CN107815295A - A kind of silica nanometer negative oxygen ion purification cream and its preparation technology - Google Patents
A kind of silica nanometer negative oxygen ion purification cream and its preparation technology Download PDFInfo
- Publication number
- CN107815295A CN107815295A CN201710945796.1A CN201710945796A CN107815295A CN 107815295 A CN107815295 A CN 107815295A CN 201710945796 A CN201710945796 A CN 201710945796A CN 107815295 A CN107815295 A CN 107815295A
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- Prior art keywords
- oxygen ion
- negative oxygen
- silica nanometer
- cream
- foaming
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/18—Materials not provided for elsewhere for application to surfaces to minimize adherence of ice, mist or water thereto; Thawing or antifreeze materials for application to surfaces
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Combustion & Propulsion (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
The invention discloses a kind of silica nanometer negative oxygen ion of antifog purification cream technical field to purify cream, and the raw material of silica nanometer negative oxygen ion purification cream are according to mass ratio：SiO 2 powder：Deionized water：Foaming agent：Antioxidant：Preservative=45：50：2：1：2, the foaming agent is CBA, the CBA is azo-compound, nitroso compound, sulfonyl hydrazines compound, one or more in carbonate, the carbonate is calcium carbonate, one kind in magnesium carbonate or sodium acid carbonate, the preservative is the substituent of phenol, the substituent of the phenol is cresols or xylenols, silica nanometer negative oxygen ion purification cream utilizes Nano sol technology, one layer of porous nanometer layer is formed in glass surface, when porous nano layer runs into water smoke, water smoke is quickly absorbed, it is strong with antifog power, the advantages of effect is lasting, realize chemical bond, the antifog time is lasting.
Description
Technical field
The present invention relates to purification cream technical field, specially a kind of silica nanometer negative oxygen ion purification cream and its preparation
Technique.
Background technology
The development of Modern Car external form and the development of glass technology are closely bound up.Before more than 40 years, car front windshield glass
Glass is using single-piece bending windshield, and gradually abandoned the windshield of plane.The car windshield of today
The general large curved surface type for all doing integral width formula, there is certain radian up and down.No matter this bend glass is from processing
Process is still all a kind of very high product of technical requirements from the point of view of the cooperation of assembly because it be related to vehicle, intensity,
The problems such as heat-insulated, assembling, into autumn and winter, the easy upper water smoke of automobile door glass and front windshield is cold by a night
Freeze and easily freeze, so influence the sight of driver, and be difficult to clear up, influence the normal driving of driver, therefore, it is proposed that
A kind of silica nanometer negative oxygen ion purification cream and its preparation technology.
The content of the invention
It is an object of the invention to provide a kind of silica nanometer negative oxygen ion purification cream and its preparation technology, to solve
What is proposed in above-mentioned background technology enters autumn and winter, the easy upper water smoke of automobile door glass and front windshield, cold by a night
Freeze and easily freeze, so the sight of influence driver, and be difficult to clear up, the problem of influenceing the normal driving of driver.
To achieve the above object, the present invention provides following technical scheme：A kind of silica nanometer negative oxygen ion purifies cream,
The silica nanometer negative oxygen ion purification cream raw material be according to mass ratio：SiO 2 powder：Deionized water：Foaming
Agent：Antioxidant：Preservative=45：50：2：1：2.
Preferably, the foaming agent is CBA, and the CBA is azo-compound, nitroso chemical combination
One or more in thing, sulfonyl hydrazines compound, carbonate.
Preferably, the carbonate is one kind in calcium carbonate, magnesium carbonate or sodium acid carbonate.
Preferably, the preservative is the substituent of phenol, and the substituent of the phenol is cresols or xylenols.
A kind of its preparation technology of silica nanometer negative oxygen ion purification cream, silica nanometer negative oxygen ion purification
Its preparation technology's of cream comprises the following steps that：
S1：45 parts of SiO 2 powders, 50 parts of deionized waters, 2 parts of foaming agents are placed in foaming bucket, to 45 parts of dioxies
SiClx powder, 50 parts of deionized waters, 2 parts of foaming agents carry out foaming effects, while carry out negative oxygen ion and have an effect, to negative oxygen from
Son purifying；
S2：Negative oxygen ion will be passed through in mixture after foaming, be stirred, overturns during being passed through, negative oxygen ion
It is passed through and negative oxygen ion is uniformly sufficiently blown into the mixture after foaming using porous type endless tube；
S3：Catalyst is added during mixing into the mixture after mixed negative oxygen ion and foaming to carry out
Hydrolysis and polycondensation, Nano sol is made by raw materials such as silica；
S4：1 part of antioxidant, 2 portions of preservatives will be added in manufactured Nano sol in step S3, stirred, and
Stood, wait bubble to be discharged to be fitted into manufactured finished product in closed container into paste, be stored in what cool place was dried
In storage chamber.
Preferably, the catalyst in the step S3 is germanium dioxide.
Preferably, the time stood in the step S4 is 2-3 hours.
Preferably, the container in the step S4 is glass container.
Compared with prior art, the beneficial effects of the invention are as follows：Silica nanometer negative oxygen ion purification cream, which utilizes, to be received
Rice colloidal sol technology, one layer of porous nanometer layer is formed in glass surface, when porous nano layer runs into water smoke, utilizes its duct
Capillary force, water smoke is quickly absorbed, realize antifog, had antifog power strong, the advantages of effect is lasting, realize chemical bond, it is antifog
Time is lasting.
Brief description of the drawings
Fig. 1 is present invention process flow chart.
Embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete
Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.It is based on
Embodiment in the present invention, those of ordinary skill in the art are obtained every other under the premise of creative work is not made
Embodiment, belong to the scope of protection of the invention.
Referring to Fig. 1, the present invention provides a kind of technical scheme：A kind of silica nanometer negative oxygen ion purifies cream, and this two
Silica nanometer negative-oxygen ion purification cream raw material be according to mass ratio：SiO 2 powder：Deionized water：Foaming agent：It is anti-
Oxidant：Preservative=45：50：2：1：2.
Wherein, the foaming agent is CBA, the CBA be azo-compound, nitroso compound,
One or more in sulfonyl hydrazines compound, carbonate, the carbonate are in calcium carbonate, magnesium carbonate or sodium acid carbonate
One kind, the preservative be phenol substituent, the substituent of the phenol is cresols or xylenols.
A kind of its preparation technology of silica nanometer negative oxygen ion purification cream, silica nanometer negative oxygen ion purification
Its preparation technology's of cream comprises the following steps that：
S1：45 parts of SiO 2 powders, 50 parts of deionized waters, 2 parts of foaming agents are placed in foaming bucket, to 45 parts of dioxies
SiClx powder, 50 parts of deionized waters, 2 parts of foaming agents carry out foaming effects, while carry out negative oxygen ion and have an effect, to negative oxygen from
Son purifying；
S2：Negative oxygen ion will be passed through in mixture after foaming, be stirred, overturns during being passed through, negative oxygen ion
It is passed through and negative oxygen ion is uniformly sufficiently blown into the mixture after foaming using porous type endless tube；
S3：Catalyst is added during mixing into the mixture after mixed negative oxygen ion and foaming to carry out
Hydrolysis and polycondensation, catalyst are germanium dioxide, and the raw materials such as silica are made into Nano sol；
S4：1 part of antioxidant, 2 portions of preservatives will be added in manufactured Nano sol in step S3, stirred, and
Stood, the time of standing is 2-3 hours, waits bubble to be discharged that manufactured finished product is loaded to closed glass into paste
In glass container, it is stored in the shady and cool storage chamber dried.
Embodiment
(1), group is set：Three identical vehicles are chosen, three groups of vehicles are respectively defined as the first experimental group, second
Experimental group and control group；
(2) variable, is controlled：Common diaphragm will be bonded on the front windshield of first experimental group, in the second experimental group
The purification cream that even application this programme is produced on front windshield, do not process on control group；
(3), tested in autumn and winter, by the front windshield of the first experimental group, the second experimental group and control group
Water smoke is uniformly sprayed by sprayer, the first experimental group, the second experimental group and control group are continuously placed two nights, observation the
The water smoke situation of the front windshield of one experimental group, the second experimental group and control group；
(4), got according to Germicidal efficacy, the globule is covered with the front windshield of the first experimental group, and trickle knot occur
Ice phenomenon, the front windshield of the second experimental group are having slight water smoke, frozen on the front windshield of control group, and
The immersion of hot water is just slowly melted under melting.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (8)
1. a kind of silica nanometer negative oxygen ion purifies cream, it is characterised in that：The silica nanometer negative oxygen ion purifies cream
Raw material be according to mass ratio：SiO 2 powder：Deionized water：Foaming agent：Antioxidant：Preservative=45：50：2：1：
2。
A kind of 2. silica nanometer negative oxygen ion purification cream according to claim 1, it is characterised in that：The foaming agent
For CBA, the CBA is in azo-compound, nitroso compound, sulfonyl hydrazines compound, carbonate
One or more.
A kind of 3. silica nanometer negative oxygen ion purification cream according to claim 2, it is characterised in that：The carbonate
For one kind in calcium carbonate, magnesium carbonate or sodium acid carbonate.
A kind of 4. silica nanometer negative oxygen ion purification cream according to claim 1, it is characterised in that：The preservative
For the substituent of phenol, the substituent of the phenol is cresols or xylenols.
A kind of 5. its preparation technology of silica nanometer negative oxygen ion purification cream, it is characterised in that：The silica nanometer is born
Its preparation technology's of oxonium ion purification cream comprises the following steps that：
S1：45 parts of SiO 2 powders, 50 parts of deionized waters, 2 parts of foaming agents are placed in foaming bucket, to 45 parts of silica
Powder, 50 parts of deionized waters, 2 parts of foaming agents carry out foaming effect, while carry out negative oxygen ion and have an effect, pure to negative oxygen ion
Change；
S2：Negative oxygen ion will be passed through in mixture after foaming, be stirred, overturns during being passed through, negative oxygen ion is passed through
Negative oxygen ion is uniformly sufficiently blown into the mixture after foaming using porous type endless tube；
S3：Catalyst is added during mixing into the mixture after mixed negative oxygen ion and foaming to be hydrolyzed
And polycondensation, Nano sol is made in the raw materials such as silica；
S4：Will in manufactured Nano sol in step S3 add 1 part of antioxidant, 2 portions of preservatives, stir, and by its
Stand, wait bubble to be discharged to be fitted into manufactured finished product in closed container into paste, be stored in the shady and cool storage dried
It is indoor.
6. a kind of its preparation technology of silica nanometer negative oxygen ion purification cream according to claim 5, its feature exist
In：Catalyst in the step S3 is germanium dioxide.
7. a kind of its preparation technology of silica nanometer negative oxygen ion purification cream according to claim 5, its feature exist
In：The time stood in the step S4 is 2-3 hours.
8. a kind of its preparation technology of silica nanometer negative oxygen ion purification cream according to claim 5, its feature exist
In：Container in the step S4 is glass container.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710945796.1A CN107815295A (en) | 2017-10-12 | 2017-10-12 | A kind of silica nanometer negative oxygen ion purification cream and its preparation technology |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710945796.1A CN107815295A (en) | 2017-10-12 | 2017-10-12 | A kind of silica nanometer negative oxygen ion purification cream and its preparation technology |
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| CN107815295A true CN107815295A (en) | 2018-03-20 |
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| CN201710945796.1A Pending CN107815295A (en) | 2017-10-12 | 2017-10-12 | A kind of silica nanometer negative oxygen ion purification cream and its preparation technology |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108530644A (en) * | 2018-04-18 | 2018-09-14 | 河南科技学院 | A kind of Multifunctional coordination copolymer nanometer material and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103013197A (en) * | 2012-12-19 | 2013-04-03 | 江苏博斯腾纳米涂层有限公司 | Preparation method of nano anti-fogging agent |
| CN103626463A (en) * | 2013-12-06 | 2014-03-12 | 徐伟 | Environment-friendly diatom ooze composite material and production method for decorative plates |
| CN104147631A (en) * | 2014-07-31 | 2014-11-19 | 赵海银 | Haze-proof technical method and product for purifying in-car air with oxygen-derived negative ions |
| CN105176156A (en) * | 2015-09-17 | 2015-12-23 | 苏州智见新材料技术有限公司 | Nano antifogging paint composition and preparation method thereof |
-
2017
- 2017-10-12 CN CN201710945796.1A patent/CN107815295A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103013197A (en) * | 2012-12-19 | 2013-04-03 | 江苏博斯腾纳米涂层有限公司 | Preparation method of nano anti-fogging agent |
| CN103626463A (en) * | 2013-12-06 | 2014-03-12 | 徐伟 | Environment-friendly diatom ooze composite material and production method for decorative plates |
| CN104147631A (en) * | 2014-07-31 | 2014-11-19 | 赵海银 | Haze-proof technical method and product for purifying in-car air with oxygen-derived negative ions |
| CN105176156A (en) * | 2015-09-17 | 2015-12-23 | 苏州智见新材料技术有限公司 | Nano antifogging paint composition and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108530644A (en) * | 2018-04-18 | 2018-09-14 | 河南科技学院 | A kind of Multifunctional coordination copolymer nanometer material and preparation method thereof |
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Application publication date: 20180320 |
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