The content of the invention
For above-mentioned technical problem, the present invention has designed and developed a kind of residual detection pretreating device of the high agriculture for the treatment of effeciency.
Technical scheme provided by the invention is:
A kind of residual detection pretreating device of agriculture, including:
Sample stage, thereon formed with a fixing groove, the inside of the sample stage, it is being sitting at the lower section of the fixing groove
Position be provided with cooling water pipe, the cooling water pipe is connected to recirculated cooling water supply equipment;
Container, its bottom are equipped in the fixing groove, and the container is by plastic material, in cylinder;
Concrete vibrating mechanism, its hammer that includes vibrating, vibrate support and the cylinder that vibrates, and the support that vibrates is arranged at the fixation
The side of groove, and the hammer that vibrates be arranged in a manner of it can vertically reciprocatingly move it is described vibrate on support, it is described
The hammer that vibrates includes cylindrical hammer and is sheathed on the baffle ring of the hammer body bottom, and the hammer that vibrates is described by being made up of rubber
The bottom of hammer body is provided with a packed layer, and water, the outstanding setting in lower surface of the hammer body are filled with the packed layer
There is crisscross a plurality of cutting rod, and the diameter of the hammer body is smaller 0.5cm than the internal diameter of the container, the baffle ring is inclined
Set, the outer ledge of the baffle ring is higher than the inside edge of the baffle ring, and the cylinder that vibrates is connected to the hammer body, to drive
Move the hammer body and be downwardly into the container or the upward out container, when the hammer body is downwardly into the container and institute
State that container is coaxial, and contacted with the bottom of the container, and the outer ledge of the baffle ring contacts with the inwall of the container;
Wherein, the lower end of the support that vibrates has the first external screw thread, and the first screw, the support that vibrates are offered on the sample stage
It is threadedly connected in first screw, and the sample stage is fixed under the tightening of the first nut;
Rabbling mechanism, it includes puddler and the stirring vane being arranged on the puddler, and the stirring motor connects
The rear end of the puddler is connected to, to drive the puddler to rotate, the puddler is in a manner of it can vertically move
It is arranged on a stirring support, the lower end of the stirring support has the second external screw thread, and the second spiral shell is offered on the sample stage
Hole, the stirring support is threadedly connected in second screw, and the sample stage is fixed under the tightening of the second nut;
Solvent liquid pump, the outlet end of the solvent liquid pump are connected to the side wall of the container, the solvent by feed tube
The liquid feeding end of liquid pump is connected to solvent tank;
Liquid pump is sampled, the liquid feeding end of the sampling liquid pump is connected to the side wall of the container by probe tube, and described takes
The outlet end of sample liquid pump is connected to a sampling bottle, and the liquid feeding end of the probe tube is provided with a filter;And
Controller, it is connected to vibrate cylinder, the stirring motor, the solvent liquid pump and the sampling liquid pump,
Wherein, in the case where the holder pivots that vibrate cause the hammer that vibrates to be rocked to the top of the container, the controller
The hammer that vibrated described in the cylinder that vibrated described in control driving moves reciprocatingly a period of time, then controls the solvent liquid pump to the container
The solvent of certain volume is inside pumped into, causes the stirring vane to stretch in the container in the stirring holder pivots, it is described
Controller controls the stirring motor spin for some time, then the sample liquid for controlling the sampling liquid pump to extract certain volume.
Preferably, in the residual detection pretreating device of described agriculture, the solvent liquid pump is the first measuring pump;The sampling
Liquid pump is the second measuring pump.
Preferably, in the residual detection pretreating device of described agriculture, cylinder driving institute of being vibrated described in the controller control
The hammer that vibrates is stated to move reciprocatingly 1~3min.
Preferably, in the residual detection pretreating device of described agriculture, the controller controls the solvent liquid pump to described
50~100mL solvent is pumped into container.
Preferably, in the residual detection pretreating device of described agriculture, the controller control sampling liquid pump extracts 1mL
Sample liquid.
The residual detection pretreating device of agriculture of the present invention devises concrete vibrating mechanism, solvent liquid pump and sampling liquid pump, shakes
Stamper structure can vibrate to vegetable sample, and solvent liquid pump adds solvent, the vegetables that solvent will be smashed to pieces from trend container
Remains of pesticide in sample is dissolved out, and sampling liquid pump automatically extracts the sample liquid of preparation into sampling bottle.The present invention improves
Pre-treatment efficiency and processing accuracy to vegetable sample, and then improve the accuracy of detection to residues of pesticides.
Embodiment
The present invention is described in further detail below in conjunction with the accompanying drawings, to make those skilled in the art with reference to specification text
Word can be implemented according to this.
As depicted in figs. 1 and 2, the present invention provides a kind of residual detection pretreating device of agriculture, including:Sample stage 6, is formed thereon
There is a fixing groove 7, the inside of the sample stage, the position for the lower section for being sitting at the fixing groove is provided with cooling water pipe
18, the cooling water pipe 18 is connected to recirculated cooling water supply equipment;Container 3, its bottom is equipped in the fixing groove, described
Container is by plastic material, in cylinder;Concrete vibrating mechanism, its hammer 12 that includes vibrating, vibrate support 2 and the cylinder 1 that vibrates, described to shake
The side that support is arranged at the fixing groove is smash, and the hammer that vibrates is arranged in a manner of it can vertically reciprocatingly move
Described to vibrate on support, the hammer that vibrates includes cylindrical hammer 4 and is sheathed on the baffle ring 5 of the hammer body bottom, described to shake
For beater by being made up of rubber, the bottom of the hammer body is provided with a packed layer 17, and water, the hammer are filled with the packed layer
The lower surface 19 of body is outstanding to be provided with crisscross a plurality of cutting rod 20, and the diameter of the hammer body is than the container
The small 0.5cm of internal diameter, the baffle ring 5 are inclined to set, and the outer ledge of the baffle ring is higher than the inside edge of the baffle ring, described
The cylinder that vibrates is connected to the hammer body, to drive the hammer body to be downwardly into the container or the upward out container, institute
State hammer body and be downwardly into coaxial with the container during container, and contacted with the bottom of the container, and the baffle ring
Outer ledge contacts with the inwall of the container;Wherein, the lower end of the support 2 that vibrates has the first external screw thread, the sample
The first screw is offered on platform 6, the support that vibrates is threadedly connected in first screw, and under the tightening of the first nut
It is fixed on the sample stage;Rabbling mechanism, it includes puddler 14 and the stirring vane being arranged on the puddler 16, institute
The rear end that stirring motor 13 is connected to the puddler is stated, to drive the puddler to rotate, the puddler is with can be along vertical
The mode of direction movement is arranged on a stirring support 15, and the lower end of the stirring support has the second external screw thread, the sample
The second screw is offered on platform, the stirring support is threadedly connected in second screw, and under the tightening of the second nut
It is fixed on the sample stage;Solvent liquid pump 9, the outlet end of the solvent liquid pump 9 are connected to the side of the container by feed tube
Wall, the liquid feeding end of the solvent liquid pump are connected to solvent tank 8;Liquid pump 11 is sampled, the liquid feeding end of the sampling liquid pump passes through sampling
Pipe is connected to the side wall of the container, and the outlet end of the sampling liquid pump is connected to a sampling bottle 10, and the probe tube enters
Liquid end is provided with a filter;And controller, it is connected to vibrate cylinder, the stirring motor, the solvent liquid pump
With the sampling liquid pump, wherein, the holder pivots that vibrate cause the hammer that vibrates be rocked to the container top feelings
Under condition, the hammer that vibrated described in cylinder driving of being vibrated described in controller control moves reciprocatingly a period of time, then controls described molten
Agent liquid pump is pumped into the solvent of certain volume into the container, causes the stirring vane to stretch in the stirring holder pivots
In the container, the controller controls the stirring motor spin for some time, then controls the sampling liquid pump to extract necessarily
The sample liquid of volume.
When being handled before being carried out to vegetable sample, vegetable sample is placed in container, the first nut is unclamped, will be vibrated
Holder pivots certain angle, the hammer that makes to vibrate is rocked to above container, then the first nut is tightened;Controller controls concrete vibrating mechanism work
Make, the hammer that vibrates moves back and forth under the driving for the cylinder that vibrates, so as to which vegetable sample be smashed to pieces;Treat that vegetable sample is smashed to pieces to certain journey
Degree, the first nut is unclamped manually, will vibrate holder pivots certain angle, so that the hammer that vibrates is avoided above container;Solvent liquid
Pump is worked automatically under the control of the controller, and the solvent in solvent tank is pumped into container, afterwards manually unclamps the second nut,
Holder pivots certain angle will be stirred, stirring vane be located at container top, adjusts puddler afterwards, make puddler to moving down
It is dynamic, stirring vane is immersed in solvent, then equipment is started, by controller control stirring motor stirring a period of time, so that will
Remains of pesticide in the vegetable sample smashed to pieces is dissolved out;Afterwards, sampling liquid pump extracts sample liquid to sample liquid bottle automatically.Detection is set
Standby can be done to sample liquid pump further tests and analyzes.
The hammer that vibrates includes cylindrical hammer and baffle ring, and hammer body contacts when moving to the position of bottom with container, to vegetables
Sample is hammered.During hammering, vegetable sample can outwards splash, and the bottom of hammer body is arranged with baffle ring, moreover, gear
Ring is inclined to set, and outer ledge is higher than inside edge, and baffle ring can block the vegetable sample sputtered, and the sample that will be sputtered
Fragment is kept off back below hammer body, so as to improve vibration efficiency, improves effect of vibrating, and avoids vibrating for generation vegetable sample uneven.
Once it is uneven to vibrate, then solvent may be caused all to dissolve remains of pesticide, and then influence the detection to remains of pesticide.
Cooling water pipe can cool to container, avoid the temperature of vegetable sample in process of vibrating too high.Hammering into shape simultaneously
The bottom of body is also equipped with one layer of packed layer, fills water in the packed layer, avoids the temperature of hammer body too high.
Crisscross cutting rod is provided with the lower surface of hammer body is outstanding, cutting rod plays cutting to vegetable sample
Effect, the effect of vibrating to vegetable sample can be promoted, and then improve the extraction effect residual to agriculture.
Container is made of plastic, is not easy in process of vibrating damaged.Container is fastened in fixing groove, can be removed, so as to
Cleaned in container.
The liquid feeding end of probe tube is provided with a filter, and filter can be filtered with sample liquid, so as to avoid vegetables slag from entering
Enter sample liquid bottle.
Preferably, in the residual detection pretreating device of described agriculture, the solvent liquid pump is the first measuring pump;The sampling
Liquid pump is the second measuring pump.
Preferably, in the residual detection pretreating device of described agriculture, cylinder driving institute of being vibrated described in the controller control
The hammer that vibrates is stated to move reciprocatingly 1~3min.
Preferably, in the residual detection pretreating device of described agriculture, the controller controls the solvent liquid pump to described
50~100mL solvent is pumped into container.It is quantitative that solution is supplied into container, to prepare the sample liquid of standardization.
Preferably, in the residual detection pretreating device of described agriculture, the controller control sampling liquid pump extracts 1mL
Sample liquid.
Although embodiment of the present invention is disclosed as above, it is not restricted in specification and embodiment listed
With it can be applied to various suitable the field of the invention completely, can be easily for those skilled in the art
Other modification is realized, therefore under the universal limited without departing substantially from claim and equivalency range, it is of the invention and unlimited
In specific details and shown here as the legend with description.