改性丝蛋白12-24份、聚氧乙烯多胺25-42份、异丙醇钛1-8份、银杏叶提取物25-38份、椰油酰单乙醇胺8-18份、聚乙二醇3-8份、对苯二甲酸二甲酯24-38份、十六烷基一甲基二乙羟基溴化铵1-8份、丙烯酸乙酯18-25份、油酸钠1-5份。
2.根据权利要求1所述的丝绸织物抗静电整理剂，其特征在于，包括以下按重量份数计的组分：壳聚糖6份、改性丝蛋白20份、聚氧乙烯多胺32份、异丙醇钛6份、银杏叶提取物30份、椰油酰单乙醇12份、聚乙二醇4份、对苯二甲酸二甲酯32份、十六烷基一甲基二乙羟基溴化铵4份、丙烯酸乙酯20份、油酸钠3份。
3.根据权利要求1所述的丝绸织物抗静电整理剂，其特征在于，所述壳聚糖的分子量为1500-2000。
4.根据权利要求1或2所述的丝绸织物抗静电整理剂，其特征在于，所述改性丝蛋白的制备方法，包括以下步骤：步骤1，将废蚕丝去除杂质，脱胶处理后捞出，自然晾干，清水洗涤2-5次至无滑腻感；步骤2，将洁净处理后的蚕丝置于醋酸锌溶液中，微波溶解10-20min后，移入旋转蒸发仪中浓缩至含水率20-30%的丝素溶液；步骤3，向丝素溶液中加入泡沫铝和马来酸接枝剂，搅拌均匀得到改性丝蛋白。
5.根据权利要求4所述的丝绸织物抗静电整理剂，其特征在于，步骤1中脱胶处理所用的溶液为5-8g/L的碳酸氢钠溶，且碳酸氢钠的加入量为废蚕丝的1.5-5倍。
6.根据权利要求4所述的丝绸织物抗静电整理剂，其特征在于，步骤2中醋酸锌溶液的密度为1-2g/L。
7.根据权利要求4所述的丝绸织物抗静电整理剂，其特征在于，步骤2中浓缩所用的温度为40-60℃。
8.根据权利要求4所述的丝绸织物抗静电整理剂，其特征在于，步骤3中泡沫铝的加入量为废蚕丝干重的0.2-0.8倍，马来酸接枝剂的加入量为废蚕丝干重的0.01-0.05倍。
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