CN107572802A - A kind of glazing process for colorful pottery - Google Patents
A kind of glazing process for colorful pottery Download PDFInfo
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- CN107572802A CN107572802A CN201710892711.8A CN201710892711A CN107572802A CN 107572802 A CN107572802 A CN 107572802A CN 201710892711 A CN201710892711 A CN 201710892711A CN 107572802 A CN107572802 A CN 107572802A
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- glaze slip
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Abstract
A kind of glazing process for colorful pottery, include the preparation and glazing of glaze, comprise the following steps that：Step 1: the preparation of glaze：It will be dried after the raw material ball milling of white glaze slip and red glaze slip, uniformly mixed with sodium carboxymethylcellulose sodium carboxymethyl cellulose solution, obtain white glaze slip and red glaze slip；White glaze slip is poured into container, red glaze slip is added toward white glaze slip is interior, after red glaze slip uniformly diffusion, white glaze slip is slowly dropped into the middle part of red glaze slip, is so superimposed 24 times, is finally unidirectionally pulled repeatedly along glaze slip center line repeatedly, much color glaze slurry；Step 2: glazing：Pick after qualified plain tire removing floating dust is dried and insert in centrifuge, carry out inwall glazing；The plain tire of inner chamber glazing is turned clockwise in polychrome glaze slip and taken out after 360 °, unnecessary glaze is removed after air-drying.In summary, while uniform glazing is ensured, the color of colorful glaze in itself will not be destroyed again.
Description
Technical field
The invention belongs to pottery field, more particularly to a kind of glazing process for colorful pottery.
Background technology
An ancient unit of weight kiln is one of Chinese five big kilns of Song Dynasty, is run neck and neck with you, official, brother, fixed all kilns, its moulding is with dignified, muddy
It is thick, simple and unsophisticated, be delicately characteristic, corner angle are clearly demarcated, and lines are graceful, and decorative pattern is terse, air.Pottery traditional work honor, ancient cooking vessel, alms bowl, wash, bottle
Deng stuff, the front yard room put is splendid, and houseful blazes；Old several cases, pleasing, graceful rhythm people.The enamel of pottery is deep
Thoroughly living, sparkling and crystal-clear smooth as jade, in sintering procedure, glaze colours obtains auberigin, sea using copper, iron as main coloring element by " transmutation "
Chinese bush cherry is red, chicken blood is red, Vermilion, famille rose, the glaze paint of fresh green unglazed ten color such as blue or green, sky blue, bluish white, the device having is of the same colour, has
One device polychrome, but can not find identical product.Here it is so-called " unparalleled to match somebody with somebody ", and pottery unique artistic style
One side, the unique artistic style of pottery, always appreciated by domestic and international people from all walks of life, its economic value is more gone together institute
Pay attention to.
The content of the invention
It is an object of the invention to provide a kind of glazing process for colorful pottery.
In order to realize the above object the technical solution adopted in the present invention is：A kind of glazing process for colorful pottery,
Preparation and glazing including glaze, are comprised the following steps that：
Step 1: the preparation of glaze：
A, the raw material of white glaze slip and red glaze slip is added respectively water to insert ball milling in ball mill, the material after ball milling crosses 300-
Dried after 400 mesh sieves, it is standby；
B, sodium carboxymethylcellulose is slowly added in the deionized water that temperature is 50-60 DEG C, it is stirring while adding, continue after mixing
Constant temperature stirs 1-2 hours, obtains sodium carboxymethyl cellulose solution, standby；
C, by dried two kinds of materials in step a respectively with the sodium carboxymethyl cellulose solution in step b according to 1:5-1:3
Ratio uniform mixing, obtain white glaze slip and red glaze slip, it is standby；
D, white glaze slip is poured into container, then toward adding red glaze slip in white glaze slip, after red glaze slip uniformly diffusion,
White glaze slip is slowly dropped into the middle part of red glaze slip, is so superimposed 2-4 times, is finally unidirectionally drawn repeatedly along glaze slip center line repeatedly
Dynamic, much color glaze is starched；
Step 2: glazing：
E, the floating dust picked in qualified plain tire is cleaned out and inserted in centrifuge after being dried, then by step c
White glaze slip be scooped into plain tire inner chamber, starting centrifuge makes glaze layer uniformly be scattered in plain tire inwall, is carried out after pouring out unnecessary glaze slip
Dry；
F, it will turn clockwise in the plain tire of inner chamber glazing in step c polychrome glaze slip in stepb and take out after 360 °, wait to air-dry
Unnecessary glaze is removed afterwards.
Further optimization, the raw material weight number of the white enamel are：The white feldspar of 34-47 parts, 25-27 parts quartz,
12-14 parts calcite, 7-9 parts zircon, 3-5 part alkali stone, 3-5 parts smoothers, 7-9 parts Copper Ores and 3-7 part talcums.
Further optimize, the lithium carbonate that composition by weight is 0.1-0.3 parts is also included in the raw material of the white enamel.
Further optimization, the raw material weight number of the red glaze slip are：2-4 parts iron chloride, 1-3 parts cupric oxide, 1-3
Part potassium chloride, 3-5 parts zinc oxide, 1-3 parts tin oxide, 1-3 parts barium monoxide and 1-3 part glass frits.
Further optimization, the weight ratio of affiliated sodium carboxymethylcellulose and water is 1：240-1：260.
Further optimize, when glaze slip is superimposed in the step d, the dosage of last layer glaze slip is three points of next layer of glaze slip amount
One of.
Further optimize, the plain tire of glazing naturally cools to 200- after 0-1300 DEG C of grand feu in the step f
300 DEG C, then placed 12-24 hours in the sealing container of constant temperature and pressure.
Further optimization, the pressure of the sealing container is 120-140MPa, temperature is 80-110 DEG C.
Beneficial effects of the present invention are broadly divided into four aspects：
First, white enamel is improved into glaze slip with being mixed respectively with sodium carboxymethyl cellulose solution after red glaze material ball mill grinding
Viscosity, more colour glazes caused by helping to prevent the short time internal cause Action of Gravity Field after glazing are broken in pottery surface crossing current
Bad decorative pattern, in addition, because glaze is general mainly using water as dispersant, so cellulose solution concentration is relatively low in the present invention, prevent glaze
Starch influences the absorbability of pottery biscuit because viscosity is excessive, causes glazing difficult；
2nd, white glaze slip and red glaze slip prepare the colorful slurry having a sense of hierarchy by the way of garland is superimposed, and utilize liquid
Stronger mobile performance itself, simple, quick, the effective color effect for meeting needs；
3rd, the constitutive material of white enamel adds lithium carbonate, and lithia, the fluxing effect pole of lithia are introduced by lithium carbonate
It is good, it can strengthen 3-5 times than potassium oxide, sodium oxide molybdena, the coefficient of expansion, high temperature viscosity, melting temperature, softening temperature and solidification can be reduced
Temperature, improve the glossiness of glaze paint；
4th, inwall uniformly smears white glaze slip by the way of centrifuge rotation during glazing, and outer wall rotates pottery element using 360 °
The mode of tire imposes colorful glaze slip to it, which compare brushing glazing, pour glaze, leaching glaze, that the mode of glaze spraying is more conducive to protection is more
Color decorative pattern is not destroyed；
In summary, compared with prior art, pottery glaze slip uses sodium carboxymethyl cellulose solution as adhesion agent to the present invention, and two
The glaze slip of kind of color hybrid modulation by the way of garland, method is simple, easily operated, plain tire inner and outer wall be respectively adopted from
Core type and 360 ° of rotary glazings, while uniform glazing is ensured, the color of colorful glaze in itself will not be destroyed again.
Embodiment
With reference to implementing in detail below, the present invention is described in further detail, and protection scope of the present invention is not limited to
Embodiment once.Process, condition, reagent, the experimental method etc. of the present invention, is ability in addition to the following content specially referred to
The universal knowledege in domain, the content that the present invention is not particularly limited.
Embodiment 1
A kind of glazing process for colorful pottery, include the preparation and glazing of glaze, comprise the following steps that：
Step 1: the preparation of glaze：
A, prepared by white glaze slip, by 34 parts of white feldspars, 25 parts of quartzs, 12 parts of calcites, 7 parts of zircons, 3 parts of alkali stones, 3 parts of cunnings
Powder, 7 parts of Copper Ores, 3 parts of talcums, 0.1 part of lithium carbonate, it is mixed into ball mill and adds water for ball milling, the material after ball milling is crossed 300
Dried after mesh sieve, it is standby；
The preparation of red glaze slip, by 2 parts of iron chloride, 1 part of cupric oxide, 1 part of potassium chloride, 3 parts of zinc oxide, 1 part of tin oxide, 1 part of oxygen
Change barium and 1 part of glass frit, be mixed into ball mill and add water for ball milling, dried after the material after ball milling is crossed into 300 mesh sieves, it is standby
With；
B, it is 1 by ratio:After 240 sodium carboxymethylcellulose uniformly mixes with 50 DEG C of deionized water, it is small to continue constant temperature stirring 1
When, sodium carboxymethyl cellulose solution is obtained, it is standby；
C, by the material of dried two kinds of colors in step a respectively with sodium carboxymethyl cellulose solution according to 1:5 ratio
Uniformly mixing, obtains white glaze slip and red glaze slip, standby；
D, white glaze slip is poured into clean container, then toward red glaze slip is added in white glaze slip, treats that red glaze slip is uniform
After diffusion, white glaze slip is slowly dropped into the middle part of red glaze slip, is so superimposed 2 times repeatedly, every time during two kinds of color additions, on
The dosage of one layer of glaze slip is 1/3rd of next layer of glaze slip amount, is finally unidirectionally pulled repeatedly along glaze slip center line, until being formed equal
Even polychrome glaze slip red and white；
Step 2: glazing：
E, the plain tire Jing Guo biscuiting is picked, picks the floating dust that qualified plain tire is cleared up on surface using spray mode, so
After be dried after be put into centrifuge, the white glaze slip in step c is scooped into plain tire inner chamber, starting centrifuge makes glaze layer in element
Tire inwall uniformly scatters, and is further dried after pouring out unnecessary glaze slip；
F, it will turn clockwise in the plain tire of inner chamber glazing in step c polychrome glaze slip in stepb and take out after 360 °, rotation speed
Degree can not be too fast, leave for plain tire it is enough remove unnecessary glaze after air-drying.
In the present invention, the plain tire of glazing after 0-1300 DEG C of grand feu, naturally cools to 200 DEG C, so in step f
Place it in afterwards in the sealing container that pressure is 120MPa, temperature is 80 DEG C of constant temperature and pressures 12 hours.
Embodiment 2
Step 1: the preparation of glaze：
A, prepared by white glaze slip, by 40 parts of white feldspars, 26 parts of quartzs, 13 parts of calcites, 8 parts of zircons, 4 parts of alkali stones, 3 parts of cunnings
Powder, 8 parts of Copper Ores, 4 parts of talcums, 0.2 part of lithium carbonate, it is mixed into ball mill and adds water for ball milling, the material after ball milling is crossed 350
Dried after mesh sieve, it is standby；
The preparation of red glaze slip, by 3 parts of iron chloride, 2 parts of cupric oxide, 2 parts of potassium chloride, 4 parts of zinc oxide, 2 parts of tin oxide, 2 parts of oxygen
Change barium and 2 parts of glass frits, be mixed into ball mill and add water for ball milling, dried after the material after ball milling is crossed into 350 mesh sieves, it is standby
With；
B, it is 1 by ratio:After 250 sodium carboxymethylcellulose uniformly mixes with 55 DEG C of deionized water, continue constant temperature stirring 1.5
Hour, sodium carboxymethyl cellulose solution is obtained, it is standby；
C, by the material of dried two kinds of colors in step a respectively with sodium carboxymethyl cellulose solution according to 1:5 ratio
Uniformly mixing, obtains white glaze slip and red glaze slip, standby；
D, white glaze slip is poured into clean container, then toward red glaze slip is added in white glaze slip, treats that red glaze slip is uniform
After diffusion, white glaze slip is slowly dropped into the middle part of red glaze slip, is so superimposed 3 times repeatedly, every time during two kinds of color additions, on
The dosage of one layer of glaze slip is 1/3rd of next layer of glaze slip amount, is finally unidirectionally pulled repeatedly along glaze slip center line, until being formed equal
Even polychrome glaze slip red and white；
Step 2: glazing：
E, the plain tire Jing Guo biscuiting is picked, picks the floating dust that qualified plain tire is cleared up on surface using spray mode, so
After be dried after be put into centrifuge, the white glaze slip in step c is scooped into plain tire inner chamber, starting centrifuge makes glaze layer in element
Tire inwall uniformly scatters, and is further dried after pouring out unnecessary glaze slip；
F, it will turn clockwise in the plain tire of inner chamber glazing in step c polychrome glaze slip in stepb and take out after 360 °, rotation speed
Degree can not be too fast, leave for plain tire it is enough remove unnecessary glaze after air-drying.
In the present invention, the plain tire of glazing after 0-1300 DEG C of grand feu, naturally cools to 250 DEG C, so in step f
Place it in afterwards in the sealing container that pressure is 130MPa, temperature is 95 DEG C of constant temperature and pressures 18 hours.
Embodiment 3
Step 1: the preparation of glaze：
A, prepared by white glaze slip, by 47 parts of white feldspars, 27 parts of quartzs, 14 parts of calcites, 9 parts of zircons, 5 parts of alkali stones, 5 parts of cunnings
Powder, 9 parts of Copper Ores, 7 parts of talcums, 0.3 part of lithium carbonate, it is mixed into ball mill and adds water for ball milling, the material after ball milling is crossed 400
Dried after mesh sieve, it is standby；
The preparation of red glaze slip, by 4 parts of iron chloride, 3 parts of cupric oxide, 3 parts of potassium chloride, 5 parts of zinc oxide, 3 parts of tin oxide, 2 parts of oxygen
Change barium and 2 parts of glass frits, be mixed into ball mill and add water for ball milling, dried after the material after ball milling is crossed into 400 mesh sieves, it is standby
With；
B, it is 1 by ratio:After 260 sodium carboxymethylcellulose uniformly mixes with 60 DEG C of deionized water, it is small to continue constant temperature stirring 2
When, sodium carboxymethyl cellulose solution is obtained, it is standby；
C, by the material of dried two kinds of colors in step a respectively with sodium carboxymethyl cellulose solution according to 1:3 ratio
Uniformly mixing, obtains white glaze slip and red glaze slip, standby；
D, white glaze slip is poured into clean container, then toward red glaze slip is added in white glaze slip, treats that red glaze slip is uniform
After diffusion, white glaze slip is slowly dropped into the middle part of red glaze slip, is so superimposed 4 times repeatedly, every time during two kinds of color additions, on
The dosage of one layer of glaze slip is 1/3rd of next layer of glaze slip amount, is finally unidirectionally pulled repeatedly along glaze slip center line, until being formed equal
Even polychrome glaze slip red and white；
Step 2: glazing：
E, the plain tire Jing Guo biscuiting is picked, picks the floating dust that qualified plain tire is cleared up on surface using spray mode, so
After be dried after be put into centrifuge, the white glaze slip in step c is scooped into plain tire inner chamber, starting centrifuge makes glaze layer in element
Tire inwall uniformly scatters, and is further dried after pouring out unnecessary glaze slip；
F, it will turn clockwise in the plain tire of inner chamber glazing in step c polychrome glaze slip in stepb and take out after 360 °, rotation speed
Degree can not be too fast, leave for plain tire it is enough remove unnecessary glaze after air-drying.
In the present invention, the plain tire of glazing after 0-1300 DEG C of grand feu, naturally cools to 300 DEG C, so in step f
Place it in afterwards in the sealing container that pressure is 140MPa, temperature is 110 DEG C of constant temperature and pressures 24 hours.
Claims (8)
1. a kind of glazing process for colorful pottery, it is characterised in that preparation and glazing including glaze, specific steps are such as
Under：
Step 1: the preparation of glaze：
A, the raw material of white glaze slip and red glaze slip is added respectively water to insert ball milling in ball mill, the material after ball milling crosses 300-
Dried after 400 mesh sieves, it is standby；
B, sodium carboxymethylcellulose is slowly added in the deionized water that temperature is 50-60 DEG C, it is stirring while adding, continue after mixing
Constant temperature stirs 1-2 hours, obtains cellulose aqueous solution, standby；
C, by dried two kinds of materials in step a respectively with the cellulose aqueous solution in step b according to 1:5-1:3 ratio is equal
Even mixing, white glaze slip and red glaze slip are obtained, it is standby；
D, white glaze slip is poured into container, then toward adding red glaze slip in white glaze slip, after red glaze slip uniformly diffusion,
White glaze slip is slowly dropped into the middle part of red glaze slip, is so superimposed 2-4 times, is finally unidirectionally drawn repeatedly along glaze slip center line repeatedly
Dynamic, much color glaze is starched；
Step 2: glazing：
E, the floating dust picked in qualified plain tire is cleaned out and inserted in centrifuge after being dried, then by step c
White glaze slip be scooped into plain tire inner chamber, starting centrifuge makes glaze layer uniformly be scattered in plain tire inwall, is carried out after pouring out unnecessary glaze slip
Dry；
F, it will turn clockwise in the plain tire of inner chamber glazing in step c polychrome glaze slip in stepb and take out after 360 °, wait to air-dry
Unnecessary glaze is removed afterwards.
A kind of 2. glazing process for colorful pottery as claimed in claim 1, it is characterised in that the raw material of the white enamel
Parts by weight are：The white feldspar of 34-47 parts, 25-27 parts quartz, 12-14 parts calcite, 7-9 parts zircon, 3-5 part alkali stone,
3-5 parts smoothers, 7-9 parts Copper Ores and 3-7 part talcums.
A kind of 3. glazing process for colorful pottery as claimed in claim 2, it is characterised in that the raw material of the white enamel
In also include composition by weight be 0.1-0.3 parts lithium carbonate.
A kind of 4. glazing process for colorful pottery as claimed in claim 1, it is characterised in that the raw material of the red glaze slip
Parts by weight are：2-4 parts iron chloride, 1-3 parts cupric oxide, 1-3 parts potassium chloride, 3-5 parts zinc oxide, 1-3 parts tin oxide, 1-3 parts
Barium monoxide and 1-3 part glass frits.
A kind of 5. glazing process for colorful pottery as claimed in claim 1, it is characterised in that affiliated sodium carboxymethylcellulose
Weight ratio with water is 1：240-1：260.
6. a kind of glazing process for colorful pottery as claimed in claim 1, it is characterised in that glaze slip is folded in the step d
Added-time, the dosage of last layer glaze slip is 1/3rd of next layer of glaze slip amount.
A kind of 7. glazing process for colorful pottery as claimed in claim 1, it is characterised in that glazing in the step f
Plain tire naturally cools to 200-300 DEG C after 0-1300 DEG C of grand feu, is then placed the sealing container of constant temperature and pressure
Interior 12-24 hours.
A kind of 8. glazing process for colorful pottery as claimed in claim 7, it is characterised in that the pressure of the sealing container
It it is 80-110 DEG C for 120-140MPa, temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710892711.8A CN107572802B (en) | 2017-09-27 | 2017-09-27 | Glazing process for colorful jun porcelain |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710892711.8A CN107572802B (en) | 2017-09-27 | 2017-09-27 | Glazing process for colorful jun porcelain |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107572802A true CN107572802A (en) | 2018-01-12 |
| CN107572802B CN107572802B (en) | 2020-06-26 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710892711.8A Expired - Fee Related CN107572802B (en) | 2017-09-27 | 2017-09-27 | Glazing process for colorful jun porcelain |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1224076A (en) * | 1998-12-23 | 1999-07-28 | 广东佛陶集团赛纳陶瓷有限公司 | Glaze texture forming process |
| CN104649719A (en) * | 2015-01-30 | 2015-05-27 | 许昌学院 | Glazing method of jun porcelain glaze |
| CN105036811A (en) * | 2015-07-24 | 2015-11-11 | 郏县神前传奇陶瓷钧瓷厂 | White-ground red-spot composite tangjun glaze and process of preparing jun porcelain with same |
| CN106348590A (en) * | 2016-08-26 | 2017-01-25 | 温书强 | Jun porcelain glaze and application method thereof |
-
2017
- 2017-09-27 CN CN201710892711.8A patent/CN107572802B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1224076A (en) * | 1998-12-23 | 1999-07-28 | 广东佛陶集团赛纳陶瓷有限公司 | Glaze texture forming process |
| CN104649719A (en) * | 2015-01-30 | 2015-05-27 | 许昌学院 | Glazing method of jun porcelain glaze |
| CN105036811A (en) * | 2015-07-24 | 2015-11-11 | 郏县神前传奇陶瓷钧瓷厂 | White-ground red-spot composite tangjun glaze and process of preparing jun porcelain with same |
| CN106348590A (en) * | 2016-08-26 | 2017-01-25 | 温书强 | Jun porcelain glaze and application method thereof |
Non-Patent Citations (4)
| Title |
|---|
| 仁英歌等编著: "《中华文脉：中国陶瓷艺术.钧瓷》", 31 March 2013, 黑龙江美术出版社 * |
| 孙彦春主编: "《中国钧窑志》", 31 October 2011, 中州古籍出版社 * |
| 江苏省陶瓷工业科技情报站等著: "《陶瓷译文集》", 31 December 1983, 江苏省宜兴县丁蜀人民印刷厂印刷 * |
| 池至铣编著: "《陶瓷釉色料及装饰》", 30 November 2015, 中国建材工业出版社 * |
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