CN107551444A - A kind of powder extinguishing agent and preparation method thereof - Google Patents

A kind of powder extinguishing agent and preparation method thereof Download PDF

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Publication number
CN107551444A
CN107551444A CN201710699092.0A CN201710699092A CN107551444A CN 107551444 A CN107551444 A CN 107551444A CN 201710699092 A CN201710699092 A CN 201710699092A CN 107551444 A CN107551444 A CN 107551444A
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CN
China
Prior art keywords
boron magnesium
magnesium mud
extinguishing agent
powder extinguishing
preparation
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Pending
Application number
CN201710699092.0A
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Chinese (zh)
Inventor
徐金海
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SUZHOU WUYUE SYNTHETIC FIRE SCI-TECH Co Ltd
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SUZHOU WUYUE SYNTHETIC FIRE SCI-TECH Co Ltd
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Priority to CN201710699092.0A priority Critical patent/CN107551444A/en
Publication of CN107551444A publication Critical patent/CN107551444A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a kind of powder extinguishing agent and preparation method thereof, powder extinguishing agent parts by weights ratio is made of materials described below:Boron magnesium mud 80%, sodium acid carbonate 6%, potassium nitrate 8%, sulfamic acid 1% and anti-blushing agent 5%;Method prepared by powder extinguishing agent comprises the following steps:S1:Raw material boron magnesium mud is crushed;S2:By metering, boron magnesium mud, 6% sodium acid carbonate, 8% potassium nitrate, 1% sulfamic acid and 5% anti-blushing agent that mass percent is 80% are separately added into silication device is mixed and carries out mixing silication;S3:The good material of silication is dried;S4:The material for drying completion is sieved;S5:The material being sieved excessively is packed, metering obtains finished product.The present invention is utilized caused boron magnesium mud in borax plant's production process, is rationally less than 15um using resource, the molecular particle size of boron magnesium mud, surface forms various holes, increases the contact area on surface, and adsorption capacity is strong.

Description

A kind of powder extinguishing agent and preparation method thereof
Technical field
The present invention relates to fire control technology field, specially a kind of powder extinguishing agent and preparation method thereof.
Background technology
Powder extinguishing agent is the drying for fire extinguishing and readily flowed attritive powder, by the inorganic salts with fire extinguishing effectiveness With a small amount of additive through drying, crush, mix micro-solid powder constituent.
The fire extinguishing base-material of existing BC powder extinguishing agents is mainly sodium acid carbonate, but supply falls short of demand for current sodium acid carbonate, Cause goods and materials in short supply, most of waste residue, the composition of boron magnesium mud is with the shape of carbonate caused by Peng Meinishi borax plants production borax Formula is present, and runs into high temperature dehydration, therefore the present inventor have devised a kind of powder extinguishing agent and preparation method thereof.
The content of the invention
The technical problem to be solved in the present invention is that the fire extinguishing base-material of existing BC powder extinguishing agents is mainly sodium acid carbonate, still Supply falls short of demand for current sodium acid carbonate, the defects of causing goods and materials in short supply, there is provided a kind of powder extinguishing agent and preparation method thereof, so as to Solve the above problems.
To achieve the above object, the present invention provides following technical scheme:A kind of powder extinguishing agent, parts by weights ratio is with following Raw material are made:Boron magnesium mud 80%, sodium acid carbonate 6%, potassium nitrate 8%, sulfamic acid 1% and anti-blushing agent 5%.
Further, the composition parts by weights ratio of the boron magnesium mud is magnesium carbonate 40%, magnesia 30%, silica 20%th, calcium oxide 2%, manganese oxide 1%, di-iron trioxide 5%, alundum (Al2O3) 1% and diboron trioxide 1%.
Further, the anti-blushing agent is silica gel or stearate.
A kind of preparation method of powder extinguishing agent, including following manufacturing step:
S1:Raw material boron magnesium mud is crushed;
S2:By metering, boron magnesium mud, 6% carbon that mass percent is 80% are separately added into silication device is mixed Sour hydrogen sodium, 8% potassium nitrate, 1% sulfamic acid and 5% anti-blushing agent carry out mixing silication;
S3:The good material of silication is dried;
S4:The material for drying completion is sieved;
S5:The material being sieved excessively is packed, metering obtains finished product.
Further, after the raw material boron magnesium mud in the S1 steps is crushed by pulverizer, then filled by separating The raw material that will be crushed is put to be separated.
Further, the raw material boron magnesium mud that the diameter for being more than technological requirement after separation is crushed in the S1 steps re-starts Separating twice.
Further, the molecular particle size of the boron magnesium mud raw material after being crushed in the S1 steps is less than 15um.
Further, the boron magnesium mud dry powder being sieved excessively in the S5 steps can burst into many smaller under high temperature action Particle.
Compared with prior art, the beneficial effects of the invention are as follows:This kind of powder extinguishing agent product and preparation method thereof, by boron Caused boron magnesium mud is utilized in sand factory production process, is turned waste into wealth, and is rationally less than using resource, the molecular particle size of boron magnesium mud 15um, surface form various holes, increase the contact area on surface, and adsorption capacity is strong, and boron magnesium mud dry powder particle exists Many smaller particles can be burst under high temperature action so that increase with the contact area of flame, improve extinguishing property, it is moistureproof Agent can prevent that powder from making moist caking, and the powder caking that makes moist can cause contact area to reduce, and reduce extinguishing property, boron magnesium mud Composition is more to be existed in the form of carbonate, also most oxide, meets high temperature dehydration, and substantial amounts of vapor plays fire extinguishing and made With the clay powder extinguishing agent produced of boron magnesium reduces the manufacturing cost of extinguishing chemical, saves the energy and will not cause dirt to environment Dye.
Embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, Obviously, described embodiment is only part of the embodiment of the present invention, rather than whole embodiments, based in the present invention Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all Belong to the scope of protection of the invention.
The present invention provides a kind of technical scheme:A kind of powder extinguishing agent, parts by weights ratio are made of following raw material:Boron magnesium Mud 80%, sodium acid carbonate 6%, potassium nitrate 8%, sulfamic acid 1% and anti-blushing agent 5%.
The composition parts by weights ratio of boron magnesium mud be magnesium carbonate 40%, magnesia 30%, silica 20%, calcium oxide 2%, Manganese oxide 1%, di-iron trioxide 5%, alundum (Al2O3) 1% and diboron trioxide 1%, the composition of boron magnesium mud are more with carbonate Form is present, also most oxide, meets high temperature dehydration, and substantial amounts of vapor plays fire extinguishing function.
Anti-blushing agent is silica gel or stearate, and anti-blushing agent can prevent that powder from making moist caking, and the powder caking that makes moist can cause Contact area is reduced, and reduces extinguishing property.
A kind of preparation method of powder extinguishing agent, including following manufacturing step:
S1:Raw material boron magnesium mud is crushed;
S2:By metering, boron magnesium mud, 6% carbon that mass percent is 80% are separately added into silication device is mixed Sour hydrogen sodium, 8% potassium nitrate, 1% sulfamic acid and 5% anti-blushing agent carry out mixing silication;
S3:The good material of silication is dried;
S4:The material for drying completion is sieved;
S5:The material being sieved excessively is packed, metering obtains finished product.
After raw material boron magnesium mud in S1 steps is crushed by pulverizer, the original that then will be crushed by separator Material is separated, and boron magnesium mud is ground into little particle, separator isolates the boron magnesium mud particle for reaching and preparing and requiring.
The raw material boron magnesium mud that the diameter for being more than technological requirement after separation is crushed in S1 steps re-starts separating twice, will not have There is the coarse granule boron magnesium mud progress separating twice for reaching and preparing and requiring, making up to preparation is required, save resource, reduction is manufactured into This.
The molecular particle size of boron magnesium mud raw material after being crushed in S1 steps is less than 15um, and boron magnesium mud particle surface, which is formed, is permitted many More holes, increase the contact area on surface.
The boron magnesium mud dry powder being sieved is crossed in S5 steps can burst into many smaller particles, boron magnesium mud under high temperature action Dry powder particle can burst into many smaller particles under high temperature action so that increase with the contact area of flame, raising is gone out Fiery performance.
During concrete operations, Peng Meinishi borax plants are in waste residue caused by production borax, the transport boron magnesium mud original from factory Material, boron magnesium mud raw material is poured into pulverizer and crushed by staff, after the completion of crushing, is isolated point by separator Seed footpath is less than 15um boron magnesium mud particles, and boron magnesium mud particle surface of the particle diameter less than 15um can form various holes, increase The big contact area on surface, then coarse grained boron magnesium mud of the remaining particle diameter more than 15um is poured into pulverizer carry out again Separating twice, then isolate remaining qualified boron magnesium mud particle again by separator, continue aforesaid operations, until crushing Boron magnesium mud particle afterwards is all qualified, and then by Weighing, in silication device is mixed being separately added into mass percent is 80% boron magnesium mud, 6% sodium acid carbonate, 8% potassium nitrate, 1% sulfamic acid and 5% anti-blushing agent carries out mixing silicon Change, the product of sulfamic acid and boron magnesium mud reaction can not only absorb the partial heat of flame, and the carbon dioxide that generates and Water can the concentration of dilute combustion area oxygen play a part of fire extinguishing, anti-blushing agent can prevent that powder from making moist caking, if powder The end caking that makes moist can cause contact area to reduce, and reduce extinguishing property, the material completed by drying machine to silication is done Dry processing, after drying process after the completion of, material is sieved, filters out qualified material, to sieving after qualified material Measured, then packed, come into operation.
Finally it should be noted that:The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention, Although the present invention is described in detail with reference to the foregoing embodiments, for those skilled in the art, it still may be used To be modified to the technical scheme described in foregoing embodiments, or equivalent substitution is carried out to which part technical characteristic, Within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., it should be included in the present invention's Within protection domain.

Claims (8)

1. a kind of powder extinguishing agent, it is characterised in that parts by weights ratio is made of following raw material:Boron magnesium mud 80%, bicarbonate Sodium 6%, potassium nitrate 8%, sulfamic acid 1% and anti-blushing agent 5%.
A kind of 2. powder extinguishing agent according to claim 1, it is characterised in that the composition parts by weights ratio of the boron magnesium mud Aoxidized for magnesium carbonate 40%, magnesia 30%, silica 20%, calcium oxide 2%, manganese oxide 1%, di-iron trioxide 5%, three Two aluminium 1% and diboron trioxide 1%.
3. a kind of powder extinguishing agent according to claim 1, it is characterised in that the anti-blushing agent is silica gel or stearic acid Salt.
4. a kind of preparation method of powder extinguishing agent, it is characterised in that including following manufacturing step:
S1:Raw material boron magnesium mud is crushed;
S2:By metering, boron magnesium mud, 6% bicarbonate that mass percent is 80% are separately added into silication device is mixed Sodium, 8% potassium nitrate, 1% sulfamic acid and 5% anti-blushing agent carry out mixing silication;
S3:The good material of silication is dried;
S4:The material for drying completion is sieved;
S5:The material being sieved excessively is packed, metering obtains finished product.
A kind of 5. preparation method of powder extinguishing agent according to claim 4, it is characterised in that the original in the S1 steps After material boron magnesium mud is crushed by pulverizer, then the raw material crushed is separated by separator.
6. the preparation method of a kind of powder extinguishing agent according to claim 5, it is characterised in that crushed in the S1 steps The raw material boron magnesium mud of diameter after separation more than technological requirement re-starts separating twice.
7. the preparation method of a kind of powder extinguishing agent according to claim 6, it is characterised in that crushed in the S1 steps The molecular particle size of boron magnesium mud raw material afterwards is less than 15um.
8. the preparation method of a kind of powder extinguishing agent according to claim 4, it is characterised in that sieved in the S5 steps Good boron magnesium mud dry powder can burst into many smaller particles under high temperature action.
CN201710699092.0A 2017-08-15 2017-08-15 A kind of powder extinguishing agent and preparation method thereof Pending CN107551444A (en)

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CN107551444A true CN107551444A (en) 2018-01-09

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112807600A (en) * 2020-12-15 2021-05-18 华夏永侒(西安)控股集团有限公司 Combined action micro-particle temperature-sensing fire extinguishing agent and preparation method thereof
WO2022034580A1 (en) 2020-08-09 2022-02-17 Bioma Ltd Firefighting compositions

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3523893A (en) * 1967-03-22 1970-08-11 Stop Fire Inc Fire extinguishing powder composition
CN102247684A (en) * 2011-06-13 2011-11-23 上海百友得机械设备有限公司 Production technology of powder extinguishing agent
CN102512779A (en) * 2011-11-24 2012-06-27 苏州大学 Dry powder fire extinguishing agent
CN105944275A (en) * 2016-05-25 2016-09-21 李涛 Dry powder extinguishing agent and preparation method

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3523893A (en) * 1967-03-22 1970-08-11 Stop Fire Inc Fire extinguishing powder composition
CN102247684A (en) * 2011-06-13 2011-11-23 上海百友得机械设备有限公司 Production technology of powder extinguishing agent
CN102512779A (en) * 2011-11-24 2012-06-27 苏州大学 Dry powder fire extinguishing agent
CN105944275A (en) * 2016-05-25 2016-09-21 李涛 Dry powder extinguishing agent and preparation method

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
张宝瑞: "用硼镁泥配制干粉灭火剂", 《无机盐工业》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2022034580A1 (en) 2020-08-09 2022-02-17 Bioma Ltd Firefighting compositions
CN112807600A (en) * 2020-12-15 2021-05-18 华夏永侒(西安)控股集团有限公司 Combined action micro-particle temperature-sensing fire extinguishing agent and preparation method thereof

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Application publication date: 20180109