CN107648874A - A kind of volatile solvent condensate recycling device - Google Patents

A kind of volatile solvent condensate recycling device Download PDF

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Publication number
CN107648874A
CN107648874A CN201711034460.6A CN201711034460A CN107648874A CN 107648874 A CN107648874 A CN 107648874A CN 201711034460 A CN201711034460 A CN 201711034460A CN 107648874 A CN107648874 A CN 107648874A
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CN
China
Prior art keywords
cooling cylinder
cavity
dividing plate
volatile solvent
pipe
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201711034460.6A
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Chinese (zh)
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CN107648874B (en
Inventor
黄爱军
阳杨
赵静
张瑜
汪小飞
许桂连
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XINZHONGTIAN ENVIRONMENTAL PROTECTION Co Ltd
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XINZHONGTIAN ENVIRONMENTAL PROTECTION Co Ltd
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Priority to CN201711034460.6A priority Critical patent/CN107648874B/en
Publication of CN107648874A publication Critical patent/CN107648874A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/0011Heating features
    • B01D1/0041Use of fluids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/30Accessories for evaporators ; Constructional details thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0003Condensation of vapours; Recovering volatile solvents by condensation by using heat-exchange surfaces for indirect contact between gases or vapours and the cooling medium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0003Condensation of vapours; Recovering volatile solvents by condensation by using heat-exchange surfaces for indirect contact between gases or vapours and the cooling medium
    • B01D5/0012Vertical tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0057Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
    • B01D5/006Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with evaporation or distillation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0057Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
    • B01D5/0075Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with heat exchanging

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treating Waste Gases (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The present patent application discloses a kind of volatile solvent condensate recycling device, including evaporator, pipeline, air-introduced machine and cooling cylinder, the cavity for being used for being put into solvent is provided with inside evaporator, multiple dividing plates being obliquely installed are provided with cooling cylinder, the low side of dividing plate and the side wall of cooling cylinder one end are fixed, the high-end and cooling cylinder other end side wall of dividing plate is communicated with chamber, and multiple baffle intervals are arranged in two side walls relative in cooling cylinder;Cooling cylinder is divided into multiple cavities by dividing plate, is connected between multiple cavities by connecting chamber, and cooling cylinder is outer to be provided with the collecting pipe connected with cavity with dividing plate low side corresponding position;Evenly spaced multiple condenser pipes are provided with cavity, from top to bottom the condenser pipe increased number in cavity, the bottom of cooling cylinder is provided with blast pipe, and adsorption filter layer is provided with blast pipe.Compared with prior art, the present apparatus substantially increases the efficiency of volatile solvent recycling, and this process reduces environmental pollution, and makes each component purity isolated higher.

Description

A kind of volatile solvent condensate recycling device
Technical field
The invention belongs to solvent recovery technical field, specifically discloses a kind of volatile solvent condensate recycling device.
Background technology
In water-absorbing material carries out surface hydrophobicity modifying process, typically led to using equipment in host material inner and outer surfaces Cross chemical reaction and be grafted or coated one or more layers hydrophobic group or organic matter, these hydrophobic groups or organic matter are reacting Purpose before to host surface for dissolving, dilution needs to add one or more volatile solvents, to improve reaction effect Rate and quality.In above process, volatile solvent is the consumptive material in course of reaction, is completed after above-mentioned reaction terminates, need by Volatile solvent recycling.Otherwise, volatilize have solvent can will be serious environmental pollution and produce potential safety hazard, together When also result in substantial amounts of waste.
When being recycled to such volatile solvent, volatilization is heated using the volatility of solvent, then will wave To send out into gaseous solvent and carry out condensation process, condensed solution is purified or separating treatment, separates its each component, so as to It is easy to reuse.Condensation process is mainly carried out using condenser at present, and condenser internal temperature is relatively low, can be by most of gas The solvent of state is condensed into solution.Because solution has the characteristic of volatilization, if being separated again after by its most of component condensation Or purification process, contained constituent part will continue to volatilize in the process in solution, cause the pollution of working environment.Simultaneously The processes such as condensation, separation are separately handled, complex procedures, less efficient, so that the recycling of solvent is less efficient.
The content of the invention
The purpose of the present invention is providing a kind of volatile solvent condensate recycling device, to solve volatile solvent recycling The problem of efficiency is low.
In order to achieve the above object, base case of the invention is:A kind of volatile solvent condensate recycling device, including steam Send out device, pipeline, air-introduced machine and cooling cylinder, be provided with the cavity for being used for being put into solvent inside the evaporator, evaporator be provided with into The mouth of pipe, base of evaporator are provided with hot-water cavity, and the upper end of the upper end of evaporator and cooling cylinder passes through pipeline communication, the air inducing Machine is arranged at pipeline and cooling cylinder junction;Multiple dividing plates being obliquely installed, adjacent separator inclination side are provided with the cooling cylinder To on the contrary, the low side and the side wall of cooling cylinder one end of the dividing plate are fixed, the high-end and side of the cooling cylinder other end of the dividing plate Wall is communicated with chamber, and multiple baffle intervals are arranged in two side walls relative in cooling cylinder;Cooling cylinder is divided into by the dividing plate Multiple cavities, connected by connecting chamber between multiple cavities, the cooling cylinder is outer to be provided with and cavity company with dividing plate low side corresponding position Logical collecting pipe;Evenly spaced multiple condenser pipes are provided with the cavity, from top to bottom the condenser pipe increased number in cavity, The bottom of cooling cylinder is provided with blast pipe, and adsorption filter layer is provided with the blast pipe.
The operation principle of this base case is:It after use, can be passed through evaporation by volatile solvent by entering the mouth of pipe In the cavity of device, now to hot water is passed through in heating chamber, volatile solvent is heated by hot water, volatile solvent will Heated volatilization;Simultaneously because heated using hot water, the moisture in solvent can only evaporate on a small quantity.Upper end of evaporator and The upper end of cooling cylinder is passed through in cooling cylinder by pipeline communication, the gaseous solvent of volatilization through pipeline, can also start air-introduced machine to waving The gaseous solvent of hair is aspirated, and can accelerate the volatilization process of solvent.
Gaseous solvent after volatilization will be passed through in cooling cylinder from the upper end of cooling cylinder, due to being provided with multiple inclinations in cooling cylinder The dividing plate of setting, adjacent separator incline direction is on the contrary, the low side and the side wall of cooling cylinder one end of the dividing plate are fixed, the dividing plate It is high-end be communicated with chamber with cooling cylinder other end side wall, multiple baffle intervals are arranged on two side walls relative in cooling cylinder On;Cooling cylinder is divided into multiple cavities by the dividing plate, is connected between multiple cavities by connecting chamber;In the presence of air-introduced machine, Gaseous solvent will pass sequentially through cavity from top to bottom.Due to being provided with evenly spaced multiple condenser pipes in the cavity, from upper Condenser pipe increased number in lower chamber, so that cavity temperature from top to bottom reduces successively, gaseous solvent leads to successively When crossing cavity from top to bottom, suffered temperature is more and more lower, so that the component of boiling point from high to low condenses successively, realizes Separation to each component.Because the low side and the side wall of cooling cylinder one end of dividing plate are fixed, the high-end and cooling cylinder of the dividing plate is another The side wall of one end is communicated with chamber, and cooling cylinder is outer to be provided with the collecting pipe connected with cavity with dividing plate low side corresponding position;It is condensed Component will flow down along dividing plate, by collecting condensed each component at collecting pipe.
The higher component of boiling point, and gas contained in some air, will not be condensed, in cavity from top to bottom Interior by rear, this part gaseous solvent is discharged by the inside in cooling cylinder, and by blast pipe, and adsorption filter layer will before discharge Adsorption filtration processing can be carried out to it, so as to avoid causing harmful substance to discharge, cause environmental pollution.
The beneficial effect of this base case is:When the present apparatus is handled volatile solvent, condensation and separation can be same Shi Jinhang, it is different according to the boiling point of each component in solvent, it through in the cavity gradually reducing successively, realized to different boiling Component carry out condensation collection, so as to complete in solvent each component separate processing;The process that this process reduces separation, from And improve the efficiency of solvent recovery processing.During the present apparatus is handled volatile solvent, solvent volatilization, it is cold Solidifying, separation process slitless connection, avoids solvent from evaporateing into the process in air, causes the pollution of working environment.This dress Put by boiling point come each component contained in separating volatile solvent, separating obtained compositional purity can be made higher, constituent part Use can be direct plungeed into, without working process again, greatlys save the manufacturing procedure of solvent.Compared with prior art, this dress The efficiency for greatly improving volatile solvent recycling of knowing clearly is put, this process reduces environmental pollution, and makes each group isolated Divide purity higher.
Preferred scheme one:Based on scheme preferred, in addition to multiple temperature conditioning units, the quantity of temperature conditioning unit and cavity Corresponding, the temperature conditioning unit includes temperature inductor within the cavity and the temperature indicator being fixed on outside cooling cylinder, institute Temperature indicator is stated to be electrically connected with temperature inductor.Due to the present apparatus be mainly used each cavity temperature difference come realize to boiling The different each component of point is separated, and temperature conditioning unit can monitor the temperature in each cavity in time, consequently facilitating adjusting each chamber The temperature of body, realize the preferably condensation to each component in volatile solvent.
Preferred scheme two:Based on scheme it is preferred, it is described connection intracavitary be provided with check valve, the end of the collecting pipe Provided with door.Check valve can ensure in each cavity, the gaseous solvent of flowing, will not flow back, and avoid backflow from making the present apparatus With impacting.When the component condensed in some cavity is less, usable door blocks collecting pipe, component to be condensed compared with Collected together when more.
Preferred scheme three:Based on scheme it is preferred, the condenser pipe is vertically arranged, condenser pipe outer cover be provided with it is more Porous materials.Porous material make to be passed through gaseous solvent in cavity will not direct condensation by contact pipe surface, so as to avoid due to condensation The relatively low component for causing boiling point relatively low of pipe surface condenses here.
Preferred scheme four:Based on scheme it is preferred, the adsorption filter layer includes active carbon layer and spongy layer.Can be more Adsorption filtration effect is carried out to gas well, pollution of the gas to environment in environment is discharged into so as to further reduce.
Brief description of the drawings
Fig. 1 is a kind of structural representation of volatile solvent condensate recycling device embodiment of the present invention.
Embodiment
Below by embodiment, the present invention is further detailed explanation:
Reference in Figure of description includes:Evaporator 10, cavity 11, enter the mouth of pipe 12, hot-water cavity 13, pipeline 20, Air-introduced machine 30, cooling cylinder 40, dividing plate 41, cavity 42, connection chamber 43, check valve 44, condenser pipe 50, porous material 51, collecting pipe 60th, door 61, blast pipe 70, active carbon layer 71, spongy layer 72, temperature indicator 80, temperature inductor 81.
As shown in figure 1, a kind of volatile solvent condensate recycling device, including it is evaporator 10, pipeline 20, air-introduced machine 30, cold Solidifying case 40 and temperature conditioning unit, the inside of evaporator 10 are provided with the cavity 11 for being used for being put into solvent, inlet pipe are provided with evaporator 10 Mouth 12, the bottom of evaporator 10 is provided with hot-water cavity 13, and the upper end of evaporator 10 is connected with the upper end of cooling cylinder 40 by pipeline 20, Air-introduced machine 30 is arranged at pipeline 20 and the junction of cooling cylinder 40.Multiple dividing plates 41 being obliquely installed are provided with cooling cylinder 40, this Embodiment median septum 41 is preferably five, and the incline direction of adjacent separator 41 is opposite;The low side of dividing plate 41 and the one end of cooling cylinder 40 Side wall is fixed, and the side wall of the other end of high-end and cooling cylinder 40 of dividing plate 41, which is provided with, connects chamber 43, and five dividing plates 41 are arranged at intervals In cooling cylinder 40 in two relative side walls.Dividing plate 41 divides cooling cylinder 40 for five cavitys 42, leads between five cavitys 42 Cross connection chamber 43 to connect, check valve 44 is provided with connection chamber 43;What check valve 44 can ensure to flow in each cavity 42 is gaseous state Solvent, it will not flow back, the use for avoiding flowing back to the present apparatus impacts.Cooling cylinder 40 is outer and the low side corresponding position of dividing plate 41 is set The collecting pipe 60 connected with cavity 42, the end of collecting pipe 60 are provided with door 61;The component of condensation in some cavity 42 When less, door 61 can be used to block collecting pipe 60, component to be condensed is collected together when more.It is respectively provided with each cavity 42 Multiple evenly spaced condenser pipes 50, the increased number of condenser pipe 50 in cavity 42 from top to bottom, the bottom of cooling cylinder 40 is set Blast pipe 70 has been put, adsorption filter layer is provided with blast pipe 70;Condenser pipe 50 is vertically arranged, and the outer cover of condenser pipe 50 is provided with Porous material 51;Porous material 51 make the gaseous solvent that is passed through in cavity 42 will not the direct surface of condensation by contact pipe 50, so as to keep away Exempt to cause the relatively low component of boiling point to condense here because the surface of condenser pipe 50 is relatively low.Adsorption filter layer includes the He of active carbon layer 71 Spongy layer 72, preferably can carry out adsorption filtration effect to gas, and gas is discharged into environment to environment so as to further reduce Pollution.Temperature conditioning unit is corresponding with the quantity of cavity 42, and temperature conditioning unit is including the temperature inductor 81 in cavity 42 and admittedly The temperature indicator 80 being scheduled on outside cooling cylinder 40, temperature indicator 80 are electrically connected with temperature inductor 81.
It after use, can be passed through in the cavity 11 of evaporator 10 by volatile solvent by entering the mouth of pipe 12, is now given and is added Hot intracavitary is passed through hot water, and volatile solvent is heated by hot water, and volatile solvent will be heated volatilization;Simultaneously because Heated using hot water, the moisture in solvent can only evaporate on a small quantity.The upper end of evaporator 10 and the upper end of cooling cylinder 40 lead to Piping 20 is connected, and the gaseous solvent of volatilization is passed through in cooling cylinder 40 through pipeline 20, can also start gas of the air-introduced machine 30 to volatilization State solvent is aspirated, and can accelerate the volatilization process of solvent.
Gaseous solvent after volatilization will be passed through in cooling cylinder 40 from the upper end of cooling cylinder 40, due to being provided with cooling cylinder 40 Five dividing plates 41 being obliquely installed, the low side and the side wall of the one end of cooling cylinder 40 of dividing plate 41 are fixed, the high-end and condensation of dividing plate 41 The side wall of the other end of case 40 is provided with connection 43 5 dividing plates 41 of chamber and is disposed in two side walls relative in cooling cylinder 40; Dividing plate 41 divides cooling cylinder 40 for five cavitys 42, is connected between five cavitys 42 by connecting chamber 43;In the work of air-introduced machine 30 Under, gaseous solvent will pass sequentially through cavity 42 from top to bottom.Due to being provided with evenly spaced multiple condensations in cavity 42 Pipe 50, the increased number of condenser pipe 50 in cavity 42 from top to bottom, so that the temperature of cavity 42 from top to bottom reduces successively, When gaseous solvent passes sequentially through cavity 42 from top to bottom, suffered temperature is more and more lower, so that boiling point is from high to low Component condenses successively, realizes the separation to each component.Because the low side and the side wall of the one end of cooling cylinder 40 of dividing plate 41 are fixed, dividing plate The side wall of 41 other end of high-end and cooling cylinder 40, which is provided with, connects chamber 43, and cooling cylinder 40 is outer and the low side corresponding position of dividing plate 41 is set The collecting pipe 60 that is connected with cavity 42;Condensed component will flow down along dividing plate 41, cold by being collected at collecting pipe 60 Each component after solidifying.
The higher component of boiling point, and gas contained in some air, will not be condensed, in cavity from top to bottom By rear in 42, this part gaseous solvent will discharge in the inside of cooling cylinder 40, and by blast pipe 70, be adsorbed before discharge Filtering layer will carry out adsorption filtration processing to it, so as to avoid causing harmful substance to discharge, cause environmental pollution.Due to the present apparatus The temperature difference of mainly used each cavity 42 realizes that each component different to boiling point separates, and temperature conditioning unit can be timely The temperature in each cavity 42 is monitored, consequently facilitating adjusting the temperature of each cavity 42, is realized preferably in volatile solvent The condensation of each component.
Above-described is only embodiments of the invention, and the general knowledge such as known concrete structure and characteristic is not made herein in scheme Excessive description., without departing from the structure of the invention, can be with it should be pointed out that for those skilled in the art Several modifications and improvements are made, these should also be considered as protection scope of the present invention, and these are implemented all without the influence present invention Effect and practical applicability.

Claims (5)

1. a kind of volatile solvent condensate recycling device, it is characterised in that including evaporator, pipeline, air-introduced machine and cooling cylinder, institute The cavity for being provided with inside evaporator and being used for being put into solvent is stated, evaporator is provided with into the mouth of pipe, base of evaporator and is provided with hot-water cavity, institute The upper end for stating upper end of evaporator and cooling cylinder is arranged at pipeline and cooling cylinder junction by pipeline communication, the air-introduced machine; Multiple dividing plates being obliquely installed are provided with the cooling cylinder, adjacent separator incline direction is on the contrary, low side and the condensation of the dividing plate The side wall of case one end is fixed, and the high-end and cooling cylinder other end side wall of the dividing plate is communicated with chamber, and multiple baffle intervals are set Put in relative two side walls in cooling cylinder;Cooling cylinder is divided into multiple cavities by the dividing plate, passes through company between multiple cavities Cavity connects, and the cooling cylinder is outer to be provided with the collecting pipe connected with cavity with dividing plate low side corresponding position;Between being provided with the cavity Every uniform multiple condenser pipes, the condenser pipe increased number in cavity from top to bottom, the bottom of cooling cylinder is provided with blast pipe, described Adsorption filter layer is provided with blast pipe.
2. a kind of volatile solvent condensate recycling device as claimed in claim 1, it is characterised in that also including multiple temperature control lists Member, temperature conditioning unit is corresponding with the quantity of cavity, and the temperature conditioning unit includes temperature inductor within the cavity and is fixed on cold Temperature indicator outside solidifying case, the temperature indicator are electrically connected with temperature inductor.
3. a kind of volatile solvent condensate recycling device as claimed in claim 1, it is characterised in that the connection intracavitary is provided with Check valve, the end of the collecting pipe are provided with door.
4. a kind of volatile solvent condensate recycling device as claimed in claim 1, it is characterised in that the condenser pipe is vertical Set, condenser pipe outer cover is provided with porous material.
A kind of 5. volatile solvent condensate recycling device as claimed in claim 1, it is characterised in that the adsorption filter layer bag Include active carbon layer and spongy layer.
CN201711034460.6A 2017-10-30 2017-10-30 Volatile solvent condensation recovery device Active CN107648874B (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108380138A (en) * 2018-04-13 2018-08-10 浙江国森精细化工科技有限公司 A kind of retracting device of the reaction kettle of environment-friendlyacrylic acrylic acid esters adhesive production
CN109612292A (en) * 2019-01-15 2019-04-12 海安艾拉新材料有限公司 Condensing plant is used in a kind of processing of new material
CN111170387A (en) * 2018-11-13 2020-05-19 上海景峰制药有限公司 Drawer type split water organic solvent evaporation device
CN111318047A (en) * 2020-04-24 2020-06-23 东营银桥化工有限责任公司 Dichloroacetyl chloride cooling and purifying device and method
CN113413629A (en) * 2021-07-01 2021-09-21 合肥工业大学 Organic solvent separation device and system method for flat panel display based on condensation method
CN115282619A (en) * 2022-05-24 2022-11-04 温州市康泰生物科技有限公司 System for rapidly removing volatile solvent

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH09262403A (en) * 1996-03-27 1997-10-07 Hayashi Denko Kk Washing solvent recovering device
CN106643238A (en) * 2016-11-17 2017-05-10 广东工业大学 Multistage liquid-separation plate-type condenser
CN206463527U (en) * 2017-02-05 2017-09-05 江西仙康药业有限公司 A kind of Chemical Manufacture integrated distillation kettle

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH09262403A (en) * 1996-03-27 1997-10-07 Hayashi Denko Kk Washing solvent recovering device
CN106643238A (en) * 2016-11-17 2017-05-10 广东工业大学 Multistage liquid-separation plate-type condenser
CN206463527U (en) * 2017-02-05 2017-09-05 江西仙康药业有限公司 A kind of Chemical Manufacture integrated distillation kettle

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108380138A (en) * 2018-04-13 2018-08-10 浙江国森精细化工科技有限公司 A kind of retracting device of the reaction kettle of environment-friendlyacrylic acrylic acid esters adhesive production
CN111170387A (en) * 2018-11-13 2020-05-19 上海景峰制药有限公司 Drawer type split water organic solvent evaporation device
CN111170387B (en) * 2018-11-13 2021-12-17 上海景峰制药有限公司 Drawer type split water organic solvent evaporation device
CN109612292A (en) * 2019-01-15 2019-04-12 海安艾拉新材料有限公司 Condensing plant is used in a kind of processing of new material
CN111318047A (en) * 2020-04-24 2020-06-23 东营银桥化工有限责任公司 Dichloroacetyl chloride cooling and purifying device and method
CN111318047B (en) * 2020-04-24 2024-05-28 东营银桥化工有限责任公司 Device and method for cooling and purifying dichloroacetyl chloride
CN113413629A (en) * 2021-07-01 2021-09-21 合肥工业大学 Organic solvent separation device and system method for flat panel display based on condensation method
CN113413629B (en) * 2021-07-01 2022-04-19 合肥工业大学 Organic solvent separation device and system method for flat panel display based on condensation method
CN115282619A (en) * 2022-05-24 2022-11-04 温州市康泰生物科技有限公司 System for rapidly removing volatile solvent

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