CN107760433A - A kind of water-base metal cutting fluid and preparation method thereof - Google Patents
A kind of water-base metal cutting fluid and preparation method thereof Download PDFInfo
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- CN107760433A CN107760433A CN201711269399.3A CN201711269399A CN107760433A CN 107760433 A CN107760433 A CN 107760433A CN 201711269399 A CN201711269399 A CN 201711269399A CN 107760433 A CN107760433 A CN 107760433A
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Abstract
The invention provides a kind of preparation method of water-base metal cutting fluid, according to the following steps：S1. 30 50 DEG C are heated water to, magnesium chromate, neopelex, dinonyl naphthalene sulfonate barium and sodium heavy alkyl benzene sulfonate is then sequentially added while stirring, is filtrated to get mixed solution A；S2. by dinonylnaphthalene disulfonic acid, maleic anhydride, 1,2 propylene carbonates, polyoxyethylated alkyl phenol, lauric acid amide of ethanol, fumaric acid, fatty alcohol-ether sodium sulfate, triethanolamine, magnesium chromate, 1,2 propane diols and ethanol mixing, ultrasonic shear, obtain mixed solution B；S3. mixed solution B is slowly added in mixed solution A, first the 20min of ultrasonic shear 10 in the case where power is 800 1000W, then the 10min of ultrasonic shear 5 under 200 500W, last solution adjust pH.This metal water-base cutting fluid excellent performance.
Description
Technical field
The present invention relates to cutting fluid, and in particular to a kind of water-base metal cutting fluid and preparation method thereof.
Background technology
Metal working fluid refers to be used for metal and its alloy is various processed in cutting, grinding, punching press, rolling and drawing etc.
Lubricant used in journey.Metal working fluid can be divided into metalworking fluid according to the characteristic used and metal forming liquid two is big
Class.Each kind is further divided into water base and oil type.Oil type cutting fluid is mainly prevented by mineral oil and oiliness improver, a small amount of oil-soluble
Become rusty the composition such as agent, extreme pressure agent, is characterized in greasy property and good antirust property, but easily produces mist of oil, easily catches fire.In recent years
Come, as low energy consumption, low cost, low nuisanceless require increasingly strict, metalworking fluid is just rapidly to water-base cutting fluid transition.Mesh
Preceding water-base cutting fluid has obtained swift and violent development.To reduce metal in process because of the loss that abrasion is brought, each production
Performance requirement more and more higher of the enterprise to metalworking fluid；Simultaneously as the attention of Environmental protection, it is proposed that cleaning life
The requirement such as production, energy-saving and emission-reduction, metalworking fluid is promoted to develop towards environmental protection, energy-conservation, efficient direction.
The content of the invention
Technical problems to be solved：It is an object of the invention to provide a kind of water-base metal cutting fluid, the cutting fluid are comprehensive
Energy is excellent, green, service life length, and production is simple and cost is low, can meet the needs of domestic market.
Technical scheme：A kind of water-base metal cutting fluid, it is formed by following parts by weight：Neopelex 3-10
Part, dinonyl naphthalene sulfonate barium 2-8 parts, sodium heavy alkyl benzene sulfonate 3-6 parts, dinonylnaphthalene disulfonic acid 1-6 parts, maleic anhydride 2-
7 parts, 1,2- propylene carbonate 5-10 parts, polyoxyethylated alkyl phenol 3-8 parts, lauric acid amide of ethanol 1-5 parts, rich horse
Sour 3-8 parts, fatty alcohol-ether sodium sulfate 4-10 parts, triethanolamine 3-10 parts, magnesium chromate 4-12 parts, 1,2- propane diols 10-15 parts, second
Alcohol 10-20 parts, water 20-40 parts.
Further, described a kind of water-base metal cutting fluid, formed by following parts by weight：Neopelex 5-
8 parts, dinonyl naphthalene sulfonate barium 4-6 parts, sodium heavy alkyl benzene sulfonate 4-6 parts, dinonylnaphthalene disulfonic acid 2-5 parts, maleic anhydride
3-6 parts, 1,2- propylene carbonate 6-9 parts, polyoxyethylated alkyl phenol 5-7 parts, lauric acid amide of ethanol 2-4 parts, rich horse
Sour 4-7 parts, fatty alcohol-ether sodium sulfate 6-8 parts, triethanolamine 6-9 parts, magnesium chromate 6-10 parts, 1,2- propane diols 11-14 parts, ethanol
13-17 parts, water 25-35 parts.
A kind of preparation method of water-base metal cutting fluid, according to the following steps：
S1. 30-50 DEG C is heated water to, then sequentially adds magnesium chromate, neopelex, dinonyl naphthalene while stirring
Barium sulfonate and sodium heavy alkyl benzene sulfonate, are filtrated to get mixed solution A；
S2. by dinonylnaphthalene disulfonic acid, maleic anhydride, 1,2- propylene carbonates, polyoxyethylated alkyl phenol, coconut oil
Diglycollic amide, fumaric acid, fatty alcohol-ether sodium sulfate, triethanolamine, magnesium chromate, 1,2-PD and ethanol mixing, ultrasonic wave
30-60min is sheared, shearing power 500-1500W, obtains mixed solution B；
S3. mixed solution B is slowly added in mixed solution A, first the ultrasonic shear 10- in the case where power is 800-1000W
20min, then the ultrasonic shear 5-10min under 200-500W, last solution adjust pH to 7-9.
Further, the preparation method of described a kind of water-base metal cutting fluid, the step（2）Middle ultrasonic shear
Time is 40-50min, shearing power 800-1200W.
Further, the preparation method of described a kind of water-base metal cutting fluid, the step（3）Middle elder generation is in power
Ultrasonic shear 12-16min under 850-950W, then the ultrasonic shear 8min under 300-400W.
Beneficial effect：The present invention cutting formula of liquid it is simple, easily prepare, without natrium nitrosum, chlorine and other to human body
The material being harmful to environmental toxic, it is easy to workpieces processing and keeps the cleaning of processing environment.The cutting fluid excellent combination property,
And production cost is very low, there are wide market prospects.
Embodiment
Embodiment 1
A kind of water-base metal cutting fluid, it is formed by following parts by weight：3 parts of neopelex, dinonyl naphthalene sulfonate barium 8
Part, 3 parts of sodium heavy alkyl benzene sulfonate, 6 parts of dinonylnaphthalene disulfonic acid, 2 parts of maleic anhydride, 10 parts of 1,2- propylene carbonates,
3 parts of polyoxyethylated alkyl phenol, 5 parts of lauric acid amide of ethanol, 3 parts of fumaric acid, 10 parts of fatty alcohol-ether sodium sulfate, triethanolamine
3 parts, 12 parts of magnesium chromate, 10 parts of 1,2- propane diols, 20 parts of ethanol, 20 parts of water；
Its preparation method, according to the following steps：
S1. 30 DEG C are heated water to, then sequentially adds magnesium chromate, neopelex, dinonyl naphthalene sulphur while stirring
Sour barium and sodium heavy alkyl benzene sulfonate, are filtrated to get mixed solution A；
S2. by dinonylnaphthalene disulfonic acid, maleic anhydride, 1,2- propylene carbonates, polyoxyethylated alkyl phenol, coconut oil
Diglycollic amide, fumaric acid, fatty alcohol-ether sodium sulfate, triethanolamine, magnesium chromate, 1,2-PD and ethanol mixing, ultrasonic wave
30min is sheared, shearing power 1500W, obtains mixed solution B；
S3. mixed solution B is slowly added in mixed solution A, first ultrasonic shear 20min, Ran Hou in the case where power is 800W
Ultrasonic shear 5min under 200W, last solution adjust pH to 7.
Embodiment 2
A kind of water-base metal cutting fluid, it is formed by following parts by weight：10 parts of neopelex, dinonyl naphthalene sulfonate barium
2 parts, 6 parts of sodium heavy alkyl benzene sulfonate, 1 part of dinonylnaphthalene disulfonic acid, 7 parts of maleic anhydride, 5 parts of 1,2- propylene carbonates,
8 parts of polyoxyethylated alkyl phenol, 1 part of lauric acid amide of ethanol, 8 parts of fumaric acid, 4 parts of fatty alcohol-ether sodium sulfate, triethanolamine
10 parts, 4 parts of magnesium chromate, 15 parts of 1,2- propane diols, 10 parts of ethanol, 40 parts of water；
Its preparation method, according to the following steps：
S1. 50 DEG C are heated water to, then sequentially adds magnesium chromate, neopelex, dinonyl naphthalene sulphur while stirring
Sour barium and sodium heavy alkyl benzene sulfonate, are filtrated to get mixed solution A；
S2. by dinonylnaphthalene disulfonic acid, maleic anhydride, 1,2- propylene carbonates, polyoxyethylated alkyl phenol, coconut oil
Diglycollic amide, fumaric acid, fatty alcohol-ether sodium sulfate, triethanolamine, magnesium chromate, 1,2-PD and ethanol mixing, ultrasonic wave
60min is sheared, shearing power 500W, obtains mixed solution B；
S3. mixed solution B is slowly added in mixed solution A, first ultrasonic shear 10min, Ran Hou in the case where power is 1000W
Ultrasonic shear 10min under 500W, last solution adjust pH to 9.
Embodiment 3
A kind of water-base metal cutting fluid, it is formed by following parts by weight：5 parts of neopelex, dinonyl naphthalene sulfonate barium 6
Part, 4 parts of sodium heavy alkyl benzene sulfonate, 5 parts of dinonylnaphthalene disulfonic acid, 3 parts of maleic anhydride, 9 parts of 1,2- propylene carbonates, gather
5 parts of oxygen vinyl alkyl phenolic ether, 4 parts of lauric acid amide of ethanol, 4 parts of fumaric acid, 8 parts of fatty alcohol-ether sodium sulfate, triethanolamine 6
Part, 10 parts of magnesium chromate, 11 parts of 1,2- propane diols, 17 parts of ethanol, 25 parts of water；
Its preparation method, according to the following steps：
S1. 35 DEG C are heated water to, then sequentially adds magnesium chromate, neopelex, dinonyl naphthalene sulphur while stirring
Sour barium and sodium heavy alkyl benzene sulfonate, are filtrated to get mixed solution A；
S2. by dinonylnaphthalene disulfonic acid, maleic anhydride, 1,2- propylene carbonates, polyoxyethylated alkyl phenol, coconut oil
Diglycollic amide, fumaric acid, fatty alcohol-ether sodium sulfate, triethanolamine, magnesium chromate, 1,2-PD and ethanol mixing, ultrasonic wave
40min is sheared, shearing power 1200W, obtains mixed solution B；
S3. mixed solution B is slowly added in mixed solution A, first ultrasonic shear 12min, Ran Hou in the case where power is 850W
Ultrasonic shear 8min under 400W, last solution adjust pH to 7.
Embodiment 4
A kind of water-base metal cutting fluid, it is formed by following parts by weight：8 parts of neopelex, dinonyl naphthalene sulfonate barium 4
Part, 6 parts of sodium heavy alkyl benzene sulfonate, 2 parts of dinonylnaphthalene disulfonic acid, 6 parts of maleic anhydride, 6 parts of 1,2- propylene carbonates, gather
7 parts of oxygen vinyl alkyl phenolic ether, 2 parts of lauric acid amide of ethanol, 7 parts of fumaric acid, 6 parts of fatty alcohol-ether sodium sulfate, triethanolamine 9
Part, 6 parts of magnesium chromate, 14 parts of 1,2- propane diols, 13 parts of ethanol, 35 parts of water；
Its preparation method, according to the following steps：
S1. 45 DEG C are heated water to, then sequentially adds magnesium chromate, neopelex, dinonyl naphthalene sulphur while stirring
Sour barium and sodium heavy alkyl benzene sulfonate, are filtrated to get mixed solution A；
S2. by dinonylnaphthalene disulfonic acid, maleic anhydride, 1,2- propylene carbonates, polyoxyethylated alkyl phenol, coconut oil
Diglycollic amide, fumaric acid, fatty alcohol-ether sodium sulfate, triethanolamine, magnesium chromate, 1,2-PD and ethanol mixing, ultrasonic wave
50min is sheared, shearing power 800W, obtains mixed solution B；
S3. mixed solution B is slowly added in mixed solution A, first ultrasonic shear 16min, Ran Hou in the case where power is 950W
Ultrasonic shear 8min under 300W, last solution adjust pH to 8.
Embodiment 5
A kind of water-base metal cutting fluid, it is formed by following parts by weight：7 parts of neopelex, dinonyl naphthalene sulfonate barium 5
Part, 5 parts of sodium heavy alkyl benzene sulfonate, 4 parts of dinonylnaphthalene disulfonic acid, 5 parts of maleic anhydride, 8 parts of 1,2- propylene carbonates, gather
6 parts of oxygen vinyl alkyl phenolic ether, 3 parts of lauric acid amide of ethanol, 6 parts of fumaric acid, 7 parts of fatty alcohol-ether sodium sulfate, triethanolamine 7
Part, 8 parts of magnesium chromate, 12 parts of 1,2- propane diols, 15 parts of ethanol, 30 parts of water；
Its preparation method, according to the following steps：
S1. 40 DEG C are heated water to, then sequentially adds magnesium chromate, neopelex, dinonyl naphthalene sulphur while stirring
Sour barium and sodium heavy alkyl benzene sulfonate, are filtrated to get mixed solution A；
S2. by dinonylnaphthalene disulfonic acid, maleic anhydride, 1,2- propylene carbonates, polyoxyethylated alkyl phenol, coconut oil
Diglycollic amide, fumaric acid, fatty alcohol-ether sodium sulfate, triethanolamine, magnesium chromate, 1,2-PD and ethanol mixing, ultrasonic wave
45min is sheared, shearing power 1000W, obtains mixed solution B；
S3. mixed solution B is slowly added in mixed solution A, first ultrasonic shear 14min, Ran Hou in the case where power is 900W
Ultrasonic shear 8min under 360W, last solution adjust pH to 8.
Comparative example 1
A kind of water-base metal cutting fluid, it is formed by following parts by weight：3 parts of neopelex, dinonyl naphthalene sulfonate barium 8
Part, 3 parts of sodium heavy alkyl benzene sulfonate, 10 parts of 1,2- propylene carbonates, 3 parts of polyoxyethylated alkyl phenol, coconut oil diethanol acyl
5 parts of amine, 3 parts of fumaric acid, 10 parts of fatty alcohol-ether sodium sulfate, 3 parts of triethanolamine, 12 parts of magnesium chromate, 10 parts of 1,2- propane diols, ethanol
20 parts, 20 parts of water；
Its preparation method, according to the following steps：
S1. 30 DEG C are heated water to, then sequentially adds magnesium chromate, neopelex, dinonyl naphthalene sulphur while stirring
Sour barium and sodium heavy alkyl benzene sulfonate, are filtrated to get mixed solution A；
S2. by 1,2- propylene carbonates, polyoxyethylated alkyl phenol, lauric acid amide of ethanol, fumaric acid, fatty alcohol ether sulphur
Sour sodium, triethanolamine, magnesium chromate, 1,2-PD and ethanol mixing, ultrasonic shear 30min, shearing power 1500W, are obtained
To mixed solution B；
S3. mixed solution B is slowly added in mixed solution A, first ultrasonic shear 20min, Ran Hou in the case where power is 800W
Ultrasonic shear 5min under 200W, last solution adjust pH to 7.
Comparative example 2
A kind of water-base metal cutting fluid, it is formed by following parts by weight：10 parts of neopelex, dinonyl naphthalene sulfonate barium
2 parts, 6 parts of sodium heavy alkyl benzene sulfonate, 1 part of dinonylnaphthalene disulfonic acid, 7 parts of maleic anhydride, 8 parts of polyoxyethylated alkyl phenol,
8 parts of fumaric acid, 4 parts of fatty alcohol-ether sodium sulfate, 10 parts of triethanolamine, 4 parts of magnesium chromate, 15 parts of 1,2- propane diols, 10 parts of ethanol, water
40 parts；
Its preparation method, according to the following steps：
S1. 50 DEG C are heated water to, then sequentially adds magnesium chromate, neopelex, dinonyl naphthalene sulphur while stirring
Sour barium and sodium heavy alkyl benzene sulfonate, are filtrated to get mixed solution A；
S2. by dinonylnaphthalene disulfonic acid, maleic anhydride, polyoxyethylated alkyl phenol, fumaric acid, fatty alcohol-ether sodium sulfate,
Triethanolamine, magnesium chromate, 1,2-PD and ethanol mixing, ultrasonic shear 60min, shearing power 500W, are mixed
Solution B；
S3. mixed solution B is slowly added in mixed solution A, first ultrasonic shear 10min, Ran Hou in the case where power is 1000W
Ultrasonic shear 10min under 500W, last solution adjust pH to 9.
The property indices of this water-base cutting fluid are tested according to standard GB/T 6144-2010, as can be seen from Table 1
The water-base metal cutting fluid of the present invention has excellent antiseptic property and rustless property.
The properties of the water-base metal cutting fluid of the present invention of table 1
Claims (5)
1. a kind of water-base metal cutting fluid, it is characterised in that formed by following parts by weight：Neopelex 3-10 parts
（Table is lived）, dinonyl naphthalene sulfonate barium 2-8 parts, sodium heavy alkyl benzene sulfonate 3-6 parts（Cut composition）, dinonylnaphthalene disulfonic acid 1-6 parts
（Table is lived）, maleic anhydride 2-7 parts, 1,2- propylene carbonate 5-10 parts, polyoxyethylated alkyl phenol 3-8 parts, coconut oil
Diglycollic amide 1-5 parts, fumaric acid 3-8 parts, fatty alcohol-ether sodium sulfate 4-10 parts, triethanolamine 3-10 parts, magnesium chromate 4-12 parts,
1,2- propane diols 10-15 parts, ethanol 10-20 parts, water 20-40 parts.
2. a kind of water-base metal cutting fluid according to claim 1, it is characterised in that formed by following parts by weight：12
Sodium alkyl benzene sulfonate 5-8 parts, dinonyl naphthalene sulfonate barium 4-6 parts, sodium heavy alkyl benzene sulfonate 4-6 parts, dinonylnaphthalene disulfonic acid 2-5
Part, maleic anhydride 3-6 parts, 1,2- propylene carbonate 6-9 parts, polyoxyethylated alkyl phenol 5-7 parts, coconut oil diethanol
Acid amides 2-4 parts, fumaric acid 4-7 parts, fatty alcohol-ether sodium sulfate 6-8 parts, triethanolamine 6-9 parts, magnesium chromate 6-10 parts, 1,2- the third two
Alcohol 11-14 parts, ethanol 13-17 parts, water 25-35 parts.
3. a kind of preparation method of water-base metal cutting fluid, it is characterised in that according to the following steps：
S1. 30-50 DEG C is heated water to, then sequentially adds magnesium chromate, neopelex, dinonyl naphthalene while stirring
Barium sulfonate and sodium heavy alkyl benzene sulfonate, are filtrated to get mixed solution A；
S2. by dinonylnaphthalene disulfonic acid, maleic anhydride, 1,2- propylene carbonates, polyoxyethylated alkyl phenol, coconut oil
Diglycollic amide, fumaric acid, fatty alcohol-ether sodium sulfate, triethanolamine, magnesium chromate, 1,2-PD and ethanol mixing, ultrasonic wave
30-60min is sheared, shearing power 500-1500W, obtains mixed solution B；
S3. mixed solution B is slowly added in mixed solution A, first the ultrasonic shear 10- in the case where power is 800-1000W
20min, then the ultrasonic shear 5-10min under 200-500W, last solution adjust pH to 7-9.
A kind of 4. preparation method of water-base metal cutting fluid according to claim 3, it is characterised in that：The step（2）
The time of middle ultrasonic shear is 40-50min, shearing power 800-1200W.
A kind of 5. preparation method of water-base metal cutting fluid according to claim 3, it is characterised in that：The step（3）
Middle elder generation is ultrasonic shear 12-16min under 850-950W in power, then the ultrasonic shear 8min under 300-400W.
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Citations (7)
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| US4880552A (en) * | 1987-04-24 | 1989-11-14 | Societe Nationale Elf Aquitaine (Production) | Water-soluble additives having extreme pressure effect for aqueous functional fluids, functional fluids and concentrated aqueous compositions containing the additives |
| CN102433210A (en) * | 2011-10-27 | 2012-05-02 | 姜堰市华润化工厂 | Water-based working liquid for electrical discharge wire cutting and preparation method thereof |
| CN103242946A (en) * | 2013-05-06 | 2013-08-14 | 长沙好的机电科技有限公司 | Formula and preparation technology of machine tool working solution |
| CN104087406A (en) * | 2014-07-26 | 2014-10-08 | 梁胜光 | Cooling liquid for cutting solar silicon wafer through diamond wire |
| CN104611118A (en) * | 2013-11-01 | 2015-05-13 | 沈阳工业大学 | Aluminum and aluminum alloy water-based cutting fluid |
| CN105567399A (en) * | 2016-01-18 | 2016-05-11 | 清华大学 | Water-based titanium alloy processing liquid and application thereof |
| CN106244295A (en) * | 2016-07-13 | 2016-12-21 | 天长市润达金属防锈助剂有限公司 | A kind of extreme boundary lubrication metalworking fluid |
-
2017
- 2017-12-05 CN CN201711269399.3A patent/CN107760433A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4880552A (en) * | 1987-04-24 | 1989-11-14 | Societe Nationale Elf Aquitaine (Production) | Water-soluble additives having extreme pressure effect for aqueous functional fluids, functional fluids and concentrated aqueous compositions containing the additives |
| CN102433210A (en) * | 2011-10-27 | 2012-05-02 | 姜堰市华润化工厂 | Water-based working liquid for electrical discharge wire cutting and preparation method thereof |
| CN103242946A (en) * | 2013-05-06 | 2013-08-14 | 长沙好的机电科技有限公司 | Formula and preparation technology of machine tool working solution |
| CN104611118A (en) * | 2013-11-01 | 2015-05-13 | 沈阳工业大学 | Aluminum and aluminum alloy water-based cutting fluid |
| CN104087406A (en) * | 2014-07-26 | 2014-10-08 | 梁胜光 | Cooling liquid for cutting solar silicon wafer through diamond wire |
| CN105567399A (en) * | 2016-01-18 | 2016-05-11 | 清华大学 | Water-based titanium alloy processing liquid and application thereof |
| CN106244295A (en) * | 2016-07-13 | 2016-12-21 | 天长市润达金属防锈助剂有限公司 | A kind of extreme boundary lubrication metalworking fluid |
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Application publication date: 20180306 |