CN107630351A - A kind of preparation method of Anti-static cap cloth - Google Patents
A kind of preparation method of Anti-static cap cloth Download PDFInfo
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- CN107630351A CN107630351A CN201710903047.2A CN201710903047A CN107630351A CN 107630351 A CN107630351 A CN 107630351A CN 201710903047 A CN201710903047 A CN 201710903047A CN 107630351 A CN107630351 A CN 107630351A
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Abstract
The invention discloses a kind of preparation method of Anti-static cap cloth, including following aspect：It is configured to packet into including modified bamboo fibre, modified acrylic fibre, silk, burnt flaxen fiber, chitin fiber, the rabbit hair by following, and Anti-static cap cloth is made through blending；Wherein modified bamboo fibre and modified acrylic fibre procedure of processing include：（1）Low-temperature carbonization, polyacrylonitrile fibre is placed in carbide furnace and carries out carbonization treatment；（2）Antistatic treatment, bamboo fibre and carbonized polyacrylonitrile fibre are respectively put into clear water heating, then immerse antistatic agent solution respectively again and are impregnated；（3）Ionization dipping, the bamboo fibre after antistatic treatment and carbonized polyacrylonitrile fibre are immersed into conductive agent solution and ionized；（4）Carburizing, ionization bamboo fibre are placed in vapor tight tank and are evacuated to vacuum, are passed through atomization carbon black solution and carry out Carburization Treatment；（5）Solidification, carburizing bamboo fibre and ionization polyacrylonitrile fibre are put into vacuum tank and aoxidized.
Description
Technical field
The invention belongs to fibre processing technologies field, and in particular to a kind of preparation method of Anti-static cap cloth.
Background technology
Electrostatic, for the electric charge to remain static, when charge collection will form electrostatic phenomenon on object or surface, press
It can be divided into positive electrostatic and negative electrostatic according to electrostatic charge property；Object is rubbed by the external world, kinetic energy, potential energy, heat energy, chemical energy etc.
Form effect so that the positive negative electricity of atom is uneven, object is produced electrostatic charge, electrostatic in nature and daily life
Phenomenon generally existing, the phase mutual friction especially between dry season, object can produce electrostatic.Appropriate electrostatic can be to skin
Disease plays remission effect, and applies also for industrial and agricultural production；But static state is chronically at without controlling, electrostatic meeting
Internal blood neutral and alkali is caused to raise, blood calcium declines, and causes pruitus, pigment deposition, causes body physiological state to lose
Weighing apparatus, larger interference is caused to people's mood；Due to cardiovascular Aging, poor anti jamming capability, electrostatic can improve old man and suffer from painstaking effort old man
Pipe disease probability, induce premature beat and phenomena such as myocardial abnormality, larger harm is caused to health.And conventional cap, it is daily to make
It has preferably insulation and sun-screening function in, but more electrostatic can be produced by being contacted in wearing with hair, easy adsorption of dust
And pathogenic bacteria, and excessive static electricity meeting health causes damage；And by increasing electric conductivity to fiber coat method, when long
Between using obscission is occurred, persistence is poor；And silver-plated, copper method, persistence and electric conductivity are preferable, but heavy metal
Health is impacted into branch.
The content of the invention
The present invention is directed to the problem of existing：Static state is chronically at, blood calcium declines, and causes pruitus, pigment
Deposition, causes body physiological state unbalance, larger interference is caused to people's mood；Electrostatic can improve old man and suffer from angiocardiopathy machine
Rate, induce premature beat and phenomena such as myocardial abnormality, larger harm is caused to health.And conventional cap, its in routine use have
There are preferably insulation and sun-screening function, but more electrostatic can be produced by being contacted in wearing with hair, easy adsorption of dust and pathogenic bacteria,
And excessive static electricity meeting health causes damage；And by increasing fiber coat method electric conductivity, meeting is used for a long time
There is obscission, persistence is poor；And silver-plated, copper method, persistence and electric conductivity are preferable, but heavy metal component can be right
Health impacts.To solve the above problems, the present invention provides a kind of preparation method of Anti-static cap cloth.
The present invention is achieved by the following technical solutions：
A kind of preparation method of Anti-static cap cloth, it is respectively configured to sub-prime gauge part and is：Modified bamboo fibre 41-45 parts, change
Property polyacrylonitrile fibre 23-27 parts, silk 11-15 parts, burnt flaxen fiber 7-10 parts, chitin fiber 5-8 parts, rabbit hair 2-4 parts；Will
Anti-static cap cloth is made in above-mentioned raw materials after blending, and fiber has preferable electric conductivity after modified, can make caused
Electrostatic charge is neutralized by electric current transmission, so as to reduce electrostatic effect in cap, and can improve the antibacterial and fire resistance of cap
Energy.
Described modification bamboo fibre and modified acrylic fibre, its procedure of processing include following aspect：
（1）Low-temperature carbonization：Polyacrylonitrile fibre is placed in carbide furnace and carries out carbonization treatment, oxygen volumetric concentration is 32%-34%,
Programming rate is 5 DEG C/min, is first heated to 210-230 DEG C of holding 105-110min, then heats to 530-560 DEG C of holding 4-
5h, cooling rate are 7 DEG C/min, then are cooled to 300-320 DEG C of holding 75-80min, and carbon content raises in fibre composition, conductive
Performance increase, and there is excellent anti-flammability and fire resistance, carbonized polyacrylonitrile fibre is made after being down to room temperature；
（2）Antistatic treatment：Bamboo fibre and carbonized polyacrylonitrile fibre, which are respectively put into clear water, to be heated, and is then soaked respectively again
Enter in antistatic agent solution and impregnated, filamentary conductive can increase after impregnation, so as to which electrostatic charge leaks in time, avoid
Fiber surface charge collection, 68-73 DEG C of temperature, time 40-45min；
（3）Ionization dipping：Bamboo fibre after antistatic treatment and carbonized polyacrylonitrile fibre are immersed in conductive agent solution
Row ionization, 56-60 DEG C of temperature, on-load voltage 120-124V, both positive and negative polarity alternating 2 times/min of the frequency, time 40-43min, use two
Valency Mg and Zn ion its it is conductive can be good, safe, the electric conductivity of fiber can be improved by infiltrating into after fibrous inside, system
Bamboo fibre and ionization polyacrylonitrile fibre must be ionized；
（4）Carburizing：Ionization bamboo fibre is placed in vapor tight tank and is evacuated to vacuum, is passed through atomization carbon black solution and carries out Carburization Treatment, temperature
270-300 DEG C, carbon black has compared with Thief zone ability under high temperature, can increase carbon black component content in fiber, improve its electric conductivity,
Magnetic frequency is 0.5-0.6MHz, and caused high-intensity magnetic field can improve the osmotic effect of atomization carbon black, time 2-3h, carburizing bamboo be made
Fiber；
（5）Solidification：Carburizing bamboo fibre and ionization polyacrylonitrile fibre are put into vacuum tank and aoxidized, ozone volumetric concentration is
13%-16%, 114-117 DEG C of temperature, pressure 0.6-0.8Mpa, time 40-45min, make fiber sheath aoxidize to form diaphragm, make
Fibrous inside composition solidifies, and improves electric conductivity, and conductive bamboo fibre and conducting polypropylene nitrile fiber is made after cooling.
Step（2）Described heating, its temperature are 44-48 DEG C, time 22-24min.
Step（2）Described antistatic agent solution, it is respectively configured to sub-prime gauge part and is：Deionized water 100-110 parts, nothing
Water-ethanol 20-25 parts, odium stearate 7-10 parts, sucrose ester 6-9 parts, glycine betaine 5-7 parts.
Step（3）Described conductive agent solution, wherein magnesium chloride：Zinc chloride quality proportioning is 2-3:1, its mass concentration is
7%-9%。
Step（4）Described carbon black solution, wherein carbon black：Zinc chloride quality proportioning is 8-10:1, its mass concentration is
10%-12%, wherein carbon black pellet degree are 8-15nm.
The present invention has advantages below compared with prior art：Preparation raw material, it is fine to be modified bamboo fibre and modified polyacrylonitrile
Tie up mainly to process raw material, after modified with preferable electric conductivity, can make caused by during electrostatic charge transmitted by electric current
With so as to reduce electrostatic effect in cap, and the antibacterial and fire resistance of cap can be improved；And use silk, the rabbit hair, crust
Cellulose fiber etc. can improve the comfort level and antibiotic property of cap.Low-temperature carbonization, by the way that polyacrylonitrile fibre is carried out in retort
It is carbonized, carbon content raises in its fibre composition, electric conductivity increase, and has excellent anti-flammability and fire resistance.It is antistatic
Processing, filamentary conductive can increase after antistatic agent solution impregnation, so as to which electrostatic charge leaks in time, avoid fiber
Surface charge is gathered, and improves the antistatic property of cap.Dipping method is ionized, it has conduction using divalence Mg and Zn ion
Performance is good, safe, and the electric conductivity of bamboo fibre and polyacrylonitrile fibre can be improved by infiltrating into after fibrous inside, and heat and
Both positive and negative polarity method is converted, the irregular movement of effects of ion can be improved, improves the osmosis of ion pair fiber, increase is conductive
Performance.Method for carburizing, utter misery black method persistence in surface is poor, and carbon black blending mode high processing costs, passes through vacuum high-temperature bar
The high osmosis of carbon black solution is atomized under part, content of carbon black in fiber can be increased, the electric conductivity of fiber can be improved；And use magnetic
Change method, its caused high-intensity magnetic field can improve the osmotic effect of atomization carbon black.Curing, fibre is made by ozone strong oxidizing ability
Tie up superficial oxidation and form diaphragm, fibrous inside composition is solidified for a long time, improve electric conductivity, and fiber table can be made
Face feel is more smooth, comfortable.
Embodiment
Embodiment 1：
A kind of preparation method of Anti-static cap cloth, it is respectively configured to sub-prime gauge part and is：Modified 42 parts of bamboo fibre, it is modified and gathers
24 parts of Dralon, 12 parts of silk, 8 parts of burnt flaxen fiber, 6 parts of chitin fiber, 2.3 parts of the rabbit hair；By above-mentioned raw materials through blending
Anti-static cap cloth is made afterwards, fiber has preferable electric conductivity after modified, and caused electrostatic charge can be made to pass through electricity
Stream, which transmits, to be neutralized, and so as to reduce electrostatic effect in cap, and can improve the antibacterial and fire resistance of cap.
Described modification bamboo fibre and modified acrylic fibre, its procedure of processing include following aspect：
（1）Low-temperature carbonization：Polyacrylonitrile fibre is placed in carbide furnace and carries out carbonization treatment, oxygen volumetric concentration is 32.4%, is risen
Warm speed is 5 DEG C/min, is first heated to 217 DEG C of holding 106min, then heats to 540 DEG C of holding 4.5h, cooling rate 7
DEG C/min, then 305 DEG C of holding 76min are cooled to, carbon content raises in fibre composition, electric conductivity increase, and with excellent
Anti-flammability and fire resistance, be down to after room temperature and carbonized polyacrylonitrile fibre be made；
（2）Antistatic treatment：Bamboo fibre and carbonized polyacrylonitrile fibre, which are respectively put into clear water, to be heated, and is then soaked respectively again
Enter in antistatic agent solution and impregnated, filamentary conductive can increase after impregnation, so as to which electrostatic charge leaks in time, avoid
Fiber surface charge collection, 69 DEG C of temperature, time 41min；
（3）Ionization dipping：Bamboo fibre after antistatic treatment and carbonized polyacrylonitrile fibre are immersed in conductive agent solution
Row ionization, 57 DEG C, on-load voltage 121V of temperature, both positive and negative polarity alternating the frequency 2 times/min, time 41min, using divalence Mg and Zn from
Son its it is conductive can be good, safe, the electric conductivity of fiber can be improved by infiltrating into after fibrous inside, and it is fine that ionization bamboo is made
Peacekeeping ionizes polyacrylonitrile fibre；
（4）Carburizing：Ionization bamboo fibre is placed in vapor tight tank and is evacuated to vacuum, is passed through atomization carbon black solution and carries out Carburization Treatment, temperature 280
DEG C, carbon black has compared with Thief zone ability under high temperature, can increase carbon black component content in fiber, improves its electric conductivity, magnetization frequency
Rate is 0.55MHz, and caused high-intensity magnetic field can improve the osmotic effect of atomization carbon black, time 2.5h, carburizing bamboo fibre be made；
（5）Solidification：Carburizing bamboo fibre and ionization polyacrylonitrile fibre are put into vacuum tank and aoxidized, ozone volumetric concentration is
14%, 115 DEG C of temperature, pressure 0.62Mpa, time 41min, make fiber sheath aoxidize to form diaphragm, consolidate fibrous inside composition
Change, improve electric conductivity, conductive bamboo fibre and conducting polypropylene nitrile fiber is made after cooling.
Step（2）Described heating, its temperature are 45 DEG C, time 23min.
Step（2）Described antistatic agent solution, it is respectively configured to sub-prime gauge part and is：103 parts of deionized water, anhydrous second
21 parts of alcohol, 8 parts of odium stearate, 7 parts of sucrose ester, 5.2 parts of glycine betaine.
Step（3）Described conductive agent solution, wherein magnesium chloride：Zinc chloride quality proportioning is 2:1, its mass concentration is
7.4%。
Step（4）Described carbon black solution, wherein carbon black：Zinc chloride quality proportioning is 9:1, its mass concentration is 10.5%,
Wherein carbon black pellet degree is 8-15nm.
Embodiment 2：
Compared with embodiment 1, step changes in the following areas the present embodiment 2：
Step（1）Described in carbonization treatment, its parameter is：Oxygen volumetric concentration is 33.6%, and programming rate is 5 DEG C/min, first
225 DEG C of holding 108min are heated to, then heat to 550 DEG C of holding 5h, cooling rate is 7 DEG C/min, then is cooled to 317 DEG C of guarantors
Hold 78min.
Step（2）Described dipping, its parameter are：71 DEG C of temperature, time 44min.
Step（2）Described heating, its temperature are 47 DEG C, time 24min.
Step（2）Described antistatic agent solution, it is respectively configured to sub-prime gauge part and is：109 parts of deionized water, anhydrous second
24 parts of alcohol, 9 parts of odium stearate, 8 parts of sucrose ester, 6.5 parts of glycine betaine.
Step（3）Described ionization, its parameter are：59 DEG C, on-load voltage 123V of temperature, the both positive and negative polarity alternating frequency 2 times/
Min, time 42min.
Step（3）Described conductive agent solution, wherein magnesium chloride：Zinc chloride quality proportioning is 3:1, its mass concentration is
8.7%。
Step（4）Described Carburization Treatment, its parameter are：290 DEG C of temperature, magnetic frequency are 0.6 MHz, time 3h.
Step（4）Described carbon black solution, wherein carbon black：Zinc chloride quality proportioning is 10:1, its mass concentration is
11.6%, wherein carbon black pellet degree is 8-15nm.
Step（5）Described oxidation, its parameter are：Ozone volumetric concentration is 15%, 116 DEG C, pressure 0.75Mpa of temperature, when
Between 44min.
Contrast 1：
This contrast 1 does not carry out step compared with embodiment 1（1）Middle low-temperature carbonization, other steps are same as Example 1.
Contrast 2：
This contrast 2 does not carry out step compared with embodiment 1（2）Middle dipping, other steps are same as Example 1.
Contrast 3：
This contrast 3 does not carry out step compared with embodiment 2（3）Middle ionization, other steps are same as Example 2.
Contrast 4：
This contrast 4 does not carry out step compared with embodiment 2（4）Middle Carburization Treatment, other steps are same as Example 2.
Contrast 5：
This contrast 5 does not carry out step compared with embodiment 2（5）Middle oxidation, other steps are same as Example 2.
Control group：
Be processed in control group using bamboo fibre and polyacrylonitrile fibre, be not used low-temperature carbonization, dipping, ionization, at carburizing
Reason and method for oxidation.
To embodiment 1, embodiment 2, contrast 1, contrast 2, contrast 3, contrast 4, contrast 5 and control group experimental program, statistics
The fabric resistor rate of cap, electrostatic charge（Electrostatic tester）, absorbability（48h, water are placed under the conditions of humidity is 70%-75%
Divide increase ratio）, stain be compared.
It is stain：Wherein ﹢ ﹢ ﹢ ﹢ ﹢ are fine that preferably, ﹢ ﹢ ﹢ are general to ﹢ ﹢ ﹢ ﹢, and ﹢ ﹢ are poor, and ﹢ is very poor；Each evaluation sample
Capacity is 130, is defined by the super evaluation result of sample 2/3.
Experimental data：
| Project | Fabric resistor rate Ω m | Electrostatic charge V | Water imbibition % | It is stain |
| Embodiment 1 | 102 | 0.32 | 12.30 | ﹢ ﹢ ﹢ ﹢ |
| Embodiment 2 | 105 | 0.28 | 12.10 | ﹢ ﹢ ﹢ ﹢ |
| Contrast 1 | 188 | 0.91 | 12.50 | ﹢ ﹢ |
| Contrast 2 | 155 | 0.68 | 10.38 | ﹢ ﹢ ﹢ |
| Contrast 3 | 175 | 0.75 | 9.28 | ﹢ ﹢ |
| Contrast 4 | 183 | 0.81 | 8.19 | ﹢ ﹢ |
| Contrast 5 | 147 | 0.56 | 7.25 | ﹢ ﹢ ﹢ |
| Control group | 431 | 2.56 | 25.60 | ﹢ |
Synthesis result：The Anti-static cap that the inventive method is produced, compared with control group, its fabric resistor rate declines 329
Ω m, electrostatic charge decline 2.24V, and absorbability declines 13.3%, have stain well.It is fine using low-temperature carbonization method
Tieing up resistivity reduces by 86 Ω m, and electrostatic charge reduces 0.59V；And dipping and ionization method are used, fabric resistor rate reduces by 53
Ω m, 70 Ω m, electrostatic charge reduce 0.36V, 0.47 V, and water imbibition reduces by 1.7%, 2.8%；Use carburizing and solidification side
Method, fabric resistor rate reduce by 78 Ω m, 42 Ω m, and electrostatic charge reduces 0.53V, 0.28V, and water imbibition reduces by 3.9%, 4.9%.
Claims (6)
1. a kind of preparation method of Anti-static cap cloth, it is characterised in that it is respectively configured to sub-prime gauge part and is：Modified bamboo is fine
Tie up 41-45 parts, modified acrylic fibre 23-27 parts, silk 11-15 parts, burnt flaxen fiber 7-10 parts, chitin fiber 5-8 parts,
Rabbit hair 2-4 parts；Anti-static cap cloth is made in above-mentioned raw materials after blending.
2. the preparation method of Anti-static cap cloth as claimed in claim 1, it is characterised in that described modification bamboo fibre and
Modified acrylic fibre, its procedure of processing include following aspect：
（1）Low-temperature carbonization：Polyacrylonitrile fibre is placed in carbide furnace and carries out carbonization treatment, oxygen volumetric concentration is 32%-34%,
Programming rate is 5 DEG C/min, is first heated to 210-230 DEG C of holding 105-110min, then heats to 530-560 DEG C of holding 4-
5h, cooling rate are 7 DEG C/min, then are cooled to 300-320 DEG C of holding 75-80min, and silicon carbide/polypropylene nitrile is made after being down to room temperature
Fiber；
（2）Antistatic treatment：Bamboo fibre and carbonized polyacrylonitrile fibre, which are respectively put into clear water, to be heated, and is then soaked respectively again
Enter in antistatic agent solution and impregnated, 68-73 DEG C of temperature, time 40-45min；
（3）Ionization dipping：Bamboo fibre after antistatic treatment and carbonized polyacrylonitrile fibre are immersed in conductive agent solution
Row ionization, 56-60 DEG C of temperature, on-load voltage 120-124V, both positive and negative polarity the alternating frequency 2 times/min, time 40-43min, electricity is made
From bamboo fibre and ionization polyacrylonitrile fibre；
（4）Carburizing：Ionization bamboo fibre is placed in vapor tight tank and is evacuated to vacuum, is passed through atomization carbon black solution and carries out Carburization Treatment, temperature
270-300 DEG C, magnetic frequency is 0.5-0.6 MHz, time 2-3h, and carburizing bamboo fibre is made；
（5）Solidification：Carburizing bamboo fibre and ionization polyacrylonitrile fibre are put into vacuum tank and aoxidized, ozone volumetric concentration is
13%-16%, 114-117 DEG C of temperature, pressure 0.6-0.8Mpa, time 40-45min, conductive bamboo fibre and conduction are made after cooling
Polyacrylonitrile fibre.
3. the preparation method of Anti-static cap cloth as claimed in claim 2, it is characterised in that step（2）Described heating
Processing, its temperature are 44-48 DEG C, time 22-24min.
4. the preparation method of Anti-static cap cloth as claimed in claim 2, it is characterised in that step（2）Described is anti-quiet
Electric agent solution, it is respectively configured to sub-prime gauge part and is：Deionized water 100-110 parts, absolute ethyl alcohol 20-25 parts, odium stearate 7-
10 parts, sucrose ester 6-9 parts, glycine betaine 5-7 parts.
5. the preparation method of Anti-static cap cloth as claimed in claim 2, it is characterised in that step（3）Described conduction
Agent solution, wherein magnesium chloride：Zinc chloride quality proportioning is 2-3:1, its mass concentration is 7%-9%.
6. the preparation method of Anti-static cap cloth as claimed in claim 2, it is characterised in that step（4）Described carbon black
Solution, wherein carbon black：Zinc chloride quality proportioning is 8-10:1, its mass concentration is 10%-12%, and wherein carbon black pellet degree is 8-
15nm。
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| CN201710903047.2A CN107630351A (en) | 2017-09-29 | 2017-09-29 | A kind of preparation method of Anti-static cap cloth |
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| CN201710903047.2A CN107630351A (en) | 2017-09-29 | 2017-09-29 | A kind of preparation method of Anti-static cap cloth |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108411624A (en) * | 2018-02-06 | 2018-08-17 | 天津兴华织造有限公司 | A kind of manufacturing process of antistatic magic tape |
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