CN107555917A - A kind of water-proof plugging material and preparation method thereof - Google Patents

A kind of water-proof plugging material and preparation method thereof Download PDF

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Publication number
CN107555917A
CN107555917A CN201710702896.1A CN201710702896A CN107555917A CN 107555917 A CN107555917 A CN 107555917A CN 201710702896 A CN201710702896 A CN 201710702896A CN 107555917 A CN107555917 A CN 107555917A
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parts
water
cement
plugging material
proof plugging
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CN107555917B (en
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张宁
常英
吴应林
耿刚
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Oriental Yuhong Civil Building Materials LLC
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Oriental Yuhong Civil Building Materials LLC
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Abstract

The invention discloses a kind of water-proof plugging material and preparation method thereof, it is related to building material technical field.The water-proof plugging material of the present invention includes following components:300 600 parts of sulphate aluminium cement, 200 400 parts of perhafnate cement, 100 200 parts of powdered whiting, wash 100 200 parts of river sand, 0.2 1 parts of accelerator, 0.2 0.5 parts of water-loss reducer, 0.5 2 parts of water reducer, 36 parts of re-dispersible glue powder, 0.3 0.5 parts of defoamer, 13 parts of powder levelling agent, 0.1 0.2 parts of polypropylene fibre.The loss circulation material combination property of the present invention is stronger, meets basic reinforcement demand, and water impermeability is good, short construction period, cheap, solves the levelling problem of worker's construction, has better effects for basic unit's leak stopping.

Description

A kind of water-proof plugging material and preparation method thereof
Technical field
The present invention relates to building material field, more particularly to a kind of water-proof plugging material and preparation method thereof.
Background technology
The construction of water-repellent paint is broadly divided into brushing, roller coat, blade coating, the form of construction work of spraying.But no matter which kind of construction party Formula, the state of basic unit can all directly affect the effect of waterproof construction, and basic unit is loose, and cracking, dusting, water absorption rate is too high, and basic unit Can have a great impact to the adhesive strength of water-repellent paint, put aside the settlement issues of later stage building, it is this obvious Basic unit's problem can all cause water-repellent paint to play drum, and cracking, pinprick, phenomena such as peeling, these phenomenons can substantially reduce water-repellent paint Integral waterproofing effect.
Basic reinforcement material on the market is broadly divided into now:1st, the liquid surface inorganic agent of polymer, this interfacial agents There can be preferable consolidation effect to basic unit, can play and fix the sand, reduce the effect of basic unit's water absorption rate, but this inorganic agent runs into base Layer can not be handled when having crack, it is still necessary to basic reinforcement can be just carried out after crack is repaired.2nd, cement mortar is handled, Cement mortar, which has carried out base treatment, can solve the problems, such as that basic unit has crack or dusting, but a slow drying speed, long construction period, Human cost is high, and whether can reach requirement in the presence of consolidation effect caused by the difference of construction gimmick.3rd, waterproof mortar, waterproof Mortar although have waterproof and it is levelling the effect of, but waterproof mortar is not particularly suited for the earth construction of building, heavy with building Drop, rigid waterproof mortar course occur crack, entered without waterproof effect.
The first common at present rapid-hardening loss circulation material is sulphate aluminium cement cement system, because it is mainly used in blocking up Leakage, product do not possess mobility, and for largely plus after water, present leak stopping product can to cause because the ratio of mud is excessive Powder is played, bonding is insecure, is not used to basic reinforcement.Second is self-leveling material, and it has larger mobility, can be used for Basic unit is levelling and reinforces, but because its construction requirement is higher, so longer operable time is needed, and its levelling agent mechanism is logical Crossing adjustment amount of water makes mortar have higher fluidity, but still needs to manually strike off, and needs certain thickness, in cost and manually Etc. inferior position be present.
The content of the invention
In view of this, the embodiments of the invention provide a kind of water-proof plugging material and preparation method thereof, main purpose is to carry The combination property of high water-proof plugging material.
To reach above-mentioned purpose, invention broadly provides following technical scheme:
On the one hand, the embodiments of the invention provide a kind of water-proof plugging material, in parts by weight, the water-proof plugging material Including following components:
Sulphate aluminium cement 300-600 parts, perhafnate cement 200-400 parts, powdered whiting 100-200 parts, washing River sand 100-200 parts, accelerator 0.5-1 parts, water-loss reducer 0.2-0.5 parts, water reducer 0.5-2 parts, re-dispersible glue powder 3-6 parts, Defoamer 0.3-0.5 parts, powder levelling agent 1-3 parts, polypropylene fibre 0.1-0.2 parts.
Preferably, the sulphate aluminium cement is 450-550 parts, the perhafnate cement is 250-350 parts, described Powdered whiting is 150-200 parts, and the washing river sand is 150-200 parts, and the accelerator is 0.8-1 parts, the water-loss reducer For 0.3-0.5 parts, the water reducer is 1-2 parts, and the re-dispersible glue powder is 4-6 parts, and the defoamer is 0.4-0.5 parts, The powder levelling agent is 2-3 parts.
Preferably, in parts by weight, the sulphate aluminium cement is 400-450 parts, the perhafnate cement is 200-250 parts, the powdered whiting are 180-200 parts, and the washing river sand is 180-200 parts, the re-dispersible glue powder For 5-6 parts, the powder levelling agent is 2-3 parts.
Preferably, the weight ratio of the sulphate aluminium cement and the perhafnate cement is 2:1.
Preferably, the sulphate aluminium cement and the perhafnate cement are 42.5 grades;The accelerator is lithium Salt cement hardener.
Preferably, the water-loss reducer is hydroxypropylcelluloether ether water-loss reducer, the water reducer is polycarboxylic acids powder diminishing Agent, the defoamer are high effective antifoaming agent.
On the other hand, the embodiments of the invention provide the preparation method of above-mentioned water-proof plugging material, methods described include with Lower step:
Prepare each raw material by composition of raw materials;
Sulphate aluminium cement and perhafnate cement mixing are obtained into cement admixture;
Accelerator, water-loss reducer, water reducer, re-dispersible glue powder, powder are added into the cement admixture of a part of parts by weight Last levelling agent, polypropylene fibre and defoamer, the cement admixture, heavy carbonic acid of residuals weight part are added after stirring for the first time Calcium and washing river sand, the product after second of stirring is the water-proof plugging material.
Preferably, a part of parts by weight of the cement admixture and the ratio of described residuals weight part are 1:1.
Preferably, the time of the first time stirring is 10 minutes, rotating speed 1000r/min;Second of stirring Time be 8 minutes, rotating speed 1000r/min.
Compared with prior art, the beneficial effects of the invention are as follows:
The present invention is for existing loss circulation material bad adhesion, poor to basic reinforcement effect, processing basic crack effect is poor, does Dry speed is slow, the shortcomings of long construction period, have studied a kind of multifunctional water-proofing loss circulation material, and it is simultaneously simultaneous to be mainly used in base treatment Has the waterproof material of leak stopping effect.The present invention water-proof plugging material can meet master worker in work progress needs to base The demand reinforced of layer, there is certain water impermeability, and short construction period, works are simple, cheap, while after solving worker The levelling problem of construction of phase, basic reinforcement and the levelling effect for settling at one go, reaching multiple material compound use can be achieved, can lead to Different amount of water is crossed to meet various construction requirements.
Embodiment
Be further illustrate the present invention to reach the technological means and effect that predetermined goal of the invention is taken, below with compared with Good embodiment, to the embodiment according to the present patent application, technical scheme, feature and its effect, describe in detail as after.Under State it is bright in multiple embodiments in special characteristic, structure, or feature can combine by any suitable form.
Embodiment 1
Prepare raw material:In parts by weight, 300 parts of 42.5 sulphate aluminium cement, 42.5 300 parts of perhafnate cement, heavy 200 parts of calcium carbonate, wash river sand 150#200 parts, 0.5 part of salts cement hardener, hydroxypropylcelluloether ether water-loss reducer 0.2 Part, 1 part of polycarboxylic acids powder water reducer, 3 parts of re-dispersible glue powder, 0.3 part of high effective antifoaming agent, 1 part of powder levelling agent, polypropylene fibre 0.1 part of dimension;
Sulphate aluminium cement and perhafnate cement mixing are obtained into cement admixture;First by 300 parts of cement admixture Add in stirred tank, then add into stirred tank accelerator, water-loss reducer, water reducer, re-dispersible glue powder, powder levelling agent, poly- Tacryl and defoamer, after being stirred 10 minutes with 1000r/min rotating speeds, stop stirring, then remaining 300 parts of cement is mixed Compound, powdered whiting and washing river sand are sequentially added in stirred tank, after stirring 8 minutes with 1000r/min rotating speeds, stop stirring Mix, discharging is water-proof plugging material.
Embodiment 2
Prepare raw material:In parts by weight, 400 parts of 42.5 sulphate aluminium cement, 42.5 200 parts of perhafnate cement, heavy 200 parts of calcium carbonate, wash river sand 150#200 parts, 0.2 part of salts cement hardener, hydroxypropylcelluloether ether water-loss reducer 0.2 Part, 1 part of polycarboxylic acids powder water reducer, 3 parts of re-dispersible glue powder, 0.3 part of high effective antifoaming agent, 1 part of powder levelling agent, polypropylene fibre 0.1 part of dimension;
Sulphate aluminium cement and perhafnate cement mixing are obtained into cement admixture;First by 300 parts of cement admixture Add in stirred tank, then add into stirred tank accelerator, water-loss reducer, water reducer, re-dispersible glue powder, powder levelling agent, poly- Tacryl and defoamer, after being stirred 10 minutes with 1000r/min rotating speeds, stop stirring, then remaining 300 parts of cement is mixed Compound, powdered whiting and washing river sand are sequentially added in stirred tank, after stirring 8 minutes with 1000r/min rotating speeds, stop stirring Mix, discharging is water-proof plugging material.
Embodiment 3
Prepare raw material:In parts by weight, 500 parts of 42.5 sulphate aluminium cement, 42.5 100 parts of perhafnate cement, heavy 200 parts of calcium carbonate, wash river sand 150#200 parts, 0.5 part of salts cement hardener, hydroxypropylcelluloether ether water-loss reducer 0.2 Part, 1 part of polycarboxylic acids powder water reducer, 5 parts of re-dispersible glue powder, 0.3 part of high effective antifoaming agent, 1 part of powder levelling agent, polypropylene fibre 0.1 part of dimension;
Sulphate aluminium cement and perhafnate cement mixing are obtained into cement admixture;First by 300 parts of cement admixture Add in stirred tank, then add into stirred tank accelerator, water-loss reducer, water reducer, re-dispersible glue powder, powder levelling agent, poly- Tacryl and defoamer, after being stirred 10 minutes with 1000r/min rotating speeds, stop stirring, then remaining 300 parts of cement is mixed Compound, powdered whiting and washing river sand are sequentially added in stirred tank, after stirring 8 minutes with 1000r/min rotating speeds, stop stirring Mix, discharging is water-proof plugging material.
Embodiment 4
Prepare raw material:In parts by weight, 400 parts of 42.5 sulphate aluminium cement, 42.5 200 parts of perhafnate cement, heavy 200 parts of calcium carbonate, wash river sand 150#200 parts, 0.5 part of salts cement hardener, hydroxypropylcelluloether ether water-loss reducer 0.2 Part, 1 part of polycarboxylic acids powder water reducer, 6 parts of re-dispersible glue powder, 0.3 part of high effective antifoaming agent, 3 parts of powder levelling agent, polypropylene fibre 0.1 part of dimension;
A mixing bowl will be added after 200 parts of sulphate aluminium cements and 100 parts of perhafnate cement premix, add accelerator, Water-loss reducer, water reducer, re-dispersible glue powder, powder levelling agent, polypropylene fibre and defoamer, stirred with 1000r/min rotating speeds After 10 minutes, stop stirring, add 200 parts of sulphate aluminium cements and 100 parts of perhafnate cement, powdered whiting and washing River sand is sequentially added in stirred tank, after being stirred 8 minutes with 1000r/min rotating speeds, stops stirring, feeding is waterproofing and leakage-stopping material Material.
Above-described embodiment 1-4 water-proof plugging material performances prepared are tested, test result is shown in Table 1.
The performance test results of water-proof plugging material prepared by the embodiment 1-4 of table 1.
By the test result of table 1, water-proof plugging material drying time, mechanical property and heat resistance of the invention It is good.
The design principle of the present invention is by sulphate aluminium cement and perhafnate acid salt cement collocation washing river sand and heavy Calcium carbonate adds a variety of auxiliary agents, improves formula intensity and application effect, adds re-dispersible glue powder, and rubber powder is dissolved in water with cement and entered OK, cement carries out hydration, surface evaporation or basic unit's absorption, causes the free moisture of internal voids constantly to consume, makes latex Continuous film not soluble in water is formed after particle drying, so that mixing and stirring material more densification after hardening, there is excellent globality. Using powder levelling agent, the process such as levelling is on the one hand easier to after pouring, while the pinprick on surface can be reduced using levelling agent Phenomenon, increases the adhesive property of glue for tile or waterproof material and this material, while can strengthen case hardness.Manually the later stage does not scrape It is flat, you can to realize the effect of automatic levelling.Either big surface construction or small range construction can use.Using water-loss reducer, It can meet not settle under higher amount of water, while can meet that product is used for that basic unit to be levelling and basic unit under high amount of water Reinforce, bright water blocking is used under amount of water and is leaked, inner corner trim smears the techniques such as arc.
Water-proof plugging material of the present invention is compounded using sulphate aluminium cement and perhafnate cement, because of sulphate aluminium cement and Perhafnate cement self-characteristic, material have excellent anti-permeability performance in itself, and two kinds of cementitious composites are compared to normal silicate Cement is finer and close, there is faster rate of set, and setting time is fast, and getting up early intensity is high, effectively shortens construction period, accelerates to apply Work progress.
The water-proof plugging material of the present invention uses modified glue powder, on the one hand improves the bulk strength of material, simultaneously modified Rubber powder is more closely knit after material solidification, there is certain water-fast anti-permeability performance.
The water-proof plugging material of the present invention uses powder levelling agent:It is simple to can reach construction, surfacing can be straight after final set Tap into the processes such as row ceramic tile plaster.
The water-proof plugging material of the present invention uses powdered whiting:Gap that can be effectively between filling powder, make material into Type is finer and close, and powdered whiting and modified glue powder combination excellent effect.
Disclosed above is only the embodiment of the present invention, but protection scope of the present invention is not limited thereto, and is appointed What those familiar with the art the invention discloses technical scope in, change or replacement can be readily occurred in, all should It is included within the scope of the present invention.Therefore, protection scope of the present invention should using above-mentioned scope of the claims as It is accurate.

Claims (9)

1. a kind of water-proof plugging material, it is characterised in that in parts by weight, the water-proof plugging material includes following components:
Sulphate aluminium cement 300-600 parts, perhafnate cement 200-400 parts, powdered whiting 100-200 parts, wash river sand 100-200 parts, accelerator 0.2-1 parts, water-loss reducer 0.2-0.5 parts, water reducer 0.5-2 parts, re-dispersible glue powder 3-6 parts, defoaming Agent 0.3-0.5 parts, powder levelling agent 1-3 parts, polypropylene fibre 0.1-0.2 parts.
A kind of 2. water-proof plugging material according to claim 1, it is characterised in that in parts by weight, the aluminium sulfate Cement is 450-550 parts, and the perhafnate cement is 250-350 parts, and the powdered whiting is 150-200 parts, the water It is 150-200 parts to wash river sand, and the accelerator is 0.8-1 parts, and the water-loss reducer is 0.3-0.5 parts, and the water reducer is 1-2 Part, the re-dispersible glue powder is 4-6 parts, and the defoamer is 0.4-0.5 parts, and the powder levelling agent is 2-3 parts.
A kind of 3. water-proof plugging material according to claim 1, it is characterised in that in parts by weight, the aluminium sulfate Cement is 400-450 parts, and the perhafnate cement is 200-250 parts, and the powdered whiting is 180-200 parts, the water It is 180-200 parts to wash river sand, and the re-dispersible glue powder is 5-6 parts, and the powder levelling agent is 2-3 parts.
4. a kind of water-proof plugging material according to claim 1, it is characterised in that the sulphate aluminium cement and the height Aluminate cement weight ratio is 2:1.
5. a kind of water-proof plugging material according to claim 1, it is characterised in that the sulphate aluminium cement and the height Aluminate cement is 42.5 grades;The accelerator is salts cement hardener.
6. a kind of water-proof plugging material according to claim 1, it is characterised in that the water-loss reducer is hydroxypropyl cellulose Ether water-loss reducer, the water reducer are polycarboxylic acids powder water reducer, and the defoamer is high effective antifoaming agent.
7. the preparation method of the water-proof plugging material described in claim any one of 1-6, it is characterised in that methods described include with Lower step:
Prepare each raw material by composition of raw materials;
Sulphate aluminium cement and perhafnate cement mixing are obtained into cement admixture;
Accelerator, water-loss reducer, water reducer, re-dispersible glue powder, powder stream are added into the cement admixture of a part of parts by weight Flat agent, polypropylene fibre and defoamer, added after stirring for the first time the cement admixture of residuals weight part, powdered whiting and River sand is washed, the product after second of stirring is the water-proof plugging material.
8. the preparation method of water-proof plugging material according to claim 7, it is characterised in that the one of the cement admixture The ratio of moiety by weight part and described residuals weight part is 1:1.
9. the preparation method of water-proof plugging material according to claim 7, it is characterised in that first time stirring when Between be 10 minutes, rotating speed 1000r/min;The time of second of stirring is 8 minutes, rotating speed 1000r/min.
CN201710702896.1A 2017-08-16 2017-08-16 Waterproof plugging material and preparation method thereof Active CN107555917B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112624712A (en) * 2020-12-23 2021-04-09 广东龙马新材料科技有限公司 Temperature-resistant pressure-resistant cement-based plugging material and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012143221A1 (en) * 2011-04-21 2012-10-26 Henkel Ag & Co. Kgaa Mineral composition for producing electric heating layers
CN105622029A (en) * 2015-12-25 2016-06-01 江苏蓝圈新材料有限公司 Cement-based self-leveling mortar
CN106145835A (en) * 2016-06-30 2016-11-23 安徽固维特材料科技有限公司 A kind of fast setting sealing loss circulation material and preparation method thereof, application process

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012143221A1 (en) * 2011-04-21 2012-10-26 Henkel Ag & Co. Kgaa Mineral composition for producing electric heating layers
CN105622029A (en) * 2015-12-25 2016-06-01 江苏蓝圈新材料有限公司 Cement-based self-leveling mortar
CN106145835A (en) * 2016-06-30 2016-11-23 安徽固维特材料科技有限公司 A kind of fast setting sealing loss circulation material and preparation method thereof, application process

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112624712A (en) * 2020-12-23 2021-04-09 广东龙马新材料科技有限公司 Temperature-resistant pressure-resistant cement-based plugging material and preparation method thereof

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