CN107827797A - The technique that bata-carotene is extracted from capsicum red pigment - Google Patents
The technique that bata-carotene is extracted from capsicum red pigment Download PDFInfo
- Publication number
- CN107827797A CN107827797A CN201710926492.0A CN201710926492A CN107827797A CN 107827797 A CN107827797 A CN 107827797A CN 201710926492 A CN201710926492 A CN 201710926492A CN 107827797 A CN107827797 A CN 107827797A
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- CN
- China
- Prior art keywords
- bata
- carotene
- red pigment
- capsicum red
- capsicum
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C403/00—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone
- C07C403/24—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone having side-chains substituted by six-membered non-aromatic rings, e.g. beta-carotene
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0096—Purification; Precipitation; Filtration
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
It is the technique that bata-carotene is extracted in extraction from capsicum red pigment from capsicum red pigment the invention discloses the technical solution adopted in the present invention.Using capsicum red pigment as raw material, addition ethanol, water, acetone, the mixed liquor of phosphoric acid, to excite the activity of bata-carotene, then using isopropyl alcohol extracting, the isopropanol containing bata-carotene is evaporated under reduced pressure, obtains bata-carotene powder.
Description
Technical field
The invention belongs to pepper extract to finish field, and bata-carotene is particularly extracted from chilli products.
Background technology
Bata-carotene is a kind of replenishing vitamins A healthcare items in food, after taking in human digestive organ, can be converted
It is current most safe replenishing vitamins A product into vitamin A.It can maintain the health of eyes and skin, improve yctalopia
Disease, the situation of pachylosis, contribute to body from the injury of free radical.Possess and be widely applied red space, especially as β recklessly
The source of radish element, all it is to refine and go out using carrot, while also has a small amount of algae to extract bata-carotene.So β is recklessly
The yield of radish element is severely limited.
The content of the invention
To overcome above mentioned problem, the invention discloses the technique that bata-carotene is extracted from capsicum red pigment, in capsanthin
The bata-carotene of high value is isolated in pigment, improves the yield of bata-carotene and the added value of capsicum.
The technical solution adopted in the present invention is that the technique of bata-carotene is extracted from capsicum red pigment, and its step is with peppery
Green pepper haematochrome is raw material, and mixed liquor is added in capsicum red pigment, and mixed liquor quality is 4%-the 7% of quality of capsicum red pigment, is mixed
It is ethanol, water, acetone, phosphoric acid to close liquid component, and its volumetric ratio is 32:40:20:8, stir, be warmed to 45-50 degrees Celsius,
To excite the activity of bata-carotene；Then isopropanol is added, addition is 3-5 times of capsicum red pigment and mixed liquor volume,
Continue to be warming up to 60-70 degrees Celsius, after standing 3 hours, isolate the isopropanol layer that bata-carotene has been dissolved in lower floor, Ran Houjin
Row is evaporated under reduced pressure, and obtains bata-carotene powder.
The beneficial effects of the invention are as follows whole extraction process, made with the capsicum red pigment extracted in the capsicum that grows naturally
For raw material, after isolating bata-carotene, make the content of capsicum red pigment higher, improve the added value of capsicum red pigment；The same time-division
The bata-carotene separated out, the added value of capsicum is improved, create wide profit margin.
Embodiment
Embodiment 1, with the capsicum red pigment raw material of Xinjiang pimento, capsicum red pigment 400kg is put into reactor, by it
It is 32 that quality 7%, which puts into volume fraction,:40:20:8 ethanol, water, acetone, the mixed liquor 28kg of phosphoric acid, 50 are warming up to after stirring
Degree Celsius, by capsicum red pigment and mixed liquor：Isopropanol volumetric ratio is 1:5,2140L isopropanols are added, continues to be warming up to 70 and takes the photograph
Family name's degree, 3 hours are stood, the isopropanol layer that bata-carotene has been dissolved in lower floor is isolated, depressurizes and evaporate isopropanol to obtain β carrots
Plain powder 52kg.
Embodiment 2, with the capsicum red pigment raw material of Gansu plate green pepper, capsicum red pigment 400kg is put into reactor, by it
It is 32 that quality 5%, which puts into volume fraction,:40:20:8 ethanol, water, acetone, the mixed liquor 20kg of phosphoric acid, 45 are warming up to after stirring
Degree Celsius, then by capsicum red pigment and mixed liquor：Isopropanol is according to volumetric ratio 1：4,1680L isopropanols are added, continue to be warming up to
65 degrees Celsius, 3 hours are stood, isolates the isopropanol layer that bata-carotene has been dissolved in lower floor, depressurized and isopropanol is evaporated to obtain β recklessly
Radish element powder 54kg.
Embodiment 3, with the capsicum red pigment raw material in Dezhou Yidu, capsicum red pigment 400kg is put into reactor, by it
It is 32 that quality 3%, which puts into volume fraction,:40:20:8 ethanol, water, acetone, the mixed liquor 12kg of phosphoric acid, 45 are warming up to after stirring
Degree Celsius, then by capsicum red pigment and mixed liquor：Isopropanol is according to volumetric ratio 1：3,1236L isopropanols are added, continue to be warming up to
60 degrees Celsius, 3 hours are stood, isolates the isopropanol layer that bata-carotene has been dissolved in lower floor, depressurized and isopropanol is evaporated to obtain β recklessly
Radish element powder 53kg.
Claims (1)
1. the technique of bata-carotene is extracted from capsicum red pigment, it is characterized in that：It is red in capsicum using capsicum red pigment as raw material
Mixed liquor is added in element, mixed liquor quality is 4%-the 7% of quality of capsicum red pigment, and mixed liquor component is ethanol, water, acetone, phosphorus
Acid, its volumetric ratio are 32:40:20:8, stir, be warmed to 45-50 degrees Celsius, to excite the activity of bata-carotene；So
After add isopropanol, addition is 3-5 times of capsicum red pigment and mixed liquor volume, continues to be warming up to 60-70 degrees Celsius, quiet
After putting 3 hours, the isopropanol layer that bata-carotene has been dissolved in lower floor is isolated, is then evaporated under reduced pressure, obtains bata-carotene powder
End.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710926492.0A CN107827797A (en) | 2017-10-07 | 2017-10-07 | The technique that bata-carotene is extracted from capsicum red pigment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710926492.0A CN107827797A (en) | 2017-10-07 | 2017-10-07 | The technique that bata-carotene is extracted from capsicum red pigment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107827797A true CN107827797A (en) | 2018-03-23 |
Family
ID=61647842
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710926492.0A Pending CN107827797A (en) | 2017-10-07 | 2017-10-07 | The technique that bata-carotene is extracted from capsicum red pigment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107827797A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109852098A (en) * | 2019-02-12 | 2019-06-07 | 黑龙江八一农垦大学 | The method of wintercherry red pigment is extracted in a kind of calyx of groundcherry place |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1242417A (en) * | 1998-07-21 | 2000-01-26 | 云南省烟草工业研究所 | Method for preparing tobacco aromatics using extracted natural carotenoid |
| CN1578628A (en) * | 2001-09-04 | 2005-02-09 | 利库德天然产品工业有限公司 | Carotenoid extraction process |
-
2017
- 2017-10-07 CN CN201710926492.0A patent/CN107827797A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1242417A (en) * | 1998-07-21 | 2000-01-26 | 云南省烟草工业研究所 | Method for preparing tobacco aromatics using extracted natural carotenoid |
| CN1578628A (en) * | 2001-09-04 | 2005-02-09 | 利库德天然产品工业有限公司 | Carotenoid extraction process |
Non-Patent Citations (1)
| Title |
|---|
| 史晓博 等: "一种降低辣椒红色素不溶物含量的方法", 《中国食品添加剂》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109852098A (en) * | 2019-02-12 | 2019-06-07 | 黑龙江八一农垦大学 | The method of wintercherry red pigment is extracted in a kind of calyx of groundcherry place |
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| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180323 |