CN107616295A - A kind of spray coating liquor for reducing Semen sojae atricolor enzymatic protein foaming characteristic and its application - Google Patents
A kind of spray coating liquor for reducing Semen sojae atricolor enzymatic protein foaming characteristic and its application Download PDFInfo
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- CN107616295A CN107616295A CN201711087287.6A CN201711087287A CN107616295A CN 107616295 A CN107616295 A CN 107616295A CN 201711087287 A CN201711087287 A CN 201711087287A CN 107616295 A CN107616295 A CN 107616295A
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- spray coating
- semen sojae
- sojae atricolor
- coating liquor
- enzymatic protein
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Abstract
The invention belongs to soybean protein production technical field, and in particular to and it is a kind of to reduce the spray coating liquor of Semen sojae atricolor enzymatic protein foaming characteristic, and its preparation method and application are further disclosed.The spray coating liquor of the present invention for reducing Semen sojae atricolor enzymatic protein foaming characteristic, using phosphatide, sucrose fatty ester and defoamer as main component, solvent is done instead of soybean oil with the process water Jing Guo osmosis filtration simultaneously, gained aqueous phase spray coating liquor for the oil phase spray coating liquor of solvent is done with soybean oil in the prior art, the solubility property of gained Semen sojae atricolor enzymatic protein is substantially improved, the foaming characteristic of Semen sojae atricolor enzymatic protein is effectively reduced, improves its injection property.
Description
Technical field
The invention belongs to soybean protein production technical field, and in particular to a kind of spray for reducing Semen sojae atricolor enzymatic protein foaming characteristic
Masking liquid, and its preparation method and application are further disclosed.
Background technology
Semen sojae atricolor enzymatic protein be using soybean as raw material, with biotechnology carry out conversion processing and through high temperature drying and
Into, a high-quality protein of adaptation young animal digestive physiology characteristic.In Semen sojae atricolor enzymatic protein protein content 90% with
On, amino acid classes have nearly 20 kinds, and contain a variety of essential amino acids.Semen sojae atricolor enzymatic protein is nutritious, meets children
Age animal and flesh-eater, aquatic livestock are to the particular/special requirement of protein quality.
In Semen sojae atricolor enzymatic protein, due to eliminating most raffinose and stachyose, the anti-of glycinin is eliminated
Originality, and other ANFs such as SNSP and phytic acid are also handled, so, the anti-nutrition in Semen sojae atricolor enzymatic protein
The factor is relatively low；And because the original spherical structure of soybean protein has been destroyed, peptide chain is in extended position, internal enzyme effect position
Point fully exposure so that its digestibility is improved；In addition, Semen sojae atricolor enzymatic protein has unique fragrance, it is favorably improved
Palatability so that animal prefers to search for food, and the extremely digestible characteristic of Semen sojae atricolor enzymatic protein, also make it that its feed intake is high and holds
Long.
In the prior art, the typical production process of Semen sojae atricolor enzymatic protein is alkali extraction-acid precipitation, i.e., soaks dregs of beans with weak lye
40 minutes or so so that protein dissolution is separated after removing insoluble fiber with seperator, left containing albumen in weak lye
Solution, then flocculant (be usually food grade hydrochloric acid) is added into protein solution, albumen precipitation is out reclaimed, then right
The albumen of recovery carries out ferment treatment, and Semen sojae atricolor enzymatic protein is obtained after obtaining protein enzymatic hydrolyzate drying and processing.But by above-mentioned first
The Semen sojae atricolor enzymatic protein powder that step processing obtains only has the general performance of Semen sojae atricolor enzymatic protein, for many application fields,
Its performance can not meet process requirements, it is necessary to by carrying out spray treatment to dried enzymolysis protein powder, to be fitted
It is suitable for the Semen sojae atricolor enzymatic protein of different manufacture field performance requirements.
The content of the invention
Therefore, the technical problems to be solved by the invention are to provide a kind of spraying for reducing Semen sojae atricolor enzymatic protein foaming characteristic
Liquid, the spray coating liquor help to reduce the foaming characteristic of the Semen sojae atricolor enzymatic protein.
In order to solve the above technical problems, a kind of spray coating liquor for reducing Semen sojae atricolor enzymatic protein foaming characteristic of the present invention, institute
Stating spray coating liquor includes the component of following parts by weight：The parts by weight of phosphatidase 5-10, sucrose fatty ester 1-4 parts by weight, defoamer 2-6 weights
Measure part, water 20-30 parts by weight.
Preferably, the spray coating liquor for reducing Semen sojae atricolor enzymatic protein foaming characteristic includes the component of following parts by weight：Phosphatidase 6-9
Parts by weight, sucrose fatty ester 2-3 parts by weight, defoamer 3-5 parts by weight, water 22-28 parts by weight.
More excellent, the spray coating liquor includes the component of following parts by weight：The parts by weight of phosphatide 7.8, the weight of sucrose fatty ester 2.4
Measure part, the parts by weight of defoamer 4, the parts by weight of water 25.8.
The water is the process water by osmosis filtration.
The defoamer includes dimethyl silicone polymer, Tween 80 or defoamer containing vegetable oil, can also be that other meet
The defoamer of international standard.
The invention also discloses a kind of method for the spray coating liquor for preparing described reduction Semen sojae atricolor enzymatic protein foaming characteristic, including
A selected amount of water is heated to 60-70 DEG C, and sequentially adds the step of a selected amount of phosphatide, sucrose fatty ester and defoamer
Suddenly, mix, produce.
While the preparation method is additionally included in the addition phosphatide and sucrose fatty ester, carried out with high speed shear pump
The step of shear treatment.
The preparation method also includes carrying out gained spray coating liquor into the step of insulation preserves in 70 DEG C.
The invention also discloses a kind of method for reducing Semen sojae atricolor enzymatic protein foaming characteristic, that is, includes to weigh described spray coating liquor
The step of being sprayed to the Semen sojae atricolor enzymatic protein.
In terms of the Semen sojae atricolor enzymatic protein butt, the quantity for spray of the spray coating liquor is 1-3 ‰.
The spray coating liquor is sprayed by measuring pump by two Fluid sprayers.
Methods described is additionally included in spraying process the step of carrying out continuing insulation and stirring to the spray coating liquor, to prevent
The spray coating liquor layering and precipitating.
The spray coating liquor of the present invention for reducing Semen sojae atricolor enzymatic protein foaming characteristic, with phosphatide, sucrose fatty ester and defoaming
Agent is main component, while makees solvent instead of soybean oil with the process water Jing Guo osmosis filtration, and gained aqueous phase spray coating liquor is compared
For the oil phase spray coating liquor of solvent is done with soybean oil in the prior art, the solubility property of gained Semen sojae atricolor enzymatic protein significantly carries
Rise, effectively reduce the foaming characteristic of Semen sojae atricolor enzymatic protein, improve its injection property.
The spray coating liquor of the present invention for reducing Semen sojae atricolor enzymatic protein foaming characteristic, with the process water generation Jing Guo osmosis filtration
Solvent is made for soybean oil, after testing, total plate count ＜ 500cfu/g, E.coli LT .LT.LT 3.0cfu/g, mould and the ferment of process water
In female bacterium ＜ 50cfu/g, add and play defoamer (typically to Microbiological requirements total plate count ＜ 500cfu/g E.coli LTs .LT.LT
3.0cfu/g yeast and mold ＜ 50cfu/g) defoaming and foam-inhibiting effect, while microbial growth is avoided reduce dissolving
Protein foam height, improves dissolving and injection effect.
Brief description of the drawings
In order that present disclosure is more likely to be clearly understood, specific embodiment and combination below according to the present invention
Accompanying drawing, the present invention is further detailed explanation, wherein,
Fig. 1 is the schematic diagram that the present invention is sprayed using two Fluid sprayers.
Embodiment
Embodiment 1
The spray coating liquor of reduction Semen sojae atricolor enzymatic protein foaming characteristic described in the present embodiment, including following component：Phosphatidase 5 kg, sugarcane
Sugar fatty acid ester 4kg, defoamer (dimethyl silicone polymer) 2kg, process water 30kg.
The method that the present embodiment prepares the spray coating liquor of described reduction Semen sojae atricolor enzymatic protein foaming characteristic, including：By selected amount
Water be heated to 60-70 DEG C, and sequentially add a selected amount of phosphatide, sucrose fatty ester and defoamer, while with a high speed
Shear pump carries out shear treatment to solution uniform dissolution, produces the spray coating liquor, and gained spray coating liquor is placed in into 70 DEG C of insulation water
Insulation preservation is carried out in bath interlayer.
Embodiment 2
The spray coating liquor of reduction Semen sojae atricolor enzymatic protein foaming characteristic described in the present embodiment, including following component：Phosphatidase 1 0kg, sugarcane
Sugar fatty acid ester 1kg, defoamer (dimethyl silicone polymer) 6kg, process water 20kg.
The preparation method of the spray coating liquor of Semen sojae atricolor enzymatic protein foaming characteristic is reduced described in the present embodiment with embodiment 1.
Embodiment 3
The spray coating liquor of reduction Semen sojae atricolor enzymatic protein foaming characteristic described in the present embodiment, including following component：Phosphatidase 6 kg, sugarcane
Sugar fatty acid ester 3kg, defoamer (Tween 80) 3kg, process water 28kg.
The preparation method of the spray coating liquor of Semen sojae atricolor enzymatic protein foaming characteristic is reduced described in the present embodiment with embodiment 1.
Embodiment 4
The spray coating liquor of reduction Semen sojae atricolor enzymatic protein foaming characteristic described in the present embodiment, including following component：Phosphatide 9kg, sugarcane
Sugar fatty acid ester 2kg, defoamer (vegetable oil defoamer) 5kg, process water 22kg.
The preparation method of the spray coating liquor of Semen sojae atricolor enzymatic protein foaming characteristic is reduced described in the present embodiment with embodiment 1.
Embodiment 5
The spray coating liquor of reduction Semen sojae atricolor enzymatic protein foaming characteristic described in the present embodiment, including following component：Phosphatide 7.8kg,
Sucrose fatty ester 2.4kg, defoamer (Tween 80) 4kg, process water 25.8kg.
The preparation method of the spray coating liquor of Semen sojae atricolor enzymatic protein foaming characteristic is reduced described in the present embodiment with embodiment 1.
Comparative example 1
The spray coating liquor of reduction Semen sojae atricolor enzymatic protein foaming characteristic described in this comparative example, including following component：Phosphatidase 5 .4kg,
Sucrose fatty ester 1.8kg, soybean oil 4.8kg.
Application examples
The spraying process of spray coating liquor of the present invention is that two Fluid sprayer commonly used in the prior art is sprayed, that is, presses
Sprayed according to the application method of two Fluid sprayers.The process that two Fluid sprayers as giving Fig. 1 are sprayed is shown
It is intended to, liquid (spray coating liquor) is transported to nozzle by flow channel for liquids under pressure, and compressed air is arrived by gas flow
Up to nozzle, both mix at nozzle produces atomization mass (circular spray pattern), and in " B " distance, atomization mass can keep ratio
More regular sectorial area, such as " A ", after beyond distance " D ", atomization mass becomes turbulent flow to angular dimension, and shape changes, attached
A, B, D parameter can change according to second fluid nozzle model difference in figure, as long as spray coating liquor is atomized uniformly and selects any type
Number nozzle.
Spraying schematic diagram as shown in Figure 1, respectively with spray coating liquor made from embodiment 1-5 and comparative example 1, led to by measuring pump
Cross the two Fluid sprayers Semen sojae atricolor enzymatic protein commercially available to prior art and carry out spray treatment, respectively obtain corresponding protein sample.
In terms of the Semen sojae atricolor enzymatic protein butt, the quantity for spray for controlling the spray coating liquor is 2 ‰, and is needed in spraying process to institute
State spray coating liquor to carry out continuing insulation, and be formulated stirrer gear in tank and persistently stir, prevent spray coating liquor layering and precipitating.
Experimental example spumescence detects
Inject formula of liquid：Distinguish obtained Semen sojae atricolor enzymatic protein sample 22.6g, trimerization in Example 1-5 and comparative example
Phosphoric acid 7.5g, glucose 3.1g, salt (NaCl) 1.8g, injection water 442.5g.
Above-mentioned dispensing is fully dissolved in agitator respectively, then the parenteral solution 1000ml dissolved is moved into glass,
With static 30min after the parenteral solution 30s in glass bar stirring glass, foam height is measured with ruler.
After testing, the foam height ＜ of the Semen sojae atricolor enzymatic protein sample obtained is handled through spray coating liquor described in embodiment 1-5
10mm, and the foam height for the Semen sojae atricolor enzymatic protein sample that the processing of spray coating liquor described in example obtains is then between 20-50mm by contrast.
It can be seen that aqueous phase spray coating liquor of the present invention effectively reduces soybean enzymolysis compared to oiliness spray coating liquor common in the art
The foaming characteristic of albumen, the solute effect and injection effect of albumen greatly improved.
Obviously, above-described embodiment is only intended to clearly illustrate example, and is not the restriction to embodiment.It is right
For those of ordinary skill in the art, can also make on the basis of the above description it is other it is various forms of change or
Change.There is no necessity and possibility to exhaust all the enbodiments.And the obvious change thus extended out or
Among changing still in the protection domain of the invention.
Claims (10)
1. a kind of spray coating liquor for reducing Semen sojae atricolor enzymatic protein foaming characteristic, it is characterised in that the spray coating liquor includes following parts by weight
Component：The parts by weight of phosphatidase 5-10, sucrose fatty ester 1-4 parts by weight, defoamer 2-6 parts by weight, water 20-30 parts by weight.
2. the spray coating liquor according to claim 1 for reducing Semen sojae atricolor enzymatic protein foaming characteristic, it is characterised in that the spray coating liquor
Include the component of following parts by weight：The parts by weight of phosphatide 7.8, the parts by weight of sucrose fatty ester 2.4, the parts by weight of defoamer 4, water 25.8
Parts by weight.
3. the spray coating liquor according to claim 1 or 2 for reducing Semen sojae atricolor enzymatic protein foaming characteristic, it is characterised in that the water
For the process water Jing Guo osmosis filtration.
4. the spray coating liquor of the reduction Semen sojae atricolor enzymatic protein foaming characteristic according to claim any one of 1-3, it is characterised in that institute
Stating defoamer includes dimethyl silicone polymer, Tween 80 or defoamer containing vegetable oil.
5. a kind of method of the spray coating liquor of the reduction Semen sojae atricolor enzymatic protein foaming characteristic prepared described in claim any one of 1-4, its
It is characterised by, including a selected amount of water is heated to 60-70 DEG C, and sequentially adds a selected amount of phosphatide, sucrose-fatty
The step of ester and defoamer, mix, produce.
6. preparation method according to claim 5, it is characterised in that be additionally included in and add the phosphatide and sucrose-fatty
While ester, with high speed shear pump carry out shear treatment the step of.
A kind of 7. method for reducing Semen sojae atricolor enzymatic protein foaming characteristic, it is characterised in that including with described in claim any one of 1-4
Spray coating liquor the step of being sprayed to the Semen sojae atricolor enzymatic protein.
8. the method according to claim 7 for reducing Semen sojae atricolor enzymatic protein foaming characteristic, it is characterised in that with the soybean enzyme
Albumen butt meter is solved, the quantity for spray of the spray coating liquor is 1-3 ‰.
9. the method for the reduction Semen sojae atricolor enzymatic protein foaming characteristic according to claim 7 or 8, it is characterised in that the spraying
Liquid is sprayed by measuring pump by two Fluid sprayers.
10. the method for the reduction Semen sojae atricolor enzymatic protein foaming characteristic according to claim any one of 7-9, it is characterised in that also
It is included in spraying process the step of carrying out continuing insulation and stirring to the spray coating liquor, to prevent the spray coating liquor layering heavy
Form sediment.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711087287.6A CN107616295B (en) | 2017-11-07 | 2017-11-07 | Spraying liquid for reducing foaming property of soybean enzymolysis protein and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201711087287.6A CN107616295B (en) | 2017-11-07 | 2017-11-07 | Spraying liquid for reducing foaming property of soybean enzymolysis protein and application thereof |
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| CN107616295A true CN107616295A (en) | 2018-01-23 |
| CN107616295B CN107616295B (en) | 2021-04-02 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108782942A (en) * | 2018-06-27 | 2018-11-13 | 山东禹王生态食业有限公司 | A kind of production method of Instant soyabean protein powder |
| CN108925744A (en) * | 2018-09-28 | 2018-12-04 | 山东禹王生态食业有限公司 | A kind of preparation method of polymolecularity soy protein concentrate |
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| CN101642185B (en) * | 2009-09-07 | 2012-05-02 | 哈高科大豆食品有限责任公司 | Injection type soybean protein isolate and preparation method thereof |
| CN104304641A (en) * | 2014-10-01 | 2015-01-28 | 谷神生物科技集团有限公司 | Preparation method of low-viscosity isolated soy protein |
| CN106942385A (en) * | 2017-03-23 | 2017-07-14 | 黑龙江省北大荒绿色健康食品有限责任公司 | A kind of preparation method of anti-fatigue effect soy milk powder |
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2017
- 2017-11-07 CN CN201711087287.6A patent/CN107616295B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101642185B (en) * | 2009-09-07 | 2012-05-02 | 哈高科大豆食品有限责任公司 | Injection type soybean protein isolate and preparation method thereof |
| CN104304641A (en) * | 2014-10-01 | 2015-01-28 | 谷神生物科技集团有限公司 | Preparation method of low-viscosity isolated soy protein |
| CN106942385A (en) * | 2017-03-23 | 2017-07-14 | 黑龙江省北大荒绿色健康食品有限责任公司 | A kind of preparation method of anti-fatigue effect soy milk powder |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108782942A (en) * | 2018-06-27 | 2018-11-13 | 山东禹王生态食业有限公司 | A kind of production method of Instant soyabean protein powder |
| CN108925744A (en) * | 2018-09-28 | 2018-12-04 | 山东禹王生态食业有限公司 | A kind of preparation method of polymolecularity soy protein concentrate |
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| CN107616295B (en) | 2021-04-02 |
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