CN107746335A - A kind of production method of the organic foliage fertilizer based on the antibacterial insecticidal action of Chinese medicine - Google Patents

A kind of production method of the organic foliage fertilizer based on the antibacterial insecticidal action of Chinese medicine Download PDF

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Publication number
CN107746335A
CN107746335A CN201711170202.0A CN201711170202A CN107746335A CN 107746335 A CN107746335 A CN 107746335A CN 201711170202 A CN201711170202 A CN 201711170202A CN 107746335 A CN107746335 A CN 107746335A
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chinese medicine
concentrate
humic acid
foliage fertilizer
temperature
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解安庆
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Suzhou Fengyuan Biotechnology Co Ltd
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Suzhou Fengyuan Biotechnology Co Ltd
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Priority to CN201711170202.0A priority Critical patent/CN107746335A/en
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Health & Medical Sciences (AREA)
  • Soil Sciences (AREA)
  • Plant Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Molecular Biology (AREA)
  • Fertilizers (AREA)

Abstract

A kind of organic foliage fertilizer based on the antibacterial insecticidal action of Chinese medicine, it is characterised in that first using rhizoma atractylodis, the tuber of stemona, kuh-seng, the achene of Siberian cocklebur, cloves, Heterostemonous Biebersteinia as raw material, concentrate of the extraction with antimicrobial and insecticidal activity;Then it is furfural dregs are decomposed, using alkali lye extracted humic acid, obtain humic acid extract solution;Finally using humic acid extract solution as chelating agent, a great number of elements and trace element built needed for concentrate, crop with antimicrobial and insecticidal activity, a kind of organic foliage fertilizer based on the antibacterial insecticidal action of Chinese medicine is obtained.The organic foliage fertilizer of the present invention, with the addition of the Chinese medicine concentrate with antimicrobial and insecticidal activity, while making it have fertilizer function, also with insecticidal function, substantially reduce the disease of crops, scientific formulation, nutrition is comprehensive, promote crop growth, increasing both production and income, improving quality.

Description

A kind of production method of the organic foliage fertilizer based on the antibacterial insecticidal action of Chinese medicine
Technical field
The invention belongs to fertilizer field, and in particular to a kind of organic foliage fertilizer based on the antibacterial insecticidal action of Chinese medicine Production method.
Background technology
Foliage dressing is the important supplement of soil application technology.The traditional approach of soil root fertilizer has been broken in foliage dressing, Can be described as most flexibly, most easily fertilization mode.But in recent years, most foliar fertilizer effective contents of domestic production are low, battalion Foster effect is single, element utilization rate is not high, effect is not sufficiently stable.Foliar fertilizer is not high in technological content high, to be finally embodied in whether It can make in peasant's increasing both production and income, this requires that foliar fertilizer provides more nutritional ingredient as far as possible, to there is higher multielement micro-fertilizer, foot The hard water resistance humic acid of Available Amino Acids and high activity enough measured, will also there is appropriate nitrogen, phosphorus, potassium certainly, but so more Composition compounding also want together it is soluble in water without go out precipitation, it goes without saying that be need it is high-tech.Therefore, concentration is developed The composite multifunction type foliar fertilizer high, nutrition is complete, utilization rate is high is extremely urgent.
The content of the invention
It is an object of the invention to provide a kind of organic foliar fertilizer of nutrition comprehensively based on the antibacterial insecticidal action of Chinese medicine The production method of material.
To achieve these goals, the present invention adopts the following technical scheme that:
A kind of organic foliage fertilizer based on the antibacterial insecticidal action of Chinese medicine, it is characterised in that first with rhizoma atractylodis, the tuber of stemona, kuh-seng, The achene of Siberian cocklebur, cloves, Heterostemonous Biebersteinia are raw material, concentrate of the extraction with antimicrobial and insecticidal activity;Then it is furfural dregs are decomposed, using alkali Liquid extracted humic acid, obtain humic acid extract solution;Finally using humic acid extract solution as chelating agent, there is the dense of antimicrobial and insecticidal activity A great number of elements and trace element built needed for contracting liquid, crop, obtain a kind of organic leaf based on the antibacterial insecticidal action of Chinese medicine Leaven material.
The described organic foliage fertilizer based on the antibacterial insecticidal action of Chinese medicine, it is characterised in that it is by following steps system It is standby to form:
(1)By rhizoma atractylodis, the tuber of stemona, kuh-seng, the achene of Siberian cocklebur, cloves, Heterostemonous Biebersteinia with 1:0.95-1.05:0.95-1.05:0.45-0.55: 0.45-0.55:0.24-0.26 mass ratio mixing, attrition grinding crosses 60-80 mesh sieves, every time using the 95% of 3-4 times of parts by weight Ethanol solution be heated to flowing back, extract 2-3 times, extract 1-2h every time, merging filtrate, abandon residue, flung to Rotary Evaporators Ethanol and concentrate, obtain concentrate;
(2)Furfural dregs are crossed to the sieve in 5mm apertures, add HM microbial inoculums, after being mixed evenly, regulation humidity is 45-55%, is piled Taper heap body, 1 temperature is respectively surveyed early, middle and late, the turning 1 time when mean temperature reaches 50 DEG C, heap body temperature is controlled by turning Degree is no more than 70 DEG C, no longer rises in heap temperature, you can stops turning, obtains the furfural dregs of fermentation maturity;Weighed using 6-8 times The potassium hydroxide solution of amount part 10% is heated to 75-85 DEG C, extracts the furfural dregs of fermentation maturity, extracts 5-6h, centrifuges, abandons Residue, obtain humic acid extract solution;
(3)Humic acid extract solution is added into reactor, agitator is opened, then opens vavuum pump, be 0.07- in vacuum 0.08MPa, temperature are 80-90 DEG C, and stirring is concentrated by evaporation 40-60min, stop being evaporated under reduced pressure;Sequentially add calcirm-fluoride, sulfuric acid Magnesium, manganese sulfate, zinc sulfate, copper sulphate, ferrous sulfate, boric acid and ammonium molybdate, continue anti-in 80-90 DEG C of temperature constant magnetic stirring chelating Answer 30-40min;
(4)By step(3)Product be cooled to 50-60 DEG C, sequentially add urea, potassium dihydrogen phosphate, potassium nitrate, Arabic gum and Concentrate, continue in 50-60 DEG C of temperature constant magnetic stirring chelatropic reaction 30-40min, reduce temperature to room temperature, obtain being based on Chinese medicine The organic foliage fertilizer of the antibacterial insecticidal action of material.
The preparation method of the described organic foliage fertilizer based on the antibacterial insecticidal action of Chinese medicine, it is characterised in that step (3)Middle humic acid extract solution, calcirm-fluoride, magnesium sulfate, manganese sulfate, zinc sulfate, copper sulphate, ferrous sulfate, boric acid and ammonium molybdate Mass ratio is 1:0.04-0.05:0.03-0.04:0.02-0.03:0.02-0.03:0.02-0.03:0.03-0.04:0.02- 0.03:0.01-0.02.
The preparation method of the described organic foliage fertilizer based on the antibacterial insecticidal action of Chinese medicine, it is characterised in that step (4)Middle step(3)Product, urea, potassium dihydrogen phosphate, potassium nitrate, the mass ratio of Arabic gum and concentrate be 1:0.15- 0.2:0.12-0.15:0.1-0.12:0.05-0.06:0.05-0.06.
Using above-mentioned technical scheme, beneficial effects of the present invention are:
The present invention with the traditional Chinese medicinal material raw materials such as rhizoma atractylodis, the tuber of stemona, kuh-seng, the achene of Siberian cocklebur, cloves, Heterostemonous Biebersteinia, extraction there is antibacterial desinsection to live The Chinese medicine concentrate of property, adds it in organic liquid fertilizer material, meets crop cycle by foliage-spray to reach To the demand of nutrient, while the generation of pest and disease damage also can be effectively prevented to a certain extent;Before utilization rate of fertilizer is improved Putting and can reduces the use of chemical industry agricultural chemicals, reach apply fertilizers scientifically, science prevents the generation of pest and disease damage, reduce the dirt to environment Dye, improve crop yield and improving quality.The present invention is decomposed by furfural dregs, using alkali lye extracted humic acid, obtains humic acid and carries Take liquid;Furfural dregs are to be produced using the leftover bits and pieces of the agricultural byproducts such as corncob, cornstalk, straw and Wheat Straw as raw material to produce chemical industry The solid waste remained after product furfural;Undergo microbial fermentation technology, and the cellulose macromolecule in furfural dregs is degradable to be small Molecular organic material such as humic acid etc..It is small for molecular weight the advantages of the humic acid compared with the humic acid extracted in weathered coal, more Be advantageous to plant absorption, it is safer to soil and plant without heavy metal.The present invention using humic acid extract solution as chelating agent, And Arabic gum is added to its synergy, the certain viscosity of foliar fertilizer is on the one hand imparted, increase foliar fertilizer is on blade face Adhesive force, anti-rain drop erosion are lost in, and on the other hand, improve the antagonism between nutrient, improve the stabilization of foliar fertilizer Property.The organic foliage fertilizer of the present invention, with the addition of the Chinese medicine concentrate with antimicrobial and insecticidal activity, makes it have fertilizer function While, also with insecticidal function, the disease of crops is substantially reduced, scientific formulation, nutrition is comprehensive, promotes plant growth hair Educate, increasing both production and income, improving quality.
Embodiment
The organic foliage fertilizer based on the antibacterial insecticidal action of Chinese medicine of the present embodiment, it is prepared by following steps:
(1)By rhizoma atractylodis, the tuber of stemona, kuh-seng, the achene of Siberian cocklebur, cloves, Heterostemonous Biebersteinia with 1:1:1:0.5:0.5:0.25 mass ratio mixing, powder Breakdown mill crosses 60 mesh sieves, is heated to flowing back using 95% ethanol solution of 4 times of parts by weight every time, extracts 3 times, extracts 2h every time, Merging filtrate, residue is abandoned, fling to ethanol with Rotary Evaporators and concentrate, obtain concentrate;
(2)Furfural dregs are crossed to the sieve in 5mm apertures, add HM microbial inoculums, after being mixed evenly, regulation humidity is 55%, is cocked Heap body, 1 temperature is respectively surveyed early, middle and late, the turning 1 time when mean temperature reaches 50 DEG C, heap temperature is controlled not by turning More than 70 DEG C, no longer rise in heap temperature, you can stop turning, obtain the furfural dregs of fermentation maturity;Using 8 times of parts by weight 10% potassium hydroxide solution is heated to 85 DEG C, extracts the furfural dregs of fermentation maturity, extracts 6h, centrifuges, abandons residue, obtain Humic acid extract solution;
(3)Humic acid extract solution is added into reactor, agitator is opened, then opens vavuum pump, be in vacuum 0.08MPa, temperature are 85 DEG C, and stirring is concentrated by evaporation 40min, stop being evaporated under reduced pressure;Sequentially add calcirm-fluoride, magnesium sulfate, sulfuric acid Manganese, zinc sulfate, copper sulphate, ferrous sulfate, boric acid and ammonium molybdate, continue in 85 DEG C of temperature constant magnetic stirring chelatropic reaction 40min;
(4)By step(3)Product be cooled to 60 DEG C, sequentially add urea, potassium dihydrogen phosphate, potassium nitrate, Arabic gum and dense Contracting liquid, continue in 60 DEG C of temperature constant magnetic stirring chelatropic reaction 40min, reduce temperature to room temperature, obtain killing based on Chinese medicine is antibacterial The organic foliage fertilizer of worm effect.
The step of the present embodiment(3)Middle humic acid extract solution, calcirm-fluoride, magnesium sulfate, manganese sulfate, zinc sulfate, copper sulphate, sulphur The mass ratio of sour ferrous, boric acid and ammonium molybdate is 1:0.05:0.04:0.03:0.03:0.02:0.03:0.02:0.01.
The step of the present embodiment(4)Middle step(3)Product, urea, potassium dihydrogen phosphate, potassium nitrate, Arabic gum and dense The mass ratio of contracting liquid is 1:0.2:0.15:0.12:0.06:0.05.

Claims (4)

1. a kind of organic foliage fertilizer based on the antibacterial insecticidal action of Chinese medicine, it is characterised in that first with rhizoma atractylodis, the tuber of stemona, hardship Ginseng, the achene of Siberian cocklebur, cloves, Heterostemonous Biebersteinia are raw material, concentrate of the extraction with antimicrobial and insecticidal activity;Then it is furfural dregs are decomposed, adopt With alkali lye extracted humic acid, humic acid extract solution is obtained;Finally using humic acid extract solution as chelating agent, there is antimicrobial and insecticidal activity Concentrate, a great number of elements and trace element built needed for crop, obtain a kind of having based on the antibacterial insecticidal action of Chinese medicine Machine foliar fertilizer.
2. the organic foliage fertilizer based on the antibacterial insecticidal action of Chinese medicine according to claims 1, it is characterised in that its It is prepared by following steps:
(1)By rhizoma atractylodis, the tuber of stemona, kuh-seng, the achene of Siberian cocklebur, cloves, Heterostemonous Biebersteinia with 1:0.95-1.05:0.95-1.05:0.45-0.55: 0.45-0.55:0.24-0.26 mass ratio mixing, attrition grinding crosses 60-80 mesh sieves, every time using the 95% of 3-4 times of parts by weight Ethanol solution be heated to flowing back, extract 2-3 times, extract 1-2h every time, merging filtrate, abandon residue, flung to Rotary Evaporators Ethanol and concentrate, obtain concentrate
(2)Furfural dregs are crossed to the sieve in 5mm apertures, add HM microbial inoculums, after being mixed evenly, regulation humidity is 45-55%, is piled Taper heap body, 1 temperature is respectively surveyed early, middle and late, the turning 1 time when mean temperature reaches 50 DEG C, heap body temperature is controlled by turning Degree is no more than 70 DEG C, no longer rises in heap temperature, you can stops turning, obtains the furfural dregs of fermentation maturity;Weighed using 6-8 times The potassium hydroxide solution of amount part 10% is heated to 75-85 DEG C, extracts the furfural dregs of fermentation maturity, extracts 5-6h, centrifuges, abandons Residue, obtain humic acid extract solution;
(3)Humic acid extract solution is added into reactor, agitator is opened, then opens vavuum pump, be 0.07- in vacuum 0.08MPa, temperature are 80-90 DEG C, and stirring is concentrated by evaporation 40-60min, stop being evaporated under reduced pressure;Sequentially add calcirm-fluoride, sulfuric acid Magnesium, manganese sulfate, zinc sulfate, copper sulphate, ferrous sulfate, boric acid and ammonium molybdate, continue anti-in 80-90 DEG C of temperature constant magnetic stirring chelating Answer 30-40min;
(4)By step(3)Product be cooled to 50-60 DEG C, sequentially add urea, potassium dihydrogen phosphate, potassium nitrate, Arabic gum and Concentrate, continue in 50-60 DEG C of temperature constant magnetic stirring chelatropic reaction 30-40min, reduce temperature to room temperature, obtain being based on Chinese medicine The organic foliage fertilizer of the antibacterial insecticidal action of material.
3. the preparation method of the organic foliage fertilizer based on the antibacterial insecticidal action of Chinese medicine according to claims 2, its It is characterised by, step(3)Middle humic acid extract solution, calcirm-fluoride, magnesium sulfate, manganese sulfate, zinc sulfate, copper sulphate, ferrous sulfate, boron The mass ratio of acid and ammonium molybdate is 1:0.04-0.05:0.03-0.04:0.02-0.03:0.02-0.03:0.02-0.03:0.03- 0.04:0.02-0.03:0.01-0.02.
4. the preparation method of the organic foliage fertilizer based on the antibacterial insecticidal action of Chinese medicine according to claims 2, its It is characterised by, step(4)Middle step(3)Product, urea, potassium dihydrogen phosphate, potassium nitrate, the quality of Arabic gum and concentrate Than for 1:0.15-0.2:0.12-0.15:0.1-0.12:0.05-0.06:0.05-0.06.
CN201711170202.0A 2017-11-22 2017-11-22 A kind of production method of the organic foliage fertilizer based on the antibacterial insecticidal action of Chinese medicine Pending CN107746335A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108503476A (en) * 2018-06-21 2018-09-07 蚌埠天河花卉市场开发有限公司 A kind of liquid organic fertilizer and preparation method thereof
CN109265219A (en) * 2018-11-13 2019-01-25 广东新维生物科技股份有限公司 A kind of lignin fertilizer and preparation method of chelated microelement

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN85103993A (en) * 1984-05-07 1986-11-19 舍林股份公司 Selectively long-term application is in the fertilizer of leaf
CN1289743A (en) * 2000-11-17 2001-04-04 解俊峰 Composite organic liquid fertilizer
CN101148375A (en) * 2006-09-22 2008-03-26 李树春 Nano medical stone highly effective foliage fertilizer
CN102040408A (en) * 2010-06-25 2011-05-04 厦门三和利生物技术有限公司 Foliar fertilizer
CN104478574A (en) * 2014-12-01 2015-04-01 宁夏共享生物化工有限公司 Method for preparing fertilizer containing humic acid concentrated chelating trace elements
CN104529624A (en) * 2014-12-12 2015-04-22 重庆惠民生物工程有限公司 Plant-source traditional Chinese medicinal herbal biological leaf fertilizer and preparation method thereof
CN105130702A (en) * 2015-08-18 2015-12-09 宁夏共享生物化工有限公司 Method used for preparing solid composite chelated water-soluble fertilizer containing humic acid from furfural residue
CN106490017A (en) * 2016-10-23 2017-03-15 张颂忠 A kind of foliage fertilizer plant pesticide of preventing and treating tetranychus viennensis

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN85103993A (en) * 1984-05-07 1986-11-19 舍林股份公司 Selectively long-term application is in the fertilizer of leaf
CN1289743A (en) * 2000-11-17 2001-04-04 解俊峰 Composite organic liquid fertilizer
CN101148375A (en) * 2006-09-22 2008-03-26 李树春 Nano medical stone highly effective foliage fertilizer
CN102040408A (en) * 2010-06-25 2011-05-04 厦门三和利生物技术有限公司 Foliar fertilizer
CN104478574A (en) * 2014-12-01 2015-04-01 宁夏共享生物化工有限公司 Method for preparing fertilizer containing humic acid concentrated chelating trace elements
CN104529624A (en) * 2014-12-12 2015-04-22 重庆惠民生物工程有限公司 Plant-source traditional Chinese medicinal herbal biological leaf fertilizer and preparation method thereof
CN105130702A (en) * 2015-08-18 2015-12-09 宁夏共享生物化工有限公司 Method used for preparing solid composite chelated water-soluble fertilizer containing humic acid from furfural residue
CN106490017A (en) * 2016-10-23 2017-03-15 张颂忠 A kind of foliage fertilizer plant pesticide of preventing and treating tetranychus viennensis

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108503476A (en) * 2018-06-21 2018-09-07 蚌埠天河花卉市场开发有限公司 A kind of liquid organic fertilizer and preparation method thereof
CN109265219A (en) * 2018-11-13 2019-01-25 广东新维生物科技股份有限公司 A kind of lignin fertilizer and preparation method of chelated microelement

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Application publication date: 20180302