CN107841390A - A kind of bentonite cleaning agent and preparation method thereof - Google Patents
A kind of bentonite cleaning agent and preparation method thereof Download PDFInfo
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- CN107841390A CN107841390A CN201711171759.6A CN201711171759A CN107841390A CN 107841390 A CN107841390 A CN 107841390A CN 201711171759 A CN201711171759 A CN 201711171759A CN 107841390 A CN107841390 A CN 107841390A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/90—Betaines
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/44—Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/1226—Phosphorus containing
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
- C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/14—Fillers; Abrasives ; Abrasive compositions; Suspending or absorbing agents not provided for in one single group of C11D3/12; Specific features concerning abrasives, e.g. granulometry or mixtures
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
- C11D3/225—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin etherified, e.g. CMC
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
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Abstract
The invention belongs to daily-use chemical industry technical field, more particularly to a kind of bentonite cleaning agent and preparation method thereof.Each constituent of bentonite cleaning agent and its ratio of weight and number are:70 ~ 80 parts of bentonite in powder, 30 ~ 45 parts of hydroxylapatite powder, 20 ~ 25 parts of bamboo charcoal powder, 18 ~ 20 parts of hydroxyethyl cellulose, 15 ~ 18 parts of alkyl betaine, 10 ~ 15 parts of yellow cinnamon leaf, cover it is close spend 10 ~ 15 parts, 15 ~ 20 parts of osmund, 10 ~ 15 parts of Chinese lantern, the Fen, pivots of Celastrus angulatus 8 ~ 12 store 15 ~ 18 parts, 10 ~ 12 parts of Chinese honey locust, 8 ~ 10 parts of leek, 12 ~ 14 parts of lemon-grass;Then preparation method is extracted to plant material to be first modified to bentonite, is finally well mixed modified alta-mud, plant extraction liquid and residual components, the bentonite cleaning agent of the present invention is produced after dry, pulverize.The present invention cleaning agent clean effect it is good, it is green, can disinfection, to human body fanout free region.
Description
Technical field
The invention belongs to daily-use chemical industry technical field, more particularly to a kind of bentonite cleaning agent and preparation method thereof.
Background technology
As the improvement of people's living standards, the requirement also more and more higher for home environment sanitation and hygiene consciousness.Market
On the house cleaning agent liquid sold it is more and more, increasingly refine, if any kitchen oil stain agent, floor cleaner, marble cleaning
Agent and bath of glass etc., the cleaning agent of multi-functional unification are commercially more rare.In order to reach strong detergency, easy mesh is rinsed
, most of cleaning agent on the market still contains chemical composition excitatory, is unfavorable for health, also causes dirt to environment
Dye.Raising with people's environmental consciousness and the attention to health problem, a kind of good, the green cleaning agent of clean effect is more
Meet the demand of consumers in general.
The content of the invention
The present invention provides a kind of bentonite cleaning agent and preparation method thereof, and the bentonite cleaning agent clean effect is good, can
Disinfection, repel mosquitoes and flies, it is green to human body without health hazard.
What the present invention was realized in:A kind of bentonite cleaning agent, each constituent of bentonite cleaning agent and its weight
Portion rate is:70 ~ 80 parts of bentonite in powder, 30 ~ 45 parts of hydroxylapatite powder, 20 ~ 25 parts of bamboo charcoal powder, hydroxyethyl cellulose 18 ~ 20
Part, 15 ~ 18 parts of alkyl betaine, 10 ~ 15 parts of yellow cinnamon leaf, cover it is close spend 10 ~ 15 parts, it is 15 ~ 20 parts of osmund, 10 ~ 15 parts of Chinese lantern, bitter
15 ~ 18 parts of the Fen, pivots of skin rattan 8 ~ 12 storage, 10 ~ 12 parts of Chinese honey locust, 8 ~ 10 parts of leek, 12 ~ 14 parts of lemon-grass.
As a further improvement on the present invention, described bentonite in powder, hydroxylapatite powder, the particle size of bamboo charcoal powder are
240 mesh.
A kind of method for preparing bentonite cleaning agent, comprises the following steps:
(1) it is bentonite modified:70 ~ 80 parts of bentonite in powder and 120 ~ 150 parts of ultra-pure waters are taken to be configured to medicinal bentonite suspension, in magnetic force
Stirred on mixer, then weigh natrium carbonicum calcinatum be added to be configured in medicinal bentonite suspension 20% slurries, by slurries
Progress heating stirring reaction is put into water-bath, heating-up temperature is 75 ~ 80 DEG C, and mixing speed is 20 ~ 40r/min, mixing time
For 60 ~ 90min, centrifuge washing, high-temperature roasting is carried out after drying, sintering temperature is 200 ~ 300 DEG C, and ball mill is put into after roasting and is entered
Row is ground, and produces modified alta-mud powder;
(2) preparation of plant extraction liquid:Take 10 ~ 15 parts of yellow cinnamon leaf, cover it is close spend 10 ~ 15 parts, 15 ~ 20 parts of osmund, Chinese lantern 10 ~ 15
Part, 15 ~ 18 parts of the Fen, pivots of Celastrus angulatus 8 ~ 12 storage, 10 ~ 12 parts of Chinese honey locust, 8 ~ 10 parts of leek, 12 ~ 14 parts of lemon-grass are ground crushing,
Plant material after grinding is added to 150 ~ 180 parts of water, is put into ultrasonic unit and carries out ultrasonic-leaching, after ultrasound
Feed liquid is filtered, and it is plant extraction liquid to be then condensed into volume as the 1/5 of extract solution;
(3) in the modified alta-mud powder being prepared toward step 1) add 30 ~ 45 parts of hydroxylapatite powder, 20 ~ 25 parts of bamboo charcoal powder,
18 ~ 20 parts of hydroxyethyl cellulose, 15 ~ 18 parts of alkyl betaine, plant extraction liquid, stirring are sufficiently mixed uniformly, are placed in drying box
Middle drying, as bentonite cleaning agent is ground into after 180 ~ 200 mesh.
As a further improvement on the present invention, described ultrasonic wave extraction water temperature be 40 ~ 50 DEG C, ultrasonic frequency be 20 ~
30zH, it is 50 ~ 60min 400 ~ 500W extraction times that ultrasonic power, which is,.
The present invention technical principle be:The present invention material and other materials based on bentonite are compounded clear to prepare
Clean dose.Due in raw material bentonite be mostly calcium-base bentonite, calcium-base bentonite water imbibition, dilatancy, plasticity, heat endurance
It is strong etc. no sodium bentonite, it is necessary to be modified to raw material bentonite, improve bentonitic value.It is swollen to raw material first
Profit soil carries out sodium modification, and the calcium-base bentonite contained in raw material is modified as into sodium bentonite, improves between bentonite crystal layer
Layer away from improving bentonite water absorption rate and expansion multiple, ion exchange capacity improved, so as to improve bentonitic adsorption effect.Make
With price is relatively low, wide material sources and easily removes in modifying process, the Na that sodium effect is good2CO3As sodium agent, using magnetic force
Mixer makes bentonite be uniformly dispersed in ultra-pure water, is advantageous to Na2CO3Sodium agent fully contacts with bentonite.It is configured to 20%
Slurries, there is provided suitably free Na+Concentration, be advantageous to Na+With Ca2+Exchange reaction, natridization reaction is promoted to be moved to positive direction,
Be advantageous to the progress of natridization reaction, while be advantageous to the drying in later stage.If the concentration of slurries improves again, Na+Na during excessive concentration+
Ionization rate is big, and electro kinetic potential is high, and activity is strong, makes the Na for having reached balance originally+With Ca2+Swap status is destroyed, excessively
Na+Make to be modified sodium bentonite Quality Down on the contrary, influence sodium effect.Water-bath heating can make reaction mass heated equal
It is even, and temperature can be controlled preferably, and the phenomenon of bumping will not be caused.Sodium effect can be improved in 75 ~ 80 DEG C of temperature
Fruit, bentonitic expansion capacity and colloid index gradually step up after sodium, and too high temperature can aggravate ion motion, destroy sodium ion
With the exchange equilibrium of calcium ions and magnesium ions, sodium effect is set to be deteriorated.Bentonite after sodium modification carries out high-temperature roasting, can make
Bentonite successively loses the combination water in surface water, water of hydration and structural framework, reduces absorption resistance of the moisture film to polluter;
Part is located at the impurity in bentonite passage and space, is pulled away together with the moisture lost, and passage and space are opened, so as to
Bentonite adsorption performance is set to change, sintering temperature will not undergo phase transition bentonite at 250 ~ 300 DEG C, will not destroy swollen
Moisten soil skeleton structure, its specific surface area is reached maximum.Crushed again after roasting, make the increase of bentonite surface area, increase is inhaled
Attached action site.
Hydroxylapatite biology compatibility is good, while there is excellent ion-exchange performance and adsorption capacity to make its right
Most of heavy metal ion, anion and organic pollution have good absorption fixation;Bamboo charcoal powder has loose more
The structure in hole, its molecule is fine and closely woven porous, and quality is hard;Have very strong adsorption capacity, greasy dirt can be adsorbed, moreover it is possible to purify air,
Eliminate that peculiar smell, moisture absorption be mould proof, antibacterial expelling parasite.Bentonite, hydroxyapatite, bamboo charcoal powder are compounded, hydroxyl phosphorus can be improved
The particle dispersion of lime stone reduces agglomeration traits, improves interface compatibility, hydroxyapatite is possessed more preferable adsorption capacity.Bamboo
Charcoal contains adsorption hole, but hole count is insufficient, and aperture is not big enough, and the ability of adsorption removal stink substance is not strong enough, by compounding,
The adsorption hole of cleaning agent can be made to increase significantly, have expansion to whole cleaning agent, can not only make the absorption of cleaning agent clear
Removing solid capacity strengthens, and the dosage of cleaning agent can also be reduced when reaching identical adsorption removal effect.
In the plant material of addition, yellow cinnamon leaf has the function that analgesic, antibacterial, drive are compacted;Covering close flower has antibacterial, anti-inflammatory
Effect, moreover it is possible to play a part of wind and heat dispersing, nourish the liver to improve visual acuity, move back screen;Osmund can remove stench;Chinese lantern have heat-clearing and fire-reducing,
The effect that anti-inflammatory is drawn out pus by applying a plaster to the affected part, moreover it is possible to treat hemorrhoid;Pivot, which stores, has the function that desinsection removing dampness to relieve itching;Celastrus angulatus is a kind of chlordane,
The insects in environment can be killed;Chinese honey locust contains triterpenoid saponin(Gledinin, gleditschiasaponin), tannin, ceryl alcohol, nonacosane, stigmasterol,
Sitosterol etc., clean effect is good, leek and lemon-grass have good result to repelling mosquitoes and flies.Enhanced by the addition of plant material
The function of cleaning agent, can also be played while can degrease antibacterial, anti-inflammatory, desinsection, mosquito repellent fly etc. effect, also have
There is wind and heat dispersing, the effect to nourish the liver to improve visual acuity.These plant material wide material sources, suitable natural disposition is strong, readily available, can significantly drop
The cost of low cleaning agent.
The present invention possesses following good result:
1. the raw material that the present invention uses, chemical agent is not added, it is green, there is no any harm for environment and human body.
2. the cleaning agent raw material sources of the present invention are abundant, green safe, dirt-removing power is strong, can be widely used in household room
Decontamination.
3. bentonite is developed, technical support is provided for my area's bentonite ore deep processing, has been widened bentonitic
Application value.
Embodiment
A kind of bentonite cleaning agent of the description present invention and preparation method thereof with reference to embodiments, these descriptions are not pair
Present invention is further limited.
Embodiment 1
It is bentonite modified:Take 78 parts of bentonite in powder and 120 parts of ultra-pure waters to be configured to medicinal bentonite suspension, stirred on magnetic stirrer
Mix uniformly, then weigh natrium carbonicum calcinatum be added to be configured in medicinal bentonite suspension 20% slurries, slurries are put into water-bath
Middle progress heating stirring reaction, heating-up temperature are 76 DEG C, mixing speed 20r/min, mixing time 85min, centrifuge washing,
High-temperature roasting is carried out after drying, sintering temperature is 250 DEG C, and ball mill is put into after roasting and is ground crushing, produces bentone
Native powder.
The preparation of plant extraction liquid:Take 15 parts of yellow cinnamon leaf, cover it is close spend 11 parts, 13 parts of osmund, 14 parts of Chinese lantern, Celastrus angulatus 11
17 parts of Fen, pivots storage, 10 parts of Chinese honey locust, 9.5 parts of leek, 13 parts of lemon-grass are ground crushing, and the plant material after grinding is added
165 parts of water, it is put into ultrasonic unit and carries out ultrasonic-leaching, ultrasonic wave extraction water temperature is 40 DEG C, and ultrasonic frequency is
24H, ultrasonic power be 480W extraction times be 52min, the feed liquid after ultrasound is filtered, is then condensed into volume to carry
It is plant extraction liquid to take the 1/5 of liquid.
35 parts of hydroxylapatite powder, 25 parts of bamboo charcoal powder, hydroxy ethyl fiber are added into the modified alta-mud powder being prepared
19.5 parts of element, 17 parts of alkyl betaine, plant extraction liquid, stirring are sufficiently mixed uniformly, are placed in drying box and dry, be ground into
It is bentonite cleaning agent after 200 mesh.
The cleaning agent that the present embodiment is prepared is used for the cleaning of lavatory, takes the product of the present invention to be uniformly sprinkled into lavatory
In, a small amount of water wetting is added, crosses in 2min and lavatory is cleaned, the lavatory after cleaning does not have dirt residual, clean smooth.
Embodiment 2
It is bentonite modified:Take 70 parts of bentonite in powder and 150 parts of ultra-pure waters to be configured to medicinal bentonite suspension, stirred on magnetic stirrer
Mix uniformly, then weigh natrium carbonicum calcinatum be added to be configured in medicinal bentonite suspension 20% slurries, slurries are put into water-bath
Middle progress heating stirring reaction, heating-up temperature are 78 DEG C, mixing speed 25r/min, mixing time 60min, centrifuge washing,
High-temperature roasting is carried out after drying, sintering temperature is 200 DEG C, and ball mill is put into after roasting and is ground crushing, produces bentone
Native powder.
The preparation of plant extraction liquid:Take 15 parts of yellow cinnamon leaf, cover it is close spend 11 parts, 13 parts of osmund, 14 parts of Chinese lantern, Celastrus angulatus 11
17 parts of Fen, pivots storage, 12 parts of Chinese honey locust, 8 parts of leek, 13.5 parts of lemon-grass are ground crushing, and the plant material after grinding is added
170 parts of water, it is put into ultrasonic unit and carries out ultrasonic-leaching, ultrasonic wave extraction water temperature is 50 DEG C, and ultrasonic frequency is
20zH, ultrasonic power be 460W extraction times be 60min, the feed liquid after ultrasound is filtered, being then condensed into volume is
The 1/5 of extract solution is plant extraction liquid.
35 parts of hydroxylapatite powder, 25 parts of bamboo charcoal powder, hydroxy ethyl fiber are added into the modified alta-mud powder being prepared
18 parts of element, 15 parts of alkyl betaine, plant extraction liquid, stirring are sufficiently mixed uniformly, are placed in drying box and dry, be ground into 180
It is bentonite cleaning agent after mesh.
The cleaning agent that the present embodiment is prepared is used for the cleaning of smoke exhaust ventilator, using preceding smoke exhaust ventilator full of dust and
Grease, the cleaning agent that the present embodiment is prepared is put into rag, and after adding water fully to soak, smearing is obtained in smoke exhaust ventilator,
Cleaning agent is wiped with rag after friction, after use, smoke exhaust ventilator is without dirt, neat and tidy.
Embodiment 3
It is bentonite modified:Take 80 parts of bentonite in powder and 125 parts of ultra-pure waters to be configured to medicinal bentonite suspension, stirred on magnetic stirrer
Mix uniformly, then weigh natrium carbonicum calcinatum be added to be configured in medicinal bentonite suspension 20% slurries, slurries are put into water-bath
Middle progress heating stirring reaction, heating-up temperature are 79 DEG C, mixing speed 35r/min, mixing time 90min, centrifuge washing,
High-temperature roasting is carried out after drying, sintering temperature is 280 DEG C, and ball mill is put into after roasting and is ground crushing, produces bentone
Native powder.
The preparation of plant extraction liquid:Take 15 parts of yellow cinnamon leaf, cover it is close spend 11 parts, 13 parts of osmund, 14 parts of Chinese lantern, Celastrus angulatus 11
17 parts of Fen, pivots storage, 10.5 parts of Chinese honey locust, 10 parts of leek, 12 parts of lemon-grass are ground crushing, and the plant material after grinding is added
175 parts of water, it is put into ultrasonic unit and carries out ultrasonic-leaching, ultrasonic wave extraction water temperature is 42 DEG C, and ultrasonic frequency is
30zH, ultrasonic power be 400W extraction times be 50min, the feed liquid after ultrasound is filtered, being then condensed into volume is
The 1/5 of extract solution is plant extraction liquid.
35 parts of hydroxylapatite powder, 25 parts of bamboo charcoal powder, hydroxy ethyl fiber are added into the modified alta-mud powder being prepared
20 parts of element, 16 parts of alkyl betaine, plant extraction liquid, stirring are sufficiently mixed uniformly, are placed in drying box and dry, be ground into 200
It is bentonite cleaning agent after mesh.
The cleaning agent that the present embodiment is prepared is used for the cleaning of kitchen range, and cleaning agent is uniformly applied into the kitchen range top
On, soaked with water, rubbed after waiting 5min with rag, the cleaning agent on the kitchen range top is finally cleaned out with clean rag, used
The kitchen range top after cleaning agent cleans is clean, no mosquitos and flies.
Embodiment 4
It is bentonite modified:Take 75 parts of bentonite in powder and 130 parts of ultra-pure waters to be configured to medicinal bentonite suspension, stirred on magnetic stirrer
Mix uniformly, then weigh natrium carbonicum calcinatum be added to be configured in medicinal bentonite suspension 20% slurries, slurries are put into water-bath
Middle progress heating stirring reaction, heating-up temperature are 75 DEG C, mixing speed 30r/min, mixing time 80min, centrifuge washing,
High-temperature roasting is carried out after drying, sintering temperature is 300 DEG C, and ball mill is put into after roasting and is ground crushing, produces bentone
Native powder.
The preparation of plant extraction liquid:Take 15 parts of yellow cinnamon leaf, cover it is close spend 11 parts, 13 parts of osmund, 14 parts of Chinese lantern, Celastrus angulatus 11
17 parts of Fen, pivots storage, 11.5 parts of Chinese honey locust, 8.5 parts of leek, 14 parts of lemon-grass are ground crushing, and the plant material after grinding is added
Enter 150 parts of water, be put into ultrasonic unit and carry out ultrasonic-leaching, ultrasonic wave extraction water temperature is 48 DEG C, and ultrasonic frequency is
22zH, ultrasonic power be 500W extraction times be 56min, the feed liquid after ultrasound is filtered, being then condensed into volume is
The 1/5 of extract solution is plant extraction liquid.
35 parts of hydroxylapatite powder, 25 parts of bamboo charcoal powder, hydroxy ethyl fiber are added into the modified alta-mud powder being prepared
19 parts of element, 16 parts of alkyl betaine, plant extraction liquid, stirring are sufficiently mixed uniformly, are placed in drying box and dry, be ground into 180
It is bentonite cleaning agent after mesh.
The cleaning agent that the present embodiment is prepared is used for the cleaning on floor, after cleaning agent is fully soaked with water, divides and spreads
Onto floor, wiped with mop, finally the cleaning agent on floor is removed totally with clean rag, uses this hair
Floor is clean after bright cleaning agent, pollution-free.
Embodiment 5
It is bentonite modified:Take 73 parts of bentonite in powder and 140 parts of ultra-pure waters to be configured to medicinal bentonite suspension, stirred on magnetic stirrer
Mix uniformly, then weigh natrium carbonicum calcinatum be added to be configured in medicinal bentonite suspension 20% slurries, slurries are put into water-bath
Middle progress heating stirring reaction, heating-up temperature are 80 DEG C, mixing speed 40r/min, mixing time 75min, centrifuge washing,
High-temperature roasting is carried out after drying, sintering temperature is 220 DEG C, and ball mill is put into after roasting and is ground crushing, produces bentone
Native powder.
The preparation of plant extraction liquid:Take 15 parts of yellow cinnamon leaf, cover it is close spend 11 parts, 13 parts of osmund, 14 parts of Chinese lantern, Celastrus angulatus 11
17 parts of Fen, pivots storage, 11 parts of Chinese honey locust, 9 parts of leek, 12.5 parts of lemon-grass are ground crushing, and the plant material after grinding is added
180 parts of water, it is put into ultrasonic unit and carries out ultrasonic-leaching, ultrasonic wave extraction water temperature is 45 DEG C, and ultrasonic frequency is
27zH, ultrasonic power be 430W extraction times be 58min, the feed liquid after ultrasound is filtered, being then condensed into volume is
The 1/5 of extract solution is plant extraction liquid.
35 parts of hydroxylapatite powder, 25 parts of bamboo charcoal powder, hydroxy ethyl fiber are added into the modified alta-mud powder being prepared
18.5 parts of element, 18 parts of alkyl betaine, plant extraction liquid, stirring are sufficiently mixed uniformly, are placed in drying box and dry, be ground into
It is bentonite cleaning agent after 200 mesh.
The cleaning agent that the present embodiment is prepared is used for the cleaning of frying pan, after the cleaning agent wetting of the present invention, with smearing
Cloth dips wipe frying pan four weeks after, cleaned with water, bright as new using frying pan after the cleaning agent of the present invention, surface does not have
Cut.
The above embodiment of the present invention scheme is only the description of the invention and can not limit the present invention, is pointed out in claim
Product form composition of the present invention, component ratio, the scope of preparation method parameter, and above-mentioned explanation does not point out ginseng of the present invention
Several scopes, therefore, any change within the meaning and scope equivalent to the claims of the present invention, all it is considered to be
It is included within the scope of the claims.
The present invention is by multidigit daily-use chemical industry processing staff's long-term work experience accumulation, and is created by creative work
And go out, cleaning agent of the invention is green safe healthy, pollution-free, and cleaning effect is notable, can extensive use, for bentonitic
Deep processing has far-reaching influence.
Claims (5)
1. a kind of bentonite cleaning agent, it is characterized in that, each constituent of bentonite cleaning agent and its ratio of weight and number are:Swelling
Native 70 ~ 80 parts of powder, 30 ~ 45 parts of hydroxylapatite powder, 20 ~ 25 parts of bamboo charcoal powder, 18 ~ 20 parts of hydroxyethyl cellulose, alkyl betaine
15 ~ 18 parts, 10 ~ 15 parts of yellow cinnamon leaf, cover it is close spend 10 ~ 15 parts, 15 ~ 20 parts of osmund, 10 ~ 15 parts of Chinese lantern, the Fen, pivots of Celastrus angulatus 8 ~ 12
15 ~ 18 parts of storage, 10 ~ 12 parts of Chinese honey locust, 8 ~ 10 parts of leek, 12 ~ 14 parts of lemon-grass.
2. a kind of bentonite cleaning agent according to claim 1, it is characterized in that, described bentonite in powder, hydroxyapatite
Powder, the particle size of bamboo charcoal powder are 240 mesh.
3. a kind of method of the bentonite cleaning agent prepared described in claim 1 or 2, it is characterized in that, preparation method step includes:
Step 1) is bentonite modified:70 ~ 80 parts of bentonite in powder and 120 ~ 150 parts of ultra-pure waters are taken to be configured to medicinal bentonite suspension,
Stirred on magnetic stirrer, then weigh natrium carbonicum calcinatum be added to be configured in medicinal bentonite suspension 20% slurries, will
Slurries are put into progress heating stirring reaction in water-bath, and heating-up temperature is 75 ~ 80 DEG C, and mixing speed is 20 ~ 40r/min, stirring
Time is 60 ~ 90min, centrifuge washing, high-temperature roasting is carried out after drying, and sintering temperature is 200 ~ 300 DEG C, and ball milling is put into after roasting
Machine is ground crushing, produces modified alta-mud powder;
The preparation of step 2) plant extraction liquid:Take 10 ~ 15 parts of yellow cinnamon leaf, cover it is close spend 10 ~ 15 parts, 15 ~ 20 parts of osmund, Chinese lantern 10
~ 15 parts, the Fen, pivots of Celastrus angulatus 8 ~ 12 store 15 ~ 18 parts, 10 ~ 12 parts of Chinese honey locust, 8 ~ 10 parts of leek, 12 ~ 14 parts of lemon-grass be ground powder
It is broken, the plant material after grinding is added to 150 ~ 180 parts of water, is put into ultrasonic unit and carries out ultrasonic-leaching, by ultrasound
Feed liquid afterwards is filtered, and it is plant extraction liquid to be then condensed into volume as the 1/5 of extract solution;
30 ~ 45 parts of hydroxylapatite powder, bamboo charcoal powder 20 ~ 25 are added in the modified alta-mud powder that step 3) is prepared toward step 1)
Part, 18 ~ 20 parts of hydroxyethyl cellulose, 15 ~ 18 parts of alkyl betaine, plant extraction liquid, stirring are sufficiently mixed uniformly, are placed in drying
Dried in case, be ground into after 180 ~ 200 mesh as bentonite cleaning agent.
4. the method according to claim 3 for preparing bentonite cleaning agent, it is characterized in that, described ultrasonic wave extraction water temperature
For 40 ~ 50 DEG C, ultrasonic frequency is 20 ~ 30zH, and it is 50 ~ 60min 400 ~ 500W extraction times that ultrasonic power, which is,.
5. the method according to claim 3 for preparing bentonite cleaning agent, it is characterized in that, the bentonite cleaning being prepared
Agent is mainly used in kitchen and its apparatus cleaning, the decontamination of smoking cigarette machine, the cleaning on floor, the cleaning of lavatory.
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN108624416A (en) * | 2018-05-11 | 2018-10-09 | 肥西县碧涛建材有限公司 | A kind of preparation method of door glass efficient cleaner |
CN108659971A (en) * | 2018-06-15 | 2018-10-16 | 河北晨晨环境科技股份有限公司 | Detergent for toilet and preparation method thereof |
CN109247246A (en) * | 2018-09-26 | 2019-01-22 | 芜湖市鹏磊新材料有限公司 | A kind of bentonitic processing method of cat litter |
CN113058547A (en) * | 2021-04-15 | 2021-07-02 | 南京大学 | Efficient phosphorus removal agent, preparation method and application thereof |
CN115558558A (en) * | 2022-10-29 | 2023-01-03 | 兰溪市屹达化工试剂有限公司 | Preparation method of detergent |
Citations (1)
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CN106978272A (en) * | 2017-05-03 | 2017-07-25 | 安徽万宝玻璃有限公司 | A kind of glass cleaner and preparation method thereof |
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Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN106978272A (en) * | 2017-05-03 | 2017-07-25 | 安徽万宝玻璃有限公司 | A kind of glass cleaner and preparation method thereof |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108624416A (en) * | 2018-05-11 | 2018-10-09 | 肥西县碧涛建材有限公司 | A kind of preparation method of door glass efficient cleaner |
CN108659971A (en) * | 2018-06-15 | 2018-10-16 | 河北晨晨环境科技股份有限公司 | Detergent for toilet and preparation method thereof |
CN109247246A (en) * | 2018-09-26 | 2019-01-22 | 芜湖市鹏磊新材料有限公司 | A kind of bentonitic processing method of cat litter |
CN113058547A (en) * | 2021-04-15 | 2021-07-02 | 南京大学 | Efficient phosphorus removal agent, preparation method and application thereof |
CN115558558A (en) * | 2022-10-29 | 2023-01-03 | 兰溪市屹达化工试剂有限公司 | Preparation method of detergent |
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