Antibacterial soft liner materials for denture
Technical field
The present invention relates to soft liner materials for denture technical field, especially a kind of antibacterial soft liner materials for denture.
Background technology
Soft liner materials for denture, also known as flexible denture gasket material, can utilize its elastic deformation buffering snap-in force, close artificial tooth
Tissue surface and tooth grain mucosal contact relation, and improve denture retention using tissue undercut area, it is that clinically common alleviate lives
The important measures for the symptoms such as Malretention that dynamic artificial tooth occurs during wearing, repeatedly tenderness, masticatory efficiency be low.Can as one kind
Long-time service and the material contacted with oral mucosa surface, the stability of its performance and the disease of cari oris mucosa easily triggered are limitations
Its principal element applied.The relation that soft liner materials for denture occurs with denture stomatitis, is the major issue of clinician's concern,
And the key for causing denture stomatitis to occur is adhesion of the microorganism especially Candida albicans to soft lining material.Therefore, research and develop
It is a kind of to keep stablizing under physiological status, there is bonds well performance and be resistant to the denture soft lining material of candida albicans infection
Material, has important clinical meaning.
The content of the invention
The purpose of the present invention is:A kind of stabilization under physiological status is provided, there is good adhesive property and be resistant to white
The soft liner materials for denture of monilial infection.
In order to solve the above technical problems, the technical solution adopted by the present invention is as follows:
A kind of antibacterial soft liner materials for denture, its mass parts composition are as follows:80-100 parts of rubber mass, vulcanizing activator 1.2-
2.8 parts, 0.8-3.2 parts of stearic acid, 0.2-0.8 parts of magnesia, 0.1-0.9 parts of vitamin E;
The rubber mass is made of holly glue, olive glue and butadiene rubber, the matter of holly glue, olive glue and butadiene rubber
Amount is than being 10:1-1.8:5.
Preferably, the antibacterial soft liner materials for denture is handled using the mixed solution of seaweed and dietary alkali, in mixed solution
The mass fraction of seaweed is 20%, and the mass fraction of dietary alkali is 30%.
Preferably, the holly glue is made using following methods:By leaf of Chinese ilex spontaneous fermentation 15-18d, by ripe Chinese ilex
Fruit is mixed in a certain ratio with the leaf of Chinese ilex to ferment, adds water infusion, after filtering, it is 1.1g/cm that filtrate, which is endured to concentration,3, obtain the winter
Blue or green glue.
Preferably, the olive glue is made using following methods:By olive fruit spontaneous fermentation 15-18d, remove dento liva,
Add water infusion, after filtering, it is 1.1g/cm that filtrate, which is endured to concentration,3, obtain olive glue.
Preferably, the mass ratio of the holly glue, olive glue and butadiene rubber is 10:1.5:5.
The beneficial effect of technical solution using the present invention is:
1st, rubber mass is made in holly glue, olive glue and butadiene rubber in the present invention, improves sterilization, the suppression of rubber mass
Bacterium effect, helps to protect gum, improves oral health.
2nd, the preparation method of holly glue and olive glue is simple and environmentally-friendly pollution-free in the present invention, and obtained product health is harmless,
Improve safety in utilization.
Embodiment
With reference to embodiment, the invention will be further described.
Embodiment 1
A kind of antibacterial soft liner materials for denture, its mass parts composition are as follows:It is 80 parts of rubber mass, 1.2 parts of vulcanizing activator, hard
0.8 part of resin acid, 0.2 part of magnesia, 0.1 part of vitamin E;Rubber mass is made of holly glue, olive glue and butadiene rubber, Chinese ilex
The mass ratio of glue, olive glue and butadiene rubber is 10:1:5, holly glue is made using following methods in the present embodiment:By leaf of Chinese ilex
Spontaneous fermentation 15d, ripe holly berry is mixed in a certain ratio with the leaf of Chinese ilex to ferment, adds water infusion, after filtering, filtrate is endured
It is 1.1g/cm to concentration3, obtain holly glue.
Olive glue is made using following methods in the present embodiment:By olive fruit spontaneous fermentation 15d, remove dento liva, add water
Infusion, after filtering, it is 1.1g/cm that filtrate, which is endured to concentration,3, obtain olive glue.
Antibacterial soft liner materials for denture is handled using the mixed solution of seaweed and dietary alkali in the present embodiment, sea in mixed solution
The mass fraction of algae is 20%, and the mass fraction of dietary alkali is 30%.
Embodiment 2
A kind of antibacterial soft liner materials for denture, its mass parts composition are as follows:90 parts of rubber mass, 2 parts of vulcanizing activator, tristearin
2 parts of acid, 0.5 part of magnesia, 0.5 part of vitamin E;Rubber mass is made of holly glue, olive glue and butadiene rubber, holly glue,
The mass ratio of olive glue and butadiene rubber is 10:1.5:5, holly glue is made using following methods in the present embodiment:By leaf of Chinese ilex
Spontaneous fermentation 16d, ripe holly berry is mixed in a certain ratio with the leaf of Chinese ilex to ferment, adds water infusion, after filtering, filtrate is endured
It is 1.1g/cm to concentration3, obtain holly glue.
Olive glue is made using following methods in the present embodiment:By olive fruit spontaneous fermentation 16d, remove dento liva, add water
Infusion, after filtering, it is 1.1g/cm that filtrate, which is endured to concentration,3, obtain olive glue.
Antibacterial soft liner materials for denture is handled using the mixed solution of seaweed and dietary alkali in the present embodiment, sea in mixed solution
The mass fraction of algae is 20%, and the mass fraction of dietary alkali is 30%.
Embodiment 3
A kind of antibacterial soft liner materials for denture, its mass parts composition are as follows:100 parts of rubber mass, 2.8 parts of vulcanizing activator,
3.2 parts of stearic acid, 0.8 part of magnesia, 0.9 part of vitamin E;The rubber mass is by holly glue, olive glue and butadiene rubber group
Into the mass ratio of holly glue, olive glue and butadiene rubber is 10:1.8:5, holly glue uses following methods system in the present embodiment
:By leaf of Chinese ilex spontaneous fermentation 18d, ripe holly berry is mixed in a certain ratio with the leaf of Chinese ilex to ferment, adds water infusion, mistake
After filter, it is 1.1g/cm that filtrate, which is endured to concentration,3, obtain holly glue.
Olive glue is made using following methods in the present embodiment:By olive fruit spontaneous fermentation 18d, remove dento liva, add water
Infusion, after filtering, it is 1.1g/cm that filtrate, which is endured to concentration,3, obtain olive glue.
Antibacterial soft liner materials for denture is handled using the mixed solution of seaweed and dietary alkali in the present embodiment, sea in mixed solution
The mass fraction of algae is 20%, and the mass fraction of dietary alkali is 30%.
Antibacterial soft liner materials for denture in embodiment 1-3 is made using common preparation method.
Water imbibition, dissolubility test, in this experiment, Wo Menxuan are carried out to the antibacterial soft liner materials for denture in the present invention
Selecting two kinds, clinically common acrylic resin and silastic material are as reference object, respectively in distilled water and artificial saliva
Place 7-30 days in two media, contrasted with the material of the present invention (in embodiment 2).
(1) preparation of artificial saliva
The formula of artificial saliva is as shown in table 1, adds 1l distilled water, adjusts pH to 7.0, manually work saliva is put after configuration completion
Enter and be mixed evenly in 37 DEG C of waters bath with thermostatic control, it is spare.
Table 1
Component |
Content mg/l |
Potassium chloride |
11200 |
Sodium chloride |
6700 |
Disodium hydrogen phosphate |
260 |
Potassium dihydrogen phosphate |
200 |
Saleratus |
1500 |
Potassium rhodanate |
330 |
(2) specific experiment:
The sample prepared is cleaned by ultrasonic 10min by a in distilled water, is then disappeared under the conditions of 3 atmospheric pressure, 121 DEG C
Malicious 20min, is then placed in 30 DEG C of drier and stores 24h, after move in the drier of room temperature and store 30min, then weigh,
Record weight m1;
Each group sample is put into 37 DEG C of distilled water and artificial saliva stores 30d respectively by b, then respectively by sample from water
Middle taking-up, is gently done solid work macroscopic water stain with blotting paper, dries 15s in atmosphere, when taking out 1min or so in water, is claimed
Weight, record weight m2;
Sample is placed again into drier by c, when quality is constant again, records weight m3;
Sample water absorption rate and dissolution rate are calculated respectively;
The water absorption rate and meltage of the present invention meets regulation.
It is complete by above-mentioned description, relevant staff using the above-mentioned desirable embodiment according to the present invention as enlightenment
Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention
Property scope is not limited to the content on specification, it is necessary to determines its technical scope according to right.