CN107727488A - A kind of multifactor explosive reaction instrument of multichannel - Google Patents

A kind of multifactor explosive reaction instrument of multichannel Download PDF

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Publication number
CN107727488A
CN107727488A CN201711176565.5A CN201711176565A CN107727488A CN 107727488 A CN107727488 A CN 107727488A CN 201711176565 A CN201711176565 A CN 201711176565A CN 107727488 A CN107727488 A CN 107727488A
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China
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stress
unit
multifactor
loading unit
air bath
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CN201711176565.5A
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Chinese (zh)
Inventor
刘琦
董明
陆蔺辉
谢尧尧
王晓强
谢德
刘瑜嘉
刘斌
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Institute of Chemical Material of CAEP
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Institute of Chemical Material of CAEP
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Priority to CN201711176565.5A priority Critical patent/CN107727488A/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/02Details
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N17/00Investigating resistance of materials to the weather, to corrosion, or to light

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  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Analytical Chemistry (AREA)
  • Pathology (AREA)
  • Immunology (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • General Health & Medical Sciences (AREA)
  • Biodiversity & Conservation Biology (AREA)
  • Ecology (AREA)
  • Environmental Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)

Abstract

The invention discloses a kind of multifactor explosive reaction instrument of multichannel, mainly it is made up of reaction tank, stress loading unit, Stress Control unit, stress measurement unit and remote monitoring unit, the stress loading unit that the control of Stress Control unit is connected with Stress Control unit, stress loading unit provides various stress loadings for reaction tank, stress measurement unit is provided with reaction tank, the stress data value of stress measurement unit measurement is transferred to Stress Control unit, and remote monitoring unit is connected with Stress Control unit.The present invention has multiple passages, and a reaction instrument can configure multiple reaction cavities, and once multiple identical or different samples to be tested can be carried out with the stress loading experiment of the same terms;The experiment condition of combined stress, including temperature, humidity, mechanical compression, gas component and pressure iso-stress can be loaded, more truly simulates the environment of explosive aging.

Description

A kind of multifactor explosive reaction instrument of multichannel
Technical field
The present invention relates to a kind of explosive to react instrument, and in particular to a kind of multifactor explosive reaction instrument of multichannel, belongs to measurement Control device technical field.
Background technology
Chemical reactivity experiment (i.e. gas chromatography) is a kind of method of produced gas componant after identification explosive reaction, And the important method of the research stability of explosive, compatibility and aging characteristics.Explosive reaction instrument is to carry out chemical reactivity The stress loading experimental facilities used is tested, it acts on the experiment condition being to provide needed for chemistry of explosives reaction.
Traditional explosive reaction instrument is merely able to provide temperature stress loading for laboratory sample, and temperature load mode is also It is single heated at constant temperature mode.It is well known that the environmental factor of explosive aging is complicated and various.If explosive reacts instrument energy More, variable stress is enough loaded, more truly the environmental condition of Dynamite aging, then the examination of chemical reactivity experiment Result is tested just closer to truth, and this is to studying the aging characteristics of explosive and more having actual meaning with the compatibility of contact material Justice.
The content of the invention
The defects of it is an object of the invention to overcome prior art, there is provided one kind can provide a variety of combined stresses for sample Loading, and the multifactor explosive reaction instrument of multichannel that multiple samples can be tested simultaneously.
What the present invention was specifically realized in:
A kind of multifactor explosive reaction instrument of multichannel, mainly by reaction tank, stress loading unit, Stress Control unit, should Power measuring unit and remote monitoring unit composition, the stress loading list that the control of Stress Control unit is connected with Stress Control unit Member, stress loading unit provide various stress loadings for reaction tank, and stress measurement unit, stress measurement list are provided with reaction tank The stress data value of member measurement is transferred to Stress Control unit, and remote monitoring unit is connected with Stress Control unit.
Further scheme is:
The stress loading unit includes temperature loading unit, humidity loading unit, mechanical stress loading unit, gas group Divide and air pressure loading unit.
Further scheme is:
The stress measurement unit includes Temperature Humidity Sensor, mechanical stress sensor, gas pressure sensor.
Further scheme is:
The temperature loading unit enters what trip temperature loaded by air bath, including an air bath body and outside air Shell is bathed, heat-preservation cotton is provided between air bath body and air bath shell, air bath body surrounding is provided with cooling coil, it is cold But coil pipe intake-outlet is connected with Cool-water Machine for Industry, and heating plate is provided with air bath body bottom, and air bath body top is provided with Multiple air bath chambers.
Further scheme is:
The humidity loading unit is by connected humidity controller, humid control solenoid valve block into humidity controller passes through Humid control magnetic valve is connected with reaction cavity.
Further scheme is:
Pressure cylinder by specific gas component of the gas component and air pressure loading unit, pressure control solenoid valve block Into the pressure cylinder of specific gas component is connected by pressure control magnetic valve with reaction cavity.
Further scheme is:
Reaction cavity of the reaction tank by least one air bath chamber and positioned at air bath intracavitary portion forms, on reaction cavity It is mounted on Temperature Humidity Sensor, mechanical stress sensor, gas pressure sensor.
Further scheme is:
The mechanical stress loading unit is made up of upper gliding mass and backspin body;Laboratory sample is positioned over the upper end of backspin body Face, the rotation of backspin body are tightened, and laboratory sample will head on gliding mass and compress mechanical strain gauge;Regulation backspin body tightens journey Degree can be achieved to load the mechanical stress of laboratory sample.
Further scheme is:
The Stress Control unit includes a single-chip microcomputer, and the liquid crystal display being connected with single-chip microcomputer, in single-chip microcomputer On, received by analog-digital converter and the Monitoring Data of diversion stress detection unit transmission, single-chip microcomputer also drive with relay Dynamic circuit is connected, and relay drive circuit also controls magnetic valve point by pressure control magnetic valve, humid control magnetic valve, cold water It is not connected with pressure cylinder, humidity controller, Cool-water Machine for Industry;Single-chip microcomputer is also connected with digital analog converter, passes through numeral Analog converter is linked in sequence with controllable silicon, heating plate.
Further scheme is:
The single-chip microcomputer is also connected with remote industrial control computer.
The invention has the advantages that:
1st, there are multiple passages, a reaction instrument can configure multiple reaction cavities, can be once to multiple identical or different Sample to be tested carry out the same terms stress loading experiment;
2nd, the experiment condition of combined stress, including temperature, humidity, mechanical compression, gas component and pressure can be loaded Iso-stress, more truly simulate the environment of explosive aging;
3rd, change the temperature controlling mode of the tradition reaction single heated at constant temperature of instrument, it is cold not only to realize program computer heating control, program But control, and improve temperature controlled precision;
4th, the mechanical structure portion for reacting instrument uses modular design concept, is easy to reaction cavity processing and passage to expand Exhibition;
5th, Stress Control unit uses SCM Based embedded control system, efficiently solves sensor output signal It is weaker, the problem of being not suitable for long-distance transmissions, and each Stress Control cycle is shortened, improve Stress Control precision;
6th, control system has nearly distal end two places human-computer interaction interface, human users easy to operation, uses industrial computer As distal end host computer, the safety issue of explosive operation was both efficiently solved, and personnel easy to operation are carried out to experimental data Subsequent analysis processing.
Brief description of the drawings
Fig. 1 is overall structure diagram of the present invention;
Fig. 2 is temperature loading unit structural representation of the present invention;
Fig. 3 is reaction cavity structural representation of the present invention;
Fig. 4 is Stress Control cellular construction schematic diagram of the present invention.
Embodiment
The present invention is further illustrated with specific embodiment below in conjunction with the accompanying drawings.
As shown in Figure 1, a kind of multichannel multifactor explosive reaction instrument, mainly by reaction tank 1, stress loading unit 2, should Power control unit 3, stress measurement unit 4 and remote monitoring unit 5 form, the control of Stress Control unit 3 and Stress Control unit 3 Connected stress loading unit 2, stress loading unit 2 are that reaction tank 1 provides various stress loadings, and being provided with reaction tank 1 should Power measuring unit 4, the stress data value that stress measurement unit 4 measures are transferred to Stress Control unit 3, remote monitoring unit 5 with Stress Control unit 3 is connected.
Wherein, stress loading unit 2 includes temperature loading unit 21, humidity loading unit 22, mechanical stress loading unit 23rd, gas component and air pressure loading unit 24, stress measurement unit 4 include Temperature Humidity Sensor 41, mechanical stress sensor 42, Gas pressure sensor 43.
The temperature loading unit 21 enters what trip temperature loaded by air bath, including an air bath body 211 and outside Air bath shell 212, heat-preservation cotton 217 is provided between air bath body 211 and air bath shell 212, in air bath body 211 Surrounding is provided with cooling coil 215, and the intake-outlet of cooling coil 215 is connected with Cool-water Machine for Industry 216, is set in air bath body bottom Heating plate 214 is equipped with, air bath body top is provided with multiple air bath chambers 213.
The humidity loading unit 22 is made up of connected humidity controller 16, humid control magnetic valve 15, humid control Instrument 16 is connected by humid control magnetic valve 15 with reaction cavity 11.
Pressure cylinder 18, the pressure control magnetic valve of the gas component and air pressure loading unit 24 by specific gas component 17 compositions, the pressure cylinder 18 of specific gas component are connected by pressure control magnetic valve 17 with reaction cavity 11.
Reaction tank 1 is made up of at least one air bath chamber 213 and the reaction cavity 11 inside air bath chamber 213, Temperature Humidity Sensor 41, mechanical stress sensor 42, gas pressure sensor 43 are mounted on reaction cavity 11.
The mechanical stress loading unit 23 is made up of upper gliding mass 13 and backspin body 12;Laboratory sample 14 is positioned over backspin body 12 upper surface, the rotation of backspin body 12 are tightened, and laboratory sample 14 will head on gliding mass 13 and compress mechanical strain gauge 42;Adjust The degree of tightening of section backspin body can realize the mechanical stress loading to laboratory sample.
The Stress Control unit includes a single-chip microcomputer 31, and the liquid crystal display 32 being connected with single-chip microcomputer, in list On piece machine, by analog-digital converter 33 receive and diversion stress detection unit 4 transmit Monitoring Data, single-chip microcomputer also with after Electrical apparatus driving circuit 34 is connected, and relay drive circuit 34 is also by pressure control magnetic valve 17, humid control magnetic valve 15, cold Water management magnetic valve 19 is connected with pressure cylinder 18, humidity controller 16, Cool-water Machine for Industry 216 respectively;Single-chip microcomputer also with numeral Analog converter 35 is connected, and is linked in sequence by digital analog converter 35 and controllable silicon 218, heating plate 214.
Single-chip microcomputer is also connected with remote industrial control computer 51.
In the embodiment of the present invention, reaction tank is the support container that sample to be tested chemically reacts;Stress loading unit bag Include temperature, humidity, mechanical compression, gas component and pressure-loaded etc.;Stress Control unit can control each according to sets requirement The loading of item stress;Stress measurement unit includes Temperature Humidity Sensor, mechanical stress sensor and gas pressure sensor, in real time Monitor the numerical value of every stress;Remote monitoring unit can remotely record the numerical value of every stress in real time, to analyze experiment knot Fruit.
Reaction instrument enters trip temperature loading from air bath, and the structure of temperature loading unit is as shown in Figure 2.In an air bath Multiple air bath chambers are provided with body, realizing reaction instrument has the requirement of multichannel, and heater block and cooling-part are unified direct Load on air bath body, simultaneously multiple reaction tanks can so be entered with trip temperature loading, and ensure that each reaction tank as far as possible The uniformity of temperature.Heater block selects heating plate, and heating plate is placed in air bath body bottom, and such heat can pass through thicker sky Gas bath body bottom is conducted, and more homogenization ground heats each air bath chamber, reduces the difference between each air bath chamber temperature It is different.Cooling-part selects Cool-water Machine for Industry, cooling water is introduced into air bath body using cooling coil, increase cooling-part not only may be used The scope loaded with extended temperature, can also provide facility for temperature control.It is provided with and protects between air bath shell and air bath body Wen Mian, to strengthen the heat insulation effect of air bath body, reduce influence of the external environment to air bath chamber temperature.
The structure of reaction cavity is as shown in Figure 3.Temperature Humidity Sensor, baroceptor and stress are installed on reaction cavity Sensor, the mechanical compression that humiture, air pressure and the tablet sample of measurable reaction cavity are born.Humidity loading unit by Humidifier, magnetic valve and associated pipe composition;Electromagnetic valve for adjusting can realize the humidity loading to laboratory sample.Air pressure-loading unit It is made up of the pressure cylinder, magnetic valve and associated pipe of specific gas component;Electromagnetic valve for adjusting can realize the spy to laboratory sample Determine gas atmosphere loading.Stress loading unit is made up of upper gliding mass and backspin body;Laboratory sample is positioned over the upper surface of backspin body, The rotation of backspin body is tightened, and laboratory sample will head on gliding mass compressive stres sensor;The degree of tightening for adjusting backspin body can be real Now the mechanical stress of laboratory sample is loaded.The sealing property of reaction cavity is must assure that, the main seal measure taken for this Have:Movable part is sealed using brass shim spacer, including the upper end cover of reaction cavity, strain gauge and Temperature Humidity Sensor Installation place;Inactive pipeline uses welding manner.
Stress Control unit uses the embedded control system based on STM32 single-chip microcomputers, and its frame structure is as shown in Figure 4. The analog signal of sensor output is converted to data signal through digital analog converter, and data signal is taken by monolithic is machine-readable again, single Piece machine controls each stress to be added according to the numerical value of each sensor and the intelligent proportional integral differential control method algorithm of design Carry.It is weaker can effectively to solve sensor output signal using such Stress Control system, the problem of being not suitable for long-distance transmissions. The adjusting actuator of gas atmosphere and humidity is all magnetic valve;The adjusting actuator of temperature includes magnetic valve and controllable silicon, monolithic The temperature heating signal of machine output is converted to (0~5v) analog voltage, analog voltage input controllable silicon through digital analog converter Heater plate is controlled, the temperature cooling signal of single-chip microcomputer output directly inputs driving circuit for electromagnetic valve control solenoid closure, Control flow of cooling water;The regulation of mechanical stress needs operating personnel to be loaded in advance to laboratory sample.LCDs is Near-end man-machine interaction device, the numerical value of each sensor can be both shown, allow operating personnel to operate control system again, such as The setting value of each stress is set, experimental period, control system start and stop etc. are set.Two places control is blasting explosive secure behaviour The basic demand of work, using industrial computer as distal end host computer, host computer is led to slave computer by RS485 buses Letter, labVIEW software developments distal end man-machine interface being used on industrial computer, its function is similar with near-end man-machine interface, and The functions such as data storage, report generation are added, to facilitate operating personnel to carry out subsequent analysis processing to experimental data.
Although reference be made herein to invention has been described for explanatory embodiment of the invention, and above-described embodiment is only this hair Bright preferable embodiment, embodiments of the present invention are simultaneously not restricted to the described embodiments, it should be appreciated that people in the art Member can be designed that a lot of other modifications and embodiment, and these modifications and embodiment will fall in principle disclosed in the present application Within scope and spirit.

Claims (10)

1. a kind of multifactor explosive reaction instrument of multichannel, it is characterised in that mainly by reaction tank, stress loading unit, Stress Control Unit, stress measurement unit and remote monitoring unit composition, the stress that the control of Stress Control unit is connected with Stress Control unit Loading unit, stress loading unit provide various stress loadings for reaction tank, stress measurement unit, stress are provided with reaction tank The stress data value of measuring unit measurement is transferred to Stress Control unit, and remote monitoring unit is connected with Stress Control unit.
2. the multifactor explosive reaction instrument of multichannel according to claim 1, it is characterised in that:
The stress loading unit include temperature loading unit, humidity loading unit, mechanical stress loading unit, gas component and Air pressure-loading unit.
3. the multifactor explosive reaction instrument of multichannel according to claim 1, it is characterised in that:
The stress measurement unit includes Temperature Humidity Sensor, mechanical stress sensor, gas pressure sensor.
4. the multifactor explosive reaction instrument of multichannel according to claim 2, it is characterised in that:
The temperature loading unit enters what trip temperature loaded by air bath, including outside an air bath body and outside air bath Shell, heat-preservation cotton is provided between air bath body and air bath shell, air bath body surrounding is provided with cooling coil, cooler pan Pipe intake-outlet is connected with Cool-water Machine for Industry, and heating plate is provided with air bath body bottom, and air bath body top is provided with multiple Air bath chamber.
5. the multifactor explosive reaction instrument of multichannel according to claim 2, it is characterised in that:
The humidity loading unit is by connected humidity controller, humid control solenoid valve block into humidity controller passes through humidity Control magnetic valve is connected with reaction cavity.
6. the multifactor explosive reaction instrument of multichannel according to claim 2, it is characterised in that:
The gas component and air pressure loading unit are by the pressure cylinder of specific gas component, pressure control solenoid valve block into special The pressure cylinder for determining gas component is connected by pressure control magnetic valve with reaction cavity.
7. the multifactor explosive reaction instrument of multichannel according to claim 4, it is characterised in that:
Reaction cavity of the reaction tank by least one air bath chamber and positioned at air bath intracavitary portion forms, and pacifies on reaction cavity Equipped with Temperature Humidity Sensor, mechanical stress sensor, gas pressure sensor.
8. the multifactor explosive reaction instrument of multichannel according to claim 2, it is characterised in that:
The mechanical stress loading unit is made up of upper gliding mass and backspin body;Laboratory sample is positioned over the upper surface of backspin body, under Rotation body rotation is tightened, and laboratory sample will head on gliding mass and compress mechanical strain gauge;The degree of tightening for adjusting backspin body can Realize and the mechanical stress of laboratory sample is loaded.
9. the multifactor explosive reaction instrument of multichannel according to claim 1, it is characterised in that:
The Stress Control unit includes a single-chip microcomputer, and the liquid crystal display being connected with single-chip microcomputer, on single-chip microcomputer, leads to Cross analog-digital converter receive and diversion stress detection unit transmission Monitoring Data, single-chip microcomputer also with relay drive circuit Be connected, relay drive circuit also by pressure control magnetic valve, humid control magnetic valve, cold water control magnetic valve respectively with pressure Strength bottle, humidity controller, Cool-water Machine for Industry are connected;Single-chip microcomputer is also connected with digital analog converter, is turned by digital simulation Parallel operation is linked in sequence with controllable silicon, heating plate.
10. the multifactor explosive reaction instrument of multichannel according to claim 9, it is characterised in that:
The single-chip microcomputer is also connected with remote industrial control computer.
CN201711176565.5A 2017-11-22 2017-11-22 A kind of multifactor explosive reaction instrument of multichannel Pending CN107727488A (en)

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Application Number Priority Date Filing Date Title
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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108388289A (en) * 2018-03-26 2018-08-10 中国工程物理研究院化工材料研究所 The full dimension security protection system of the hot Combined Loading of explosive power and method
CN108444526A (en) * 2018-03-14 2018-08-24 中国工程物理研究院化工材料研究所 The hot Combined Loading environment multi-channel multi-parameter high frequency sound data network structure of explosive power
CN109443447A (en) * 2018-12-20 2019-03-08 中国工程物理研究院化工材料研究所 The hot Combined Loading control system of explosive power
CN109489730A (en) * 2018-12-20 2019-03-19 中国工程物理研究院化工材料研究所 The hot Combined Loading equipment operation multi-screen display method of explosive power
CN109975121A (en) * 2019-04-19 2019-07-05 中国工程物理研究院化工材料研究所 A kind of fast appraisement method characterizing PBX modeling powder compressibility

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108444526A (en) * 2018-03-14 2018-08-24 中国工程物理研究院化工材料研究所 The hot Combined Loading environment multi-channel multi-parameter high frequency sound data network structure of explosive power
CN108388289A (en) * 2018-03-26 2018-08-10 中国工程物理研究院化工材料研究所 The full dimension security protection system of the hot Combined Loading of explosive power and method
CN108388289B (en) * 2018-03-26 2020-05-22 中国工程物理研究院化工材料研究所 Explosive force-heat composite loading full-dimensional safety protection method
CN109443447A (en) * 2018-12-20 2019-03-08 中国工程物理研究院化工材料研究所 The hot Combined Loading control system of explosive power
CN109489730A (en) * 2018-12-20 2019-03-19 中国工程物理研究院化工材料研究所 The hot Combined Loading equipment operation multi-screen display method of explosive power
CN109975121A (en) * 2019-04-19 2019-07-05 中国工程物理研究院化工材料研究所 A kind of fast appraisement method characterizing PBX modeling powder compressibility
CN109975121B (en) * 2019-04-19 2021-07-27 中国工程物理研究院化工材料研究所 Rapid evaluation method for representing compressibility of PBX molding powder

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