CN107793860A - A kind of acrylic acid composite coating and preparation method thereof - Google Patents
A kind of acrylic acid composite coating and preparation method thereof Download PDFInfo
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- CN107793860A CN107793860A CN201710893215.4A CN201710893215A CN107793860A CN 107793860 A CN107793860 A CN 107793860A CN 201710893215 A CN201710893215 A CN 201710893215A CN 107793860 A CN107793860 A CN 107793860A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D187/00—Coating compositions based on unspecified macromolecular compounds, obtained otherwise than by polymerisation reactions only involving unsaturated carbon-to-carbon bonds
- C09D187/005—Block or graft polymers not provided for in groups C09D101/00 - C09D185/04
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Paints Or Removers (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
Abstract
The present invention relates to a kind of acrylic acid composite coating and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：60 75 parts of acrylic resin, 15 25 parts of acrylic emulsion, 5 10 parts of carbon black, 10 15 parts of hollow glass microbead, 10 15 parts of terpene resin, 10 15 parts of Petropols, 69 parts of hydroxyethyl cellulose, 46 parts of butyl acetate, 35 parts of disodium ethylene diamine tetraacetate, 6 10 parts of deionized water.Material of the present invention is easy to get, and cost is low, and environment-friendly and green, lubricity is strong, construction is simple, high temperature resistant, corrosion-resistant with the good saturating effect of waterproof, seepage control, ageing resistance is strong, has and maintains cohesive force and good tack, heat endurance is strong, rapid-curing cutback, and cleannes are high, usage time length.
Description
Technical field
The present invention relates to paint field, and in particular to a kind of acrylic acid composite coating and preparation method thereof.
Background technology
Concrete is one of material that dosage is maximum in modern architecture, purposes is most wide.This is due to that it not only has raw material
Abundant, cheap, the characteristics of simple production process, but also, good endurance high with compression strength, strength grade scope are wide
The advantages of.Little by little, concrete is posted with very high great expectations by people.But in fact, it can occur in concrete hydrating hardening process
Volume contraction deforms, while can also cause inside concrete tension to be more than tensile strength, the cracking and phenomenon that seeps water, seriously
Influence the security of the durability of concrete, the stability of reinforcing bar and building.Therefore, it is that people grind to solve cracking and seepage problem
Study carefully one of important directions of concrete.
Waterproof is the key for solving concrete cracking and seepage problem, and water is a kind of polar substances, and surface tension is about
72mN/m, diffusivity is very strong, can soak many kinds of substance, can not only be flowed under gravity by larger interstitial channels,
And it can be spread by pore to all directions.In order to prevent infiltration of the water to some positions of building, people are typically
It is-the material waterproofing that taken measures from construction material.Mainly using architectural waterproof material, (such as waterproof is rolled up for material waterproofing
Material, water-repellent paint) block water path, with reach the purpose of waterproof or increase anti-leakage ability.Waterproof roll is mainly
For construction wall, roofing etc., play and resist extraneous rainwater, a kind of rollable flexible building materials into web-like of underground water seepage produce
Product, but there is the problem of such：Coiled material poor toughness, seam crossing imprecision, easy seepage.Water-repellent paint is primarily referred to as applying
For brush on building surface, the chemical reaction of volatilization or two kinds of components through solvent or moisture forms thin film, makes building
Surface completely cuts off with water, so as to play a part of waterproof, sealing.The waterproofing membrane formed after water-repellent paint is cured has certain
Extensibility, elastoplasticity, crack resistance, impermeability and weatherability, waterproof can be played, prevent blending protective effect.Conventional water-repellent paint
Have：Polyurethane water-proof paint, epoxy resin waterproof coating and acrylate waterproof paint.Wherein, acrylate flood coat applies
Material is and one-component water-emulsifying type waterproof coatings prepared by add other additives using acrylate polymer emulsion as base-material.
It has excellent weatherability, heat resistance and ultra-violet resistance, and performance is substantially unchanged in the range of -30 DEG C to 80 DEG C, and
Adapt to the craze and transfiguration of basal plane certain amplitude.But there is a kind of simple macromolecule emulsion to be deposited for acrylate waterproof paint
Limitation, such as：Film compactness is poor, bad to the shielding of vapor and oxygen, and tensile strength is relatively low, elongation percentage compared with
Small, service life is shorter, limits its application to a certain extent.Therefore, want to widen answering for acrylate waterproof paint
Applied with scope, it is necessary to develop other materials and acrylate waterproof paint is modified so as to obtain the good waterproof of combination property
Material.
The content of the invention
A kind of acrylic acid composite coating and preparation method thereof is provided the invention aims to overcome the shortcomings of the above.
Technical scheme includes：A kind of acrylic acid composite coating and preparation method thereof, raw material constituent is by weight
Amount number is made up of following ratio：Acrylic resin 60-75 parts, acrylic emulsion 15-25 parts, carbon black 5-10 parts, double glazing
Microballon 10-15 parts, terpene resin 10-15 parts, Petropols 10-15 parts, hydroxyethyl cellulose 6-9 parts, butyl acetate 4-6 parts,
Disodium ethylene diamine tetraacetate 3-5 parts, deionized water 6-10 parts.
Further improvement of the present invention is：Its preparation method is as follows：
A, acrylic resin, terpene resin and Petropols are merged, polycondensation, temperature is set to 80-140 DEG C, add carbon black,
Hydroxyethyl cellulose and hollow glass microbead are stirred, and stir speed (S.S.) 600-800r/min, after stirring, obtain mixture
A；
B, butyl acetate and disodium ethylene diamine tetraacetate are added into deionized water to be stirred, stir speed (S.S.) 400-500r/
Min, is stirring evenly and then adding into acrylic emulsion, and redistillation goes out excessive moisture to thick, obtains mixture B；
C, mixture B additions mixture A is stirred, adds centrifugal treating in centrifuge, frequency 8000-9500HZ, 10-
Viscous liquid is taken after 15min, obtains product.
Beneficial effects of the present invention：Material of the present invention is easy to get, and cost is low, and environment-friendly and green, lubricity is strong, construction is simple, tool
There is a saturating effect of good waterproof, seepage control, high temperature resistant, corrosion-resistant, ageing resistance is strong, has and maintains cohesive force and good first viscous
Property, heat endurance is strong, rapid-curing cutback, and cleannes are high, usage time length.
Embodiment：
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, and the embodiment is only used
In explaining the present invention, it is not intended to limit the scope of the present invention..
Embodiment 1
A kind of acrylic acid composite coating and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：Propylene
60 parts of acid resin, 18 parts of acrylic emulsion, 7 parts of carbon black, 13 parts of hollow glass microbead, 10 parts of terpene resin, 14 parts of Petropols,
7 parts of hydroxyethyl cellulose, 5 parts of butyl acetate, 3 parts of disodium ethylene diamine tetraacetate, 8 parts of deionized water.
Its preparation method is as follows：
A, acrylic resin, terpene resin and Petropols are merged, polycondensation, temperature is set to 120 DEG C, adds carbon black, hydroxyl
Ethyl cellulose and hollow glass microbead are stirred, stir speed (S.S.) 650r/min, after stirring, obtain mixture A；
B, butyl acetate and disodium ethylene diamine tetraacetate are added into deionized water to be stirred, stir speed (S.S.) 480r/min, stirred
Acrylic emulsion is added after mixing uniformly, redistillation goes out excessive moisture to thick, obtains mixture B；
C, mixture B is added into mixture A to stir, centrifugal treating in addition centrifuge, after frequency 9500HZ, 13min
Viscous liquid is taken, obtains product.
Embodiment 2
A kind of acrylic acid composite coating and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：Propylene
60 parts of acid resin, 25 parts of acrylic emulsion, 5 parts of carbon black, 15 parts of hollow glass microbead, 10 parts of terpene resin, 15 parts of Petropols,
6 parts of hydroxyethyl cellulose, 4 parts of butyl acetate, 3 parts of disodium ethylene diamine tetraacetate, 10 parts of deionized water.
Its preparation method is as follows：
A, acrylic resin, terpene resin and Petropols are merged, polycondensation, temperature is set to 140 DEG C, adds carbon black, hydroxyl
Ethyl cellulose and hollow glass microbead are stirred, stir speed (S.S.) 600r/min, after stirring, obtain mixture A；
B, butyl acetate and disodium ethylene diamine tetraacetate are added into deionized water to be stirred, stir speed (S.S.) 400r/min, stirred
Acrylic emulsion is added after mixing uniformly, redistillation goes out excessive moisture to thick, obtains mixture B；
C, mixture B is added into mixture A to stir, centrifugal treating in addition centrifuge, after frequency 9500HZ, 15min
Viscous liquid is taken, obtains product.
Embodiment 3
A kind of acrylic acid composite coating and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：Propylene
75 parts of acid resin, 25 parts of acrylic emulsion, 5 parts of carbon black, 15 parts of hollow glass microbead, 10 parts of terpene resin, 10 parts of Petropols,
9 parts of hydroxyethyl cellulose, 4 parts of butyl acetate, 3 parts of disodium ethylene diamine tetraacetate, 10 parts of deionized water.
Its preparation method is as follows：
A, acrylic resin, terpene resin and Petropols are merged, polycondensation, temperature is set to 80 DEG C, adds carbon black, hydroxyl second
Base cellulose and hollow glass microbead are stirred, stir speed (S.S.) 800r/min, after stirring, obtain mixture A；
B, butyl acetate and disodium ethylene diamine tetraacetate are added into deionized water to be stirred, stir speed (S.S.) 500r/min, stirred
Acrylic emulsion is added after mixing uniformly, redistillation goes out excessive moisture to thick, obtains mixture B；
C, mixture B is added into mixture A to stir, centrifugal treating in addition centrifuge, after frequency 9500HZ, 10min
Viscous liquid is taken, obtains product.
Embodiment 4
A kind of acrylic acid composite coating and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：Propylene
70 parts of acid resin, 20 parts of acrylic emulsion, 8 parts of carbon black, 13 parts of hollow glass microbead, 14 parts of terpene resin, 13 parts of Petropols,
8 parts of hydroxyethyl cellulose, 5 parts of butyl acetate, 4 parts of disodium ethylene diamine tetraacetate, 8 parts of deionized water.
Its preparation method is as follows：
A, acrylic resin, terpene resin and Petropols are merged, polycondensation, temperature is set to 110 DEG C, adds carbon black, hydroxyl
Ethyl cellulose and hollow glass microbead are stirred, stir speed (S.S.) 750r/min, after stirring, obtain mixture A；
B, butyl acetate and disodium ethylene diamine tetraacetate are added into deionized water to be stirred, stir speed (S.S.) 450r/min, stirred
Acrylic emulsion is added after mixing uniformly, redistillation goes out excessive moisture to thick, obtains mixture B；
C, mixture B is added into mixture A to stir, centrifugal treating in addition centrifuge, after frequency 9000HZ, 13min
Viscous liquid is taken, obtains product.
In above example, embodiment 4 is most preferred embodiment, has an excellent saturating effect of waterproof, seepage control, in above-mentioned steps C
It is very high to centrifuge unit frequency, can effective product mix, improve the stability of internal structure.
Explanation embodiments of the present invention are the foregoing is only, are not intended to limit the invention, for the technology of this area
For personnel, within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., it should be included in
Within protection scope of the present invention.
Claims (2)
- A kind of 1. acrylic acid composite coating and preparation method thereof, it is characterised in that：Raw material constituent is in parts by weight by following Ratio forms：Acrylic resin 60-75 parts, acrylic emulsion 15-25 parts, carbon black 5-10 parts, hollow glass microbead 10-15 parts, Terpene resin 10-15 parts, Petropols 10-15 parts, hydroxyethyl cellulose 6-9 parts, butyl acetate 4-6 parts, ethylenediamine tetra-acetic acid Disodium 3-5 parts, deionized water 6-10 parts.
- A kind of 2. acrylic acid composite coating according to claim 1 and preparation method thereof, it is characterised in that：Its preparation method It is as follows：A, acrylic resin, terpene resin and Petropols are merged, polycondensation, temperature is set to 80-140 DEG C, add carbon black, Hydroxyethyl cellulose and hollow glass microbead are stirred, and stir speed (S.S.) 600-800r/min, after stirring, obtain mixture A；B, butyl acetate and disodium ethylene diamine tetraacetate are added into deionized water to be stirred, stir speed (S.S.) 400-500r/ Min, is stirring evenly and then adding into acrylic emulsion, and redistillation goes out excessive moisture to thick, obtains mixture B；C, mixture B additions mixture A is stirred, adds centrifugal treating in centrifuge, frequency 8000-9500HZ, 10- Viscous liquid is taken after 15min, obtains product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710893215.4A CN107793860A (en) | 2017-09-28 | 2017-09-28 | A kind of acrylic acid composite coating and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710893215.4A CN107793860A (en) | 2017-09-28 | 2017-09-28 | A kind of acrylic acid composite coating and preparation method thereof |
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| Publication Number | Publication Date |
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| CN107793860A true CN107793860A (en) | 2018-03-13 |
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| CN201710893215.4A Withdrawn CN107793860A (en) | 2017-09-28 | 2017-09-28 | A kind of acrylic acid composite coating and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108531017A (en) * | 2018-04-24 | 2018-09-14 | 四川文希科技有限公司 | A kind of building coating of waterproof easy cleaning |
| CN109098005A (en) * | 2018-07-31 | 2018-12-28 | 合肥远科服装设计有限公司 | A kind of coating and preparation method thereof for shell fabric for fire garment |
| CN111763452A (en) * | 2020-07-23 | 2020-10-13 | 江苏大使同丰涂料有限公司 | Multifunctional refraction coating |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104119754A (en) * | 2014-08-01 | 2014-10-29 | 吴江华诚复合材料科技有限公司 | Acrylate series colorful coating material |
| CN104403455A (en) * | 2014-11-28 | 2015-03-11 | 安徽省金盾涂料有限责任公司 | Safe, environment-friendly, heat-resisting and antibacterial water-based paint |
| CN104530859A (en) * | 2014-12-11 | 2015-04-22 | 青岛佰众化工技术有限公司 | Thin-layer heat-preserving insulation coating material |
| CN105385265A (en) * | 2015-11-14 | 2016-03-09 | 合肥标兵凯基新型材料有限公司 | Corrosion-resistant and weatherproof paint specially used for pop can |
| CN106147470A (en) * | 2015-04-05 | 2016-11-23 | 泉州市合创涂料科技有限公司 | A kind of preparation method of water-borne acrylic resin heat insulating coatings |
-
2017
- 2017-09-28 CN CN201710893215.4A patent/CN107793860A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104119754A (en) * | 2014-08-01 | 2014-10-29 | 吴江华诚复合材料科技有限公司 | Acrylate series colorful coating material |
| CN104403455A (en) * | 2014-11-28 | 2015-03-11 | 安徽省金盾涂料有限责任公司 | Safe, environment-friendly, heat-resisting and antibacterial water-based paint |
| CN104530859A (en) * | 2014-12-11 | 2015-04-22 | 青岛佰众化工技术有限公司 | Thin-layer heat-preserving insulation coating material |
| CN106147470A (en) * | 2015-04-05 | 2016-11-23 | 泉州市合创涂料科技有限公司 | A kind of preparation method of water-borne acrylic resin heat insulating coatings |
| CN105385265A (en) * | 2015-11-14 | 2016-03-09 | 合肥标兵凯基新型材料有限公司 | Corrosion-resistant and weatherproof paint specially used for pop can |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108531017A (en) * | 2018-04-24 | 2018-09-14 | 四川文希科技有限公司 | A kind of building coating of waterproof easy cleaning |
| CN109098005A (en) * | 2018-07-31 | 2018-12-28 | 合肥远科服装设计有限公司 | A kind of coating and preparation method thereof for shell fabric for fire garment |
| CN111763452A (en) * | 2020-07-23 | 2020-10-13 | 江苏大使同丰涂料有限公司 | Multifunctional refraction coating |
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Application publication date: 20180313 |