CN107674759A - A kind of plant medicinal liquid extraction and Activated Carbon Production process equipment and technique - Google Patents

A kind of plant medicinal liquid extraction and Activated Carbon Production process equipment and technique Download PDF

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Publication number
CN107674759A
CN107674759A CN201711057366.2A CN201711057366A CN107674759A CN 107674759 A CN107674759 A CN 107674759A CN 201711057366 A CN201711057366 A CN 201711057366A CN 107674759 A CN107674759 A CN 107674759A
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stifling
activated carbon
gasification burner
gas
condenser
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关玉明
韩梦琪
陈浩然
钱丹
王骁
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Chengde Bao Biotechnology Co Ltd
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Chengde Bao Biotechnology Co Ltd
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Priority to CN201711057366.2A priority Critical patent/CN107674759A/en
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/12Production of fats or fatty oils from raw materials by melting out
    • C11B1/16Production of fats or fatty oils from raw materials by melting out with steam

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Carbon And Carbon Compounds (AREA)

Abstract

The invention discloses a kind of extraction of plant medicinal liquid and Activated Carbon Production process equipment and technique.The equipment includes fruit stone stifling vaporization extraction system, activated carbon production system and activated carbon system of processing;The stifling vaporization extraction system of the fruit stone includes raw material cabin, the first helical feeder, stifling gasification burner, intermediate bin, the first condenser, the first cooling-water machine, the first pump, medicine original fluid container and the first blower fan;The activated carbon production system includes the second helical feeder, activation furnace, the second blower fan, the 3rd blower fan, steam oven, the second condenser, the second cooling-water machine, the second pump and secondary medicine stoste and filled.The technique prepares fractional oil of haw kernel co-production activated carbon by raw material of Chinese hawthorn seed, realizes the comprehensive utilization of resource, avoids only focusing on production single product and ignoring the economic value of byproduct.Heat is provided in caused fuel gas circulating involuting system during Chinese hawthorn seed is pyrolyzed, the saving of raw material resources is realized, reduces the pollution to environment.

Description

A kind of plant medicinal liquid extraction and Activated Carbon Production process equipment and technique
Technical field
The invention belongs to edible fruit stone processing technique field, specifically a kind of plant medicinal liquid extraction is processed with Activated Carbon Production Equipment and technique.
Background technology
Fruit stone is wrapped in the duricrust part of seed as fruit center, there is abundant resource in China, but various fruits Pile up like a mountain for the cannery in the place of production or the fruit stone of fruit wine factory, there is no and is developed and utilized, and substantial amounts of fruit stone is as useless Thing processing, causes the pollution of environment.Modern science and technology method has confirmed there is good antibacterial from the juice of fruit stone extraction, kills The effect of bacterium and sterilization, and medical and health, food processing and each field of environmental protection are had been widely used for, such as the mountain by purification Short, bristly hair or beard core evaporates oil and is configured to ointment and creme, and treating the illnesss such as eczema, neurodermatitis, burn has the effect of obvious, while it is right Nine kinds of bacteriums such as Escherichia coli have obvious inhibitory action.In addition, Chinese hawthorn seed uses directly as Chinese medicine, hernia can be treated The diseases such as gas, difficult labour.
The utilization of Chinese hawthorn seed at present is mostly that Chinese hawthorn seed is placed in reactor, isolation air heating, with the rising of temperature Flue gas spilling is had, Chinese hawthorn seed fraction can be obtained by by condenser condensation, remaining solid thing is rough Chinese hawthorn seed charcoal.Application Numbers 201320817197.9 disclose a kind of activation fluidized bed furnace for producing activated carbon, and it is by activation furnace body and auxiliary device group Into activation furnace body includes burner hearth, heat-insulation layer, air inlet pipe, charging aperture, discharging opening, thermometer hole and peep hole.It uses gaseous mixture Body stirs the material in stove so that material can be stirred equably, fully contacted at high temperature with vapor, ensure activation Uniformly.The device uses single process, extracts single material, produces single product, without reference to raw material and product Coproduction and comprehensive utilization of resources, sufficiently complete process system is not formed using raw material, it is impossible to comprehensively utilize and make Cost improves.
The content of the invention
In view of the shortcomings of the prior art, the technical problem that the present invention intends to solve is to provide a kind of plant medicinal liquid extraction and lived Property charcoal manufacturing and processing equipment and technique.The technique prepares fractional oil of haw kernel co-production activated carbon by raw material of Chinese hawthorn seed, realizes The comprehensive utilization of resource, avoid only focusing on production single product and ignoring the economic value of byproduct.In the mistake of Chinese hawthorn seed pyrolysis Heat is provided in caused fuel gas circulating involuting system in journey, realizes the saving of raw material resources, reduces the dirt to environment Dye.
The present invention solves the problems, such as that the technical scheme of the equipment and technology is to provide a kind of plant medicinal liquid extraction and given birth to activated carbon Produce process equipment, including activated carbon system of processing, it is characterised in that the equipment also includes the stifling vaporization extraction system of fruit stone and work Property charcoal production system;The fruit stone stifling vaporization extraction system, activated carbon production system and activated carbon system of processing are sequentially connected;
The stifling vaporization extraction system of the fruit stone include raw material cabin, the first helical feeder, stifling gasification burner, intermediate bin, First condenser, the first cooling-water machine, the first pump, medicine original fluid container and the first blower fan;The raw material cabin and the first helical feeder One end connects;The other end of first helical feeder is connected with the material inlet of stifling gasification burner;The stifling vaporization The gas entry of stove is connected with extraneous gas pipeline;The discharging opening of the stifling gasification burner is connected with intermediate bin;It is described smoked The evaporation exhanst gas outlet for steaming gasification burner is connected by pipeline with the condensation tube inlet of the first condenser;First condenser it is cold Condensate outlet is connected with the first cooling-water machine;First cooling-water machine is connected by the condensing water inlet of the first pump and the first condenser Connect;The condenser pipe outlet of first condenser is connected by pipeline with medicine original fluid container;The condenser pipe of first condenser goes out The side wall of mouth vertical pipeline is connected by the first blower fan with the gas returning port of stifling gasification burner;
The activated carbon production system include the second helical feeder, activation furnace, the second blower fan, the 3rd blower fan, steam oven, Second condenser, the second cooling-water machine, the second pump and secondary medicine stoste fill;One end of second helical feeder connects with intermediate bin Connect, the material inlet connection of the other end and activation furnace;The gas entry of the activation furnace is connected with extraneous gas pipeline; The steam entry of the activation furnace is connected by pipeline with extraneous oxygen and steam oven, and the second blower fan is provided with pipeline;Institute The gas outlet side for stating activation furnace is connected by pipeline and activation air valve with the 3rd blower fan, and the gas outlet opposite side of activation furnace passes through Pipeline and evaporation smoke valve are connected with the condensation tube inlet of the second condenser;The gas returning port of 3rd blower fan and stifling gasification burner Connection;The condensation-water drain of second condenser is connected with the second cooling-water machine;Second cooling-water machine passes through the second pump and The condensing water inlet connection of two condensers;The condenser pipe outlet of second condenser passes through vertical pipeline and secondary medicine original fluid container Connection.
The present invention solves the problems, such as that the technical scheme of the technology is to provide a kind of plant medicinal liquid extraction and given birth to activated carbon Produce processing technology, it is characterised in that the technique comprises the following steps:
The first step, hawthorn nuclear fuel material is added in raw material cabin;Open the original of the first helical feeder and stifling gasification burner Expect charging aperture, by Chinese hawthorn seed feedstock transportation to fumigating in gasification burner, the evaporation that the volume of hawthorn nuclear fuel material is accounted in stifling gasification burner The 1/2-4/5 of the volume of tank;Close the first helical feeder;
Second step, the stifling vaporization extraction system work of fruit stone, activated carbon production system and activated carbon system of processing are closed;Will The material inlet of stifling gasification burner is closed, and evaporation exhanst gas outlet is opened;Gas entry is opened, firing up, makes steam stifling Change in-furnace temperature and reach 90 DEG C -350 DEG C;High temperature pyrolysis gas phase product is discharged by evaporating exhanst gas outlet from stifling gasification burner, Enter the condensation tube inlet of the first condenser by pipeline, the first pump, which is opened, makes the first water chiller work;High temperature pyrolysis gas phase is produced Fractional oil of haw kernel stoste and not condensable combustible gas are obtained after thing is condensed, fractional oil of haw kernel stoste instills medicine original along vertical pipeline In flow container, not condensable combustible gas enters the gas returning port of stifling gasification burner in the presence of the first blower fan along pipeline;To steam stifling Change stove uniformly to heat, until vaporization terminates;
3rd step, vaporization open the discharging opening of stifling gasification burner after terminating, and fumigate the rough Chinese hawthorn seed charcoal in gasification burner Into after intermediate bin, immediately pass through the second helical feeder and rough Chinese hawthorn seed charcoal is conveyed into activation furnace;
4th step, activated carbon production system work, the stifling vaporization extraction system of fruit stone and activated carbon system of processing are closed;Will The material inlet of activation furnace is closed, and gas outlet is opened;Gas entry is opened, firing up, reach activation in-furnace temperature 800 DEG C -1100 DEG C, while steam entry is opened, it is passed through 300 DEG C -450 DEG C of superheated vapour;Rough Chinese hawthorn seed charcoal is equal Preceding 1/3 period of even heating total time, evaporation smoke valve is opened, activation air valve is closed, and high temperature pyrolysis gas phase product passes through Pipeline where evaporating smoke valve enters the condensation tube inlet of the second condenser, and the second pump, which is opened, makes the second water chiller work, high temperature Fractional oil of haw kernel stoste and not condensable combustible gas are obtained after pyrolysis gas-phase product is condensed, and fractional oil of haw kernel stoste is along VERTICAL TUBE Road is instilled in secondary medicine original fluid container, and not condensable combustible gas enters returning for stifling gasification burner in the presence of the 3rd blower fan along pipeline Gas port;Rough Chinese hawthorn seed charcoal uniformly heats rear 2/3 period of total time, and activation air valve is opened, and evaporation smoke valve is closed, high Warm solution gas-phase product is discharged from the gas outlet of activation furnace, is entered in the presence of the 3rd blower fan by pipeline where activating air valve The gas returning port of stifling gasification burner;To the uniform heating of rough Chinese hawthorn seed charcoal until material becomes loose, start to switch to kermesinus, and emit Go out a large amount of white cigarettes, activation terminates, and obtains activated carbon.
Compared with prior art, beneficial effect of the present invention is:
(1) present invention co-producing active carbon while fractional oil of haw kernel is produced, realizes the comprehensive utilization of resource, avoids only Focus on production single product and ignore the economic value of byproduct.Chinese hawthorn seed is in the rough Chinese hawthorn seed charcoal base after stifling vaporization Originally original size is maintained, high quality active carbon can be prepared, but in traditional production process, most Chinese hawthorn seed profit A certain specific product is only produced with equipment or is only focused in pyrolytic process in itself, enterprise lacks multi-joint to the progress of whole thermal decomposition products The technology and system of comprehensive utilization are produced, the effective means for preparing activated carbon are lacked to rough Chinese hawthorn seed charcoal, raw material can only be used as It is outer at a low price to be sold to activated carbon factory, have a strong impact on the high value added utilization of charcoal.
(2) this technique is anti-with caused not condensable combustible gas and activation in production process during product is produced Should the combustible gas such as gas be heating raw material, make use of the calorific value of pyrolysis gas to the utmost, effectively improve the thermal efficiency of system, drop The low consumption in high-grade electric energy source, has obvious energy-saving effect.For original whole system, by Chinese hawthorn seed pyrolytic process In caused pyrolysis gas directly empty or burn up, lack the consideration to thermal balance and afterheat utilizing system, not only cause resource With the significant wastage of the energy, and certain pollution is also generated to environment, there are obvious energy-saving and emission-reduction potentiality.
(3) in this technological process, raw material can be made full use of, is disposably produced a variety of suitable for medical and health, food Processing and the product in each field of environmental protection.It is different due to fumigating used time production cycle of gasification burner and activation furnace in process of production, Can arrange in pairs or groups activation furnace multiple stifling gasification burners, also can in a production life cycle same stifling gasification burner come out of the stove it is more Secondary rough Chinese hawthorn seed charcoal, thus can be by controlling the heating-up temperature acquisition of different stifling gasification burners is a variety of to evaporate oily product, example Cut of the temperature in 80 DEG C -108 DEG C is such as controlled to do the raw material of food additives, the cut in 109 DEG C -169 DEG C can With the raw material of the light industrial goods such as perfume (or spice) processed, medicinal raw material can be produced more than 170 DEG C.
(4) material heating charing, the activation in this technique are integral, and traditional method charcoal processing and activation process are point Open, intermediate demand manually shifts, and labor intensity is big, and treatment effeciency is low, and can make rough Chinese hawthorn seed charcoal in transportation Temperature reduces, and needs to reheat when activate in next step, causes the waste of the energy.This equipment does not have motion, structure Simple with technique, continuous type commercial manufacturing equipment flow is complete, and continuity is strong, reliable, energy-conserving and environment-protective.
(5) the stifling gasification burner and activation furnace in this equipment are all conducted heat using external-heat, and furnace gas amount is small, and resistance is low, Self-produced fuel gases calorific value is high.Combustion product gases do not contact directly as heat carrier with raw material, will not be mixed into charing caused by evaporate oil and In water-gas caused by activation section, their calorific value is reduced, and gas circulation amount is little inside and outside stove, can reduce air resistance, Dust-carrying capacity is reduced.
(6) response area of the activation cylinder in this activation furnace is big, can use less mistake with air good mixing Measure air coefficient, the activated gas requirement being suitably lowered into.Activation body of heater is simple in construction, and consumable quantity is low, and heats passage Burning velocity and efficiency are higher than grate furnace, and whole body of heater heat-transfer effect is good.
(7) activation process uses physical method, compares pollution of the chemical zinc chloride activation method to environment and the corruption to equipment Erosion is lower.And chemical zinc chloride activation method easily corrodes because inboard wall of furnace body can contact with zinc chloride, produce plate face concavo-convex Uneven, tilting is even burnt, and causes body of heater service life short, it is necessary to consider the processing of waste gas and waste water and equipment in production process Anticorrosion Problems.
Brief description of the drawings
Fig. 1 is that plant medicinal liquid extraction of the present invention and the equipment of Activated Carbon Production process equipment and a kind of embodiment of technique are overall Structural representation.
Embodiment
The specific embodiment of the present invention is given below.Specific embodiment is only used for that the present invention is further described, unlimited The application scope of the claims processed.
The invention provides a kind of extraction of plant medicinal liquid and Activated Carbon Production process equipment (referring to Fig. 1, abbreviation equipment), bag Include activated carbon system of processing, it is characterised in that the equipment also includes the stifling vaporization extraction system of fruit stone and activated carbon production system; The fruit stone stifling vaporization extraction system, activated carbon production system and activated carbon system of processing are sequentially connected;
The stifling vaporization extraction system of the fruit stone includes raw material cabin 1, the first helical feeder 2, stifling gasification burner 3, centre Storehouse 4, the first condenser 5, the first cooling-water machine 6, the first pump 7, the blower fan 21 of medicine original fluid container 8 and first;The stove of the stifling gasification burner 3 Body selects carbon steel, and high 2 meters, 1 meter of diameter, material thickness is 10-20mm, and bile duct is located at body of heater center, is that the oil stream that evaporates of evaporation enters Position, 16 centimetres of bile duct diameter, air-vent size on bile duct is less than the size of Chinese hawthorn seed (2-3mm) in order to avoid mountain around it Short, bristly hair or beard core enters bile duct, and the body of heater heat resisting temperature for fumigating gasification burner 3 is higher than 350 DEG C, and assigned temperature is realized under the monitoring of each instrument; The number amount and type of first condenser 5 determine according to actual conditions;One end of the helical feeder 2 of raw material cabin 1 and first connects Connect;The other end of first helical feeder 2 is connected with the material inlet of stifling gasification burner 3;The stifling gasification burner 3 Gas entry is connected with extraneous gas pipeline, and the gas entry of coal gas from stifling gasification burner 3 is passed through;The stifling gasification burner 3 discharging opening is connected with intermediate bin 4;The evaporation exhanst gas outlet of the stifling gasification burner 3 passes through the cold of pipeline and the first condenser 5 Solidifying tube inlet connection, the heat resisting temperature of the pipeline are higher than 350 DEG C;The condensation-water drain and the first cold water of first condenser 5 Machine 6 connects;First cooling-water machine 6 is connected by the first pump 7 with the condensing water inlet of the first condenser 5;First condensation The condenser pipe outlet of device 5 is connected by vertical pipeline with medicine original fluid container 8;The condenser pipe outlet VERTICAL TUBE of first condenser 5 The side wall in road is connected by the first blower fan 21 with the gas returning port of stifling gasification burner 3;
The activated carbon production system include the second helical feeder 9, activation furnace 10, the second blower fan 22, the 3rd blower fan 23, Steam oven 11, the second condenser 12, the second cooling-water machine 13, the second pump 14 and secondary medicine stoste fill 15;The stove of the activation furnace 10 Body selects carbon steel, and high 2 meters, 1.4 meters of diameter, the body of heater heat resisting temperature of activation furnace 10 is higher than 1100 DEG C, under the monitoring of each instrument Realize assigned temperature;The number amount and type of second condenser 12 are depending on actual conditions;The one of second helical feeder 9 End is connected with intermediate bin 4, and the other end is connected with the material inlet of activation furnace 10;The gas entry of the activation furnace 10 and the external world Gas pipeline is connected, and the gas entry of coal gas from activation furnace 10 is passed through;The steam entry of the activation furnace 10 passes through pipe Road is connected with extraneous oxygen and steam oven 11, and the second blower fan 22 is provided with pipeline, and the heat resisting temperature of the pipeline is higher than 450 DEG C; The gas outlet side of the activation furnace 10 is connected by pipeline and activation air valve 24 with the 3rd blower fan 23, the gas outlet of activation furnace 10 Opposite side is connected by pipeline and evaporation smoke valve 25 with the condensation tube inlet of the second condenser 12, and the heat resisting temperature of the pipeline is high In 1100 DEG C;3rd blower fan 23 is connected with the gas returning port of stifling gasification burner 3;The condensation-water drain of second condenser 12 It is connected with the second cooling-water machine 13;Second cooling-water machine 13 is connected by the condensing water inlet of the second pump 14 and the second condenser 12 Connect;The condenser pipe outlet of second condenser 12 is connected by vertical pipeline with secondary medicine original fluid container 15;
The activated carbon system of processing includes cooler 16, pulverizer 17, screening machine 18, type extruder 19 and packaging shaping Machine 20;The pulverizer 16 is connected with the activated carbon discharging opening of activation furnace 10 by pipeline;The cooler 16 and pulverizer 17 Connection;The pulverizer 17 is connected with screening machine 18;The screening machine 18 is connected with type extruder 19;The type extruder 19 with Packaging forming machine 20 connects.
Invention also provides a kind of extraction of plant medicinal liquid and Activated Carbon Production processing technology (abbreviation technique), its feature It is that the technique comprises the following steps:
The first step, it will be added to by the hawthorn nuclear fuel material for removing sandstone impurity and simple selection processing in raw material cabin 1;Beat The material inlet of the first helical feeder 2 and stifling gasification burner 3 is opened, by Chinese hawthorn seed feedstock transportation to stifling gasification burner 3, mountain The 1/2-4/5 of the volume for the evaporator that the volume of short, bristly hair or beard nuclear fuel material is accounted in stifling gasification burner 3;Close the first helical feeder 2;
Second step, the stifling vaporization extraction system work of fruit stone, activated carbon production system and activated carbon system of processing are closed;Will The material inlet of stifling gasification burner 3 is closed, and evaporation exhanst gas outlet is opened;Gas entry is opened, firing up, makes steam stifling The evaporator temperature changed in stove 3 reaches 90 DEG C -350 DEG C;High temperature pyrolysis gas phase product is by evaporating exhanst gas outlet from stifling vaporization Discharged in stove 3, the condensation tube inlet of the first condenser 5 is entered by pipeline, the first pump 7, which is opened, makes the first water chiller 6 work;It is high Product liquid fractional oil of haw kernel stoste and not condensable combustible gas are obtained after warm solution gas-phase product is condensed, fractional oil of haw kernel is former Liquid is instilled in medicine original fluid container 8 along vertical pipeline, and not condensable combustible gas enters stifling in the presence of the first blower fan 21 along pipeline The gas returning port of gasification burner 3;Stifling gasification burner 3 can uniformly be heated 70-350 minutes, the heat time with body of heater size, process raw material Depending on amount and concrete condition, until vaporization terminates;
3rd step, vaporization terminate afterwards directly to open the discharging opening of stifling gasification burner 3, fumigate the rough mountain in gasification burner 3 After short, bristly hair or beard core charcoal enters intermediate bin 4, without waiting for immediately passing through the second helical feeder 9 and rough Chinese hawthorn seed charcoal be conveyed into activation In stove 10, the second helical feeder 9 is the batcher that can bear corresponding material temperature;
4th step, activated carbon production system work, the stifling vaporization extraction system of fruit stone and activated carbon system of processing are closed;Will The material inlet of activation furnace 10 is closed, and gas outlet is opened;Gas entry is opened, firing up, make the work in activation furnace 10 Change cylinder temperature and reach 800 DEG C -1100 DEG C, while steam entry is opened, be passed through 300 DEG C -450 DEG C of superheated vapour;Slightly Chinese hawthorn seed charcoal processed uniformly heats preceding 1/3 period of total time, and evaporation smoke valve 25 is opened, and activation air valve 24 is closed, high temperature Pyrolysis gas-phase product enters the condensation tube inlet of the second condenser 12 by evaporating the place pipeline of smoke valve 25, and the second pump 14 is opened The second water chiller 13 is worked, product liquid fractional oil of haw kernel stoste and can not be cold is obtained after high temperature pyrolysis gas phase product is condensed Solidifying combustible gas, fractional oil of haw kernel stoste are instilled in secondary medicine original fluid container 15 along vertical pipeline, and not condensable combustible gas is in the 3rd wind Enter the gas returning port of stifling gasification burner 3 in the presence of machine 23 along pipeline;When rough Chinese hawthorn seed charcoal uniformly heats rear the 2/3 of total time Between section, activation air valve 24 is opened, evaporation smoke valve 25 is closed, and high temperature pyrolysis gas phase product is arranged from the gas outlet of activation furnace 10 Go out, enter the gas returning port of stifling gasification burner 3 by activating the place pipeline of air valve 24 in the presence of the 3rd blower fan 23;To rough mountain It is 3-10 hours that short, bristly hair or beard core charcoal, which uniformly heats total time, depending on the heat time is with body of heater size, the amount of processing raw material and concrete condition, directly Become loose to material, start to switch to kermesinus, and a large amount of white cigarettes of emerging, activation terminate, and obtain activated carbon;
5th step, the activated carbon discharging opening of activation furnace 10 is opened, activated carbon pass sequentially through cooler 16, pulverizer 17, Screening machine 18, type extruder 19 and packaging forming machine 20, active carbon finished products machine.
Embodiment
A kind of plant medicinal liquid extraction and Activated Carbon Production processing technology, it is characterised in that the technique comprises the following steps:
The first step, it will be added to by the hawthorn nuclear fuel material for removing sandstone impurity and simple selection processing in raw material cabin 1;Beat The material inlet of the first helical feeder 2 and stifling gasification burner 3 is opened, by Chinese hawthorn seed feedstock transportation to stifling gasification burner 3, mountain The 1/2 of the volume for the evaporator that the volume of short, bristly hair or beard nuclear fuel material is accounted in stifling gasification burner 3;Close the first helical feeder 2;
Second step, the stifling vaporization extraction system work of fruit stone, activated carbon production system and activated carbon system of processing are closed;Will The material inlet of stifling gasification burner 3 is closed, and evaporation exhanst gas outlet is opened;Gas entry is opened, firing up, makes steam stifling The evaporator temperature changed in stove 3 reaches 180 DEG C;High temperature pyrolysis gas phase product is by evaporating exhanst gas outlet from stifling gasification burner 3 Discharge, the condensation tube inlet of the first condenser 5 is entered by pipeline, the first pump 7, which is opened, makes the first water chiller 6 work;High warm Product liquid fractional oil of haw kernel stoste and not condensable combustible gas, fractional oil of haw kernel stoste edge are obtained after solution gas-phase product is condensed Vertical pipeline is instilled in medicine original fluid container 8, and not condensable combustible gas enters stifling vaporization in the presence of the first blower fan 21 along pipeline The gas returning port of stove 3;Stifling gasification burner 3 can uniformly be heated 240 minutes, the heat time is with body of heater size, the amount of processing raw material and tool Depending on body situation, until vaporization terminates;
3rd step, vaporization terminate afterwards directly to open the discharging opening of stifling gasification burner 3, fumigate the rough mountain in gasification burner 3 After short, bristly hair or beard core charcoal enters intermediate bin 4, without waiting for immediately passing through the second helical feeder 9 and rough Chinese hawthorn seed charcoal be conveyed into activation In stove 10, the second helical feeder 9 is the batcher that can bear corresponding material temperature;
4th step, activated carbon production system work, the stifling vaporization extraction system of fruit stone and activated carbon system of processing are closed;Will The material inlet of activation furnace 10 is closed, and gas outlet is opened;Gas entry is opened, firing up, make the work in activation furnace 10 Change cylinder temperature and reach 850 DEG C, while steam entry is opened, be passed through 300 DEG C of superheated vapour;First 140 minutes will evaporation Smoke valve 25 is opened, and activation air valve 24 is closed, and high temperature pyrolysis gas phase product is by evaporating the place pipeline of smoke valve 25 into second The condensation tube inlet of condenser 12, the second pump 14, which is opened, makes the second water chiller 13 work, after high temperature pyrolysis gas phase product is condensed Product liquid fractional oil of haw kernel stoste and not condensable combustible gas are obtained, fractional oil of haw kernel stoste instills secondary medicine along vertical pipeline In original fluid container 15, not condensable combustible gas enters the gas returning port of stifling gasification burner 3 in the presence of the 3rd blower fan 23 along pipeline;Afterwards Activation air valve 24 was opened in 280 minutes, evaporation smoke valve 25 is closed, and high temperature pyrolysis gas phase product is arranged from the gas outlet of activation furnace 10 Go out, enter the gas returning port of stifling gasification burner 3 by activating the place pipeline of air valve 24 in the presence of the 3rd blower fan 23;To rough mountain Short, bristly hair or beard core charcoal uniformly heated total time as 7 hours, depending on the heat time is with body of heater size, the amount of processing raw material and concrete condition, until Material becomes loose, starts to switch to kermesinus, and a large amount of white cigarettes of emerging, activation terminate;
5th step, the activated carbon discharging opening of activation furnace 10 is opened, activated carbon pass sequentially through cooler 16, pulverizer 17, Screening machine 18, type extruder 19 and packaging forming machine 20, active carbon finished products machine.
The present invention does not address part and is applied to prior art.

Claims (7)

1. a kind of plant medicinal liquid extraction and Activated Carbon Production process equipment, including activated carbon system of processing, it is characterised in that this sets It is standby also to include the stifling vaporization extraction system of fruit stone and activated carbon production system;The stifling vaporization extraction system of the fruit stone, activated carbon Production system and activated carbon system of processing are sequentially connected;
The stifling vaporization extraction system of the fruit stone includes raw material cabin, the first helical feeder, stifling gasification burner, intermediate bin, first Condenser, the first cooling-water machine, the first pump, medicine original fluid container and the first blower fan;One end of the raw material cabin and the first helical feeder Connection;The other end of first helical feeder is connected with the material inlet of stifling gasification burner;The stifling gasification burner Gas entry is connected with extraneous gas pipeline;The discharging opening of the stifling gasification burner is connected with intermediate bin;The steam stifling The evaporation exhanst gas outlet for changing stove is connected by pipeline with the condensation tube inlet of the first condenser;The condensed water of first condenser Outlet is connected with the first cooling-water machine;First cooling-water machine is connected by the first pump with the condensing water inlet of the first condenser;Institute The condenser pipe outlet for stating the first condenser is connected by pipeline with medicine original fluid container;The condenser pipe outlet of first condenser is vertical The side wall of pipeline is connected by the first blower fan with the gas returning port of stifling gasification burner;
The activated carbon production system includes the second helical feeder, activation furnace, the second blower fan, the 3rd blower fan, steam oven, second Condenser, the second cooling-water machine, the second pump and secondary medicine stoste fill;One end of second helical feeder is connected with intermediate bin, The material inlet of the other end and activation furnace connects;The gas entry of the activation furnace is connected with extraneous gas pipeline;Institute The steam entry for stating activation furnace is connected by pipeline with extraneous oxygen and steam oven, and the second blower fan is provided with pipeline;It is described The gas outlet side of activation furnace is connected by pipeline and activation air valve with the 3rd blower fan, and the gas outlet opposite side of activation furnace passes through pipe Road and evaporation smoke valve are connected with the condensation tube inlet of the second condenser;The gas returning port of 3rd blower fan and stifling gasification burner connects Connect;The condensation-water drain of second condenser is connected with the second cooling-water machine;Second cooling-water machine passes through the second pump and second The condensing water inlet connection of condenser;The condenser pipe outlet of second condenser is connected by vertical pipeline and secondary medicine original fluid container Connect.
2. plant medicinal liquid extraction according to claim 1 and Activated Carbon Production process equipment, it is characterised in that the activity Charcoal system of processing includes cooler, pulverizer, screening machine, type extruder and packaging forming machine;The pulverizer and activation furnace Activated carbon discharging opening is connected by pipeline;The cooler is connected with pulverizer;The pulverizer is connected with screening machine;The sieve Machine is selected to be connected with type extruder;The type extruder is connected with packaging forming machine.
3. plant medicinal liquid extraction according to claim 1 and Activated Carbon Production process equipment, it is characterised in that described stifling The body of heater of gasification burner and the body of heater of activation furnace select carbon steel.
4. a kind of plant medicinal liquid extraction and Activated Carbon Production processing technology, it is characterised in that the technique comprises the following steps:
The first step, hawthorn nuclear fuel material is added in raw material cabin;The raw material for opening the first helical feeder and stifling gasification burner enters Material mouth, by Chinese hawthorn seed feedstock transportation to stifling gasification burner, evaporator that the volume of hawthorn nuclear fuel material is accounted in stifling gasification burner The 1/2-4/5 of volume;Close the first helical feeder;
Second step, the stifling vaporization extraction system work of fruit stone, activated carbon production system and activated carbon system of processing are closed;Will be stifling The material inlet of gasification burner is closed, and evaporation exhanst gas outlet is opened;Gas entry is opened, firing up, make stifling gasification burner Interior temperature reaches 90 DEG C -350 DEG C;High temperature pyrolysis gas phase product is discharged by evaporating exhanst gas outlet from stifling gasification burner, is passed through Pipeline enters the condensation tube inlet of the first condenser, and the first pump, which is opened, makes the first water chiller work;High temperature pyrolysis gas phase product passes through Fractional oil of haw kernel stoste and not condensable combustible gas are obtained after condensation, fractional oil of haw kernel stoste instills medicine original fluid container along vertical pipeline In, not condensable combustible gas enters the gas returning port of stifling gasification burner in the presence of the first blower fan along pipeline;To fumigating gasification burner Uniformly heating, until vaporization terminates;
3rd step, vaporization open the discharging opening of stifling gasification burner after terminating, and the rough Chinese hawthorn seed charcoal fumigated in gasification burner enters After intermediate bin, immediately pass through the second helical feeder and rough Chinese hawthorn seed charcoal is conveyed into activation furnace;
4th step, activated carbon production system work, the stifling vaporization extraction system of fruit stone and activated carbon system of processing are closed;Will activation The material inlet of stove is closed, and gas outlet is opened;Gas entry is opened, firing up, activation in-furnace temperature is reached 800 DEG C -1100 DEG C, while steam entry is opened, it is passed through 300 DEG C -450 DEG C of superheated vapour;Rough Chinese hawthorn seed charcoal uniformly adds Preceding 1/3 period of hot total time, evaporation smoke valve is opened, activation air valve is closed, and high temperature pyrolysis gas phase product passes through evaporation Pipeline where smoke valve enters the condensation tube inlet of the second condenser, and the second pump, which is opened, makes the second water chiller work, high temperature pyrolysis Fractional oil of haw kernel stoste and not condensable combustible gas are obtained after gas-phase product is condensed, fractional oil of haw kernel stoste is dripped along vertical pipeline Enter in secondary medicine original fluid container, not condensable combustible gas enters the return-air of stifling gasification burner in the presence of the 3rd blower fan along pipeline Mouthful;Rough Chinese hawthorn seed charcoal uniformly heats rear 2/3 period of total time, and activation air valve is opened, and evaporation smoke valve is closed, high temperature It is pyrolyzed gas-phase product to discharge from the gas outlet of activation furnace, is entered in the presence of the 3rd blower fan by pipeline where activating air valve and smoked Steam the gas returning port of gasification burner;To the uniform heating of rough Chinese hawthorn seed charcoal until material becomes loose, start to switch to kermesinus, and emerge A large amount of white cigarettes, activation terminate, and obtain activated carbon.
5. plant medicinal liquid extraction according to claim 4 and Activated Carbon Production processing technology, it is characterised in that the technique is also Including the 5th step, the activated carbon discharging opening of activation furnace is opened, activated carbon passes sequentially through cooler, pulverizer, screening machine, type and squeezed Press and packaging forming machine, active carbon finished products machine.
6. plant medicinal liquid extraction according to claim 4 and Activated Carbon Production processing technology, it is characterised in that in second step It it is 70-350 minutes to the stifling gasification burner uniform heat time.
7. plant medicinal liquid extraction according to claim 4 and Activated Carbon Production processing technology, it is characterised in that in the 4th step It is 3-10 hours that total time is uniformly heated to rough Chinese hawthorn seed charcoal.
CN201711057366.2A 2017-11-01 2017-11-01 A kind of plant medicinal liquid extraction and Activated Carbon Production process equipment and technique Pending CN107674759A (en)

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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1094915A (en) * 1993-05-11 1994-11-16 辽宁大学 With the Semen Crataegi is the processing method of feedstock production beverage, oil plant and gac
CN1275346A (en) * 2000-06-16 2000-12-06 石易 Method and equipment for destructive distillation of haw kernel to extract juice
JP2005015749A (en) * 2003-06-25 2005-01-20 Etsuo Kobayashi Carbonization tar fixation system, woody tar fixed material and its production method, and also pyroligneous acid and its production method
CN103274399A (en) * 2013-05-07 2013-09-04 韩城市金太阳花椒油脂药料有限责任公司 Method for producing active carbon by pyrolysing pepper branches
CN107022364A (en) * 2017-05-10 2017-08-08 河南省科学院能源研究所有限公司 Biomass pyrogenation gasification power generating simultaneously activated carbon process and key equipment
CN107032351A (en) * 2017-05-27 2017-08-11 山东大学 The device and method of smoke solution co-production activated carbon is produced in a kind of Chinese hawthorn seed pyrolysis
CN207227373U (en) * 2017-11-01 2018-04-13 承德本多宝生物科技有限公司 A kind of plant medicinal liquid extraction and Activated Carbon Production process equipment

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1094915A (en) * 1993-05-11 1994-11-16 辽宁大学 With the Semen Crataegi is the processing method of feedstock production beverage, oil plant and gac
CN1275346A (en) * 2000-06-16 2000-12-06 石易 Method and equipment for destructive distillation of haw kernel to extract juice
JP2005015749A (en) * 2003-06-25 2005-01-20 Etsuo Kobayashi Carbonization tar fixation system, woody tar fixed material and its production method, and also pyroligneous acid and its production method
CN103274399A (en) * 2013-05-07 2013-09-04 韩城市金太阳花椒油脂药料有限责任公司 Method for producing active carbon by pyrolysing pepper branches
CN107022364A (en) * 2017-05-10 2017-08-08 河南省科学院能源研究所有限公司 Biomass pyrogenation gasification power generating simultaneously activated carbon process and key equipment
CN107032351A (en) * 2017-05-27 2017-08-11 山东大学 The device and method of smoke solution co-production activated carbon is produced in a kind of Chinese hawthorn seed pyrolysis
CN207227373U (en) * 2017-11-01 2018-04-13 承德本多宝生物科技有限公司 A kind of plant medicinal liquid extraction and Activated Carbon Production process equipment

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Application publication date: 20180209