CN107638308A - It is a kind of to be used to manufacture mill base of nail polish glue and preparation method thereof - Google Patents
It is a kind of to be used to manufacture mill base of nail polish glue and preparation method thereof Download PDFInfo
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- CN107638308A CN107638308A CN201710873341.3A CN201710873341A CN107638308A CN 107638308 A CN107638308 A CN 107638308A CN 201710873341 A CN201710873341 A CN 201710873341A CN 107638308 A CN107638308 A CN 107638308A
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- mill base
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- polish glue
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Abstract
The invention provides a kind of mill base for being used to manufacture nail polish glue, belong to daily cosmetics field.It solve existing oil pastes be used for manufacture nail polish glue, it is poisonous to human body and not environmentally the problem of.Mill base in the present invention is prepared by the component of following mass fraction：1~7 part of aqueous high molecular dispersant, 4~15 parts of aqueous dispersion resin and deionized water.The present invention is using safety and environmental protection pigment, resin, auxiliary agent, nontoxic during its production, non-stimulated smell, green low stain, and the quality of the nail polish glue manufactured than oil pastes is more excellent.
Description
Technical field
The invention belongs to daily chemical product field, and in particular to a kind of to be used to manufacture mill base of nail polish glue and preparation method thereof.
Background technology
Nail polish glue possesses the gloss of glue and the color of oil, and nail polish glue is the symbol of newest manicure trend, and general nail polish
Compare, the Common advantages of compatible glue class and nail polish, full color is exquisitely carved, and it is convenient to smear, moment quick-drying, and gloss keeps more longlasting.
The mill base for being used to manufacture nail polish glue in the market is mostly oil pastes, and solvent is monomer or hazardous solvent, there is dense stimulation
Property smell, have very big harm to the health of environment and people during its manufacturing, manufacturing technique requirent is complicated, energy
Consumption is high.Aqueous color paste is also referred to as pigment dispersion, is using water as decentralized medium, pigment particles are dispersed in water manufactured pigment
Slurry, is typically made up of water, pigment powder, surfactant, cosolvent, NMF etc., according to using and store when needing
Also some can be added and carry high performance auxiliary agent.
Chinese patent 201510643922.9, a kind of quick-drying nail polish glue is disclosed, is calculated according to the mass fraction, by 50-80 parts
UV solidified resin A, 10-30 parts UV solidified resin B, 10-20 parts reactive diluent, 10-20 parts mill base, 0.05-
0.1 part of levelling agent, the wetting agent of 1-10 parts, 0.2-0.6 parts defoamer and the composite photoinitiator of 6-10 parts composition.
The mill base that prior art is used for nail polish glue is mostly oil pastes, and solvent is monomer or hazardous solvent, there is dense thorn
Swashing property smell, have very big harm to the health of environment and people during its manufacturing, manufacturing technique requirent is complicated,
High energy consumption.
The content of the invention
It is an object of the present invention to for the above-mentioned deficiency of prior art, propose a kind of asepsis environment-protecting be used for manufacture first
The mill base of factice.
The present invention solves the technical scheme that its technical problem uses, and proposes a kind of mill base for being used to manufacture nail polish glue, should
Mill base includes the raw material of following mass fraction：1~7 part of aqueous high molecular dispersant, 4~15 parts of aqueous dispersion resin and deionization
Water.
Preferably, 2~6 parts of the aqueous high molecular dispersant, 5~15 parts of aqueous dispersion resin and deionized water 15~50
Part.Preferably, 20~70 parts of the pigment of the raw material, 5~15 parts of NMF, 0.1~1 part of pH adjusting agent and thickener 0.1~
1.5 part.
Preferably, the aqueous high molecular dispersant is water-soluble polymer dispersant.Macromolecule dispersing agent mainly passes through
Steric hindrance obstacle disperses to pigment, is influenceed by temperature, pH small, can prevent pigment from preparing, store, use and transporting
Flocculation is produced during defeated.Macromolecule dispersing agent makes the pigment distribution in mill base uniform, improve tinting strength, tinting power, the covering power of mill base with
And the gloss and levelability formed after film, while can also avoid a variety of pigmented finisses that loose colour occurs when mixing and grows dim.High score
Sub- dispersant can significantly reduce the viscosity of system, and when dispersant dosage is optimal, system viscosity is minimum.It can so improve scattered
The rheological characteristic of system, convenient construction, save the energy.
Preferably, the aqueous dispersion resin is water soluble disperse resin.
Preferably, the water soluble disperse resin is in acrylic resin, epoxy resin, polyurethane, polyethers aldehyde ketone resin
One or more.
Preferably, the NMF is the one or more in propane diols, glycerine, polyethylene glycol, polypropylene glycol.
Preferably, described pH adjusting agent is MEA, diethanol amine, triethanolamine, 2- amino-2-methyls -1- third
One or several kinds in alcohol.
Preferably, described thickener be hydroxyethyl cellulose, it is carboxymethyl cellulose, bentonite, aerosil, poly-
One or several kinds in urethane.
For the preparation method for the mill base for manufacturing nail polish glue, comprise the following steps：There is provided raw material, it is pre-dispersed, grinding, redisperse and
Filtering.
Comprise the following steps that：
（1）Preparing raw material：The component of following mass fraction is mixed：20~70 parts of pigment, 1~7 part of macromolecule dispersing agent, disperse
4~15 parts of resin, 5~15 parts of NMF, 0.1~1 part of pH adjusting agent, 0.1~1.5 part of thickener, deionized water 15~50
Part；
（2）It is pre-dispersed：Raw material is dispersed through machine pre-dispersed 1h under 600r/min~800r/min rotating speed；
（3）Grinding：By step（2）Gained mill base through sand mill grind slurry particle diameter be less than 1 μm；
（4）Redisperse：By above-mentioned steps（3）The mill base of gained, it is dispersed through machine and is stirred under 800r/min~1100r/min rotating speeds
1h；
（5）By step（4）Gained mill base is filtered by 5 micron filter bags, obtains finished product mill base.
The present invention has the advantages that：The present invention is using water as solvent, using safety and environmental protection water-soluble resin and water-soluble
Property dispersant, nontoxic during its production, non-stimulated smell, green low stain, and than other oiliness manufacture nail polish
The quality of glue is more excellent.
Embodiment
It is the specific embodiment of the present invention below, technical scheme is further described, but the present invention is simultaneously
It is not limited to these embodiments.
Embodiment 1
Present embodiment discloses a kind of mill base for being used to manufacture nail polish glue, prepared by the component of following mass fraction：
20 parts of pigment；
1 part of macromolecule dispersing agent, macromolecule dispersing agent is water-soluble polymer dispersant；
4 parts of dispersion resin acrylic resin；
5 parts of NMF polyethylene glycol；
1 part of pH adjusting agent MEA；
1.5 parts of thickener hydroxyethyl cellulose；
50 parts of deionized water.
The method and step that mill base is prepared in the ratio of above-described embodiment is as follows：
（1）Preparing raw material：By powder pigment, macromolecule dispersing agent, dispersion resin, NMF, pH adjusting agent, thickener, go from
Sub- water mixing；
（2）It is pre-dispersed：Raw material is dispersed through machine pre-dispersed 1h under 600r/min~800r/min rotating speed；
（3）Grinding：By step（2）Gained mill base through sand mill grind slurry particle diameter be less than 1 μm；
（4）Redisperse：By above-mentioned steps（3）The mill base of gained, it is dispersed through machine and is stirred under 800r/min~1100r/min rotating speeds
1h；
（5）By step（4）Gained mill base is filtered by 5 micron filter bags, obtains finished product mill base.
Embodiment 2
Change the mass fraction of the preparation component in embodiment 1, prepared by the component of following mass fraction：
70 parts of pigment；
7 parts of water-soluble polymer dispersant；
15 parts of dispersion resin acrylic resin；
15 parts of NMF polyethylene glycol；
0.1 part of pH adjusting agent MEA；
0.1 part of thickener hydroxyethyl cellulose；
50 parts of deionized water.
Method and the embodiment 1 for preparing mill base are identical.
Embodiment 3
Change the mass fraction of the preparation component in embodiment 1, prepared by the component of following mass fraction：
40 parts of pigment；
3 parts of water-soluble polymer dispersant；
10 parts of acrylic resin dispersion resin,；
10 parts of NMF polyethylene glycol；
0.5 part of pH adjusting agent MEA；
0.5 part of thickener hydroxyethyl cellulose；
15 parts of deionized water.
Method and the embodiment 1 for preparing mill base are identical.
Embodiment 4
Change the mass fraction of the preparation component in embodiment 1, prepared by the component of following mass fraction：
50 parts of pigment；
4 parts of water-soluble polymer dispersant；
8 parts of dispersion resin acrylic resin；
8 parts of NMF polyethylene glycol；
0.8 part of pH adjusting agent MEA；
0.8 part of thickener hydroxyethyl cellulose；
30 parts of deionized water.
The method for preparing mill base is identical with embodiment.
Embodiment 5
Change the mass fraction of the preparation component in embodiment 1, prepared by the component of following mass fraction：
30 parts of pigment；
6 parts of water-soluble polymer dispersant；
15 parts of dispersion resin acrylic resin；
5 parts of NMF polyethylene glycol；
0.7 part of pH adjusting agent MEA；
1 part of thickener hydroxyethyl cellulose；
35 parts of deionized water.
Method and the embodiment 1 for preparing mill base are identical.
Comparative example 1
Change the mass fraction of the preparation component in embodiment 1, prepared by the component of following mass fraction：
10 parts of deionized water；
8 parts of dispersant polyurethane high molecule surfactant；
1 part of defoamer polyether silicones；
50 parts of filler, filler are by titanium dioxide, organobentonite, talcum powder mixing composition；
2 parts of anti-settling agent；
80 parts of pigment.
Method and the embodiment 1 for preparing mill base are identical.
Comparative example 2
Change the mass fraction of the preparation component in embodiment 1, prepared by the component of following mass fraction：
20 parts of dispersant acrylic acid；
45 parts of deionized water；
35 parts of organic pigment；
0.15 part of the chloro- 2 methyl -3- isothiazolones of preservative 5-.
Method and the embodiment 1 for preparing mill base are identical.
Comparative example 3
Change the mass fraction of the preparation component in embodiment 1, prepared by the component of following mass fraction：
75 parts of pigment；
8 parts of macromolecule dispersing agent, macromolecule dispersing agent is water-soluble polymer dispersant；
3 parts of dispersion resin, dispersion resin is acrylic resin；
20 parts of NMF, NMF is polyethylene glycol；
1.5 parts of pH adjusting agent, pH adjusting agent is MEA；
0.05 part of thickener, thickener is hydroxyethyl cellulose；
70 parts of deionized water.
Method and the embodiment 1 for preparing mill base are identical.
Evaluation method
（1）Gloss crosses test
The mill base of embodiment and the gained of comparative example is used to prepare in nail polish glue, utilizes single angle light of Instrument Ltd. of Han Consulting
Damp degree meter HP-400（60°）To above-mentioned gained nail polish glue test the glossiness after its film.
（2）Hardness test
Above-mentioned gained nail polish glue is carried out using the hard instrument of QHQ film Pencil scratch of Guangzhou Ai Sirui instruments Science and Technology Ltd.
The hardness tested after its film.
Table 1 is the glossiness and the test data explanation of hardness after prepared nail polish glue film.
Table 2 is the outward appearance explanation after prepared nail polish glue film.
Table 1
Table 2
Nail polish glue prepared by the aqueous color paste of the present invention has advantages below：
（1）, glossiness it is good；
（2）, hardness it is strong；
（3）, film forming it is uniform, it is smooth；
（4）, environmental pollution it is small, it is small to operator's actual bodily harm.
Either on single performance or combination property, it is made that the mill base prepared by the present invention is all substantially better than comparative example
Standby mill base.
Because the number range of each technological parameter involved in the present invention can not possibly all embody in the above-described embodiments,
But as long as those skilled in the art's envisioned any numerical value fallen into the above-mentioned number range completely can implement this
Invention, also include any combination of occurrence in the range of some numerical value certainly.Herein, for the consideration of length, eliminate to
Go out the embodiment of occurrence in certain one or more number range, this disclosure for being not to be construed as technical scheme is not filled
Point.
Applicant states that the present invention illustrates the detailed process equipment of the present invention and technological process by above-described embodiment,
But the invention is not limited in above-mentioned detailed process equipment and technological process, that is, it is above-mentioned detailed not mean that the present invention has to rely on
Process equipment and technological process could be implemented.Person of ordinary skill in the field it will be clearly understood that any improvement in the present invention,
The addition of equivalence replacement and auxiliary element to each raw material of product of the present invention, concrete mode selection etc., fall the protection in the present invention
In the range of.
Claims (10)
- A kind of 1. mill base for being used to manufacture nail polish glue, it is characterised in that：The mill base includes the raw material of following mass fraction：Water-based height 1~7 part of dispersal agent molecule, 4~15 parts of aqueous dispersion resin and deionized water.
- 2. the mill base as claimed in claim 1 for being used to manufacture nail polish glue, it is characterised in that：The aqueous high molecular dispersant 2 15~50 parts of~6 parts, 5~15 parts of aqueous dispersion resin and deionized water.
- 3. the mill base as claimed in claim 1 or 2 for being used to prepare nail polish glue, it is characterised in that the pigment 20~70 of the raw material Part, 5~15 parts of NMF, 0.1~1 part of pH adjusting agent and 0.1~1.5 part of thickener.
- 4. the mill base as claimed in claim 1 or 2 for being used to manufacture nail polish glue, it is characterised in that：The aqueous high molecular disperses Agent is water-soluble polymer dispersant.
- 5. the mill base as claimed in claim 1 or 2 for being used to manufacture nail polish glue, it is characterised in that：The aqueous dispersion resin is Water soluble disperse resin.
- 6. the mill base as claimed in claim 4 for being used to manufacture nail polish glue, it is characterised in that：The water soluble disperse resin is third One or more in olefin(e) acid resin, epoxy resin, polyurethane, polyethers aldehyde ketone resin.
- 7. the mill base as claimed in claim 3 for being used to manufacture nail polish glue, it is characterised in that：The NMF is propane diols, third One or more in triol, polyethylene glycol, polypropylene glycol.
- 8. the mill base as claimed in claim 3 for being used to manufacture nail polish glue, it is characterised in that：Described pH adjusting agent is monoethanol One or several kinds in amine, diethanol amine, triethanolamine, 2-amino-2-methyl-1-propanol.
- 9. the mill base as claimed in claim 3 for being used to manufacture nail polish glue, it is characterised in that：Described thickener is ethoxy fibre Tie up the one or several kinds in element, carboxymethyl cellulose, bentonite, aerosil, polyurethane.
- A kind of 10. preparation method for being used to manufacture the mill base of nail polish glue as described in claim 1~9 is any, it is characterised in that： Comprise the following steps：Raw material, pre-dispersed, grinding, redisperse and filtering are provided.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710873341.3A CN107638308B (en) | 2017-09-25 | 2017-09-25 | Color paste for manufacturing nail polish glue and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710873341.3A CN107638308B (en) | 2017-09-25 | 2017-09-25 | Color paste for manufacturing nail polish glue and preparation method thereof |
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| CN107638308A true CN107638308A (en) | 2018-01-30 |
| CN107638308B CN107638308B (en) | 2020-09-11 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111621202A (en) * | 2020-05-25 | 2020-09-04 | 浙江大利实业有限公司 | Production process of water-based environment-friendly red brown color paste |
| CN115975435A (en) * | 2022-12-27 | 2023-04-18 | 广东英科集团股份有限公司 | High-concentration superfine color paste and preparation method thereof |
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| CN111621202A (en) * | 2020-05-25 | 2020-09-04 | 浙江大利实业有限公司 | Production process of water-based environment-friendly red brown color paste |
| CN115975435A (en) * | 2022-12-27 | 2023-04-18 | 广东英科集团股份有限公司 | High-concentration superfine color paste and preparation method thereof |
| CN115975435B (en) * | 2022-12-27 | 2024-02-02 | 广东英科集团股份有限公司 | High-concentration superfine color paste and preparation method thereof |
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Denomination of invention: The invention relates to a color paste for manufacturing nail polish glue and a preparation method thereof Effective date of registration: 20211202 Granted publication date: 20200911 Pledgee: Zhejiang Anji Rural Commercial Bank Co.,Ltd. Zhuanshan sub branch Pledgor: ZHEJIANG NAMEI MATERIAL TECHNOLOGY Co.,Ltd. Registration number: Y2021330002415 |
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Date of cancellation: 20220325 Granted publication date: 20200911 Pledgee: Zhejiang Anji Rural Commercial Bank Co.,Ltd. Zhuanshan sub branch Pledgor: ZHEJIANG NAMEI MATERIAL TECHNOLOGY Co.,Ltd. Registration number: Y2021330002415 |