CN107557798A - A kind of fastener raw material acid cleaning process - Google Patents

A kind of fastener raw material acid cleaning process Download PDF

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Publication number
CN107557798A
CN107557798A CN201711013213.8A CN201711013213A CN107557798A CN 107557798 A CN107557798 A CN 107557798A CN 201711013213 A CN201711013213 A CN 201711013213A CN 107557798 A CN107557798 A CN 107557798A
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CN
China
Prior art keywords
raw material
pickling
kept
minutes
soaked
Prior art date
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Pending
Application number
CN201711013213.8A
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Chinese (zh)
Inventor
徐建华
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suzhou Huafeng Stainless Steel Fastener Co Ltd
Original Assignee
Suzhou Huafeng Stainless Steel Fastener Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Suzhou Huafeng Stainless Steel Fastener Co Ltd filed Critical Suzhou Huafeng Stainless Steel Fastener Co Ltd
Priority to CN201711013213.8A priority Critical patent/CN107557798A/en
Publication of CN107557798A publication Critical patent/CN107557798A/en
Pending legal-status Critical Current

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  • Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)

Abstract

The invention discloses a kind of fastener raw material acid cleaning process, comprise the following steps that:Pickling, washing, oxalic acid immersion, epithelium processing, washing, coating lubricant;Fastener raw material are soaked in No.1 pickling tube, kept for 5 minutes, are taken out, it is soaked in No. two pickling tubes, kept for 5 minutes, take out, be soaked in No. three pickling tubes, kept for five minutes, take out, washed, the corrosion product on the raw material surface is removed, then it is immersed in oxalic acid pond, kept for 10 minutes, taken out, be soaked into progress epithelium processing in phosphoric acid salt pond, kept for 15 minutes, take out, washed again, remove residue, coating lubricant is taken out after cleaning, the lubricant is soda soap.Through the above way; the present invention can remove the oxide-film on fastener raw material surface; and form one layer of phosphate film on raw material surface; with reliable protective value; it can prevent from taking out line in wire rod and cut scratch of the stages such as material, punching press to raw material surface; and the acid cleaning process process is simple, excellent effect, can effectively reduce production cost.

Description

A kind of fastener raw material acid cleaning process
Technical field
The present invention relates to pickling field, more particularly to a kind of fastener raw material acid cleaning process.
Background technology
It is referred to as pickling using the oxide skin on acid solution removal steel surface and the method for rust.It is cleaning metal surface A kind of method.Generally carried out together with pre- film.Product is typically immersed to the aqueous solution of sulfuric acid etc., to remove the oxygen of metal surface The films such as compound.It is pre-treatment or the intermediate treatment of the techniques such as plating, enamel, rolling.The acid cleaning process used at this stage removes Stainless steel surfaces heavy scale, temperature in use is high, pickling time length, causes processing cost to remain high;And normal temperature descales Technique to except thin oxide skin effect it is good, undesirable to heavy scale effect, particularly the black slag of weld is not substantially except falling.
How to design that a kind of descale effect is good, while the pickling that fastener raw material can be given to provide high-quality diaphragm Technique, it is to need to solve the problems, such as.
The content of the invention
The present invention solves the technical problem of a kind of fastener raw material acid cleaning process is provided, fastener can be removed The oxide-film on raw material surface, and one layer of phosphate film is formed on raw material surface, there is reliable protective value, can be to prevent Only line is taken out in wire rod and cut scratch of the stages such as material, punching press to raw material surface, and the acid cleaning process process is simple, Excellent effect, it can effectively reduce production cost.
In order to solve the above technical problems, one aspect of the present invention is:A kind of fastener raw material acid is provided Technique is washed, is comprised the following steps that:Pickling, washing, oxalic acid immersion, epithelium processing, washing, coating lubricant;By fastener former material Material is soaked in No.1 pickling tube, is kept for 5 minutes, is taken out, is soaked in No. two pickling tubes, is kept for 5 minutes, is taken out, is soaked in In No. three pickling tubes, kept for five minutes, take out, washed, the corrosion product on the raw material surface is removed, then soaked In oxalic acid pond, kept for 10 minutes, taken out, be soaked into progress epithelium processing in phosphoric acid salt pond, kept for 15 minutes, taken out, again Washed, remove residue, coating lubricant is taken out after cleaning, the lubricant is soda soap.
In a preferred embodiment of the present invention, the No.1 pickling tube, No. two pickling tubes, in No. three pickling tubes be salt Acid solution.
In a preferred embodiment of the present invention, the No.1 pickling tube, No. two pickling tubes, hydrochloric acid is molten in No. three pickling tubes Liquid concentration is respectively 22%, 23%, 25%.
In a preferred embodiment of the present invention, concentration of oxalic acid is 28% in the oxalic acid pond.
The beneficial effects of the invention are as follows:The present invention can remove the oxide-film on fastener raw material surface, and in raw material Surface forms one layer of phosphate film, has reliable protective value, can prevent from taking out line in wire rod and cut the ranks such as material, punching press Scratch of the section to raw material surface, and the acid cleaning process process is simple, excellent effect, can effectively reduce and be produced into This.
Embodiment
Presently preferred embodiments of the present invention is described in detail below so that advantages and features of the invention can be easier to by It will be appreciated by those skilled in the art that apparent clearly defined so as to be made to protection scope of the present invention.
The embodiment of the present invention includes:
A kind of fastener raw material acid cleaning process, is comprised the following steps that:Pickling, washing, oxalic acid immersion, epithelium processing, washing, painting Cover lubricant;Fastener raw material are soaked in No.1 pickling tube, kept for 5 minutes, takes out, is soaked in No. two pickling tubes, Kept for 5 minutes, take out, be soaked in No. three pickling tubes, kept for five minutes, taken out, washed, by the raw material surface Corrosion product removes, and is then immersed in oxalic acid pond, is kept for 10 minutes, takes out, and is soaked into progress epithelium processing in phosphoric acid salt pond, Kept for 15 minutes, take out, washed again, remove residue, coating lubricant is taken out after cleaning, the lubricant is Soda soap.The coefficient of friction of phosphate coating is higher, by coating soda soap, can effectively improve greasy property, facilitate next step work The progress of sequence.
Further illustrate, the No.1 pickling tube, No. two pickling tubes, in No. three pickling tubes be hydrochloric acid solution.Hydrochloric acid is molten Liquid energy is enough by chemical reaction, the oxide-film in quick acidolysis materials statement face, plays scavenging action.
Further illustrate, the No.1 pickling tube, No. two pickling tubes, concentration of hydrochloric acid solution is respectively in No. three pickling tubes 22%、23%、25%.Experiment proves that for concentration of hydrochloric acid when between 20% to 25%, its reaction rate, the extent of reaction are optimal.
Illustrate further, concentration of oxalic acid is 28% in oxalic acid pond.Steel surface with oxalic acid by reacting, it is possible to increase its Metal active so that caused epithelium more compact and firm in subsequent processing.
The present invention can remove the oxide-film on fastener raw material surface, and thin in raw material surface one layer of phosphate of formation Film, there is reliable protective value, can prevent from taking out line in wire rod and cut wiping of the stages such as material, punching press to raw material surface Wound, and the acid cleaning process process is simple, excellent effect, can effectively reduce production cost.
Embodiments of the invention are the foregoing is only, are not intended to limit the scope of the invention, it is every to utilize this hair The equivalent structure or equivalent flow conversion that bright description is made, or directly or indirectly it is used in other related technology necks Domain, it is included within the scope of the present invention.

Claims (4)

1. a kind of fastener raw material acid cleaning process, it is characterised in that comprise the following steps that:Pickling, washing, oxalic acid immersion, skin Film process, washing, coating lubricant;Fastener raw material are soaked in No.1 pickling tube, kept for 5 minutes, takes out, is soaked in In No. two pickling tubes, kept for 5 minutes, take out, be soaked in No. three pickling tubes, kept for five minutes, taken out, washed, by institute The corrosion product for stating raw material surface removes, and is then immersed in oxalic acid pond, is kept for 10 minutes, takes out, is soaked into phosphoric acid salt pond Interior progress epithelium processing, is kept for 15 minutes, takes out, washed again, remove residue, and coating lubrication is taken out after cleaning Agent, the lubricant are soda soap.
2. fastener raw material acid cleaning process according to claim 1, it is characterised in that the No.1 pickling tube, No. two It is hydrochloric acid solution in pickling tube, No. three pickling tubes.
3. fastener raw material acid cleaning process according to claim 1, it is characterised in that the No.1 pickling tube, No. two Concentration of hydrochloric acid solution is respectively 22%, 23%, 25% in pickling tube, No. three pickling tubes.
4. fastener raw material acid cleaning process according to claim 1, it is characterised in that concentration of oxalic acid in the oxalic acid pond For 28%.
CN201711013213.8A 2017-10-25 2017-10-25 A kind of fastener raw material acid cleaning process Pending CN107557798A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711013213.8A CN107557798A (en) 2017-10-25 2017-10-25 A kind of fastener raw material acid cleaning process

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711013213.8A CN107557798A (en) 2017-10-25 2017-10-25 A kind of fastener raw material acid cleaning process

Publications (1)

Publication Number Publication Date
CN107557798A true CN107557798A (en) 2018-01-09

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CN201711013213.8A Pending CN107557798A (en) 2017-10-25 2017-10-25 A kind of fastener raw material acid cleaning process

Country Status (1)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110760648A (en) * 2019-11-14 2020-02-07 北京金兆博高强度紧固件有限公司 Weather-resistant bolt production process
CN112921332A (en) * 2021-03-25 2021-06-08 海盐万达汽车配件股份有限公司 Screw pickling system

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104209705A (en) * 2014-08-22 2014-12-17 无锡市第二标准件制造有限公司 Manufacturing process of screw
CN104862717A (en) * 2015-05-08 2015-08-26 青岛锻艺金属有限公司 Closed internal acid washing process
CN106555189A (en) * 2015-09-30 2017-04-05 明光市久鼎五金制品有限公司 A kind of screw pickling processing method

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104209705A (en) * 2014-08-22 2014-12-17 无锡市第二标准件制造有限公司 Manufacturing process of screw
CN104862717A (en) * 2015-05-08 2015-08-26 青岛锻艺金属有限公司 Closed internal acid washing process
CN106555189A (en) * 2015-09-30 2017-04-05 明光市久鼎五金制品有限公司 A kind of screw pickling processing method

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110760648A (en) * 2019-11-14 2020-02-07 北京金兆博高强度紧固件有限公司 Weather-resistant bolt production process
CN112921332A (en) * 2021-03-25 2021-06-08 海盐万达汽车配件股份有限公司 Screw pickling system

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Application publication date: 20180109