CN107780302A - A kind of cork paper and preparation method with sweet taste antiseep - Google Patents
A kind of cork paper and preparation method with sweet taste antiseep Download PDFInfo
- Publication number
- CN107780302A CN107780302A CN201710933223.7A CN201710933223A CN107780302A CN 107780302 A CN107780302 A CN 107780302A CN 201710933223 A CN201710933223 A CN 201710933223A CN 107780302 A CN107780302 A CN 107780302A
- Authority
- CN
- China
- Prior art keywords
- antiseep
- cigarette
- paper
- sweet taste
- cork paper
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/80—Paper comprising more than one coating
- D21H19/82—Paper comprising more than one coating superposed
- D21H19/824—Paper comprising more than one coating superposed two superposed coatings, both being non-pigmented
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The present invention provides a kind of cork paper and preparation method with sweet taste antiseep, for cigarette filter, cigarette filter includes filter wire fasces, including outer layer forming paper, outer layer forming paper includes anti-oil reservoir and oleophobic hydrophilic layer, anti- oil reservoir and oleophobic hydrophilic layer is cascadingly set at least one side of outer layer forming paper, and filter wire fasces both ends filling acetate silk, acetate silk is bonded by adhesive and outer layer forming paper.The present invention can increase the sense of flue gas sweet tea, improves flue gas mildness and improve pleasant impression, the effect of significantly enhancing cigarette sweet sense can be reached, and the material can be sprayed directly on tow and be prepared into cigarette filter tip, it is not involved in burning, avoids and result from the uncoordinated miscellaneous gas of tobacco this perfume because material participates in cigarette burning in itself.The low raw-material cost of the present invention simultaneously, preparation is simple, and it is applied to cigarette industry mature production technology, is had a wide range of applications in tobacco business.
Description
Technical field
The invention belongs to cigarette supplementary material technical field, and in particular to a kind of cork paper with sweet taste antiseep and preparation
Method.
Background technology
Sweet taste is generally liked for masses always, also in this way, sweet tea sense can lift the comfortableness of cigarette smoking on cigarette, by
Consumers.Researcher generally increases the sweet tea sense of cigarette smoke by tobacco perfuming feeding technique, but flavoring and casing can companion
Burnt with suction, often bring other miscellaneous tastes.
Important component of the filter stick as cigarette, to increasing flue gas concentration, cigarette perfume is enriched, lifts flue gas moisture feeling, is improved
Cigarette smoking quality plays vital effect.The cigarette filter rod used at present in industry has cellulose acetate filter rod, paper
Matter filter stick and polypropylene filter.Cellulose acetate filter rod is current most popular a kind of cigarette filter rod, and such filter stick is to flue gas
Grain phase component has certain intercepting efficiency, and larger negative effect will not be produced to cigarette odor-absorbing, but as cigarette industry is to volume
The continuous improvement of cigarette flavouring humectation requirement, simple cellulose acetate filter rod have been difficult to meet need of the cigarette industry to filter stick functionalization
Ask, and many functional powder body materials show excellent properties in terms of cigarette flavouring humectation, but produced by its solvent spinning
The limitation of technique, it is impossible to be directly carried in acetate fiber, can only in the production process that acetate fiber is prepared into filter stick with
The form of grain or line load is applied in filter stick, and the particle diameter of particle need to be typically controlled in 40-80 mesh, but above-mentioned application mode
The defects of functional material addition is limited, filter stick homogeneity is serious, production cost is high be present.Therefore, a kind of raw material sources are developed
Extensively, it is easy to a large amount of loads of function powder material, production cost is low and can effectively improve the new cigarette of cigarette smoking quality
Filter stick seems particularly urgent.
Essence and flavoring agent can be played in cigarette cover shortcoming, improve tobacco aroma and it is jealous, improve tobacco it is physical
The effect of the unique taste of cigarette and style, can be assigned, and product quality differentiation can be realized, stable cigarette smoking product
Matter, had a major impact for the style and quality responses of cigarette.With the quick-fried pearl that quick-fried pearl is applied to cigarette filter tip, centre is surrounded by cigarette
Essence, consumer can discharge essence and flavoring agent with quick-fried pearl by pinching brokenly cigarette in suction, special fragrance brought to cigarette flavor
Impression.
Because quick-fried pearl discharges a large amount of oil-based liquids, cigarette holder surface is infiltrated into, so as to result from uncoordinated miscellaneous of tobacco this perfume
Taste, influence mouthfeel.
The content of the invention
【1】Technical problems to be solved
The technical problem to be solved in the present invention is to provide one kind can play increase flue gas it is sweet degree and comfortableness, cover it is miscellaneous
Gas etc. is acted on, and is not involved in burning, and the sweetish cork paper and preparation method of any negative effect will not be come to tobacco rolling belt.
【2】The technical scheme solved the problems, such as
The present invention provides a kind of cork paper with sweet taste antiseep, and for cigarette filter, the cigarette filter includes
Filter wire fasces, including outer layer forming paper, outer layer forming paper include anti-oil reservoir and oleophobic hydrophilic layer, the anti-oil reservoir and described dredge
Oily hydrophilic layer is cascadingly set at least one side of the outer layer forming paper, and the anti-oil reservoir is crylic acid resin, gathered
One or more compositions in urethane class, polyphenylalanine, Poly(Phe), rosin resin, butyral resin and polyurethane；
The oleophobic hydrophilic layer is a kind of composition in makrolon and polyurethane, and acetate fibres are filled at the filter wire fasces both ends
Beam, the acetate silk are bonded by adhesive and the outer layer forming paper.
The above-mentioned cork paper with sweet taste antiseep, the adhesive include modifying agent and water-base cement, the modifying agent bag
Sweetener, glucono-δ-lactone, chitin-chitosan emulsion are included, the weight ratio of each component is：Glucono-δ-lactone
18%~21%, sweetener 7.2%~9.8%, chitin-chitosan emulsion 60%~84%.
The above-mentioned cork paper with sweet taste antiseep, the sweetener are in acesulfame potassium, steviol glycoside and Aspartame
One or more composition.
The above-mentioned cork paper with sweet taste antiseep, the water-base cement include Aqueous Adhesives 18%~21%, deionization
Water 42%~76%, organic amine 1%~10%, organic acid 1%~10%；The modifying agent mixes at room temperature with the water-base cement
Emulsification forms mix emulsion fluid.
The above-mentioned cork paper with sweet taste antiseep, the organic amine are ethylenediamine, propane diamine, butanediamine, monoethanolamine, guanidine
With the one or more in dimethylbiguanide；The organic acid is one kind or several in acetic acid, propionic acid, citric acid and malic acid
Kind.
Technical problem solved by the invention can be realized using following technical scheme：A kind of water with sweet taste antiseep
The preparation method of loose paper, comprises the following steps：
Step A, after organic amine, organic acid and deionized water are mixed, under agitation, it is slowly dropped to water-based gluing
In agent, ultrasonic disperse 40-60min after stirring, water-base cement emulsion is obtained；
Step B, after sweetener, glucono-δ-lactone are mixed, it is added in chitin-chitosan emulsion, stirs
After uniformly, modifying agent is obtained；
Step C, the water-base cement emulsion obtained by step A is mixed with 2 DEG C/min heating with the modifying agent obtained by step B
Speed, 60 DEG C are warming up to by normal temperature, natural cooling, then produce adhesive after flowing back, centrifuging；
Step D, the adhesive is applied in outer layer forming paper using sizer.
The preparation method of the above-mentioned cork paper with sweet taste antiseep, the step B includes step B1, by chitin-shell
Glycan emulsion is heated up to 42 DEG C, and then stirring adds sweetener, mixing time 15-20min.
The preparation method of the above-mentioned cork paper with sweet taste antiseep, the step D include：
Step D1, there is provided cork paper, the cork paper have relative two sides；
Step D2, there is provided oil-proof paint, printed in one side or be coated with the oil-proof paint, the first anti-oil reservoir is made；
Step D3, there is provided oleophobic hydrophilic coating, the oleophobic hydrophilic coating have compatible tree respectively with the oil-proof paint
Aliphatic radical body；
Step D4, printed on the described first anti-oil reservoir or be coated with the oleophobic hydrophilic coating, it is hydrophilic that the first oleophobic is made
Layer, obtains the outer layer forming paper.
The preparation method of the above-mentioned cork paper with sweet taste antiseep, the step D includes step D5, in the cork paper
Another side print or be coated with the oil-proof paint and the oleophobic hydrophilic coating successively, obtain the second anti-oil reservoir and the second oleophobic
Hydrophilic layer.
【3】Beneficial effect
This sweetish cork paper of the present invention and preparation method can increase the sense of flue gas sweet tea, improve flue gas mildness and change
Kind pleasant impression, if the effect that can reach significantly enhancing cigarette sweet sense on a small quantity is added, and also the material can be sprayed directly on
Cigarette filter tip is prepared on tow, is not involved in burning, avoids and results from tobacco this perfume because material participates in cigarette burning in itself
Uncoordinated miscellaneous gas.The low raw-material cost of the present invention simultaneously, preparation is simple, and it is applied to cigarette industry production work
Skill is ripe, is had a wide range of applications in tobacco business.
Brief description of the drawings
Fig. 1 is a kind of structural representation of the preparation method of the cork paper with sweet taste antiseep of the present invention.
Embodiment
Below in conjunction with the accompanying drawings, the embodiment of the present invention is discussed in detail.
The present invention provides a kind of cork paper with sweet taste antiseep, and for cigarette filter, the cigarette filter includes
Filter wire fasces, including outer layer forming paper, outer layer forming paper include anti-oil reservoir and oleophobic hydrophilic layer, the anti-oil reservoir and described dredge
Oily hydrophilic layer is cascadingly set at least one side of the outer layer forming paper, and the anti-oil reservoir is crylic acid resin, gathered
One or more compositions in urethane class, polyphenylalanine, Poly(Phe), rosin resin, butyral resin and polyurethane；
The oleophobic hydrophilic layer is a kind of composition in makrolon and polyurethane, and acetate fibres are filled at the filter wire fasces both ends
Beam, the acetate silk are bonded by adhesive and the outer layer forming paper.
Further, in a kind of preferred embodiment of the cork paper with sweet taste antiseep of the present invention, the adhesive bag
Modifying agent and water-base cement are included, the modifying agent includes sweetener, glucono-δ-lactone, chitin-chitosan emulsion, each group
The weight ratio of composition is：Glucono-δ-lactone 18%~21%, sweetener 7.2%~9.8%, chitin-chitosan emulsion
60%~84%.
Further, in a kind of preferred embodiment of the cork paper with sweet taste antiseep of the present invention, the sweetener is
One or more compositions in acesulfame potassium, steviol glycoside and Aspartame.
Further, in a kind of preferred embodiment of the cork paper with sweet taste antiseep of the present invention, the water-base cement bag
Include Aqueous Adhesives 18%~21%, deionized water 42%~76%, organic amine 1%~10%, organic acid 1%~10%；Institute
Stating modifying agent, mixing and emulsifying forms mix emulsion fluid at room temperature with the water-base cement.
Further, in a kind of preferred embodiment of the cork paper with sweet taste antiseep of the present invention, the organic amine is
One or more in ethylenediamine, propane diamine, butanediamine, monoethanolamine, guanidine and dimethylbiguanide；The organic acid is acetic acid, third
One or more in acid, citric acid and malic acid.
Smoke panel test experiment：Certain brand cigarette of selection with mouth rod length identical with cigarette filter tip A, cigarette filter tip B and size
As control cigarette, mouth rod therein is the solid mouth rod for being stuffed entirely with filtering material.Then by cigarette filter tip A and cigarette filter tip
Cigarette A and cigarette B is respectively prepared in B, and wherein cigarette A and cigarette B tobacco material is identical with tobacco material in control cigarette, cigarette
A and cigarette B cigarette paper and tipping paper scantling is identical with control cigarette.Then respectively to cigarette A, cigarette B and
Control cigarette is smoked panel test, and extracts each sample by GB/T5606.1, sample moisture is adjusted according to GB/T16447 before smokeing panel test.According to
《Cigarette》GB5606.4-2005 Sensory Quality of Cigarette technical requirements table evaluates the improvement of aesthetic quality, the sense organ matter of cigarette product
Amount is generally included in gloss, fragrance, harmony, miscellaneous gas, excitant and wherein each index of six technical requirements of pleasant impression, is score value
More high organoleptic quality is better.
Cross specialty to smoke panel test technical staff's evaluation, unanimously think taking out using the cigarette of composite tip stick of addition solid sweetener
Harmony, fragrance etc. do not destroy during suction, do not have negative interaction to the suction quality of cigarette, and can slightly improve the comfortableness of suction.
Contrasted by evaluation effect, it is found that the sugariness of the cigarette flue gas using the composite tip stick added with granular sweetener shows
Increase is write, is shown by analysis of experimental data and Analyses Methods for Sensory Evaluation Results, mixing sweetener is more preferable than single sweetener effect, right
The sweetening effect of flue gas becomes apparent from.And acesulfame potassium, steviol glycoside, Aspartame are according to 1:4:The sweet tea prepared after the mixing of 15 ratios
Taste agent, score value highest of smokeing panel test, the sweet tea sense lifting of flue gas are most notable.
The present invention combines the cigarette with essence and uses quick-fried pearl, added in cigarette filter tip, realizes from low cool degree to the cool degree of height
Suction experience, fragrance matter can be brought into flue gas, is not involved in burning, do not produce new harmful substance, and quantitative accurate,
Seepage is prevented, storage period imitates the features such as long.
Refering to Fig. 1, a kind of preparation method of the cork paper with sweet taste antiseep, comprise the following steps：Step A, will be organic
After amine, organic acid and deionized water mixing, under agitation, it is slowly dropped in Aqueous Adhesives, it is ultrasonic after stirring
Scattered 40-60min, obtains water-base cement emulsion；Step B, after sweetener, glucono-δ-lactone are mixed, it is added to first
In shell element-chitosan emulsion, after stirring, modifying agent is obtained；
Step C, the water-base cement emulsion obtained by step A is mixed with 2 DEG C/min heating with the modifying agent obtained by step B
Speed, 60 DEG C are warming up to by normal temperature, natural cooling, then produce adhesive after flowing back, centrifuging；
Step D, the adhesive is applied in outer layer forming paper using sizer.
Further, in a kind of preferred embodiment of the preparation method of the cork paper with sweet taste antiseep of the present invention, institute
Stating step B includes step B1, and chitin-chitosan emulsion is heated up into 42 DEG C, and then stirring adds sweetener, and mixing time is
15-20min。
Further, in a kind of preferred embodiment of the preparation method of the cork paper with sweet taste antiseep of the present invention, institute
Stating step D includes：
Step D1, there is provided cork paper, the cork paper have relative two sides；
Step D2, there is provided oil-proof paint, printed in one side or be coated with the oil-proof paint, the first anti-oil reservoir is made；
Step D3, there is provided oleophobic hydrophilic coating, the oleophobic hydrophilic coating have compatible tree respectively with the oil-proof paint
Aliphatic radical body；
Step D4, printed on the described first anti-oil reservoir or be coated with the oleophobic hydrophilic coating, it is hydrophilic that the first oleophobic is made
Layer, obtains the outer layer forming paper.
Further, in a kind of preferred embodiment of the preparation method of the cork paper with sweet taste antiseep of the present invention, institute
Stating step D includes step D5, prints or be coated with the oil-proof paint and oleophobic parent successively in the another side of the cork paper
Water paint, obtain the second anti-oil reservoir and the second oleophobic hydrophilic layer.
This sweetish cork paper of the present invention and preparation method can increase the sense of flue gas sweet tea, improve flue gas mildness and change
Kind pleasant impression, if the effect that can reach significantly enhancing cigarette sweet sense on a small quantity is added, and also the material can be sprayed directly on
Cigarette filter tip is prepared on tow, is not involved in burning, avoids and results from tobacco this perfume because material participates in cigarette burning in itself
Uncoordinated miscellaneous gas.The low raw-material cost of the present invention simultaneously, preparation is simple, and it is applied to cigarette industry production work
Skill is ripe, is had a wide range of applications in tobacco business.
Described above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, without departing from the technical principles of the invention, some improvements and modifications can also be made, these improvements and modifications
Also it should be regarded as protection scope of the present invention.
Claims (9)
1. a kind of cork paper with sweet taste antiseep, for cigarette filter, the cigarette filter includes filter wire fasces, its
It is characterised by, including outer layer forming paper, outer layer forming paper include anti-oil reservoir and oleophobic hydrophilic layer, the anti-oil reservoir and the oleophobic
Hydrophilic layer is cascadingly set at least one side of the outer layer forming paper, and the anti-oil reservoir is crylic acid resin, poly- ammonia
One or more compositions in esters, polyphenylalanine, Poly(Phe), rosin resin, butyral resin and polyurethane；Institute
Oleophobic hydrophilic layer is stated as a kind of composition in makrolon and polyurethane, acetate fibres are filled at the filter wire fasces both ends
Beam, the acetate silk are bonded by adhesive and the outer layer forming paper.
2. a kind of cork paper with sweet taste antiseep as claimed in claim 1, it is characterised in that the adhesive includes being modified
Agent and water-base cement, the modifying agent include sweetener, glucono-δ-lactone, chitin-chitosan emulsion, each component
Weight ratio is：Glucono-δ-lactone 18%~21%, sweetener 7.2%~9.8%, chitin-chitosan emulsion 60%~
84%.
3. a kind of cork paper with sweet taste antiseep as claimed in claim 2, it is characterised in that the sweetener is matched for peace
One or more compositions in honey, steviol glycoside and Aspartame.
4. a kind of cork paper with sweet taste antiseep as claimed in claim 2, it is characterised in that the water-base cement includes water-based
Adhesive 18%~21%, deionized water 42%~76%, organic amine 1%~10%, organic acid 1%~10%；The modification
Mixing and emulsifying forms mix emulsion fluid at room temperature with the water-base cement for agent.
5. a kind of cork paper with sweet taste antiseep as claimed in claim 4, it is characterised in that the organic amine is second two
One or more in amine, propane diamine, butanediamine, monoethanolamine, guanidine and dimethylbiguanide；The organic acid is acetic acid, propionic acid, lemon
One or more in lemon acid and malic acid.
6. a kind of preparation method of the cork paper with sweet taste antiseep, it is characterised in that comprise the following steps：
Step A, after organic amine, organic acid and deionized water are mixed, under agitation, it is slowly dropped to Aqueous Adhesives
In, ultrasonic disperse 40-60min after stirring, obtain water-base cement emulsion；
Step B, after sweetener, glucono-δ-lactone are mixed, it is added in chitin-chitosan emulsion, stirs
Afterwards, modifying agent is obtained；
Step C, the water-base cement emulsion obtained by step A is mixed with the modifying agent obtained by step B to the heating speed with 2 DEG C/min
Degree, 60 DEG C are warming up to by normal temperature, natural cooling, then produce adhesive after flowing back, centrifuging；
Step D, the adhesive is applied in outer layer forming paper using sizer.
A kind of 7. preparation method of the cork paper with sweet taste antiseep as claimed in claim 6, it is characterised in that the step
B includes step B1, and chitin-chitosan emulsion is heated up into 42 DEG C, and then stirring adds sweetener, mixing time 15-
20min。
A kind of 8. preparation method of the cork paper with sweet taste antiseep as claimed in claim 6, it is characterised in that the step
D includes：
Step D1, there is provided cork paper, the cork paper have relative two sides；
Step D2, there is provided oil-proof paint, printed in one side or be coated with the oil-proof paint, the first anti-oil reservoir is made；
Step D3, there is provided oleophobic hydrophilic coating, the oleophobic hydrophilic coating have compatible resin base respectively with the oil-proof paint
Body；
Step D4, printed on the described first anti-oil reservoir or be coated with the oleophobic hydrophilic coating, the first oleophobic hydrophilic layer is made, obtains
Obtain the outer layer forming paper.
A kind of 9. preparation method of the cork paper with sweet taste antiseep as claimed in claim 8, it is characterised in that the step
D includes step D5, prints or be coated with the oil-proof paint and the oleophobic hydrophilic coating successively in the another side of the cork paper,
Obtain the second anti-oil reservoir and the second oleophobic hydrophilic layer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710933223.7A CN107780302A (en) | 2017-10-10 | 2017-10-10 | A kind of cork paper and preparation method with sweet taste antiseep |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710933223.7A CN107780302A (en) | 2017-10-10 | 2017-10-10 | A kind of cork paper and preparation method with sweet taste antiseep |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107780302A true CN107780302A (en) | 2018-03-09 |
Family
ID=61434298
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710933223.7A Pending CN107780302A (en) | 2017-10-10 | 2017-10-10 | A kind of cork paper and preparation method with sweet taste antiseep |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107780302A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109322208A (en) * | 2018-09-26 | 2019-02-12 | 上海乘鹰新材料有限公司 | A kind of cork paper explosion-proof pearl infiltration water paint and preparation method thereof |
-
2017
- 2017-10-10 CN CN201710933223.7A patent/CN107780302A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109322208A (en) * | 2018-09-26 | 2019-02-12 | 上海乘鹰新材料有限公司 | A kind of cork paper explosion-proof pearl infiltration water paint and preparation method thereof |
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Application publication date: 20180309 |