CN107723141A - A kind of extraction preparation method of efficiently tea seed alkali - Google Patents
A kind of extraction preparation method of efficiently tea seed alkali Download PDFInfo
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- CN107723141A CN107723141A CN201711099647.4A CN201711099647A CN107723141A CN 107723141 A CN107723141 A CN 107723141A CN 201711099647 A CN201711099647 A CN 201711099647A CN 107723141 A CN107723141 A CN 107723141A
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- Prior art keywords
- tea
- tea oil
- oil slag
- oil
- parts
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Classifications
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D473/00—Heterocyclic compounds containing purine ring systems
- C07D473/02—Heterocyclic compounds containing purine ring systems with oxygen, sulphur, or nitrogen atoms directly attached in positions 2 and 6
- C07D473/04—Heterocyclic compounds containing purine ring systems with oxygen, sulphur, or nitrogen atoms directly attached in positions 2 and 6 two oxygen atoms
- C07D473/06—Heterocyclic compounds containing purine ring systems with oxygen, sulphur, or nitrogen atoms directly attached in positions 2 and 6 two oxygen atoms with radicals containing only hydrogen and carbon atoms, attached in position 1 or 3
- C07D473/08—Heterocyclic compounds containing purine ring systems with oxygen, sulphur, or nitrogen atoms directly attached in positions 2 and 6 two oxygen atoms with radicals containing only hydrogen and carbon atoms, attached in position 1 or 3 with methyl radicals in positions 1 and 3, e.g. theophylline
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07G—COMPOUNDS OF UNKNOWN CONSTITUTION
- C07G5/00—Alkaloids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/005—Synthetic soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of extraction preparation method of efficiently tea seed alkali, light industry technical field, mainly carried out by following step：First, raw material used：50 parts of leached tea oil slag, 5 parts of sodium hydroxide, 8 parts of commercial grease；2nd, tealeaves dregs of rice mechanical crushing will be dried into powder materials, tealeaves dregs of rice powder materials add to the clear water of 20 times of quality, rise temperature turns into mixed liquor after five minutes to 100 DEG C；3rd, mixed liquor is obtained into filtrate by filter screen, filter residue is squeezed pressed liquor and to filter out clarified solution, the filtered fluid obtained twice is merged to obtain leached tea oil slag extract solution；4th, sodium carbonate hydroxide sodium powder will be added in leached tea oil slag extract solution, will be stirred, rise temperature is distilled to 50 DEG C ~ 60 DEG C, is reduced moisture to sticky, is turned into leached tea oil slag concentration alkali lye；5th, leached tea oil slag concentration alkali lye is mixed with grease, is heated to temperature 60 C ~ 65 DEG C, dissolve fully, being uniformly mixed, pours into mould, be cooled to 10 DEG C ~ 25 DEG C condensations and form.
Description
Technical field
The present invention relates to a kind of preparation method of laundry soap, more particularly to a kind of system using leached tea oil slag as the laundry soap of raw material
Make method, belong to agricultural technology field.
Background technology
The seed of tea seed, i.e. tea oil tree, it can extract oil edible.The tea oil squeezed out is protected with high nutritive value and health
Strong effect.Tea seed, it is China's endemic species, is described as " east olive oil ".The ribes tree that tea oil tree original refers to, it is evergreen little Qiao
Wood.
Tea seed oil-containing more than 30%, edible and profit hair, adjust medicine, can candle and soap processed, can also make the substitute of machine oil.
The tea oil that tea seed is squeezed out has high nutritive value.The fatty acid composition of tea oil be oleic acid, linoleic acid, palmitic acid, stearic acid,
Linolenic acid, myristic acid etc., significantly larger than rape oil, peanut oil and soya-bean oil, doubled with olive oil than content of vitamin E.Tea seed
Squeezed tea oil also containing the specific physiological activator such as camellianin and linoleic acid, linolenic acid be maintain human body skin, hair
Growth institute is indispensable, being capable of prevention of arterial hardening.
Unrighted acid is more than more than 90%, and iodine number 112 is higher than other edible vegetable oils.Tea-seed oil is more rich in tea
The content of phenol, vitamin E and carotenoid etc., wherein vitamin E is higher than other edible vegetable oils.
Tea oil has oxidation resistance simultaneously, being capable of lowering blood pressure and blood fat and suppression artery sclerosis.The nutritive value of tea oil
Can and olive oil compare favourably, even more high some, be table oil.Due to being China's endemic species, therefore also referred to as " east
Olive oil ".
Tea oil contains a large amount of unrighted acids, and its property is stable, hermetically storing physical and chemical properties change very little after 1 year.Tea
Seed oil is than the easy storage of other plant oil.Tea-seed oil can as other edible vegetable oils cooking, cold vegetable dish in sauce etc., have uniqueness
Tea perfume.
In addition, tea seed also has many comprehensive utilization values.Contain Tea Saponin, tea seed polysaccharide, tea seed albumen etc. in leached tea oil slag,
They are all the raw materials of chemical industry, light industry, food, feed industry product etc., and tea seed episperm may also be fabricated which furfural, activated carbon etc., tea shell
Or a kind of good edible mushroom culture tea seed tree is to bloom in autumn, comes annual bearing, autumn harvesting fruit.In general tea seed is all
Cold Dew is front and rear to pluck, and imply that tea seed maturation, and some late-maturing tea seeds had been wanted the Frost's Descent and could plucked, if adopted
It is early, just it is not much oil.
For camellia oleifera cultivar " Frost's Descent seed ", plucked " Cold Dew " first 10 days, kind shell accounts for 46.3%, and benevolence accounts for 53.2%, tea
Seed oil content only accounts for 17.9%；And plucked within 5 days afterwards in " Frost's Descent ", kind shell accounts for 37.6%, and benevolence accounts for 62.4%, and tea seed oil content is reachable
28.5%.Pluck in advance, cone prematurity, tea seed oil content is low, and water content is high；Pluck too late, cone cracking, tea seed is scattered, difficult
To collect, cause to waste.So camellia oleifera fruit will be plucked in good time, and accomplish " three observations ".
First, observation kind.Different kinds, camellia oleifera fruit maturity period differ." Cold Dew seed " tree crown is small, upright, crotch angle
Less than 30 degree, leaf is small and dense, the small thin skin of fruit, the ripe harvesting at " Cold Dew " per 1~3, fruit seed." Frost's Descent seed " tree crown compared with
Greatly, the first transaction of a day's business crotch angle is generally 40~60 degree, and leaf is slightly thick greatly, and fruit is big, per 4~7, fruit seed, maturation to be adopted when " Frost's Descent "
Pluck." the Beginning of Winter seed " tree crown is big, and the first transaction of a day's business crotch angle is more than 40 degree, and leaf is big and dilute, and fruit is big, and per 7~10, fruit seed, Ying Yu is " vertical
Ripe harvesting during the winter ".
Second, observation color.In the oil tea mature period, tea seed color is conscientiously observed.The ripe surface characteristics of camellia oleifera fruit is：
Pericarp is shinny, the red red middle band of follicarpium is yellow, is taken off in rascal fruit green grass or young crops with fine hair on white, pericarp, tea fruit fine fisssure, easily stripping.To oil
In tea woods conveniently harvesting cone peel off, find tea seed it is shinny when, further peel off, see benevolence it is white in it is yellow, glossy shinny when, card
Bright cone is fully ripe, at this moment can pluck.
Third, observation landforms.Geographical position residing for oil tea is different, and maturity is also inconsistent, and usually high mountain is first ripe, low
Mountain after-ripening；Tailo is first ripe, Schattenseite after-ripening；Virgin forest is first ripe, young growth after-ripening；Barren is first ripe, cultivated land after-ripening.
Tea seed oil-containing more than 30%, edible and profit hair, adjust medicine, can candle and soap processed, can also make the substitute of machine oil.
The tea oil that tea seed is squeezed out has high nutritive value.The fatty acid composition of tea oil be oleic acid, linoleic acid, palmitic acid, stearic acid,
Linolenic acid, myristic acid etc., significantly larger than rape oil, peanut oil and soya-bean oil, doubled with olive oil than content of vitamin E.Tea seed
Squeezed tea oil also containing the specific physiological activator such as camellianin and linoleic acid, linolenic acid be maintain human body skin, hair
Growth institute is indispensable, being capable of prevention of arterial hardening.Unrighted acid in tea oil is more than more than 90%, iodine number 112,
It is higher than other edible vegetable oils.Tea-seed oil is high rich in Tea Polyphenols, vitamin E and carotenoid etc., the wherein content of vitamin E
In other edible vegetable oils.
Tea oil has oxidation resistance simultaneously, being capable of lowering blood pressure and blood fat and suppression artery sclerosis.The nutritive value of tea oil
Can and olive oil compare favourably, even more high some, be table oil.Due to being China's endemic species, therefore also referred to as " east
Olive oil ".
Tea oil contains a large amount of unrighted acids, and its property is stable, hermetically storing physical and chemical properties change very little after 1 year.Tea
Seed oil is than the easy storage of other plant oil.Tea-seed oil can as other edible vegetable oils cooking, cold vegetable dish in sauce etc., have uniqueness
Tea perfume.
In addition, tea seed also has many comprehensive utilization values.Contain Tea Saponin, tea seed polysaccharide, tea seed albumen etc. in leached tea oil slag,
They are all the raw materials of chemical industry, light industry, food, feed industry product etc., and tea seed episperm may also be fabricated which furfural, activated carbon etc., tea shell
A kind of or good culture medium of edible fungus.Research shows that oil tea saponin also has antibacterial and antioxidation base.Research shows,
Oil tea saponin also has antibacterial and antioxidation.
The content of the invention
Contain substantial amounts of alkaline matter in tea seed, the alkaline matter in tea seed has very strong dirt-removing power, but tea seed or tea
The impurity such as the cellulose in the seed dregs of rice are a lot, and extraction turns into technical barrier.
A kind of extraction preparation method of efficiently tea seed alkali solves the technical scheme that problem is taken and carried out by following step：
First, raw material used：50 parts of leached tea oil slag, 5 parts of sodium hydroxide, 8 parts of commercial grease；2nd, will dry tealeaves dregs of rice mechanical crushing into
Powder materials, tealeaves dregs of rice powder materials are added to the clear water of 20 times of quality, stirred, rise temperature cools after five minutes to 100 DEG C
Turn into mixed liquor to 40 DEG C ~ 60 DEG C；3rd, mixed liquor is obtained into filtrate by filter screen, filter residue is squeezed pressed liquor and to filter
Go out clarified solution, the filtered fluid obtained twice is merged to obtain leached tea oil slag extract solution；4th, carbonic acid will be added in leached tea oil slag extract solution
Sodium hydroxide sodium powder, is stirred, and rise temperature is distilled to 50 DEG C ~ 60 DEG C, reduces moisture to sticky, it is dense to turn into leached tea oil slag
Slack mercerizing liquid；5th, leached tea oil slag concentration alkali lye is mixed with grease, is heated to temperature 60 C ~ 65 DEG C, dissolve fully, being stirred
It is even, pour into mould, be cooled to 10 DEG C ~ 25 DEG C condensations and form.
A kind of beneficial effect of the efficiently extraction preparation method of tea seed alkali is：A kind of extraction preparation method of efficiently tea seed alkali
Distilled, concentrated by dissolving alkali lye by leached tea oil slag, then mix with sodium hydroxide increase its alkalescence, by adding industry oil
Turn into after fat mixing and condense solid, turn into the piece goods that can cooperate, easily can buy and use for people.
Embodiment
Under a kind of extraction preparation method of efficiently tea seed alkali is made further to implement explanation.
A kind of extraction preparation method of efficiently tea seed alkali is by following step progress：First, raw material used：Leached tea oil slag 50
Part, 5 parts of sodium hydroxide, 8 parts of commercial grease；2nd, tealeaves dregs of rice mechanical crushing will be dried into powder materials, tealeaves dregs of rice powder materials will be added
Enter the clear water of 20 times of quality, stir, rise temperature is cooled to 40 DEG C ~ 60 DEG C after five minutes to 100 DEG C turns into mixed liquor；
3rd, mixed liquor is obtained into filtrate by filter screen, filter residue is squeezed pressed liquor and to filter out clarified solution, the filtering that will be obtained twice
Liquid merges to obtain leached tea oil slag extract solution；4th, sodium carbonate hydroxide sodium powder will be added in leached tea oil slag extract solution, stirred, risen
High-temperature is distilled to 50 DEG C ~ 60 DEG C, is reduced moisture to sticky, is turned into leached tea oil slag concentration alkali lye；5th, leached tea oil slag is concentrated into alkali
Liquid mixes with grease, is heated to temperature 60 C ~ 65 DEG C, dissolve fully, being uniformly mixed, pours into mould, be cooled to 10 DEG C ~
25 DEG C of condensations form.
Claims (1)
- A kind of 1. extraction preparation method of efficiently tea seed alkali, it is characterized in that being carried out by following step：First, raw material used：Tea 50 parts of the seed dregs of rice, 5 parts of sodium hydroxide, 8 parts of commercial grease；2nd, tealeaves dregs of rice mechanical crushing will be dried into powder materials, by tealeaves dregs of rice powder End material adds the clear water of 20 times of quality, stirs, and rise temperature is cooled to 40 DEG C ~ 60 DEG C after five minutes to 100 DEG C turns into mixed Close feed liquid；3rd, mixed liquor is obtained into filtrate by filter screen, filter residue is squeezed pressed liquor and to filter out clarified solution, will be taken twice The filtered fluid obtained merges to obtain leached tea oil slag extract solution；4th, sodium carbonate hydroxide sodium powder, stirring will be added in leached tea oil slag extract solution Uniformly, raise temperature to be distilled to 50 DEG C ~ 60 DEG C, reduce moisture to sticky, turn into leached tea oil slag concentration alkali lye；5th, by tea seed Dregs of rice concentration alkali lye mixes with grease, is heated to temperature 60 C ~ 65 DEG C, dissolve fully, being uniformly mixed, pours into mould, drops Temperature to 10 DEG C ~ 25 DEG C condensations form.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711099647.4A CN107723141A (en) | 2017-11-09 | 2017-11-09 | A kind of extraction preparation method of efficiently tea seed alkali |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711099647.4A CN107723141A (en) | 2017-11-09 | 2017-11-09 | A kind of extraction preparation method of efficiently tea seed alkali |
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| Publication Number | Publication Date |
|---|---|
| CN107723141A true CN107723141A (en) | 2018-02-23 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711099647.4A Withdrawn CN107723141A (en) | 2017-11-09 | 2017-11-09 | A kind of extraction preparation method of efficiently tea seed alkali |
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| CN (1) | CN107723141A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113337347A (en) * | 2021-05-31 | 2021-09-03 | 湖南万象生物科技有限公司 | Washing liquid prepared from defatted tea seed meal and preparation method thereof |
-
2017
- 2017-11-09 CN CN201711099647.4A patent/CN107723141A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113337347A (en) * | 2021-05-31 | 2021-09-03 | 湖南万象生物科技有限公司 | Washing liquid prepared from defatted tea seed meal and preparation method thereof |
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| WW01 | Invention patent application withdrawn after publication | ||
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Application publication date: 20180223 |