CN107780207A - A kind of fabric softener and preparation method thereof - Google Patents
A kind of fabric softener and preparation method thereof Download PDFInfo
- Publication number
- CN107780207A CN107780207A CN201710821137.7A CN201710821137A CN107780207A CN 107780207 A CN107780207 A CN 107780207A CN 201710821137 A CN201710821137 A CN 201710821137A CN 107780207 A CN107780207 A CN 107780207A
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- parts
- fabric softener
- ethanol
- dbsa
- diatomite
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- 239000002979 fabric softener Substances 0.000 title claims abstract description 50
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 64
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims abstract description 42
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 25
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims abstract description 22
- 229920000742 Cotton Polymers 0.000 claims abstract description 21
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000004115 Sodium Silicate Substances 0.000 claims abstract description 21
- 229910021538 borax Inorganic materials 0.000 claims abstract description 21
- 229910001629 magnesium chloride Inorganic materials 0.000 claims abstract description 21
- 235000019795 sodium metasilicate Nutrition 0.000 claims abstract description 21
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 21
- 229910052911 sodium silicate Inorganic materials 0.000 claims abstract description 21
- 239000004328 sodium tetraborate Substances 0.000 claims abstract description 21
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract description 21
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000008367 deionised water Substances 0.000 claims abstract description 18
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 18
- -1 sorbitan fatty acid ester Chemical class 0.000 claims abstract description 17
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 16
- 239000000194 fatty acid Substances 0.000 claims abstract description 16
- 229930195729 fatty acid Natural products 0.000 claims abstract description 16
- 239000002994 raw material Substances 0.000 claims abstract description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 28
- 238000003756 stirring Methods 0.000 claims description 27
- 235000019441 ethanol Nutrition 0.000 claims description 26
- 239000012456 homogeneous solution Substances 0.000 claims description 14
- 239000007788 liquid Substances 0.000 claims description 14
- 229910052757 nitrogen Inorganic materials 0.000 claims description 14
- 238000007664 blowing Methods 0.000 claims description 7
- 238000005538 encapsulation Methods 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 7
- 238000003780 insertion Methods 0.000 claims description 7
- 230000037431 insertion Effects 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 7
- 230000035484 reaction time Effects 0.000 claims description 7
- 238000002242 deionisation method Methods 0.000 claims description 3
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims 3
- 239000004744 fabric Substances 0.000 abstract description 21
- 238000005452 bending Methods 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 238000011084 recovery Methods 0.000 abstract description 3
- 238000010008 shearing Methods 0.000 abstract description 3
- 230000007423 decrease Effects 0.000 abstract description 2
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 230000003000 nontoxic effect Effects 0.000 abstract description 2
- 239000000835 fiber Substances 0.000 description 11
- 239000004902 Softening Agent Substances 0.000 description 9
- 239000004753 textile Substances 0.000 description 5
- 241000220324 Pyrus Species 0.000 description 3
- 230000018044 dehydration Effects 0.000 description 3
- 238000006297 dehydration reaction Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 235000021017 pears Nutrition 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 238000009987 spinning Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 239000002253 acid Substances 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000007730 finishing process Methods 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000008447 perception Effects 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000004758 synthetic textile Substances 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
- 238000004383 yellowing Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/02—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with hydrocarbons
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
- D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
- D06M11/155—Halides of elements of Groups 2 or 12 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
- D06M11/76—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
- D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/80—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides
- D06M11/82—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides with boron oxides; with boric, meta- or perboric acids or their salts, e.g. with borax
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/144—Alcohols; Metal alcoholates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/256—Sulfonated compounds esters thereof, e.g. sultones
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/368—Hydroxyalkylamines; Derivatives thereof, e.g. Kritchevsky bases
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/25—Resistance to light or sun, i.e. protection of the textile itself as well as UV shielding materials or treatment compositions therefor; Anti-yellowing treatments
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention discloses a kind of fabric softener and preparation method thereof, the fabric softener includes the raw material of following parts by weight：Natural 20 30 parts of cotton wax, 10 15 parts of sorbitan fatty acid ester, 10 15 parts of sodium metasilicate, 5 10 parts of diatomite, 10 15 parts of sodium acid carbonate, 59 parts of borax, 13 parts of triethanolamine, 10 20 parts of ethanol, 35 parts of DBSA, 5 10 parts of magnesium chloride, 30 50 parts of deionized water.After the fabric softener application of the present invention, the stiffness of fabric declines a lot, and shearing rigidity and bending stiffness all decline a lot, and creasy recovery angle increase is a lot, and flexibility improves a lot.The fabric softener manufacturing process of the present invention is simple to operation, and low in raw material price easily obtains, and nontoxic, human body is not stimulated, volatility is low.
Description
Technical field
The invention belongs to technical field of textile auxiliary agent, specifically relates to a kind of fabric softener and preparation method thereof.
Background technology
Softening agent is a kind of quiet, the coefficient of kinetic friction chemical substance that can change fiber.When changing confficient of static friction, hand
Thoughts and feelings touches with smooth sense, is easy to move on fiber or fabric；It is fine between fiber and fiber when changing the coefficient of kinetic friction
Structure is easy to be mutually shifted, that is, fiber or fabric it is easily deformable.
Soft finish is the important finishing process in dyeing and printing process.Textile in process, through repeatedly processing after
Feel can become coarse, and general synthetic fabrics is worse, especially Superfine Fibre Fabric.In order that fabric has softness, slided
Refreshing, comfortable feel, it is necessary to arranged to it, widely used at present arranged with softening agent.In addition in chemistry
Softening agent largely is used during fibre spinning, the spinning of various fibers, weaving etc., because with textile processing
A large amount of uses of high speed and short liquor ratio mode, the phase mutual friction increase between fabric and equipment between fabric, be also easy to produce scratch,
Phenomena such as bar defect.It can make fiber that there is the flexible smooth being adapted with processing conditions to avoid damage in itself using softening agent.
Therefore fabric is a kind of important textile auxiliary with softening agent.
With the improvement of living standards, the enhancing of health perception, the requirement more and more higher to textile material, it is desirable to which fabric has
There is certain soft wrinkle resistance, to the quality requirements of softening agent also more and more higher, which also promotes the development of softening agent.
The content of the invention
It is an object of the invention to provide a kind of fabric softener and preparation method thereof, to solve to carry in above-mentioned background technology
The problem of going out.
To achieve the above object, the present invention provides following technical scheme：
A kind of fabric softener, according to parts by weight, including following components：Natural cotton wax 20-30 parts, Sorbitan alcohol ester
Fat acid esters 10-15 parts, sodium metasilicate 10-15 parts, diatomite 5-10 parts, sodium acid carbonate 10-15 parts, borax 5-9 parts, triethanolamine 1-
3 parts, ethanol 10-20 parts, DBSA 3-5 parts, magnesium chloride 5-10 parts, deionized water 30-50 parts.
Preferably, the ethanol is absolute ethyl alcohol, and purity is pure to analyze.
Preferably, described fabric softener, according to parts by weight, including following components：Natural 20 parts of cotton wax, dehydration mountain
10 parts of pears alcohol fatty acid ester, 10 parts of sodium metasilicate, 5 parts of diatomite, 10 parts of sodium acid carbonate, 5 parts of borax, 1 part of triethanolamine, ethanol 10
Part, 3 parts of DBSA, 5 parts of magnesium chloride, 30 parts of deionized water.
Preferably, described fabric softener, according to parts by weight, including following components：Natural 25 parts of cotton wax, dehydration mountain
13 parts of pears alcohol fatty acid ester, 13 parts of sodium metasilicate, 8 parts of diatomite, 13 parts of sodium acid carbonate, 7 parts of borax, 2 parts of triethanolamine, ethanol 15
Part, 4 parts of DBSA, 8 parts of magnesium chloride, 40 parts of deionized water.
Preferably, described fabric softener, according to parts by weight, including following components：Natural 30 parts of cotton wax, dehydration mountain
15 parts of pears alcohol fatty acid ester, 15 parts of sodium metasilicate, 10 parts of diatomite, 15 parts of sodium acid carbonate, 9 parts of borax, 3 parts of triethanolamine, ethanol
20 parts, 5 parts of DBSA, 10 parts of magnesium chloride, 50 parts of deionized water.
Preferably, a kind of preparation method of the fabric softener, is comprised the following steps that：
(1) natural cotton wax 20-30 parts, sorbitan fatty acid ester 10-15 parts, deionization are added inside three-necked flask
Water 30-50 parts, in 70-80 DEG C of heating of oil bath pan, nitrogen protection, the speed for being passed through nitrogen is 1-2L/min, keeps charging flatly,
Insertion agitator flatly, mixing speed are 1000-2000 revs/min, reaction time 3-4h；
(2) first by borax 5-9 parts, triethanolamine 1-3 parts, ethanol 10-20 parts, with ultrasonic disperse 10-20 minutes, ultrasonic work(
Rate is 1200-1500W, obtains homogeneous solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 500-1000 revs/min, 20-30 points of stirring
Clock；
(4) temperature is reduced to 50-60 DEG C, adds sodium metasilicate 10-15 parts, DBSA 3-5 parts, magnesium chloride 5-10
Part, 500-1000 revs/min, stir 20-30 minutes；
(5) 40-50 DEG C is cooled to, diatomite 5-10 parts, sodium acid carbonate 10-15 parts is added, 500-1000 revs/min, stirs
Mix 1-2 hours；
(6) 20-30 DEG C is cooled to, closes down stirring, the liquid fabric softener prepared；
(7) stand and be cooled in three-necked flask liquid fabric softener and be less than 20 DEG C, blowing encapsulation, finished product.
Compared with prior art, the beneficial effects of the invention are as follows：
1st, after fabric softener of the invention application, the stiffness of fabric declines a lot, shearing rigidity and bending stiffness
All decline a lot, creasy recovery angle increase is a lot, and flexibility improves a lot.
2nd, after fabric softener application fabric of the invention, fabric has excellent soft feel, the sense of touch of fabric, slides
Sense is greatly improved, and suede class, fiber, the fluffy degree of fabric are improved.
3rd, fabric softener wide adaptability of the invention, various fibers are applicable.
4th, fabric softener of the invention environmental protection, without APEO.
5th, fabric softener manufacturing process of the invention is simple to operation, and low in raw material price easily obtains, and nontoxic,
Human body is not stimulated, volatility is low.
6th, mutual compatibility, synergy between various raw materials used in fabric softener of the invention, it is excellent to collectively constitute performance
Different product.
7th, the addition of sodium acid carbonate, the softness of fabric is improved.
8th, technique is simplified, safe operation is simple, is easy to industrialized production.
9th, after softening agent application fabric of the invention, fabric is not easy yellowing, can ensure the color transparent of fabric, smoothly
It is submissive, reduce fabric ages performance.
10th, use of the invention can receive good economic benefit.
Example is embodied
The invention discloses a kind of fabric softener, according to parts by weight, including following components：Natural cotton wax 20-30 parts,
Sorbitan fatty acid ester 10-15 parts, sodium metasilicate 10-15 parts, diatomite 5-10 parts, sodium acid carbonate 10-15 parts, borax 5-9
Part, triethanolamine 1-3 parts, ethanol 10-20 parts, DBSA 3-5 parts, magnesium chloride 5-10 parts, deionized water 30-50
Part.
Present invention also offers a kind of preparation method of fabric softener, comprise the following steps that：
(1) natural cotton wax 20-30 parts, sorbitan fatty acid ester 10-15 parts, deionization are added inside three-necked flask
Water 30-50 parts, in 70-80 DEG C of heating of oil bath pan, nitrogen protection, the speed for being passed through nitrogen is 1-2L/min, keeps charging flatly,
Insertion agitator flatly, mixing speed are 1000-2000 revs/min, reaction time 3-4h；
(2) first by borax 5-9 parts, triethanolamine 1-3 parts, ethanol 10-20 parts, with ultrasonic disperse 10-20 minutes, ultrasonic work(
Rate is 1200-1500W, obtains homogeneous solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 500-1000 revs/min, 20-30 points of stirring
Clock；
(4) temperature is reduced to 50-60 DEG C, adds sodium metasilicate 10-15 parts, DBSA 3-5 parts, magnesium chloride 5-10
Part, 500-1000 revs/min, stir 20-30 minutes；
(5) 40-50 DEG C is cooled to, diatomite 5-10 parts, sodium acid carbonate 10-15 parts is added, 500-1000 revs/min, stirs
Mix 1-2 hours；
(6) 20-30 DEG C is cooled to, closes down stirring, the liquid fabric softener prepared；
(7) stand and be cooled in three-necked flask liquid fabric softener and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 1
The invention discloses a kind of fabric softener, according to parts by weight, including following components：Natural 20 parts of cotton wax, lose
10 parts of water Span, 10 parts of sodium metasilicate, 5 parts of diatomite, 10 parts of sodium acid carbonate, 5 parts of borax, 1 part of triethanolamine, second
10 parts of alcohol, 3 parts of DBSA, 5 parts of magnesium chloride, 30 parts of deionized water.
Present invention also offers a kind of preparation method of fabric softener, comprise the following steps that：
(1) natural 20 parts of cotton wax, 10 parts of sorbitan fatty acid ester, deionized water 30 are added inside three-necked flask
Part, in 70 DEG C of heating of oil bath pan, nitrogen protection, the speed for being passed through nitrogen is 1L/min, keeps charging flatly, flatly insertion stirring
Device, mixing speed are 1000 revs/min, reaction time 3h；
(2) first by 5 parts of borax, 1 part of triethanolamine, 10 parts of ethanol, with ultrasonic disperse 10 minutes, ultrasonic power 1200W,
Obtain homogeneous solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 900 revs/min, stirred 20 minutes；
(4) temperature is reduced to 50 DEG C, 10 parts of sodium metasilicate of addition, 3 parts of DBSA, 5 parts of magnesium chloride, 900 revs/min
Clock, stir 20 minutes；
(5) 40 DEG C are cooled to, 5 parts of diatomite, 10 parts of sodium acid carbonate is added, 900 revs/min, stirs 1 hour；
(6) 20 DEG C are cooled to, closes down stirring, the liquid fabric softener prepared；
(7) stand and be cooled in three-necked flask liquid fabric softener and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 2
The invention discloses a kind of fabric softener, according to parts by weight, including following components：Natural 25 parts of cotton wax, lose
13 parts of water Span, 13 parts of sodium metasilicate, 8 parts of diatomite, 13 parts of sodium acid carbonate, 7 parts of borax, 2 parts of triethanolamine, second
15 parts of alcohol, 4 parts of DBSA, 8 parts of magnesium chloride, 40 parts of deionized water.
Present invention also offers a kind of preparation method of fabric softener, comprise the following steps that：
(1) natural 25 parts of cotton wax, 13 parts of sorbitan fatty acid ester, deionized water 40 are added inside three-necked flask
Part, in 75 DEG C of heating of oil bath pan, nitrogen protection, the speed for being passed through nitrogen is 1.5L/min, keeps charging flatly, and insertion flatly is stirred
Device is mixed, mixing speed is 1500 revs/min, reaction time 3.5h；
(2) first by 7 parts of borax, 2 parts of triethanolamine, 15 parts of ethanol, with ultrasonic disperse 15 minutes, ultrasonic power 1500W,
Obtain homogeneous solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 800 revs/min, stirred 25 minutes；
(4) temperature is reduced to 55 DEG C, 13 parts of sodium metasilicate of addition, 4 parts of DBSA, 8 parts of magnesium chloride, 900 revs/min
Clock, stir 25 minutes；
(5) 45 DEG C are cooled to, 8 parts of diatomite, 13 parts of sodium acid carbonate is added, 800 revs/min, stirs 1.5 hours；
(6) 25 DEG C are cooled to, closes down stirring, the liquid fabric softener prepared；
(7) stand and be cooled in three-necked flask liquid fabric softener and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 3
The invention discloses a kind of fabric softener, according to parts by weight, including following components：Natural 30 parts of cotton wax, lose
15 parts of water Span, 15 parts of sodium metasilicate, 10 parts of diatomite, 15 parts of sodium acid carbonate, 9 parts of borax, 3 parts of triethanolamine,
20 parts of ethanol, 5 parts of DBSA, 10 parts of magnesium chloride, 50 parts of deionized water.
Present invention also offers a kind of preparation method of fabric softener, comprise the following steps that：
(1) natural 30 parts of cotton wax, 15 parts of sorbitan fatty acid ester, deionized water 50 are added inside three-necked flask
Part, in 80 DEG C of heating of oil bath pan, nitrogen protection, the speed for being passed through nitrogen is 2L/min, keeps charging flatly, flatly insertion stirring
Device, mixing speed are 2000 revs/min, reaction time 4h；
(2) first by 8 parts of borax, 3 parts of triethanolamine, 20 parts of ethanol, with ultrasonic disperse 20 minutes, ultrasonic power 1500W,
Obtain homogeneous solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 1000 revs/min, stirred 30 minutes；
(4) temperature is reduced to 60 DEG C, 15 parts of sodium metasilicate of addition, 5 parts of DBSA, 10 parts of magnesium chloride, 1000 turns/
Minute, stir 30 minutes；
(5) 50 DEG C are cooled to, 10 parts of diatomite, 15 parts of sodium acid carbonate is added, 1000 revs/min, stirs 2 hours；
(6) 30 DEG C are cooled to, closes down stirring, the liquid fabric softener prepared；
(7) stand and be cooled in three-necked flask liquid fabric softener and be less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 4
The invention discloses a kind of fabric softener, according to parts by weight, including following components：Natural 30 parts of cotton wax, lose
15 parts of water Span, 10 parts of sodium metasilicate, 5 parts of diatomite, 15 parts of sodium acid carbonate, 9 parts of borax, 3 parts of triethanolamine, second
20 parts of alcohol, 3 parts of DBSA, 5 parts of magnesium chloride, 30 parts of deionized water.
Present invention also offers a kind of preparation method of fabric softener, comprise the following steps that：
(1) natural 30 parts of cotton wax, 15 parts of sorbitan fatty acid ester, deionized water 30 are added inside three-necked flask
Part, in 80 DEG C of heating of oil bath pan, nitrogen protection, the speed for being passed through nitrogen is 2L/min, keeps charging flatly, flatly insertion stirring
Device, mixing speed are 1000 revs/min, reaction time 4h；
(2) first by 9 parts of borax, 3 parts of triethanolamine, 20 parts of ethanol, with ultrasonic disperse 20 minutes, ultrasonic power 1200W,
Obtain homogeneous solution；
(3) homogeneous solution of step (2) is added in the solution of step (1), 1000 revs/min, stirred 20 minutes；
(4) temperature is reduced to 60 DEG C, 10 parts of sodium metasilicate of addition, 3 parts of DBSA, 5 parts of magnesium chloride, 800 revs/min
Clock, stir 20 minutes；
(5) 40 DEG C are cooled to, 5 parts of diatomite, 15 parts of sodium acid carbonate is added, 900 revs/min, stirs 2 hours；
(6) 30 DEG C are cooled to, closes down stirring, the liquid fabric softener prepared；
(7) stand and be cooled in three-necked flask liquid fabric softener and be less than 20 DEG C, blowing encapsulation, finished product.
Test case
The softening agent that embodiment 1,2,3,4 is respectively adopted in the fabric of four pieces of formed objects carries out soft treatment, test result
It is as follows：
| Embodiment | Stiffness | Creasy recovery angle | Shearing rigidity | Bending stiffness |
| Former cloth | 3.32 | 130 | 1.72 | 0.8522 |
| 1 | 1.42 | 180 | 1.38 | 0.4305 |
| 2 | 1.14 | 188 | 1.23 | 0.3834 |
| 3 | 1.02 | 198 | 1.11 | 0.3443 |
| 4 | 1.08 | 192 | 1.20 | 0.3663 |
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention includes appended claims and its equivalent limits.
Claims (6)
- A kind of 1. fabric softener, it is characterised in that：The fabric softener includes the raw material of following parts by weight：Natural cotton wax 20-30 parts, sorbitan fatty acid ester 10-15 parts, sodium metasilicate 10-15 parts, diatomite 5-10 parts, sodium acid carbonate 10-15 parts, Borax 5-9 parts, triethanolamine 1-3 parts, ethanol 10-20 parts, DBSA 3-5 parts, magnesium chloride 5-10 parts, deionized water 30-50 parts.
- 2. fabric softener according to claim 1, it is characterised in that：The ethanol is absolute ethyl alcohol, and purity is analysis It is pure.
- 3. fabric softener according to claim 1, it is characterised in that：According to parts by weight, including following components：Naturally 20 parts of cotton wax, 10 parts of sorbitan fatty acid ester, 10 parts of sodium metasilicate, 5 parts of diatomite, 10 parts of sodium acid carbonate, 5 parts of borax, three 1 part of monoethanolamine, 10 parts of ethanol, 3 parts of DBSA, 5 parts of magnesium chloride, 30 parts of deionized water.
- 4. fabric softener according to claim 1, it is characterised in that：According to parts by weight, including following components：Naturally 25 parts of cotton wax, 13 parts of sorbitan fatty acid ester, 13 parts of sodium metasilicate, 8 parts of diatomite, 13 parts of sodium acid carbonate, 7 parts of borax, three 2 parts of monoethanolamine, 15 parts of ethanol, 4 parts of DBSA, 8 parts of magnesium chloride, 40 parts of deionized water.
- 5. fabric softener according to claim 1, it is characterised in that：According to parts by weight, including following components：Naturally 30 parts of cotton wax, 15 parts of sorbitan fatty acid ester, 15 parts of sodium metasilicate, 10 parts of diatomite, 15 parts of sodium acid carbonate, 9 parts of borax, three 3 parts of monoethanolamine, 20 parts of ethanol, 5 parts of DBSA, 10 parts of magnesium chloride, 50 parts of deionized water.
- A kind of 6. preparation method of any described fabric softener in 1-5 using the claims, it is characterised in that：Specifically Step is as follows：Step 1, natural cotton wax 20-30 parts, sorbitan fatty acid ester 10-15 parts, deionization are added inside three-necked flask Water 30-50 parts, in 70-80 DEG C of heating of oil bath pan, nitrogen protection, the speed for being passed through nitrogen is 1-2L/min, keeps charging flatly, Insertion agitator flatly, mixing speed are 1000-2000 revs/min, reaction time 3-4h；Step 2, first by borax 5-9 parts, triethanolamine 1-3 parts, ethanol 10-20 parts, with ultrasonic disperse 10-20 minutes, ultrasonic work( Rate is 1200-1500W, obtains homogeneous solution；Step 3, the homogeneous solution of step 2 is added in the solution of step 1,500-1000 revs/min, stirs 20-30 minutes；Step 4, temperature is reduced to 50-60 DEG C, adds sodium metasilicate 10-15 parts, DBSA 3-5 parts, magnesium chloride 5-10 Part, 500-1000 revs/min, stir 20-30 minutes；Step 5,40-50 DEG C is cooled to, diatomite 5-10 parts, sodium acid carbonate 10-15 parts is added, 500-1000 revs/min, stirs 1-2 hours；Step 6,20-30 DEG C is cooled to, closes down stirring, the liquid fabric softener prepared；Step 7, stand and be cooled in three-necked flask liquid fabric softener and be less than 20 DEG C, blowing encapsulation, finished product.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108894033A (en) * | 2018-05-30 | 2018-11-27 | 李建强 | A kind of stealth knitted sportswear fabric |
| CN109602230A (en) * | 2018-12-15 | 2019-04-12 | 南通开发区翔华纺织品织造有限公司 | A kind of quilt and its production technology improving pliability |
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| CN102965923A (en) * | 2012-12-04 | 2013-03-13 | 海泰纺织（苏州）有限公司 | Flame-retardant finishing agent for textiles and preparation method of agent |
| CN103614908A (en) * | 2013-12-02 | 2014-03-05 | 湖州金塔地纺织厂 | Fabric softener |
| CN104264465A (en) * | 2014-09-26 | 2015-01-07 | 无锡市东北塘宏良染色厂 | Softening agent for treating clothes and preparation method thereof |
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| CN102619090A (en) * | 2011-01-27 | 2012-08-01 | 上海雅运纺织助剂有限公司 | Smoothening softener composition for cotton and its blended yarns, and preparation method thereof |
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Application publication date: 20180309 |