CN107674759A - A kind of plant medicinal liquid extraction and Activated Carbon Production process equipment and technique - Google Patents
A kind of plant medicinal liquid extraction and Activated Carbon Production process equipment and technique Download PDFInfo
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- CN107674759A CN107674759A CN201711057366.2A CN201711057366A CN107674759A CN 107674759 A CN107674759 A CN 107674759A CN 201711057366 A CN201711057366 A CN 201711057366A CN 107674759 A CN107674759 A CN 107674759A
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- stifling
- activated carbon
- gasification burner
- gas
- condenser
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 139
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 47
- 238000000605 extraction Methods 0.000 title claims abstract description 38
- 238000000034 method Methods 0.000 title claims abstract description 30
- 239000007788 liquid Substances 0.000 title claims abstract description 23
- 230000004913 activation Effects 0.000 claims abstract description 74
- 238000002309 gasification Methods 0.000 claims abstract description 72
- 235000008440 Crataegus cuneata Nutrition 0.000 claims abstract description 36
- 241000657480 Crataegus pinnatifida Species 0.000 claims abstract description 36
- 235000014283 Crataegus pinnatifida var major Nutrition 0.000 claims abstract description 36
- 238000012545 processing Methods 0.000 claims abstract description 36
- 238000009834 vaporization Methods 0.000 claims abstract description 31
- 230000008016 vaporization Effects 0.000 claims abstract description 31
- 239000002994 raw material Substances 0.000 claims abstract description 29
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 25
- 239000004575 stone Substances 0.000 claims abstract description 24
- 239000003814 drug Substances 0.000 claims abstract description 23
- 239000000498 cooling water Substances 0.000 claims abstract description 19
- 241000196324 Embryophyta Species 0.000 claims abstract description 17
- 239000012530 fluid Substances 0.000 claims abstract description 17
- 239000007789 gas Substances 0.000 claims description 104
- 239000000463 material Substances 0.000 claims description 36
- 239000003610 charcoal Substances 0.000 claims description 29
- 238000001704 evaporation Methods 0.000 claims description 28
- 230000008020 evaporation Effects 0.000 claims description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- 238000000197 pyrolysis Methods 0.000 claims description 19
- 238000009833 condensation Methods 0.000 claims description 16
- 230000005494 condensation Effects 0.000 claims description 16
- 239000000779 smoke Substances 0.000 claims description 15
- 238000007599 discharging Methods 0.000 claims description 13
- 238000005516 engineering process Methods 0.000 claims description 12
- 238000010304 firing Methods 0.000 claims description 8
- 239000003758 nuclear fuel Substances 0.000 claims description 8
- 238000012216 screening Methods 0.000 claims description 8
- 238000010438 heat treatment Methods 0.000 claims description 7
- 238000004806 packaging method and process Methods 0.000 claims description 7
- 241001092040 Crataegus Species 0.000 claims description 6
- 235000009917 Crataegus X brevipes Nutrition 0.000 claims description 6
- 235000013204 Crataegus X haemacarpa Nutrition 0.000 claims description 6
- 235000009685 Crataegus X maligna Nutrition 0.000 claims description 6
- 235000009444 Crataegus X rubrocarnea Nutrition 0.000 claims description 6
- 235000009486 Crataegus bullatus Nutrition 0.000 claims description 6
- 235000017181 Crataegus chrysocarpa Nutrition 0.000 claims description 6
- 235000009682 Crataegus limnophila Nutrition 0.000 claims description 6
- 235000004423 Crataegus monogyna Nutrition 0.000 claims description 6
- 235000002313 Crataegus paludosa Nutrition 0.000 claims description 6
- 235000009840 Crataegus x incaedua Nutrition 0.000 claims description 6
- 229910052799 carbon Inorganic materials 0.000 claims description 5
- 230000000694 effects Effects 0.000 claims description 5
- 230000003213 activating effect Effects 0.000 claims description 4
- 235000019504 cigarettes Nutrition 0.000 claims description 4
- 229910000975 Carbon steel Inorganic materials 0.000 claims description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 3
- 239000010962 carbon steel Substances 0.000 claims description 3
- 229910052760 oxygen Inorganic materials 0.000 claims description 3
- 239000001301 oxygen Substances 0.000 claims description 3
- 239000000047 product Substances 0.000 abstract description 31
- 239000006227 byproduct Substances 0.000 abstract description 3
- 239000002737 fuel gas Substances 0.000 abstract description 3
- 238000001994 activation Methods 0.000 description 58
- 230000008569 process Effects 0.000 description 8
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 description 6
- 210000000013 bile duct Anatomy 0.000 description 4
- 108010066057 cabin-1 Proteins 0.000 description 4
- 230000008859 change Effects 0.000 description 4
- 235000005074 zinc chloride Nutrition 0.000 description 3
- 239000011592 zinc chloride Substances 0.000 description 3
- 241000894006 Bacteria Species 0.000 description 2
- 239000003034 coal gas Substances 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 238000012544 monitoring process Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 201000004624 Dermatitis Diseases 0.000 description 1
- 241000588724 Escherichia coli Species 0.000 description 1
- 206010019909 Hernia Diseases 0.000 description 1
- 201000009053 Neurodermatitis Diseases 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 208000010668 atopic eczema Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000012777 commercial manufacturing Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000019990 fruit wine Nutrition 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 239000008246 gaseous mixture Substances 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000002674 ointment Substances 0.000 description 1
- 244000144985 peep Species 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 239000002912 waste gas Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/12—Production of fats or fatty oils from raw materials by melting out
- C11B1/16—Production of fats or fatty oils from raw materials by melting out with steam
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Carbon And Carbon Compounds (AREA)
Abstract
The invention discloses a kind of extraction of plant medicinal liquid and Activated Carbon Production process equipment and technique.The equipment includes fruit stone stifling vaporization extraction system, activated carbon production system and activated carbon system of processing;The stifling vaporization extraction system of the fruit stone includes raw material cabin, the first helical feeder, stifling gasification burner, intermediate bin, the first condenser, the first cooling-water machine, the first pump, medicine original fluid container and the first blower fan;The activated carbon production system includes the second helical feeder, activation furnace, the second blower fan, the 3rd blower fan, steam oven, the second condenser, the second cooling-water machine, the second pump and secondary medicine stoste and filled.The technique prepares fractional oil of haw kernel co-production activated carbon by raw material of Chinese hawthorn seed, realizes the comprehensive utilization of resource, avoids only focusing on production single product and ignoring the economic value of byproduct.Heat is provided in caused fuel gas circulating involuting system during Chinese hawthorn seed is pyrolyzed, the saving of raw material resources is realized, reduces the pollution to environment.
Description
Technical field
The invention belongs to edible fruit stone processing technique field, specifically a kind of plant medicinal liquid extraction is processed with Activated Carbon Production
Equipment and technique.
Background technology
Fruit stone is wrapped in the duricrust part of seed as fruit center, there is abundant resource in China, but various fruits
Pile up like a mountain for the cannery in the place of production or the fruit stone of fruit wine factory, there is no and is developed and utilized, and substantial amounts of fruit stone is as useless
Thing processing, causes the pollution of environment.Modern science and technology method has confirmed there is good antibacterial from the juice of fruit stone extraction, kills
The effect of bacterium and sterilization, and medical and health, food processing and each field of environmental protection are had been widely used for, such as the mountain by purification
Short, bristly hair or beard core evaporates oil and is configured to ointment and creme, and treating the illnesss such as eczema, neurodermatitis, burn has the effect of obvious, while it is right
Nine kinds of bacteriums such as Escherichia coli have obvious inhibitory action.In addition, Chinese hawthorn seed uses directly as Chinese medicine, hernia can be treated
The diseases such as gas, difficult labour.
The utilization of Chinese hawthorn seed at present is mostly that Chinese hawthorn seed is placed in reactor, isolation air heating, with the rising of temperature
Flue gas spilling is had, Chinese hawthorn seed fraction can be obtained by by condenser condensation, remaining solid thing is rough Chinese hawthorn seed charcoal.Application
Numbers 201320817197.9 disclose a kind of activation fluidized bed furnace for producing activated carbon, and it is by activation furnace body and auxiliary device group
Into activation furnace body includes burner hearth, heat-insulation layer, air inlet pipe, charging aperture, discharging opening, thermometer hole and peep hole.It uses gaseous mixture
Body stirs the material in stove so that material can be stirred equably, fully contacted at high temperature with vapor, ensure activation
Uniformly.The device uses single process, extracts single material, produces single product, without reference to raw material and product
Coproduction and comprehensive utilization of resources, sufficiently complete process system is not formed using raw material, it is impossible to comprehensively utilize and make
Cost improves.
The content of the invention
In view of the shortcomings of the prior art, the technical problem that the present invention intends to solve is to provide a kind of plant medicinal liquid extraction and lived
Property charcoal manufacturing and processing equipment and technique.The technique prepares fractional oil of haw kernel co-production activated carbon by raw material of Chinese hawthorn seed, realizes
The comprehensive utilization of resource, avoid only focusing on production single product and ignoring the economic value of byproduct.In the mistake of Chinese hawthorn seed pyrolysis
Heat is provided in caused fuel gas circulating involuting system in journey, realizes the saving of raw material resources, reduces the dirt to environment
Dye.
The present invention solves the problems, such as that the technical scheme of the equipment and technology is to provide a kind of plant medicinal liquid extraction and given birth to activated carbon
Produce process equipment, including activated carbon system of processing, it is characterised in that the equipment also includes the stifling vaporization extraction system of fruit stone and work
Property charcoal production system;The fruit stone stifling vaporization extraction system, activated carbon production system and activated carbon system of processing are sequentially connected;
The stifling vaporization extraction system of the fruit stone include raw material cabin, the first helical feeder, stifling gasification burner, intermediate bin,
First condenser, the first cooling-water machine, the first pump, medicine original fluid container and the first blower fan;The raw material cabin and the first helical feeder
One end connects;The other end of first helical feeder is connected with the material inlet of stifling gasification burner;The stifling vaporization
The gas entry of stove is connected with extraneous gas pipeline;The discharging opening of the stifling gasification burner is connected with intermediate bin;It is described smoked
The evaporation exhanst gas outlet for steaming gasification burner is connected by pipeline with the condensation tube inlet of the first condenser;First condenser it is cold
Condensate outlet is connected with the first cooling-water machine;First cooling-water machine is connected by the condensing water inlet of the first pump and the first condenser
Connect;The condenser pipe outlet of first condenser is connected by pipeline with medicine original fluid container;The condenser pipe of first condenser goes out
The side wall of mouth vertical pipeline is connected by the first blower fan with the gas returning port of stifling gasification burner;
The activated carbon production system include the second helical feeder, activation furnace, the second blower fan, the 3rd blower fan, steam oven,
Second condenser, the second cooling-water machine, the second pump and secondary medicine stoste fill;One end of second helical feeder connects with intermediate bin
Connect, the material inlet connection of the other end and activation furnace;The gas entry of the activation furnace is connected with extraneous gas pipeline;
The steam entry of the activation furnace is connected by pipeline with extraneous oxygen and steam oven, and the second blower fan is provided with pipeline;Institute
The gas outlet side for stating activation furnace is connected by pipeline and activation air valve with the 3rd blower fan, and the gas outlet opposite side of activation furnace passes through
Pipeline and evaporation smoke valve are connected with the condensation tube inlet of the second condenser;The gas returning port of 3rd blower fan and stifling gasification burner
Connection;The condensation-water drain of second condenser is connected with the second cooling-water machine;Second cooling-water machine passes through the second pump and
The condensing water inlet connection of two condensers;The condenser pipe outlet of second condenser passes through vertical pipeline and secondary medicine original fluid container
Connection.
The present invention solves the problems, such as that the technical scheme of the technology is to provide a kind of plant medicinal liquid extraction and given birth to activated carbon
Produce processing technology, it is characterised in that the technique comprises the following steps:
The first step, hawthorn nuclear fuel material is added in raw material cabin;Open the original of the first helical feeder and stifling gasification burner
Expect charging aperture, by Chinese hawthorn seed feedstock transportation to fumigating in gasification burner, the evaporation that the volume of hawthorn nuclear fuel material is accounted in stifling gasification burner
The 1/2-4/5 of the volume of tank;Close the first helical feeder;
Second step, the stifling vaporization extraction system work of fruit stone, activated carbon production system and activated carbon system of processing are closed;Will
The material inlet of stifling gasification burner is closed, and evaporation exhanst gas outlet is opened;Gas entry is opened, firing up, makes steam stifling
Change in-furnace temperature and reach 90 DEG C -350 DEG C;High temperature pyrolysis gas phase product is discharged by evaporating exhanst gas outlet from stifling gasification burner,
Enter the condensation tube inlet of the first condenser by pipeline, the first pump, which is opened, makes the first water chiller work;High temperature pyrolysis gas phase is produced
Fractional oil of haw kernel stoste and not condensable combustible gas are obtained after thing is condensed, fractional oil of haw kernel stoste instills medicine original along vertical pipeline
In flow container, not condensable combustible gas enters the gas returning port of stifling gasification burner in the presence of the first blower fan along pipeline;To steam stifling
Change stove uniformly to heat, until vaporization terminates;
3rd step, vaporization open the discharging opening of stifling gasification burner after terminating, and fumigate the rough Chinese hawthorn seed charcoal in gasification burner
Into after intermediate bin, immediately pass through the second helical feeder and rough Chinese hawthorn seed charcoal is conveyed into activation furnace;
4th step, activated carbon production system work, the stifling vaporization extraction system of fruit stone and activated carbon system of processing are closed;Will
The material inlet of activation furnace is closed, and gas outlet is opened;Gas entry is opened, firing up, reach activation in-furnace temperature
800 DEG C -1100 DEG C, while steam entry is opened, it is passed through 300 DEG C -450 DEG C of superheated vapour;Rough Chinese hawthorn seed charcoal is equal
Preceding 1/3 period of even heating total time, evaporation smoke valve is opened, activation air valve is closed, and high temperature pyrolysis gas phase product passes through
Pipeline where evaporating smoke valve enters the condensation tube inlet of the second condenser, and the second pump, which is opened, makes the second water chiller work, high temperature
Fractional oil of haw kernel stoste and not condensable combustible gas are obtained after pyrolysis gas-phase product is condensed, and fractional oil of haw kernel stoste is along VERTICAL TUBE
Road is instilled in secondary medicine original fluid container, and not condensable combustible gas enters returning for stifling gasification burner in the presence of the 3rd blower fan along pipeline
Gas port;Rough Chinese hawthorn seed charcoal uniformly heats rear 2/3 period of total time, and activation air valve is opened, and evaporation smoke valve is closed, high
Warm solution gas-phase product is discharged from the gas outlet of activation furnace, is entered in the presence of the 3rd blower fan by pipeline where activating air valve
The gas returning port of stifling gasification burner;To the uniform heating of rough Chinese hawthorn seed charcoal until material becomes loose, start to switch to kermesinus, and emit
Go out a large amount of white cigarettes, activation terminates, and obtains activated carbon.
Compared with prior art, beneficial effect of the present invention is:
(1) present invention co-producing active carbon while fractional oil of haw kernel is produced, realizes the comprehensive utilization of resource, avoids only
Focus on production single product and ignore the economic value of byproduct.Chinese hawthorn seed is in the rough Chinese hawthorn seed charcoal base after stifling vaporization
Originally original size is maintained, high quality active carbon can be prepared, but in traditional production process, most Chinese hawthorn seed profit
A certain specific product is only produced with equipment or is only focused in pyrolytic process in itself, enterprise lacks multi-joint to the progress of whole thermal decomposition products
The technology and system of comprehensive utilization are produced, the effective means for preparing activated carbon are lacked to rough Chinese hawthorn seed charcoal, raw material can only be used as
It is outer at a low price to be sold to activated carbon factory, have a strong impact on the high value added utilization of charcoal.
(2) this technique is anti-with caused not condensable combustible gas and activation in production process during product is produced
Should the combustible gas such as gas be heating raw material, make use of the calorific value of pyrolysis gas to the utmost, effectively improve the thermal efficiency of system, drop
The low consumption in high-grade electric energy source, has obvious energy-saving effect.For original whole system, by Chinese hawthorn seed pyrolytic process
In caused pyrolysis gas directly empty or burn up, lack the consideration to thermal balance and afterheat utilizing system, not only cause resource
With the significant wastage of the energy, and certain pollution is also generated to environment, there are obvious energy-saving and emission-reduction potentiality.
(3) in this technological process, raw material can be made full use of, is disposably produced a variety of suitable for medical and health, food
Processing and the product in each field of environmental protection.It is different due to fumigating used time production cycle of gasification burner and activation furnace in process of production,
Can arrange in pairs or groups activation furnace multiple stifling gasification burners, also can in a production life cycle same stifling gasification burner come out of the stove it is more
Secondary rough Chinese hawthorn seed charcoal, thus can be by controlling the heating-up temperature acquisition of different stifling gasification burners is a variety of to evaporate oily product, example
Cut of the temperature in 80 DEG C -108 DEG C is such as controlled to do the raw material of food additives, the cut in 109 DEG C -169 DEG C can
With the raw material of the light industrial goods such as perfume (or spice) processed, medicinal raw material can be produced more than 170 DEG C.
(4) material heating charing, the activation in this technique are integral, and traditional method charcoal processing and activation process are point
Open, intermediate demand manually shifts, and labor intensity is big, and treatment effeciency is low, and can make rough Chinese hawthorn seed charcoal in transportation
Temperature reduces, and needs to reheat when activate in next step, causes the waste of the energy.This equipment does not have motion, structure
Simple with technique, continuous type commercial manufacturing equipment flow is complete, and continuity is strong, reliable, energy-conserving and environment-protective.
(5) the stifling gasification burner and activation furnace in this equipment are all conducted heat using external-heat, and furnace gas amount is small, and resistance is low,
Self-produced fuel gases calorific value is high.Combustion product gases do not contact directly as heat carrier with raw material, will not be mixed into charing caused by evaporate oil and
In water-gas caused by activation section, their calorific value is reduced, and gas circulation amount is little inside and outside stove, can reduce air resistance,
Dust-carrying capacity is reduced.
(6) response area of the activation cylinder in this activation furnace is big, can use less mistake with air good mixing
Measure air coefficient, the activated gas requirement being suitably lowered into.Activation body of heater is simple in construction, and consumable quantity is low, and heats passage
Burning velocity and efficiency are higher than grate furnace, and whole body of heater heat-transfer effect is good.
(7) activation process uses physical method, compares pollution of the chemical zinc chloride activation method to environment and the corruption to equipment
Erosion is lower.And chemical zinc chloride activation method easily corrodes because inboard wall of furnace body can contact with zinc chloride, produce plate face concavo-convex
Uneven, tilting is even burnt, and causes body of heater service life short, it is necessary to consider the processing of waste gas and waste water and equipment in production process
Anticorrosion Problems.
Brief description of the drawings
Fig. 1 is that plant medicinal liquid extraction of the present invention and the equipment of Activated Carbon Production process equipment and a kind of embodiment of technique are overall
Structural representation.
Embodiment
The specific embodiment of the present invention is given below.Specific embodiment is only used for that the present invention is further described, unlimited
The application scope of the claims processed.
The invention provides a kind of extraction of plant medicinal liquid and Activated Carbon Production process equipment (referring to Fig. 1, abbreviation equipment), bag
Include activated carbon system of processing, it is characterised in that the equipment also includes the stifling vaporization extraction system of fruit stone and activated carbon production system;
The fruit stone stifling vaporization extraction system, activated carbon production system and activated carbon system of processing are sequentially connected;
The stifling vaporization extraction system of the fruit stone includes raw material cabin 1, the first helical feeder 2, stifling gasification burner 3, centre
Storehouse 4, the first condenser 5, the first cooling-water machine 6, the first pump 7, the blower fan 21 of medicine original fluid container 8 and first;The stove of the stifling gasification burner 3
Body selects carbon steel, and high 2 meters, 1 meter of diameter, material thickness is 10-20mm, and bile duct is located at body of heater center, is that the oil stream that evaporates of evaporation enters
Position, 16 centimetres of bile duct diameter, air-vent size on bile duct is less than the size of Chinese hawthorn seed (2-3mm) in order to avoid mountain around it
Short, bristly hair or beard core enters bile duct, and the body of heater heat resisting temperature for fumigating gasification burner 3 is higher than 350 DEG C, and assigned temperature is realized under the monitoring of each instrument;
The number amount and type of first condenser 5 determine according to actual conditions;One end of the helical feeder 2 of raw material cabin 1 and first connects
Connect;The other end of first helical feeder 2 is connected with the material inlet of stifling gasification burner 3;The stifling gasification burner 3
Gas entry is connected with extraneous gas pipeline, and the gas entry of coal gas from stifling gasification burner 3 is passed through;The stifling gasification burner
3 discharging opening is connected with intermediate bin 4;The evaporation exhanst gas outlet of the stifling gasification burner 3 passes through the cold of pipeline and the first condenser 5
Solidifying tube inlet connection, the heat resisting temperature of the pipeline are higher than 350 DEG C;The condensation-water drain and the first cold water of first condenser 5
Machine 6 connects;First cooling-water machine 6 is connected by the first pump 7 with the condensing water inlet of the first condenser 5;First condensation
The condenser pipe outlet of device 5 is connected by vertical pipeline with medicine original fluid container 8;The condenser pipe outlet VERTICAL TUBE of first condenser 5
The side wall in road is connected by the first blower fan 21 with the gas returning port of stifling gasification burner 3;
The activated carbon production system include the second helical feeder 9, activation furnace 10, the second blower fan 22, the 3rd blower fan 23,
Steam oven 11, the second condenser 12, the second cooling-water machine 13, the second pump 14 and secondary medicine stoste fill 15;The stove of the activation furnace 10
Body selects carbon steel, and high 2 meters, 1.4 meters of diameter, the body of heater heat resisting temperature of activation furnace 10 is higher than 1100 DEG C, under the monitoring of each instrument
Realize assigned temperature;The number amount and type of second condenser 12 are depending on actual conditions;The one of second helical feeder 9
End is connected with intermediate bin 4, and the other end is connected with the material inlet of activation furnace 10;The gas entry of the activation furnace 10 and the external world
Gas pipeline is connected, and the gas entry of coal gas from activation furnace 10 is passed through;The steam entry of the activation furnace 10 passes through pipe
Road is connected with extraneous oxygen and steam oven 11, and the second blower fan 22 is provided with pipeline, and the heat resisting temperature of the pipeline is higher than 450 DEG C;
The gas outlet side of the activation furnace 10 is connected by pipeline and activation air valve 24 with the 3rd blower fan 23, the gas outlet of activation furnace 10
Opposite side is connected by pipeline and evaporation smoke valve 25 with the condensation tube inlet of the second condenser 12, and the heat resisting temperature of the pipeline is high
In 1100 DEG C;3rd blower fan 23 is connected with the gas returning port of stifling gasification burner 3;The condensation-water drain of second condenser 12
It is connected with the second cooling-water machine 13;Second cooling-water machine 13 is connected by the condensing water inlet of the second pump 14 and the second condenser 12
Connect;The condenser pipe outlet of second condenser 12 is connected by vertical pipeline with secondary medicine original fluid container 15;
The activated carbon system of processing includes cooler 16, pulverizer 17, screening machine 18, type extruder 19 and packaging shaping
Machine 20;The pulverizer 16 is connected with the activated carbon discharging opening of activation furnace 10 by pipeline;The cooler 16 and pulverizer 17
Connection;The pulverizer 17 is connected with screening machine 18;The screening machine 18 is connected with type extruder 19;The type extruder 19 with
Packaging forming machine 20 connects.
Invention also provides a kind of extraction of plant medicinal liquid and Activated Carbon Production processing technology (abbreviation technique), its feature
It is that the technique comprises the following steps:
The first step, it will be added to by the hawthorn nuclear fuel material for removing sandstone impurity and simple selection processing in raw material cabin 1;Beat
The material inlet of the first helical feeder 2 and stifling gasification burner 3 is opened, by Chinese hawthorn seed feedstock transportation to stifling gasification burner 3, mountain
The 1/2-4/5 of the volume for the evaporator that the volume of short, bristly hair or beard nuclear fuel material is accounted in stifling gasification burner 3;Close the first helical feeder 2;
Second step, the stifling vaporization extraction system work of fruit stone, activated carbon production system and activated carbon system of processing are closed;Will
The material inlet of stifling gasification burner 3 is closed, and evaporation exhanst gas outlet is opened;Gas entry is opened, firing up, makes steam stifling
The evaporator temperature changed in stove 3 reaches 90 DEG C -350 DEG C;High temperature pyrolysis gas phase product is by evaporating exhanst gas outlet from stifling vaporization
Discharged in stove 3, the condensation tube inlet of the first condenser 5 is entered by pipeline, the first pump 7, which is opened, makes the first water chiller 6 work;It is high
Product liquid fractional oil of haw kernel stoste and not condensable combustible gas are obtained after warm solution gas-phase product is condensed, fractional oil of haw kernel is former
Liquid is instilled in medicine original fluid container 8 along vertical pipeline, and not condensable combustible gas enters stifling in the presence of the first blower fan 21 along pipeline
The gas returning port of gasification burner 3;Stifling gasification burner 3 can uniformly be heated 70-350 minutes, the heat time with body of heater size, process raw material
Depending on amount and concrete condition, until vaporization terminates;
3rd step, vaporization terminate afterwards directly to open the discharging opening of stifling gasification burner 3, fumigate the rough mountain in gasification burner 3
After short, bristly hair or beard core charcoal enters intermediate bin 4, without waiting for immediately passing through the second helical feeder 9 and rough Chinese hawthorn seed charcoal be conveyed into activation
In stove 10, the second helical feeder 9 is the batcher that can bear corresponding material temperature;
4th step, activated carbon production system work, the stifling vaporization extraction system of fruit stone and activated carbon system of processing are closed;Will
The material inlet of activation furnace 10 is closed, and gas outlet is opened;Gas entry is opened, firing up, make the work in activation furnace 10
Change cylinder temperature and reach 800 DEG C -1100 DEG C, while steam entry is opened, be passed through 300 DEG C -450 DEG C of superheated vapour;Slightly
Chinese hawthorn seed charcoal processed uniformly heats preceding 1/3 period of total time, and evaporation smoke valve 25 is opened, and activation air valve 24 is closed, high temperature
Pyrolysis gas-phase product enters the condensation tube inlet of the second condenser 12 by evaporating the place pipeline of smoke valve 25, and the second pump 14 is opened
The second water chiller 13 is worked, product liquid fractional oil of haw kernel stoste and can not be cold is obtained after high temperature pyrolysis gas phase product is condensed
Solidifying combustible gas, fractional oil of haw kernel stoste are instilled in secondary medicine original fluid container 15 along vertical pipeline, and not condensable combustible gas is in the 3rd wind
Enter the gas returning port of stifling gasification burner 3 in the presence of machine 23 along pipeline;When rough Chinese hawthorn seed charcoal uniformly heats rear the 2/3 of total time
Between section, activation air valve 24 is opened, evaporation smoke valve 25 is closed, and high temperature pyrolysis gas phase product is arranged from the gas outlet of activation furnace 10
Go out, enter the gas returning port of stifling gasification burner 3 by activating the place pipeline of air valve 24 in the presence of the 3rd blower fan 23;To rough mountain
It is 3-10 hours that short, bristly hair or beard core charcoal, which uniformly heats total time, depending on the heat time is with body of heater size, the amount of processing raw material and concrete condition, directly
Become loose to material, start to switch to kermesinus, and a large amount of white cigarettes of emerging, activation terminate, and obtain activated carbon;
5th step, the activated carbon discharging opening of activation furnace 10 is opened, activated carbon pass sequentially through cooler 16, pulverizer 17,
Screening machine 18, type extruder 19 and packaging forming machine 20, active carbon finished products machine.
Embodiment
A kind of plant medicinal liquid extraction and Activated Carbon Production processing technology, it is characterised in that the technique comprises the following steps:
The first step, it will be added to by the hawthorn nuclear fuel material for removing sandstone impurity and simple selection processing in raw material cabin 1;Beat
The material inlet of the first helical feeder 2 and stifling gasification burner 3 is opened, by Chinese hawthorn seed feedstock transportation to stifling gasification burner 3, mountain
The 1/2 of the volume for the evaporator that the volume of short, bristly hair or beard nuclear fuel material is accounted in stifling gasification burner 3;Close the first helical feeder 2;
Second step, the stifling vaporization extraction system work of fruit stone, activated carbon production system and activated carbon system of processing are closed;Will
The material inlet of stifling gasification burner 3 is closed, and evaporation exhanst gas outlet is opened;Gas entry is opened, firing up, makes steam stifling
The evaporator temperature changed in stove 3 reaches 180 DEG C;High temperature pyrolysis gas phase product is by evaporating exhanst gas outlet from stifling gasification burner 3
Discharge, the condensation tube inlet of the first condenser 5 is entered by pipeline, the first pump 7, which is opened, makes the first water chiller 6 work;High warm
Product liquid fractional oil of haw kernel stoste and not condensable combustible gas, fractional oil of haw kernel stoste edge are obtained after solution gas-phase product is condensed
Vertical pipeline is instilled in medicine original fluid container 8, and not condensable combustible gas enters stifling vaporization in the presence of the first blower fan 21 along pipeline
The gas returning port of stove 3;Stifling gasification burner 3 can uniformly be heated 240 minutes, the heat time is with body of heater size, the amount of processing raw material and tool
Depending on body situation, until vaporization terminates;
3rd step, vaporization terminate afterwards directly to open the discharging opening of stifling gasification burner 3, fumigate the rough mountain in gasification burner 3
After short, bristly hair or beard core charcoal enters intermediate bin 4, without waiting for immediately passing through the second helical feeder 9 and rough Chinese hawthorn seed charcoal be conveyed into activation
In stove 10, the second helical feeder 9 is the batcher that can bear corresponding material temperature;
4th step, activated carbon production system work, the stifling vaporization extraction system of fruit stone and activated carbon system of processing are closed;Will
The material inlet of activation furnace 10 is closed, and gas outlet is opened;Gas entry is opened, firing up, make the work in activation furnace 10
Change cylinder temperature and reach 850 DEG C, while steam entry is opened, be passed through 300 DEG C of superheated vapour;First 140 minutes will evaporation
Smoke valve 25 is opened, and activation air valve 24 is closed, and high temperature pyrolysis gas phase product is by evaporating the place pipeline of smoke valve 25 into second
The condensation tube inlet of condenser 12, the second pump 14, which is opened, makes the second water chiller 13 work, after high temperature pyrolysis gas phase product is condensed
Product liquid fractional oil of haw kernel stoste and not condensable combustible gas are obtained, fractional oil of haw kernel stoste instills secondary medicine along vertical pipeline
In original fluid container 15, not condensable combustible gas enters the gas returning port of stifling gasification burner 3 in the presence of the 3rd blower fan 23 along pipeline;Afterwards
Activation air valve 24 was opened in 280 minutes, evaporation smoke valve 25 is closed, and high temperature pyrolysis gas phase product is arranged from the gas outlet of activation furnace 10
Go out, enter the gas returning port of stifling gasification burner 3 by activating the place pipeline of air valve 24 in the presence of the 3rd blower fan 23;To rough mountain
Short, bristly hair or beard core charcoal uniformly heated total time as 7 hours, depending on the heat time is with body of heater size, the amount of processing raw material and concrete condition, until
Material becomes loose, starts to switch to kermesinus, and a large amount of white cigarettes of emerging, activation terminate;
5th step, the activated carbon discharging opening of activation furnace 10 is opened, activated carbon pass sequentially through cooler 16, pulverizer 17,
Screening machine 18, type extruder 19 and packaging forming machine 20, active carbon finished products machine.
The present invention does not address part and is applied to prior art.
Claims (7)
1. a kind of plant medicinal liquid extraction and Activated Carbon Production process equipment, including activated carbon system of processing, it is characterised in that this sets
It is standby also to include the stifling vaporization extraction system of fruit stone and activated carbon production system;The stifling vaporization extraction system of the fruit stone, activated carbon
Production system and activated carbon system of processing are sequentially connected;
The stifling vaporization extraction system of the fruit stone includes raw material cabin, the first helical feeder, stifling gasification burner, intermediate bin, first
Condenser, the first cooling-water machine, the first pump, medicine original fluid container and the first blower fan;One end of the raw material cabin and the first helical feeder
Connection;The other end of first helical feeder is connected with the material inlet of stifling gasification burner;The stifling gasification burner
Gas entry is connected with extraneous gas pipeline;The discharging opening of the stifling gasification burner is connected with intermediate bin;The steam stifling
The evaporation exhanst gas outlet for changing stove is connected by pipeline with the condensation tube inlet of the first condenser;The condensed water of first condenser
Outlet is connected with the first cooling-water machine;First cooling-water machine is connected by the first pump with the condensing water inlet of the first condenser;Institute
The condenser pipe outlet for stating the first condenser is connected by pipeline with medicine original fluid container;The condenser pipe outlet of first condenser is vertical
The side wall of pipeline is connected by the first blower fan with the gas returning port of stifling gasification burner;
The activated carbon production system includes the second helical feeder, activation furnace, the second blower fan, the 3rd blower fan, steam oven, second
Condenser, the second cooling-water machine, the second pump and secondary medicine stoste fill;One end of second helical feeder is connected with intermediate bin,
The material inlet of the other end and activation furnace connects;The gas entry of the activation furnace is connected with extraneous gas pipeline;Institute
The steam entry for stating activation furnace is connected by pipeline with extraneous oxygen and steam oven, and the second blower fan is provided with pipeline;It is described
The gas outlet side of activation furnace is connected by pipeline and activation air valve with the 3rd blower fan, and the gas outlet opposite side of activation furnace passes through pipe
Road and evaporation smoke valve are connected with the condensation tube inlet of the second condenser;The gas returning port of 3rd blower fan and stifling gasification burner connects
Connect;The condensation-water drain of second condenser is connected with the second cooling-water machine;Second cooling-water machine passes through the second pump and second
The condensing water inlet connection of condenser;The condenser pipe outlet of second condenser is connected by vertical pipeline and secondary medicine original fluid container
Connect.
2. plant medicinal liquid extraction according to claim 1 and Activated Carbon Production process equipment, it is characterised in that the activity
Charcoal system of processing includes cooler, pulverizer, screening machine, type extruder and packaging forming machine;The pulverizer and activation furnace
Activated carbon discharging opening is connected by pipeline;The cooler is connected with pulverizer;The pulverizer is connected with screening machine;The sieve
Machine is selected to be connected with type extruder;The type extruder is connected with packaging forming machine.
3. plant medicinal liquid extraction according to claim 1 and Activated Carbon Production process equipment, it is characterised in that described stifling
The body of heater of gasification burner and the body of heater of activation furnace select carbon steel.
4. a kind of plant medicinal liquid extraction and Activated Carbon Production processing technology, it is characterised in that the technique comprises the following steps:
The first step, hawthorn nuclear fuel material is added in raw material cabin;The raw material for opening the first helical feeder and stifling gasification burner enters
Material mouth, by Chinese hawthorn seed feedstock transportation to stifling gasification burner, evaporator that the volume of hawthorn nuclear fuel material is accounted in stifling gasification burner
The 1/2-4/5 of volume;Close the first helical feeder;
Second step, the stifling vaporization extraction system work of fruit stone, activated carbon production system and activated carbon system of processing are closed;Will be stifling
The material inlet of gasification burner is closed, and evaporation exhanst gas outlet is opened;Gas entry is opened, firing up, make stifling gasification burner
Interior temperature reaches 90 DEG C -350 DEG C;High temperature pyrolysis gas phase product is discharged by evaporating exhanst gas outlet from stifling gasification burner, is passed through
Pipeline enters the condensation tube inlet of the first condenser, and the first pump, which is opened, makes the first water chiller work;High temperature pyrolysis gas phase product passes through
Fractional oil of haw kernel stoste and not condensable combustible gas are obtained after condensation, fractional oil of haw kernel stoste instills medicine original fluid container along vertical pipeline
In, not condensable combustible gas enters the gas returning port of stifling gasification burner in the presence of the first blower fan along pipeline;To fumigating gasification burner
Uniformly heating, until vaporization terminates;
3rd step, vaporization open the discharging opening of stifling gasification burner after terminating, and the rough Chinese hawthorn seed charcoal fumigated in gasification burner enters
After intermediate bin, immediately pass through the second helical feeder and rough Chinese hawthorn seed charcoal is conveyed into activation furnace;
4th step, activated carbon production system work, the stifling vaporization extraction system of fruit stone and activated carbon system of processing are closed;Will activation
The material inlet of stove is closed, and gas outlet is opened;Gas entry is opened, firing up, activation in-furnace temperature is reached 800
DEG C -1100 DEG C, while steam entry is opened, it is passed through 300 DEG C -450 DEG C of superheated vapour;Rough Chinese hawthorn seed charcoal uniformly adds
Preceding 1/3 period of hot total time, evaporation smoke valve is opened, activation air valve is closed, and high temperature pyrolysis gas phase product passes through evaporation
Pipeline where smoke valve enters the condensation tube inlet of the second condenser, and the second pump, which is opened, makes the second water chiller work, high temperature pyrolysis
Fractional oil of haw kernel stoste and not condensable combustible gas are obtained after gas-phase product is condensed, fractional oil of haw kernel stoste is dripped along vertical pipeline
Enter in secondary medicine original fluid container, not condensable combustible gas enters the return-air of stifling gasification burner in the presence of the 3rd blower fan along pipeline
Mouthful;Rough Chinese hawthorn seed charcoal uniformly heats rear 2/3 period of total time, and activation air valve is opened, and evaporation smoke valve is closed, high temperature
It is pyrolyzed gas-phase product to discharge from the gas outlet of activation furnace, is entered in the presence of the 3rd blower fan by pipeline where activating air valve and smoked
Steam the gas returning port of gasification burner;To the uniform heating of rough Chinese hawthorn seed charcoal until material becomes loose, start to switch to kermesinus, and emerge
A large amount of white cigarettes, activation terminate, and obtain activated carbon.
5. plant medicinal liquid extraction according to claim 4 and Activated Carbon Production processing technology, it is characterised in that the technique is also
Including the 5th step, the activated carbon discharging opening of activation furnace is opened, activated carbon passes sequentially through cooler, pulverizer, screening machine, type and squeezed
Press and packaging forming machine, active carbon finished products machine.
6. plant medicinal liquid extraction according to claim 4 and Activated Carbon Production processing technology, it is characterised in that in second step
It it is 70-350 minutes to the stifling gasification burner uniform heat time.
7. plant medicinal liquid extraction according to claim 4 and Activated Carbon Production processing technology, it is characterised in that in the 4th step
It is 3-10 hours that total time is uniformly heated to rough Chinese hawthorn seed charcoal.
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CN107022364A (en) * | 2017-05-10 | 2017-08-08 | 河南省科学院能源研究所有限公司 | Biomass pyrogenation gasification power generating simultaneously activated carbon process and key equipment |
CN107032351A (en) * | 2017-05-27 | 2017-08-11 | 山东大学 | The device and method of smoke solution co-production activated carbon is produced in a kind of Chinese hawthorn seed pyrolysis |
CN207227373U (en) * | 2017-11-01 | 2018-04-13 | 承德本多宝生物科技有限公司 | A kind of plant medicinal liquid extraction and Activated Carbon Production process equipment |
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CN1094915A (en) * | 1993-05-11 | 1994-11-16 | 辽宁大学 | With the Semen Crataegi is the processing method of feedstock production beverage, oil plant and gac |
CN1275346A (en) * | 2000-06-16 | 2000-12-06 | 石易 | Method and equipment for destructive distillation of haw kernel to extract juice |
JP2005015749A (en) * | 2003-06-25 | 2005-01-20 | Etsuo Kobayashi | Carbonization tar fixation system, woody tar fixed material and its production method, and also pyroligneous acid and its production method |
CN103274399A (en) * | 2013-05-07 | 2013-09-04 | 韩城市金太阳花椒油脂药料有限责任公司 | Method for producing active carbon by pyrolysing pepper branches |
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Application publication date: 20180209 |