CN107898000A - A kind of method for reducing reconstituted tobacco plus fiber dosage - Google Patents
A kind of method for reducing reconstituted tobacco plus fiber dosage Download PDFInfo
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- CN107898000A CN107898000A CN201711227315.XA CN201711227315A CN107898000A CN 107898000 A CN107898000 A CN 107898000A CN 201711227315 A CN201711227315 A CN 201711227315A CN 107898000 A CN107898000 A CN 107898000A
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- Prior art keywords
- fiber
- sepiolite
- inorfil
- tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
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Abstract
The invention discloses a kind of method for reducing reconstituted tobacco plus fiber dosage, it is the plus fiber (wood pulp, jute pulp) substituted with natural sepiolite inorfil part in reconstituted tobacco production, and paper substrate is manufactured paper with pulp into after being mixed with tobacco slurry, reconstituted tobacco is made after coated, dry again, cutting, so as to reduce the dosage of plus fiber.Papermaking-method reconstituted tobaccos prepared by the method for the present invention, can reduce plus fiber dosage 20% 30%, significantly reduce the exogenous xylon gas of papermaking-method reconstituted tobaccos and are remained with oral cavity, so as to significantly improve the aesthetic quality of reconstituted tobacco product.
Description
Technical field
The present invention relates to papermaking-method reconstituted tobaccos production technical field, and in particular to one kind reduces reconstituted tobacco plus fiber
The method of dosage.
Background technology
Papermaking-method reconstituted tobaccos are to use paper process principle, it is impossible to are directly used in the cigarettes such as offal, the offal of cigarette products
Grassland expects, manufacture paper with pulp, be coated with by extraction, slurrying, base, drying, cutting, the technique such as perfuming and be made.Due to tobacco material fiber
Short and few, heteroproteose cell is more, and tobacco slurry can not provide enough physical strengths during paper is manufactured paper with pulp into and manufacture paper with pulp to ensure
Journey is smoothed out, therefore, a certain amount of wood pulp of general choice addition or ramie pulp fiber in papermaking-method reconstituted tobaccos production process
To provide certain physical strength.However, difference lies in reconstituted tobacco for the core of papermaking-method reconstituted tobaccos and traditional paper industry
Finally enter cigarette product together with other natural tobacco raw materials.Therefore, the addition of additional wood pulp or ramie pulp fiber is to reproducing cigarette
The aesthetic quality of leaf product has more negative impact, such as increases exogenous miscellaneous gas, reduces oral cavity comfort level, increase irritation
Etc. distinct disadvantage.How the addition of plus fiber is reduced as far as possible on the premise of certain paper substrate physical strength is provided,
One of hot issue as reconstituted tobacco industry research.Wear chief and (wear chief, Wang Shuhua, Su Yao, wait to discard gunnysack fiber and making
Application [J] Paper Science ＆ Technologies in paper method reconstituted tobacco, 2016 (3):39-44.) et al. it have selected cheap discarded fiber crops
Bag fiber part substitutes plus fiber, obtains preferable application effect；Li Wenyu have studied sugarcane fiber partly substitute it is additional
(Li Wenyu, Xiao Xuanhu, Liu Weijuan, wait application of the sugarcane fibers in papermaking-method reconstituted tobaccos production to application effect in fiber
[J] paper and papermaking, 2014,33 (1):18-20)；(Zhang Linglong, Liang Fengling, Liu Fei, wait a kind of cotton stalk bark fibre generations to Zhang Linglong
The method that papermaking-method reconstituted tobaccos are prepared for wood pulp cellulose, CN105286078A.2016.) then invent a kind of cotton stalk bark replacement
Wood pulp prepares method of reconstituted tobacco, etc..
Although numerous studies attempt to substitute wood pulp or ramie pulp fiber using non-tobacco plant fiber to improve reconstituted tobacco
Aesthetic quality, but non-tobacco vegetative fiber can not avoid producing band in the cracking process that burns as complicated organism
There is the chemical composition of the bad breath such as xylon gas, therefore vegetalitas plus fiber limits its usage amount in chemical nature,
Constrain its using effect.
Sepiolite, as a kind of naturally occurring inorfil raw material, has been widely applied in traditional paper industry.With
On the manufacturing paper with pulp altogether of plant fiber, microexamination shows (Yan Quanxiang, Yuan Jizu, Hu Liuqiu sepiolites and plant composite papermaking fiber
Preparation [J] paper and papermaking, 2008,27 (4):40-42.), sepiolite fibre is wrapped in plant fiber with tridimensional network
Surface, obtain the effect suitable with pure wood pulp paper, natural sepiolite fiber not only has filling capacity, it is often more important that,
, can be with intensity of the substituted plant fiber without reducing paper due to its special fibre structure.Natural sepiolite fiber conduct
Paper making raw material, applied to some speciality paper production industries, possesses extremely vast potential for future development.
Research through the present invention finds that sepiolite belongs to a kind of aqueous silicic acid for possessing fibre morphology in chemical nature
Magnesium, it is possessing outside absorption, decoloration and scattered characteristic, also has high heat endurance, heat-resisting quantity is up to 1500-1700
℃.Sepiolite fibre enumerates paper strength height, heat endurance good (being not involved in burning cracking) two additional plants of reconstituted tobacco
Property fiber institute can not possibly both with core capabilities.Therefore, plus fiber of the natural sepiolite fiber as reconstituted tobacco, tool are selected
Standby stronger innovative and practicality.
The content of the invention
It is outer the purpose of the present invention is substituting the wood pulp in reconstituted tobacco, jute pulp etc. using natural sepiolite inorfil part
Add fiber, there is provided a kind of new method for reducing reconstituted tobacco plus fiber dosage, improving reconstituted tobacco product sensory quality.
The present invention solves technical problem, adopts the following technical scheme that：
The method that the present invention reduces reconstituted tobacco plus fiber dosage, is substituted again with natural sepiolite inorfil part
The plus fiber in leaf tobacco production is made, and paper substrate is manufactured paper with pulp into after being mixed with tobacco slurry, then is made after coated, dry, cutting
Reconstituted tobacco product, so as to reduce the dosage of plus fiber.
Wherein, the natural sepiolite inorfil is using natural fiber sepiolite raw ore as raw material, through discongesting removal of impurities
After be made.The natural fiber sepiolite raw ore is preferably that Turkey originates in fibrous sepiolite raw ore.Through fibre morphology point
Analysis and thermogravimetric analysis show that the high-quality sepiolite fibre length of Turkey's production is longer, length and width are higher, and thermal inertia is preferable, can
Preferably meet the requirement of reconstituted tobacco plus fiber
The plus fiber is wood pulp cellulose and/or ramie pulp fiber.
The method of the present invention specifically comprises the following steps：
(1) after natural fiber sepiolite raw ore being soaked 24h by 7.5% pulp density, addition accounts for the raw ore matter
The calgon of amount 2.0% makees dispersant, stirs 60min under the rotating speed of 500r/min, is then sonicated 30min, finally
Standing sedimentation 12h, takes upper strata suspended matter, obtains natural sepiolite inorfil；
(2) by tobacco slurry raw material (the offal, residue) defibrination in fiberizer, tobacco slurry is obtained, controls tobacco pulp
Expect beating degree in 35 ± 2 ° of SR；
(3) natural sepiolite inorfil and plus fiber are mixed with tobacco slurry, is ultrasonically treated to fiber and disperses
It is even, then manufacture paper with pulp and be dried to paper substrate；
(4) by made of the tobacco material extract coating fluid according to 38 ± 2% spreading rate to step (3) in obtain
Paper substrate is coated, and reconstituted tobacco product is made after dry, cutting.
Wherein, the addition upper limit of the natural sepiolite inorfil is to meet the minimum tensile strength of reconstituted tobacco production
It is required that.Preferably, with the addition of for natural sepiolite inorfil accounts for natural sepiolite inorfil and plus fiber gross mass
20%~30%.
The mass ratio of the gross mass and tobacco slurry of natural sepiolite inorfil and plus fiber is 1 in step (3):6
~10.
The beneficial effects of the invention are as follows：First, natural sepiolite derives from a wealth of sources, is cheap, than commercially available wood pulp, jute pulp etc.
Plus fiber has obvious cost advantage；Secondly, add the papermaking-method reconstituted tobaccos of natural sepiolite inorfil with it is common
Paper process thin slice is compared, and has that aroma quality is high, dense miscellaneous gas is few, good after-taste absolute predominance on aesthetic quality, and with sea
The increasing of afrodite natural fiber dosage, indices significantly improve；In addition, addition natural sepiolite fiber is paper-making method reconstructed
Tobacco leaf substrate can keep stronger physical property, be fully able to the needs for meeting reconstituted tobacco amplification production.
Embodiment
The present invention is described in further detail below by embodiment, but embodiment is not to the technology of the present invention
The restriction of scheme.
Embodiment 1
The method that the present embodiment reduces reconstituted tobacco plus fiber dosage, step are as follows：
(1) after Turkey being originated in fibrous sepiolite raw ore by 7.5% pulp density immersion 24h, addition accounts for raw ore
The calgon of quality 2.0% makees dispersant, and 60min is stirred under the rotating speed of 500r/min, is then sonicated 30min, most
Standing sedimentation 12h afterwards, takes upper strata suspended matter, obtains natural sepiolite inorfil；
(2) by absolute dry mass be 100g tobacco slurry raw material (offal, residue) in the highly concentrated mill of II types of KRK 2500-
Defibrination in fiberizer, fixed abrasive disk space, repeatedly measures beating degree, control tobacco slurry beating degree is in 35 ± 2 ° of SR.
(3) the natural sepiolite inorfil and broad-leaved wood fiber (sepiolite by total absolute dry mass for 10g：Leaf wood
(mass ratio, similarly hereinafter) is 1:9) mixed with 90g tobacco slurries, be ultrasonically treated 30min, journey is disperseed using microscope monitoring fiber
Degree, manufactures paper with pulp after fiber degree of scatter is preferable and is dried to paper substrate.
(4) by made of the tobacco material extract coating fluid according to 38% spreading rate to step (3) in obtained paper
Base is coated, and reconstituted tobacco is made after dry, cutting, and products obtained therefrom is labeled as C1, measure tensile strength, Filling power, pine
After the paper physical index such as thickness, cigarette is made, sense organ product are completed by professional judging panel and are inhaled.
Embodiment 2
The method that the present embodiment reduces reconstituted tobacco plus fiber dosage, its step is same as Example 1, and difference exists
The absolute dry mass of natural sepiolite inorfil and broad-leaved wood fiber ratio is 2 in step (3):8, obtained reconstituted tobacco production
Product are labeled as C2.
Embodiment 3
The method that the present embodiment reduces reconstituted tobacco plus fiber dosage, its step is same as Example 1, and difference exists
The absolute dry mass of natural sepiolite inorfil and broad-leaved wood fiber ratio is 3 in step (3):7, obtained reconstituted tobacco production
Product are labeled as C3.
Embodiment 4
The method that the present embodiment reduces reconstituted tobacco plus fiber dosage, its step is same as Example 1, and difference exists
The absolute dry mass of natural sepiolite inorfil and broad-leaved wood fiber ratio is 4 in step (3):6, obtained reconstituted tobacco production
Product are labeled as C4.
Embodiment 5
The method that the present embodiment reduces reconstituted tobacco plus fiber dosage, its step is same as Example 1, and difference exists
The absolute dry mass of natural sepiolite inorfil and broad-leaved wood fiber ratio is 5 in step (3):5, obtained reconstituted tobacco production
Product are labeled as C5.
Common reconstituted tobacco (the i.e. step that will be prepared under the obtained reconstituted tobacco of above-described embodiment and the same terms
(3) natural sepiolite inorfil, all broad-leaved wood fibers of 10g are not added in) performance comparison is carried out, its mechanics is tested respectively
Performance, filling capacity and structural behaviour, the results are shown in Table 1：
1. natural inorganic fiber part of table substitutes wood pulp cellulose reconstituted tobacco physical performance data
| Cigarette sample | Tensile strength/kNm-1 | Filling power/cm3·g-1 | Bulk cm3·g-1 |
| C1 | 1.07 | 6.25 | 2.10 |
| C2 | 0.91 | 6.27 | 2.12 |
| C3 | 0.80 | 6.31 | 2.13 |
| C4 | 0.64 | 6.29 | 2.11 |
| C5 | Less than lower limit | / | / |
| Common reconstituted tobacco product | 1.01 | 6.29 | 2.12 |
It can be obtained from table 1, substitute the reconstruction cigarette of wood pulp cellulose preparation under equal conditions by natural sepiolite inorfil part
Leaf is in tensile strength as the overall trend for first increasing and reducing afterwards, wherein C1 (10%) is presented in the increasing of natural inorganic fiber dosage
Tensile strength is maximum, and is much larger than common reconstituted tobacco product, the slightly below common reconstituted tobacco product since C2 (20%)；When
When additive amount reaches 50%, due to system intensity it is too low and can not be into paper.And for Filling power, bulk two indices, naturally
The addition of inorfil does not influence significantly.From data as can be seen that C1, C2, C3, C4 can meet reconstituted tobacco physics
The needs of performance.
Part substitutes the reconstituted tobacco product of reconstituted tobacco wood pulp cellulose and the contrast of common reconstituted tobacco product sensory is smoked panel test
The results are shown in Table 2：
2. sense organ of table contrasts smoking result
Note：" 0 " represents initial value or unchanged；"+" represents to improve；" ++ " represents to be obviously improved；"-" represents index drop
It is low.
It can be obtained from table 2, compared with common papermaking-method reconstituted tobaccos product, with the addition of the reconstituted tobacco production of natural inorganic fiber
Product have different degrees of improvement in aroma quality, perfume quantity, miscellaneous gas, irritation, mouthfeel.Wherein, C2 improves pleasant impression most bright
Aobvious, C3, C4 improve miscellaneous gas the most obvious；But C4 sample stimulus is big compared with mill run at the same time.In terms of comprehensive, in aesthetic quality
On, 20%-30% natural inorganic fiber additive amounts are more suitable.
In terms of comprehensive, additional wood pulp cellulose is substituted using natural sepiolite inorfil part to reduce reconstituted tobacco product
Outer fibre dosage, possesses preferable practicality and novelty.
The foregoing is merely the exemplary embodiment of the present invention, it is not intended to limit the invention, it is all the present invention's
All any modification, equivalent and improvement made within spirit and principle etc., should all be included in the protection scope of the present invention.
Claims (8)
1. a kind of method for reducing reconstituted tobacco plus fiber dosage, it is characterized in that：It is with natural sepiolite inorfil part
The plus fiber in reconstituted tobacco production is substituted, and paper substrate is manufactured paper with pulp into after being mixed with tobacco slurry, then coated, dry, cutting
Reconstituted tobacco is made afterwards, so as to reduce the dosage of plus fiber.
2. according to the method described in claim 1, it is characterized in that：The natural sepiolite inorfil is with natural fiber
Sepiolite raw ore is raw material, is made after discongesting removal of impurities.
3. according to the method described in claim 2, it is characterized in that：The natural fiber sepiolite raw ore originates in for Turkey
Fibrous sepiolite raw ore.
4. according to the method described in claim 2, it is characterized in that：The plus fiber is wood pulp cellulose and/or ramie pulp fiber.
5. according to the method described in claim 1, it is characterised in that it includes following steps：
(1) after natural fiber sepiolite raw ore being soaked 24h by 7.5% pulp density, addition accounts for the ore quality
2.0% calgon makees dispersant, stirs 60min under the rotating speed of 500r/min, is then sonicated 30min, last quiet
Sedimentation 12h is put, upper strata suspended matter is taken, obtains natural sepiolite inorfil；
(2) by tobacco slurry raw material in fiberizer defibrination, obtain tobacco slurry, control tobacco slurry beating degree at 35 ± 2 °
SR；
(3) natural sepiolite inorfil and plus fiber are mixed with tobacco slurry, is ultrasonically treated to fiber and is uniformly dispersed, so
After manufacture paper with pulp and be dried to paper substrate；
(4) by made of the tobacco material extract coating fluid according to 38 ± 2% spreading rate to step (3) in obtained paper substrate
It is coated, reconstituted tobacco is made after dry, cutting.
6. method according to claim 1 or 5, it is characterised in that：The addition upper limit of the natural sepiolite inorfil
To meet the minimum tensile strength requirement of reconstituted tobacco production.
7. according to the method described in claim 5, it is characterized in that：Natural sepiolite inorfil and additional fibre in step (3)
The gross mass of dimension and the mass ratio of tobacco slurry are 1:6~10.
8. according to the method described in claim 6, it is characterized in that：Natural sepiolite inorfil with the addition of in step (3)
Account for the 20%~30% of natural sepiolite inorfil and plus fiber gross mass.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711227315.XA CN107898000A (en) | 2017-11-29 | 2017-11-29 | A kind of method for reducing reconstituted tobacco plus fiber dosage |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711227315.XA CN107898000A (en) | 2017-11-29 | 2017-11-29 | A kind of method for reducing reconstituted tobacco plus fiber dosage |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110025036A (en) * | 2019-05-10 | 2019-07-19 | 湖北中烟工业有限责任公司 | A kind of preparation method of sweet orange odor type reconstituted tobacco |
| CN110679982A (en) * | 2019-11-15 | 2020-01-14 | 湖北中烟工业有限责任公司 | Method for reducing dosage of extra fiber of special sheet without burning during heating |
| CN112106729A (en) * | 2020-10-28 | 2020-12-22 | 童萍 | Modeling method for mice with depression, liver depression and spleen deficiency syndrome |
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| CN104902767A (en) * | 2012-09-21 | 2015-09-09 | R.J.雷诺兹烟草公司 | Fibrous composite tobacco-containing materials |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110025036A (en) * | 2019-05-10 | 2019-07-19 | 湖北中烟工业有限责任公司 | A kind of preparation method of sweet orange odor type reconstituted tobacco |
| CN110679982A (en) * | 2019-11-15 | 2020-01-14 | 湖北中烟工业有限责任公司 | Method for reducing dosage of extra fiber of special sheet without burning during heating |
| CN112106729A (en) * | 2020-10-28 | 2020-12-22 | 童萍 | Modeling method for mice with depression, liver depression and spleen deficiency syndrome |
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