CN107694744B - A kind of flotation combined desliming process of ultrasonic wave-shaking table- - Google Patents

A kind of flotation combined desliming process of ultrasonic wave-shaking table- Download PDF

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CN107694744B
CN107694744B CN201710887342.3A CN201710887342A CN107694744B CN 107694744 B CN107694744 B CN 107694744B CN 201710887342 A CN201710887342 A CN 201710887342A CN 107694744 B CN107694744 B CN 107694744B
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ultrasonic wave
desliming
shaking table
deslimer
flotation
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CN107694744A (en
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罗斌
曹沁波
黄余
程金华
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Kunming University of Science and Technology
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Kunming University of Science and Technology
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B03SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03BSEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
    • B03B9/00General arrangement of separating plant, e.g. flow sheets

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Abstract

The invention discloses a kind of flotation combined desliming process of ultrasonic wave-shaking table-, desliming process of the invention is that raw ore material is removed a part of sludge by ultrasonic wave deslimer first, tail is directly thrown in the overflow of ultrasonic wave deslimer, the sand setting of ultrasonic wave deslimer carries out sorting desliming using shaking table, table concentrate is as material after qualified desliming, shaking table tailing directly throws tail, shaking table chats is added into foaming agent, then flotation desliming is carried out using agitator again after mixing evenly, flotation froth is that thin mud directly throws tail, floatation underflow is the material after desliming, the ultrasonic wave deslimer that the present invention uses includes mineral-feeding pipe, give mine spray head, cowling panel, ultrasonic probe, casing ontology, overflow launder, overflow port, conducting wire, ultrasonic wave control cabinet, add water pipe, high-pressure water pipe, sand sinking port switch, sand sinking port, rectify board mount and mineral-feeding pipe bracket , desliming of the present invention is thorough, and desliming is high-efficient, can reduce consumption of the sludge to medicament in subsequent job, has wide application prospect.

Description

A kind of flotation combined desliming process of ultrasonic wave-shaking table-
Technical field
The present invention relates to a kind of flotation combined desliming process of ultrasonic wave-shaking table-, belong to technical field of mineral processing.
Background technique
The source of sludge is generally divided into two kinds, and one is primary slime, the sludge that ore is formed in mineralizing process is another Kind is that subsequent exploitation sorts secondary slime of the ore in the process due to polluting or excessively honed pulverized zone is come.Thin mud described in people Usually material of the granularity less than 10 μm, these fine granule materials have very big surface area, sort in mineral since granularity is small A large amount of medicament can be consumed in the process, can also be attached to coarse grain mineral surfaces, drastically influence subsequent sorting operation.Therefore, exist It generally requires to carry out desliming process when carrying out to mineral and sort separation, obtains better separating effect for subsequent sorting operation and provide Precondition.
For the higher ore containing mud, desliming, such as the higher zinc oxide of clay content are often first carried out before being sorted Mine will increase foam viscosity when using vulcanization-amine method flotation, foam can be difficult to eliminate, serious race if clay content is too high Slot phenomenon can make floatation indicators be deteriorated.Now for desliming using more equipment such as hydrocyclone, desliming bucket, inclined plate concentration Machine etc., however these equipment are often all single use, is not achieved a preferable desliming effect, how to existing equipment or Person's technique improves, and develops an efficient desliming device and technique will be an effective method.
Summary of the invention
The main purpose of the present invention is to provide a kind of flotation combined desliming process of ultrasonic wave-shaking table-, of the invention is super Sound wave desliming mainly utilizes ultrasonic wave deslimer to complete, and the equipment making of the ultrasonic wave deslimer is simple, and desliming is high-efficient, with The combination of the techniques such as shaking table, flotation can be handled containing the higher ore of mud, can obtain preferable desliming effect.
Concrete operations of the invention are as follows: raw ore material being removed a part of sludge by ultrasonic wave deslimer first, is surpassed Tail is directly thrown in the overflow of sound wave deslimer, and the sand setting of ultrasonic wave deslimer continues to carry out sorting desliming, table concentrate using shaking table As the material after desliming, shaking table tailing directly throws tail, and shaking table chats is added foaming agent, is then stirred evenly using agitator Carry out flotation desliming again afterwards, flotation froth is thin mud, directly throwing tail, floatation underflow be desliming after material, raw ore material it is dense Degree is 10% ~ 40%.
Ultrasonic wave desliming of the invention mainly utilizes ultrasonic wave deslimer to complete, which includes to mine Pipe gives mine spray head, cowling panel, ultrasonic probe, casing ontology, overflow launder, overflow port, conducting wire, ultrasonic wave control cabinet, water supplement Pipe, high-pressure water pipe, sand sinking port switch, sand sinking port, rectification board mount and mineral-feeding pipe bracket;
Casing ontology top is cylinder, and diameter is 0.3 ~ 5m, and lower part is inverted conical shape, and bottom cone angle is 20 ~ 70 °, The over top of casing ontology is equipped with overflow launder, and the lowest part of overflow launder is equipped with overflow port, and mineral-feeding pipe is solid by mineral-feeding pipe bracket It is scheduled on casing ontology top center, the lower end of mineral-feeding pipe, which is installed, gives mine spray head, is located in casing ontology to mine spray head, casing ontology It is interior to be equipped with upper layer and lower layer cowling panel layer, there is more than one rectification board mount on each layer of cowling panel layer, each cowling panel branch Frame is equipped with more than one cowling panel, is equipped with ultrasonic probe between two layers of cowling panel layer, ultrasonic probe by conducting wire with External ultrasonic wave control cabinet connection, more than one water pipe of adding is mounted on casing ontology side, and connect with external water source, It is equipped with sand sinking port in casing ontology bottom, sand sinking port is equipped with above sand sinking port and switchs, high-pressure water pipe is mounted on sand sinking port side, and It is connect with external water source.
The working principle of ultrasonic wave deslimer: being first turned on the power supply of ultrasonic wave control cabinet, and signal is incoming super by conducting wire Sonic probe, ultrasonic probe emit ultrasonic wave into around it 360 degree, and ore pulp is entered by feed port, are giving mine spray head Under the action of sprayed at dispersion shape, under the action of ultrasonic probe that ore pulp is loose, thin mud floats and goes forward side by side after passing through cowling panel Enter overflow launder, be finally discharged from overflow port, heavy mineral is crossed cowling panel and is discharged from sand sinking port, and sand sinking port switch can control sand setting The size of mouth, adding water pipe can according to need carry out water supplement, and high-pressure water pipe can provide high pressure water to solve desilting mouth Blockage problem.
The beneficial effects of the present invention are:
1, the present invention carries out joint desliming, simple process using ultrasonic high-efficiency deslimer, shaking table and flotation device, and desliming is done Only, it is easy to accomplish.
2, technique of the invention uses stage desliming operation, uses different equipment for the material properties of each sessions Desliming is carried out, subsequent job load can be not only reduced, but also can achieve the purpose for improving desliming efficiency.
3, the present invention carries out ultrasonic wave desliming using ultrasonic wave deslimer, and the effect of ultrasonic wave can be very good to prevent thin mud The cover phenomenon reunited with sludge surface, greatly improves desliming effect.
4, ultrasonic wave deslimer of the invention does not need stirring power, it is possible to reduce the consumption of electric energy reduces desliming cost.
Detailed description of the invention
Fig. 1 is process flow chart of the invention;
Fig. 2 is ultrasonic wave deslimer cross-sectional view of the invention;
Fig. 3 is ultrasonic wave deslimer top view of the invention;
In figure: 1-mineral-feeding pipe, 2-are overflow to mine spray head, 3-cowling panels, 4-ultrasonic probes, 5-casing ontologies, 6- Chute, 7-overflow ports, 8-conducting wires, 9-ultrasonic wave control cabinets, 10-are added water pipe, 11-high-pressure water pipes, 12-sand sinking ports and are opened Pass, 13-sand sinking ports, 14-rectification board mounts, 15-mineral-feeding pipe brackets.
Specific embodiment
Below by drawings and examples, invention is further described in detail, but protection scope of the present invention is not limited to In the content.
Embodiment 1: the flotation combined desliming process of ultrasonic wave-shaking table-, concrete operations are as follows:
Sichuan weathering iron ore primary slime clay content 30% carries out the iron ore concentrate after magnetic separation using traditional cyclone Twice after desliming process, for clay content still 5% or more, obtained iron concentrate grade is 61.63%.
Using the method for the present invention, process flow is as shown in Figure 1, carry out ultrasonic wave-shaking table-flotation for the iron ore concentrate after magnetic separation The iron ore concentrate after magnetic separation that concentration is first 10% by joint desliming removes a part of sludge, ultrasonic wave by ultrasonic wave deslimer Tail is directly thrown in the overflow of deslimer, and the sand setting of ultrasonic wave deslimer carries out sorting desliming using shaking table, and table concentrate is as qualified Desliming after material, shaking table tailing directly throws tail, and shaking table chats is added foaming agent 2#Oily 75g/t, is then stirred using agitator Flotation desliming is carried out after mixing uniformly again, flotation froth is that thin mud directly throws tail, and floatation underflow is the material after desliming, after desliming Product clay content 1% hereinafter, iron concentrate grade be 65.63%, and, using the method for the present invention carry out desliming, considerably reduce Clay content increases substantially concentrate quality.
Ultrasonic wave deslimer used in the present invention as shown in Fig. 2 ~ 3, including mineral-feeding pipe 1, to mine spray head 2, cowling panel 3, Ultrasonic probe 4, overflow launder 6, overflow port 7, conducting wire 8, ultrasonic wave control cabinet 9, adds water pipe 10, high-pressure water pipe at casing ontology 5 11, sand sinking port switch 12, sand sinking port 13, rectification board mount 14 and mineral-feeding pipe bracket 15;
5 top of casing ontology is cylinder, and diameter 0.3m, lower part is inverted conical shape, and bottom cone angle is 20 °, casing sheet The over top of body 5 is equipped with overflow launder 6, and the lowest part of overflow launder 6 is equipped with overflow port 7, and mineral-feeding pipe 1 is solid by mineral-feeding pipe bracket 15 It is scheduled on 5 top center of casing ontology, the lower end of mineral-feeding pipe 1 is installed to mine spray head 2, is located in casing ontology 5 to mine spray head 2, machine It is equipped with upper layer and lower layer cowling panel layer in shell ontology 5, there are 4 rectification board mounts 14 on each layer of cowling panel layer, outermost two Rectify board mount and be equipped with 4 cowling panels 3, intermediate two rectification board mounts equipped with 6 cowling panels 3, two layers cowling panel layer it Between be equipped with ultrasonic probe 4, ultrasonic probe 4 is connect by conducting wire 8 with external ultrasonic wave control cabinet 9, equipped with 2 water supplements Pipe 10 is mounted on 5 side of casing ontology, and connect with external water source, is equipped with sand sinking port 13, sand sinking port 13 in 5 bottom of casing ontology Top is equipped with sand sinking port switch 12, and high-pressure water pipe 11 is mounted on 13 side of sand sinking port, and connect with external water source.
Embodiment 2: the flotation combined desliming process of ultrasonic wave-shaking table-, concrete operations are as follows:
Guangxi lead-zinc clay content 25% preselects desliming using desliming bucket, and clay content is still greater than 10%, then uses Vulcanization-amine method carries out flotation, and reagent consumption amount is big, finally obtains in concentrate, Pb grade 31.50%, the rate of recovery 56%, Zn grade 25.65%, the rate of recovery 63.7%, floatation indicators are poor, and foam is relatively glutinous, and it is serious to run slot.
Using the flotation combined desliming process of ultrasonic wave-shaking table-of the present invention, process flow is as shown in Figure 1, by Guangxi The raw ore of certain lead-zinc carries out predictive desliming, and the raw ore that concentration is 40% is removed one by ultrasonic wave deslimer first Divide sludge, tail is directly thrown in the overflow of ultrasonic wave deslimer, and the sand setting of ultrasonic wave deslimer carries out sorting desliming, shaking table using shaking table Concentrate directly throws tail as material after qualified desliming, shaking table tailing, and shaking table chats is added foaming agent 2#Oily 75g/t, then Flotation desliming is carried out using agitator again after mixing evenly, flotation froth is that thin mud directly throws tail, and floatation underflow is after desliming Material, for the product clay content after desliming 1% hereinafter, carrying out flotation using vulcanization-amine method, floatation indicators are Pb grade 36.70%, the rate of recovery 78%, Zn grade 32.34%, the rate of recovery 82.4%, and amount of sodium sulfide is reduced to original 1/2, lauryl amine Dosage is original 1/3, and concentrate grade and the rate of recovery are all significantly improved, and desliming process ratio before, significantly Clay content is reduced, it is less that slot phenomenon is run in flotation.
The structure of ultrasonic wave deslimer used in the present embodiment with embodiment 1, the difference is that, on casing ontology 5 Portion is that cylindrical diameter is 4m, and lower part inverted conical shape bottom cone angle is 50 °
Embodiment 3: the flotation combined desliming process of ultrasonic wave-shaking table-, concrete operations are as follows:
Yunnan weathering titanium ore raw ore clay content 21% preselects desliming using cyclone, and clay content is still greater than 6%, after desliming Flotation is carried out using hydroximic acid collecting agent, obtains Ti grade 33.70% in ilmenite concentrate, the rate of recovery 66.83%.
Using the flotation combined desliming process of ultrasonic wave-shaking table-of the present invention, process flow is as shown in Figure 1, by Guangxi The raw ore of certain lead-zinc carries out predictive desliming, and the raw ore that concentration is 25% is removed one by ultrasonic wave deslimer first Divide sludge, tail is directly thrown in the overflow of ultrasonic wave deslimer, and the sand setting of ultrasonic wave deslimer carries out sorting desliming, shaking table using shaking table Concentrate directly throws tail as material after qualified desliming, shaking table tailing, and shaking table chats is added foaming agent 2#Oily 90g/t, then Flotation desliming is carried out using agitator again after mixing evenly, flotation froth is that thin mud directly throws tail, and floatation underflow is after desliming Material, the product clay content after desliming is 1% hereinafter, carrying out flotation using hydroximic acid collecting agent after desliming, collector dosage is not When change, Ti grade 39.20% in ilmenite concentrate, the rate of recovery 83.65% are obtained, ilmenite concentrate grade and the rate of recovery have all obtained significantly mentioning It is high.
The structure of ultrasonic wave deslimer used in the present embodiment with embodiment 1, the difference is that, on casing ontology 5 Portion's cylinder diameter is 5m, and lower part is inverted conical shape, and bottom cone angle is 70 °.

Claims (3)

1. a kind of flotation combined desliming process of ultrasonic wave-shaking table-, which comprises the following steps:
Raw ore material is removed into a part of sludge by ultrasonic wave deslimer first, tail is directly thrown in the overflow of ultrasonic wave deslimer, The sand setting of ultrasonic wave deslimer carries out sorting desliming using shaking table, and table concentrate is as material after qualified desliming, shaking table tailing Tail is directly thrown, foaming agent is added to shaking table chats, flotation desliming, flotation froth is then carried out using agitator again after mixing evenly Tail is directly thrown, floatation underflow is the material after desliming, and the ultrasonic wave deslimer includes mineral-feeding pipe (1), to mine spray head (2), whole Flowing plate (3), ultrasonic probe (4), casing ontology (5), overflow launder (6), overflow port (7), conducting wire (8), ultrasonic wave control cabinet (9), it adds water pipe (10), high-pressure water pipe (11), sand sinking port switch (12), sand sinking port (13), rectify board mount (14) and to mine Pipe holder (15);
Casing ontology (5) top is cylinder, and lower part is inverted conical shape, and the over top of casing ontology (5) is equipped with overflow launder (6), the lowest part of overflow launder (6) is equipped with overflow port (7), and mineral-feeding pipe (1) is fixed on casing ontology by mineral-feeding pipe bracket (15) (5) top center, the lower end of mineral-feeding pipe (1), which is installed, gives mine spray head (2), is located in casing ontology (5) to mine spray head (2), casing It is equipped with upper layer and lower layer cowling panel layer in ontology (5), has more than one rectification board mount (14) on each layer of cowling panel layer, it is each A rectification board mount (14) is equipped with more than one cowling panel (3), is equipped with ultrasonic probe (4) between two layers of cowling panel layer, Ultrasonic probe (4) is connect by conducting wire (8) with external ultrasonic wave control cabinet (9), more than one to add water pipe (10) peace It mounted in casing ontology (5) side, and is connect with external water source, is equipped with sand sinking port (13) in casing ontology (5) bottom, sand sinking port (13) top is equipped with sand sinking port switch (12), and high-pressure water pipe (11) is mounted on sand sinking port (13) side, and connect with external water source.
2. the flotation combined desliming process of ultrasonic wave-shaking table-according to claim 1, it is characterised in that: the ultrasonic wave is de- The bottom cone angle of the inverted conical shape of mud machine is 20 ~ 70 °, and the diameter of ultrasonic wave deslimer upper cylindrical is 0.3 ~ 5m.
3. the flotation combined desliming process of ultrasonic wave-shaking table-according to claim 1, it is characterised in that: raw ore material it is dense Degree is 10% ~ 40%.
CN201710887342.3A 2017-09-27 2017-09-27 A kind of flotation combined desliming process of ultrasonic wave-shaking table- Active CN107694744B (en)

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CN109054464B (en) * 2018-08-20 2020-11-06 西安科技大学 Physical deashing process for tire cracking carbon black
CN110227682A (en) * 2019-05-29 2019-09-13 安徽理工大学 Ultrasonic wave desliming device before a kind of coal slime flotation
CN114054200B (en) * 2021-11-18 2022-09-02 长沙矿山研究院有限责任公司 Zinc oxide flotation recovery method based on gravity-flotation combined pre-desliming

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