CN107558243A - A kind of wormwood essential oil and the microcapsules brassiere finishing agent and preparation method of Geranium Essential compounding - Google Patents
A kind of wormwood essential oil and the microcapsules brassiere finishing agent and preparation method of Geranium Essential compounding Download PDFInfo
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- CN107558243A CN107558243A CN201710780133.9A CN201710780133A CN107558243A CN 107558243 A CN107558243 A CN 107558243A CN 201710780133 A CN201710780133 A CN 201710780133A CN 107558243 A CN107558243 A CN 107558243A
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Abstract
The invention discloses a kind of wormwood essential oil and the microcapsules brassiere finishing agent and preparation method of Geranium Essential compounding, including wick and capsule skin, the wick is using wormwood essential oil, Geranium Essential as major ingredient and adds the microcapsules wick that surfactant, solvent, assistant for emulsifying agent be combined into, the capsule skin is using high polymer material as capsule leather material and with deionized water dissolving, the high score ascus leather material aqueous solution is prepared into, described high polymer material refers to natural macromolecular material or artificial synthesized high polymer material.The high polymer material of present invention non-toxic and safe gets up wormwood, Geranium Essential cladding, it is prepared into the microcapsules textile finish with slow-release function, wormwood essential oil, Geranium Essential is set to be used for the arrangement of textile, simultaneously solve the problems, such as plants essential oil be easy to volatilization, easily decomposes action time on the textile it is short, make common brassiere that there is certain antimicrobial health care function, it is not volatile and function is lasting.
Description
Technical field
The present invention relates to a kind of technical field of functions of textile fabrics finishing agent, particularly a kind of wormwood essential oil and fish pelargonium
The microcapsules brassiere finishing agent and preparation method of essential oil compounding.
Background technology
Wormwood essential oil is using wormwood herb as raw material, is extracted through steam distillation or carbon dioxide supercritical extraction method
Plants essential oil, mainly contain：A variety of Chinese herbal medicine active components such as wormwood element, rutin sophorin, wormwood essential oil have anti-inflammation, promote
Capillary blood circulates, the function such as antiallergy.
Geranium Essential extracts from fish pelargonium cauline leaf, low boiling point, high volatility, has anti-herpesvirus, anti-human nipple
Tumor virus, anti-Staphylococcus aureus isoreactivity, be a kind of preventing mammary gland hyperplasia health plant essential oil.
Brassiere is women underwear, and directly and skin contact, the invasive organism grown on brassiere often triggers mastitis, breast
The diseases such as gland hyperplasia.
Therefore the present invention is prepared into microcapsules brassiere finishing agent with wormwood essential oil and Geranium Essential compounding, by brassiere
Impregnation processability micro- glue is attached in the face liber of brassiere, with the fragrance and antibacterial of wormwood and India sunflower protect
Health-care function, and be the upgrading of yarn fabric, increase technology content and lay technical foundation.
The content of the invention
A kind of nontoxic, safe wormwood essential oil is provided the invention aims to solve above-mentioned the deficiencies in the prior art
With the microcapsules brassiere finishing agent and preparation method of Geranium Essential compounding.Present invention high polymer material is by wormwood essential oil, day
Zhu Kuihua claddings are got up, and are prepared into the textile finish with slow-release function, are enable wormwood essential oil, India sunflower to be used to weave
Arrangement.Solve plants essential oil and volatilize, easily decompose, the problems such as action time is very short on the textile, have common brassiere
There is certain antimicrobial health care function.
To achieve these goals, a kind of wormwood essential oil designed by the present invention and the microcapsules text of Geranium Essential compounding
Chest finishing agent, including wick and capsule skin, the wick are using wormwood essential oil, Geranium Essential as major ingredient and add surface-active
Agent, solvent, assistant for emulsifying agent and the microcapsules wick being combined into, the capsule skin be using high polymer material as capsule leather material and spend from
Sub- water dissolving, is prepared into the high score ascus leather material aqueous solution, and described high polymer material refers to natural macromolecular material or artificial
High polymer material is synthesized, the natural macromolecular material refers to natural animal glue, natural plant gum, one kind or more of marine organisms glue
Kind, described artificial synthesized high polymer material is acrylic acid, polyacrylic acid, methacrylic acid, polymethylacrylic acid, polyacrylic acid
The compound composition of one or both of sodium, polyethylene glycol, described surfactant are sorbitan monooleate, sorbierite
APEO, sorbitan monostearate, tetraethylene glycol monostearate, ethoxylated dodecyl alcohol, polyoxyethylene
Anhydrous sorbitol tristearate, polyoxyethylene 20 sorbitan monopalmitate, the solvent are maize germ oil, wheat
One or more double solvents in bud oil, rice skin health oil, grape-kernel oil, dihydro jasmone acid formicester, benzyl acetate.
Further, the natural macromolecular material is gelatin, xanthans, peach gum, Arabic gum, sodium alginate, chitin
One or more in glue, milk casein glue.
Further, the assistant for emulsifying agent is the one or more in propane diols, glycerine, polyethylene glycol, ethanol.
The invention also discloses the preparation side of a kind of wormwood essential oil and the microcapsules brassiere finishing agent of Geranium Essential compounding
Method, including the raw material using a kind of wormwood essential oil described above and the microcapsules brassiere finishing agent of Geranium Essential compounding,
Characterized in that, prepare the specific steps for the microcapsules brassiere finishing agent that a kind of above-mentioned wormwood essential oil compounds with Geranium Essential such as
Under：
A, the preparation of microcapsule wall material
It is gelatin, xanthans, peach gum, Arabic gum, sodium alginate, chitin glue, milk junket by natural macromolecular material
40-60 DEG C of deionized water dissolving of one or more in protein adhesive, becomes water-soluble polymers, dissolves the reaction time
30min-12h；
B, the preparation of microcapsules core
The wormwood essential oil and Geranium Essential of design flow are weighed, and the gross weight of above-mentioned two essential oil accounts for the 19- of microcapsules
80%th, 1-5% solvent, 19-50% surfactant, 19-20% assistant for emulsifying agent, heating dissolve by heating, temperature control
At 30-100 DEG C；
C, the preparation of plants essential oil core material emulsion
Core material solution after the completion of step B is heated, when temperature reaches 30-100 DEG C, isothermal reaction 10min, stirred
Mix under machine stirring, add 30-100 DEG C of deionized water 19-80%, emulsion dispersion 1-10min, and move on high-speed shearing emulsion machine
1-60min is handled, obtains core material emulsion；
D, microcapsule dressing agent synthesizes
The water-soluble polymers that step A is obtained, heating heating are measured, temperature control adds step C and obtained at 30-100 DEG C
Plants essential oil core material emulsion, with handling 1-30min on high-speed shearing emulsion machine, the isothermal reaction time under mixer stirring
1h-12h；20-25 DEG C of normal temperature is cooled to, obtains microcapsule dressing agent.
A kind of wormwood essential oil that the present invention obtains and the microcapsules brassiere finishing agent and preparation method of Geranium Essential compounding,
With advantages below：
1st, it is an advantage of the invention that wormwood, Geranium Essential cladding are got up with the high polymer material of non-toxic and safe, prepare
Into the microcapsules textile finish with slow-release function, wormwood essential oil, Geranium Essential is set to be used for the arrangement of textile.
2 at the same solve the problems, such as plants essential oil be easy to volatilization, easily decomposes action time on the textile it is short, make general
Logical brassiere has certain antimicrobial health care function, and function is lasting, not volatile.
Embodiment
The present embodiment is further illustrated below.
Embodiment 1：
A kind of wormwood essential oil that the present embodiment provides and the microcapsules brassiere finishing agent of Geranium Essential compounding, including wick
With capsule skin, the wick be using wormwood essential oil, Geranium Essential as major ingredient and add surfactant, solvent, assistant for emulsifying agent and
The microcapsules wick being combined into, the capsule skin are using high polymer material as capsule leather material and with deionized water dissolving, are prepared into height
The molecule capsule leather material aqueous solution, described high polymer material refer to natural macromolecular material or artificial synthesized high polymer material, institute
State natural macromolecular material and refer to natural animal glue, natural plant gum, the one or more of marine organisms glue, described artificial synthesized height
Molecular material is one kind in acrylic acid, polyacrylic acid, methacrylic acid, polymethylacrylic acid, Sodium Polyacrylate, polyethylene glycol
Or both compound composition, described surfactant be sorbitan monooleate, sorbitol polyoxyethylene ether, Sorbitan
Alcohol monostearate, tetraethylene glycol monostearate, ethoxylated dodecyl alcohol, the stearic acid of polyoxyethylene sorbitan three
Ester, polyoxyethylene 20 sorbitan monopalmitate, the solvent are maize germ oil, wheat-germ oil, rice skin health oil, Portugal
One or more double solvents in grape seed oil, dihydro jasmone acid formicester, benzyl acetate.
Further, the natural macromolecular material is gelatin, xanthans, peach gum, Arabic gum, sodium alginate, chitin
One or more in glue, milk casein glue.
Further, the assistant for emulsifying agent is the one or more in propane diols, glycerine, polyethylene glycol, ethanol.
The present embodiment also discloses the preparation of a kind of wormwood essential oil and the microcapsules brassiere finishing agent of Geranium Essential compounding
Method, including the former material using a kind of wormwood essential oil described above and the microcapsules brassiere finishing agent of Geranium Essential compounding
Material, it is characterised in that prepare the specific step of a kind of above-mentioned wormwood essential oil and the microcapsules brassiere finishing agent of Geranium Essential compounding
It is rapid as follows：
A, the preparation of microcapsule wall material
It is gelatin, xanthans, peach gum, Arabic gum, sodium alginate, chitin glue, milk junket by natural macromolecular material
40-60 DEG C of deionized water dissolving of one or more in protein adhesive, becomes water-soluble polymers, dissolves the reaction time
30min-12h；
B, the preparation of microcapsules core
The wormwood essential oil and Geranium Essential of design flow are weighed, and the gross weight of above-mentioned two essential oil accounts for the 19- of microcapsules
80%th, 1-5% solvent, 19-50% surfactant, 19-20% assistant for emulsifying agent, heating dissolve by heating, temperature control
At 30-100 DEG C；
C, the preparation of plants essential oil core material emulsion
Core material solution after the completion of step B is heated, when temperature reaches 30-100 DEG C, isothermal reaction 10min, stirred
Mix under machine stirring, add 30-100 DEG C of deionized water 19-80%, emulsion dispersion 1-10min, and move on high-speed shearing emulsion machine
1-60min is handled, obtains core material emulsion；
D, microcapsule dressing agent synthesizes
The water-soluble polymers that step A is obtained, heating heating are measured, temperature control adds step C and obtained at 30-100 DEG C
Plants essential oil core material emulsion, with handling 1-30min on high-speed shearing emulsion machine, the isothermal reaction time under mixer stirring
1h-12h；20-25 DEG C of normal temperature is cooled to, obtains microcapsule dressing agent.
Microcapsules brassiere finishing agent and preparation side of a kind of wormwood essential oil that the present embodiment obtains with Geranium Essential compounding
Method, there is advantages below：
3rd, advantage of this embodiment is that wormwood, Geranium Essential cladding are got up with the high polymer material of non-toxic and safe, system
For into the microcapsules textile finish with slow-release function, wormwood essential oil, Geranium Essential is set to be used for the arrangement of textile.
4 at the same solve the problems, such as plants essential oil be easy to volatilization, easily decomposes action time on the textile it is short, make general
Logical brassiere has certain antimicrobial health care function, and function is lasting, not volatile.
Natural macromolecular material alginic acid is used in the present embodiment, weighs wormwood essential oil 10g and Geranium Essential 80g,
Both are provided as 1:8, sorbitan monooleate 30g, maize germ oil 250g, glycerine 2g, altogether 372g, heating are heated
To 55 DEG C of dissolvings, then 55 DEG C of deionized water 100ml, emulsion dispersion 5min are added, and move on high-speed shearing emulsion machine and handle
5min, obtain core material emulsion；It is stand-by；
It is that sodium alginate is dissolved in 99 times of water by natural macromolecular material, heating is heated to 90 DEG C, dissolves under agitation
4h, turn into water-soluble polymers；It is standby；
582ml water-soluble polymers are added in core material emulsion, 55 DEG C of reaction time 4h of constant temperature under mixer stirring；It is cold
But to 25 DEG C, microcapsule dressing agent is obtained.
Embodiment 2：
The preparation method for the microcapsules brassiere finishing agent that a kind of wormwood essential oil of the present embodiment compounds with Geranium Essential is：
Artificial synthesized high polymer material is used in the present embodiment:Sodium Polyacrylate, weigh 112g Sodium Polyacrylates be dissolved in 550ml go from
In sub- water, heating is heated to 60 DEG C, dissolves 1h under agitation, and it is water-soluble to obtain the Sodium Polyacrylate microcapsule wall material that concentration is 2%
Liquid, as water-soluble polymers；It is standby；
Wormwood essential oil 10g and Geranium Essential 80g are weighed, both are provided as 1:8, dihydro jasmone acid formicester 250g, lose
Water sorbitol monooleate 20g；Polyoxyethylene 20 sorbitan tristearate 8g；Heating is heated to 60 DEG C of dissolving 30min, then
60 DEG C of deionized water 100ml, emulsion dispersion 10min are added, and moves into and 10min is handled on high-speed shearing emulsion machine, obtains core breast
Liquid；It is stand-by；
532ml water-soluble polymers are added in core material emulsion, after handling 2min with high-speed shearing machine, stirred in mixer
Lower 60 DEG C of reaction time 1h of constant temperature；The 3g methyl-propyls acid glycol ester drop of addition one per minute into system, after the completion of addition, after
Continuous isothermal reaction 3h, obtains microcapsule dressing agent.
Embodiment 3：
The preparation method for the microcapsules brassiere finishing agent that a kind of wormwood essential oil of the present embodiment compounds with Geranium Essential is：
It is gelatin, xanthans, peach gum, Arabic gum that natural macromolecular material is used in the present embodiment, weighs 50g gelatin, 50g xanthans
It is dissolved in 50g peach gums, 10g Arabic gums in 550ml deionized water, heating is heated to 45 DEG C, dissolves 4h under agitation, obtains
Water-soluble polymers；It is standby；
Wormwood essential oil 20g and Geranium Essential 160g are weighed, both are provided as 1:8, dihydro jasmone acid formicester 250g, rise
Temperature is heated to 75 DEG C of dissolving 15min, then adds 75 DEG C of deionized water 100ml, emulsion dispersion 10min, and moves into high speed shear breast
5min is handled on change machine, obtains core material emulsion；It is stand-by；
585ml water-soluble polymers are added in core material emulsion, after handling 15min with high-speed shearing machine, stirred in mixer
Mix lower 45 DEG C of reaction time 3h of constant temperature；Obtain microcapsule dressing agent.
Embodiment 4：
Present embodiment discloses the preparation side of a kind of wormwood essential oil and the microcapsules brassiere finishing agent of Geranium Essential compounding
Method, it is characterised in that prepare the specific step of a kind of above-mentioned wormwood essential oil and the microcapsules brassiere finishing agent of Geranium Essential compounding
It is rapid as follows：
A, the preparation of microcapsule wall material
It is the deionized water dissolving in xanthans, sodium alginate, milk casein glue with 55 DEG C by natural macromolecular material,
Water-soluble polymers are become, dissolve reaction time 8h；
B, the preparation of microcapsules core
The wormwood essential oil and Geranium Essential of design flow are weighed, and the gross weight of above-mentioned two essential oil accounts for the 80% of microcapsules,
Wherein wormwood essential oil：The ratio 1 of Geranium Essential:1,2% solvent, 40% surfactant, 19% assistant for emulsifying agent, rise
Temperature dissolves by heating, and temperature control is at 30-100 DEG C；
C, the preparation of plants essential oil core material emulsion
Core material solution after the completion of step B is heated, when temperature reaches 68 DEG C, isothermal reaction 10min, in mixer
Under stirring, 368 DEG C of deionized waters 60%, emulsion dispersion 5min are added, and moves into and 30min is handled on high-speed shearing emulsion machine, is obtained
Core material emulsion；
D, microcapsule dressing agent synthesizes
The water-soluble polymers that step A is obtained, heating heating are measured, temperature control adds the plant that step C is obtained at 80 DEG C
Thing essential oil core material emulsion, with handling 20min on high-speed shearing emulsion machine, the isothermal reaction time 4h under mixer stirring；Cooling
To 25 DEG C, microcapsule dressing agent is obtained.
The ratio of deionized water is the 19-80% of microcapsules core gross weight in above-mentioned several embodiments.
Claims (4)
1. a kind of wormwood essential oil and the microcapsules brassiere finishing agent of Geranium Essential compounding, it is characterised in that including wick and capsule
Skin, the wick are using wormwood essential oil, Geranium Essential as major ingredient and add surfactant, solvent, assistant for emulsifying agent and combine
Into microcapsules wick, the capsule skin is using high polymer material as capsule leather material and with deionized water dissolving, is prepared into macromolecule
The capsule leather material aqueous solution, described high polymer material refer to natural macromolecular material or artificial synthesized high polymer material, the day
Right high polymer material refers to natural animal glue, natural plant gum, the one or more of marine organisms glue, described artificial synthesized macromolecule
Material is one kind or two in acrylic acid, polyacrylic acid, methacrylic acid, polymethylacrylic acid, Sodium Polyacrylate, polyethylene glycol
The compound composition of person, described surfactant are sorbitan monooleate, sorbitol polyoxyethylene ether, anhydrous sorbitol list
Stearate, tetraethylene glycol monostearate, ethoxylated dodecyl alcohol, polyoxyethylene 20 sorbitan tristearate, gather
Oxygen ethene sorbitan monopalmitate, the solvent are maize germ oil, wheat-germ oil, rice skin health oil, grape pip
One or more double solvents in oil, dihydro jasmone acid formicester, benzyl acetate.
2. a kind of wormwood essential oil according to claim 1 and the microcapsules brassiere finishing agent of Geranium Essential compounding, it is special
Sign is that the natural macromolecular material is gelatin, xanthans, peach gum, Arabic gum, sodium alginate, chitin glue, milk junket
One or more in protein adhesive.
3. a kind of wormwood essential oil according to claim 1 or 2 and the microcapsules brassiere finishing agent of Geranium Essential compounding, its
It is characterised by, the assistant for emulsifying agent is the one or more in propane diols, glycerine, polyethylene glycol, ethanol.
4. the preparation method of a kind of wormwood essential oil and the microcapsules brassiere finishing agent of Geranium Essential compounding, including use above-mentioned power
Profit requires the raw material of a kind of wormwood essential oil and the microcapsules brassiere finishing agent of Geranium Essential compounding described in 3, and its feature exists
In preparing comprising the following steps that for the microcapsules brassiere finishing agent that a kind of above-mentioned wormwood essential oil compounds with Geranium Essential：
A, the preparation of microcapsule wall material
It is gelatin, xanthans, peach gum, Arabic gum, sodium alginate, chitin glue, milk casein by natural macromolecular material
40-60 DEG C of deionized water dissolving of one or more in glue, becomes water-soluble polymers, dissolves the reaction time
30min-12h；
B, the preparation of microcapsules core
The wormwood essential oil and Geranium Essential of design flow are weighed, and the gross weight of above-mentioned two essential oil accounts for 19-80%, 1- of microcapsules
5% solvent, 19-50% surfactant, 19-20% assistant for emulsifying agent, heating dissolve by heating, and temperature control is in 30-100
℃；
C, the preparation of plants essential oil core material emulsion
Core material solution after the completion of step B is heated, when temperature reaches 30-100 DEG C, isothermal reaction 10min, stirred in mixer
Mix down, add 30-100 DEG C of deionized water 19-80%, emulsion dispersion 1-10min, and move into and 1- is handled on high-speed shearing emulsion machine
60min, obtain core material emulsion；
D, microcapsule dressing agent synthesizes
The water-soluble polymers that step A is obtained, heating heating are measured, temperature control adds the plant that step C is obtained at 30-100 DEG C
Thing essential oil core material emulsion, with handling 1-30min on high-speed shearing emulsion machine, the isothermal reaction time 1h- under mixer stirring
12h；20-25 DEG C of normal temperature is cooled to, obtains microcapsule dressing agent.
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| CN109718136A (en) * | 2019-01-25 | 2019-05-07 | 重庆真艾农业有限公司 | A kind of skin liniment based on wormwood essential oil, phosphatide and pyrroloquinoline quinone |
| CN110184823A (en) * | 2019-06-15 | 2019-08-30 | 南通宏石家居用品有限公司 | A kind of natural antibacterial disappears taste Korean pine microcapsules cotton by core, manufacturing method |
| CN110205827A (en) * | 2019-06-15 | 2019-09-06 | 南通宏石家居用品有限公司 | A kind of anti-mite taste Korean pine microcapsules mattress manufacture method that disappears of natural antibacterial |
| CN110205828A (en) * | 2019-06-20 | 2019-09-06 | 东莞简越服饰有限公司 | A kind of plants essential oil microcapsules and preparation method thereof |
| CN110713614A (en) * | 2019-10-22 | 2020-01-21 | 浙江海洋大学 | Preparation method of essential oil slow-release preservative film |
| CN111621986A (en) * | 2019-12-05 | 2020-09-04 | 山东汇高智慧纺织科技有限公司 | Multifunctional fabric containing mosquito-repellent microcapsules and preparation method thereof |
| CN113684690A (en) * | 2021-09-07 | 2021-11-23 | 百事基材料（青岛）股份有限公司 | Polyester macrobiotic fabric containing jasmine active ingredients and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109718136A (en) * | 2019-01-25 | 2019-05-07 | 重庆真艾农业有限公司 | A kind of skin liniment based on wormwood essential oil, phosphatide and pyrroloquinoline quinone |
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| CN110205827A (en) * | 2019-06-15 | 2019-09-06 | 南通宏石家居用品有限公司 | A kind of anti-mite taste Korean pine microcapsules mattress manufacture method that disappears of natural antibacterial |
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| CN111621986A (en) * | 2019-12-05 | 2020-09-04 | 山东汇高智慧纺织科技有限公司 | Multifunctional fabric containing mosquito-repellent microcapsules and preparation method thereof |
| CN113684690A (en) * | 2021-09-07 | 2021-11-23 | 百事基材料（青岛）股份有限公司 | Polyester macrobiotic fabric containing jasmine active ingredients and preparation method thereof |
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Application publication date: 20180109 |
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