CN107510052A - A kind of combination product for alleviating dysmenorrhoea and beauty and preparation method thereof - Google Patents
A kind of combination product for alleviating dysmenorrhoea and beauty and preparation method thereof Download PDFInfo
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- CN107510052A CN107510052A CN201710742800.4A CN201710742800A CN107510052A CN 107510052 A CN107510052 A CN 107510052A CN 201710742800 A CN201710742800 A CN 201710742800A CN 107510052 A CN107510052 A CN 107510052A
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- 206010013935 Dysmenorrhoea Diseases 0.000 title claims abstract description 48
- 238000002360 preparation method Methods 0.000 title claims abstract description 33
- 230000003796 beauty Effects 0.000 title claims abstract description 29
- 239000013066 combination product Substances 0.000 title claims abstract description 29
- 229940127555 combination product Drugs 0.000 title claims abstract description 29
- PVXPPJIGRGXGCY-DJHAAKORSA-N 6-O-alpha-D-glucopyranosyl-alpha-D-fructofuranose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1OC[C@@H]1[C@@H](O)[C@H](O)[C@](O)(CO)O1 PVXPPJIGRGXGCY-DJHAAKORSA-N 0.000 claims abstract description 63
- 239000000463 material Substances 0.000 claims abstract description 51
- 239000012141 concentrate Substances 0.000 claims abstract description 27
- 244000241838 Lycium barbarum Species 0.000 claims abstract description 22
- 235000015459 Lycium barbarum Nutrition 0.000 claims abstract description 22
- 235000006886 Zingiber officinale Nutrition 0.000 claims abstract description 22
- 235000008397 ginger Nutrition 0.000 claims abstract description 22
- 240000001008 Dimocarpus longan Species 0.000 claims abstract description 21
- 235000000235 Euphoria longan Nutrition 0.000 claims abstract description 21
- 241000220317 Rosa Species 0.000 claims abstract description 21
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- 235000015849 Apium graveolens Dulce Group Nutrition 0.000 claims abstract description 16
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- 235000016709 nutrition Nutrition 0.000 claims abstract description 13
- 230000035764 nutrition Effects 0.000 claims abstract description 13
- 240000008866 Ziziphus nummularia Species 0.000 claims abstract 2
- 239000003795 chemical substances by application Substances 0.000 claims description 130
- 230000001954 sterilising effect Effects 0.000 claims description 87
- 238000004659 sterilization and disinfection Methods 0.000 claims description 87
- 239000011236 particulate material Substances 0.000 claims description 54
- 238000002386 leaching Methods 0.000 claims description 48
- 239000006228 supernatant Substances 0.000 claims description 35
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 31
- 238000000605 extraction Methods 0.000 claims description 25
- 238000002156 mixing Methods 0.000 claims description 24
- 241000234314 Zingiber Species 0.000 claims description 21
- 239000000284 extract Substances 0.000 claims description 19
- 238000001914 filtration Methods 0.000 claims description 18
- 238000000703 high-speed centrifugation Methods 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 14
- HOWHQWFXSLOJEF-MGZLOUMQSA-N systemin Chemical compound NCCCC[C@H](N)C(=O)N[C@@H](CCSC)C(=O)N[C@@H](CCC(N)=O)C(=O)N[C@@H]([C@@H](C)O)C(=O)N[C@@H](CC(O)=O)C(=O)OC(=O)[C@@H]1CCCN1C(=O)[C@H]1N(C(=O)[C@H](CC(O)=O)NC(=O)[C@H](CCCN=C(N)N)NC(=O)[C@H](CCCCN)NC(=O)[C@H](CO)NC(=O)[C@H]2N(CCC2)C(=O)[C@H]2N(CCC2)C(=O)[C@H](CCCCN)NC(=O)[C@H](CO)NC(=O)[C@H](CCC(N)=O)NC(=O)[C@@H](NC(=O)[C@H](C)N)C(C)C)CCC1 HOWHQWFXSLOJEF-MGZLOUMQSA-N 0.000 claims description 12
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- 238000012423 maintenance Methods 0.000 claims description 9
- 230000003750 conditioning effect Effects 0.000 claims description 7
- 238000004140 cleaning Methods 0.000 claims description 6
- 238000004821 distillation Methods 0.000 claims description 6
- 230000003821 menstrual periods Effects 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 230000003340 mental effect Effects 0.000 claims description 2
- 230000035479 physiological effects, processes and functions Effects 0.000 claims description 2
- 244000126002 Ziziphus vulgaris Species 0.000 claims 2
- 229920001817 Agar Polymers 0.000 claims 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical class OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims 1
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- 231100000957 no side effect Toxicity 0.000 abstract description 2
- 244000273928 Zingiber officinale Species 0.000 abstract 1
- 239000004480 active ingredient Substances 0.000 abstract 1
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- 235000013399 edible fruits Nutrition 0.000 description 2
- 229930003944 flavone Natural products 0.000 description 2
- -1 flavone compound Chemical class 0.000 description 2
- 235000011949 flavones Nutrition 0.000 description 2
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 2
- 239000010931 gold Substances 0.000 description 2
- 229910052737 gold Inorganic materials 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 2
- VVVDGSCGBGBGFN-UHFFFAOYSA-O 2-[decoxy(hydroxy)phosphoryl]oxyethyl-trimethylazanium Chemical group CCCCCCCCCCOP(O)(=O)OCC[N+](C)(C)C VVVDGSCGBGBGFN-UHFFFAOYSA-O 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 208000005171 Dysmenorrhea Diseases 0.000 description 1
- 206010020772 Hypertension Diseases 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- FHNINJWBTRXEBC-UHFFFAOYSA-N Sudan III Chemical group OC1=CC=C2C=CC=CC2=C1N=NC(C=C1)=CC=C1N=NC1=CC=CC=C1 FHNINJWBTRXEBC-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000000730 antalgic agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 230000013872 defecation Effects 0.000 description 1
- 201000005577 familial hyperlipidemia Diseases 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000003599 food sweetener Nutrition 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 230000004630 mental health Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000007170 pathology Effects 0.000 description 1
- 230000008855 peristalsis Effects 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000003765 sweetening agent Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/125—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives containing carbohydrate syrups; containing sugars; containing sugar alcohols; containing starch hydrolysates
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Mycology (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Molecular Biology (AREA)
- Botany (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention belongs to Gynecological health product technical field, and in particular to a kind of combination product for alleviating dysmenorrhoea and beauty and preparation method thereof, product of the present invention includes A agent, B agent and C agent, and the A agent is mainly made up of the material of following parts by weight：5 15 parts of 75 70 85 parts of type FOS concentrates, 5 15 parts of palatinose and celery stalk；The B agent is mainly made up of the material of following parts by weight：45 55 parts of 11 16 parts of old ginger, 59 parts of rose, 14 18 parts of palatinose, 10 13 parts of FOS and brown sugar；The C agent is mainly made up of the material of following parts by weight：15 20 parts of 10 15 parts of jujube, 5 10 parts of matrimony vine, 5 10 parts of longan, 50 60 parts of brown sugar and palatinose.A, B, C, tri- doses are packaged into a nutrition bag, eaten respectively in different physiological periods for adult female, it is that a kind of can effectively alleviate has no side effect product through symptom, the safety for improving the face colour of skin, product of the present invention is extracted and concentrated using ultralow temperature in preparation process, avoid degrading under active ingredient high temperature, reduce product the effect of.
Description
Technical field
The invention belongs to Gynecological health product technical field, and in particular to a kind of combination product for alleviating dysmenorrhoea and beauty and
Its preparation method.
Background technology
Dysmenorrhoea is the common pain of menstruating female, refers to that periodicity underbelly pain occurs before and after menstrual period or through row in women
Bitterly.Pain draws waist sacrum, and notably severe pain is fainted, also known as ＂ dysmenorrhea ＂.Dysmenorrhoea not only brings the pain of patient's body heart, and gives pain
Person causes larger psychology, physical stress, severely impacts daily life and the mental health of women.Traditionally many women are frequent
Drunk together with menstrual period and with brown sugar and ginger, jujube, matrimony vine etc. enduring water, to invigorate blood circulation, cold removing, warm the womb reduce dysmenorrhoea, to a certain degree
On can alleviate dysmenorrhoea caused by palace cold, but it is not that dysmenorrhoea symptom is more serious caused by palace cold that menstrual period, which drink brown sugar Jiang Shui and easily allowed,.Mesh
Preceding in the market also has the food or health products of many treatment dysmenorrhoeas, and many products with the addition of anodyne or steady in order to improve effect
Determine agent, often take with certain side effect.
The content of the invention
It is an object of the present invention to the product for treating dysmenorrhoea for above-mentioned in the market has the problem of side effect, there is provided can
Effectively alleviate dysmenorrhoea symptom, improve the product that the safety of the face colour of skin has no side effect.
To reach above-mentioned purpose, the technical solution adopted in the present invention is：
A kind of combination product for alleviating dysmenorrhoea and beauty, is mainly made up of the material of following parts by weight：Including A agent, B agent and C agent,
The A agent is mainly made up of the material of following parts by weight：75 type FOS concentrate 70-85 parts, palatinose 5-15 parts and
Celery stalk 5-15 parts；The B agent is mainly made up of the material of following parts by weight：Old ginger 11-16 parts, rose 5-9 parts, para gold
Sugared 14-18 parts, FOS 10-13 parts and brown sugar 45-55 parts；The C agent is mainly made up of the material of following parts by weight：Jujube
10-15 parts, matrimony vine 5-10 parts, longan 5-10 parts, brown sugar 50-60 parts and palatinose 15-20 parts.
In the present invention, further instruction, the combination product for alleviating dysmenorrhoea and beauty is mainly by following parts by weight
Material be made：Including A agent, B agent and C agent, the A agent is mainly made up of the material of following parts by weight：75 type FOSs are dense
Contracting liquid 74-80 parts, palatinose 8-12 parts and celery stalk 8-10 parts；The B agent is mainly made up of the material of following parts by weight：Always
Ginger 13-15 parts, rose 6-8 parts, palatinose 15-17 parts, FOS 11-12 parts and brown sugar 48-53 parts；The C agent master
To be made up of the material of following parts by weight：Jujube 12-13 parts, matrimony vine 7-9 parts, longan 7-8 parts, brown sugar 53-57 parts and para gold
Sugared 17-18 parts.
A kind of method for preparing the combination product for alleviating dysmenorrhoea and beauty, comprises the following steps：
The preparation method of A agent is as follows：
（1）Superfreeze crushes：Weigh fresh celery stalk by weight, be cut into after cleaning after 2-3mm sections be placed in minus 60 DEG C-it is negative
Superfreeze crushing is carried out under conditions of 100 DEG C, obtains granularity 1-3mm particulate material, it is standby；
（2）Vacuum ultrasonic low temperature extracts：0 DEG C of frozen water is added in the particulate material obtained toward step (1), adjustment makes the matter of particulate material
Amount concentration is 3-10%, obtains system, then by systemVacuum ultrasonic low temperature leaching device is sent into, it is negative to keep vacuum
0.05MPa- bears 0.08MPa, carries out vacuum and low temperature ultrasonic-leaching, makes system during extractionTemperature maintain 0-4 DEG C, extraction
After 30-50min, system is obtained, then make systemBeing risen under normal pressure makes temperature to 20-25 DEG C, and makes its bar at 20-25 DEG C
0-4 DEG C is rapidly cooled to after maintaining 60-90min under part, obtains system, then by systemIt is placed in a centrifuge, will be from
Mental and physical efforts rotating speed is adjusted to 6000-15000r/min, makes systemHigh speed centrifugation 5-15min is carried out, supernatant is taken, then at 0-4 DEG C
Temperature conditionss to supernatant carry out filtration sterilization, obtain system, 0-4 DEG C of stored under sterile conditions is placed on, it is standby；
（3）Vacuum ultralow temperature concentrates：The system that step (2) is obtainedIt is put into concentration tank, makes it in sterile leaching liquor temperature
For minus 60 DEG C-minus 90 DEG C, vacuum be negative 0.05MPa- bear carry out distillation under conditions of 0.08MPa and be concentrated into solid content be
75-85% concentrate；
（4）Mixing:By weight, 75 type FOSs and palatinose are weighed, 75 type FOSs and palatinose are added
In concentrate obtained by step (3), mixing 15-18min makes to be well mixed between each material, obtains system；
（5）Ultrahigh-pressure sterilization：The system that step (4) is obtainedIt is placed in ultra-high pressure sterilization device, ultra-high pressure sterilization device is boosted
To 460-480MPa, make systemAfter carrying out autoclaving 25-28min under conditions of 460-480MPa, make ultra-high pressure sterilization device
In 3-5min reduction of blood pressure in high-speed obtains A agent, then A is packed to zero；
The preparation method of B agent is as follows：
（1）Superfreeze crushes：By weight, old ginger and rose are taken, and is charged with 1-2 times of old ginger and rose is total
The pure water of parts by weight, obtains system, by systemBe placed in minus 60 DEG C-it is minus 100 DEG C under the conditions of carry out superfreeze crushing,
Granularity 1-3mm particulate material is obtained, it is standby；
（2）Vacuum ultrasonic low temperature extracts：Toward step（1）0 DEG C of frozen water is added in obtained particulate material, adjustment makes the matter of particulate material
Amount concentration is 3-10%, obtains system, then by systemIt is sent into vacuum ultrasonic low temperature leaching device, keeps vacuum
0.08MPa is born for negative 0.05MPa-, carries out vacuum and low temperature ultrasonic-leaching, carries out vacuum and low temperature ultrasonic-leaching, is made during extraction
SystemTemperature maintain 0-4 DEG C, after extracting 30-50min, obtain system, then make systemHeated up under normal pressure
To 20-25 DEG C, and it is rapidly cooled to 0-4 DEG C after maintaining 60-90min under conditions of 20-25 DEG C, obtain system, then
By systemIt is placed in a centrifuge, centrifugal force rotating speed is adjusted to 6000-15000r/min, makes systemCarry out high speed centrifugation 5-
15min, supernatant is taken, then the temperature conditionss at 0-4 DEG C carry out filtration sterilization to supernatant, obtain system, it is placed on 0-
4 DEG C of stored under sterile conditions, it is standby；
（3）Mixing:By weight, palatinose, FOS and brown sugar are weighed, palatinose, FOS and brown sugar are added
Enter step（2）Obtained systemIn, being stirred 15-18min makes to be well mixed between each material, obtains system；
（4）Ultrahigh-pressure sterilization：The system that step (3) is obtainedIt is placed in ultra-high pressure sterilization device, ultra-high pressure sterilization device is boosted
To 460-480MPa, make system25-28min is maintained under 460-480MPa pressure condition, then makes ultra-high pressure sterilization device
Reduction of blood pressure in high-speed produces B agent, B agent is packed to zero in 3-5min；
The preparation method of C agent is as follows：
（1）Superfreeze crushes：Enuleation date, matrimony vine and longan are weighed by weight and is well mixed, and are added 1-2 times and gone
The pure water of core jujube, matrimony vine and longan total weight parts, obtains system, then by systemIt is placed in minus 60 DEG C-minus 100 DEG C of conditions
Lower progress superfreeze crushing, obtains granularity 1-3mm particulate material, standby；
（2）Vacuum ultrasonic low temperature extracts：0 DEG C of frozen water is added in the particulate material obtained toward step (1), adjusts the quality of particulate material
Concentration is 3-10%, and this is system, then by systemIt is sent into vacuum ultrasonic low temperature leaching device, holding vacuum is
Negative 0.05MPa- bears 0.08MPa, carries out vacuum and low temperature ultrasonic-leaching, makes system during extractionTemperature maintain 0-4 DEG C, carry
After taking time 30-50min, system is obtained, by system30-40 DEG C is warming up under normal pressure, and makes it at 30-40 DEG C
Under the conditions of maintain 60-90min after be rapidly cooled to 0-4 DEG C of temperature, obtain system, then by systemIt is placed in a centrifuge,
Centrifugal force rotating speed is adjusted to 6000-15000r/min, makes systemHigh speed centrifugation 5-15min is carried out, supernatant is taken, then in 0-
Filtration sterilization is carried out to supernatant under conditions of 4 DEG C, obtains system, then by systemIt is placed under 0-4 DEG C of aseptic condition and stores
Deposit, it is standby；
（3）Mixing:By weight, brown sugar and palatinose are weighed, brown sugar and palatinose are added into step（2）Obtained systemIn, stirring 15-18mi makes to be well mixed between each material, obtains system；
（4）Ultrahigh-pressure sterilization：By step（3）Obtained systemIt is placed in ultra-high pressure sterilization device, by ultra-high pressure sterilization device
460-480MPa is boosted to, makes systemAfter maintaining 25-28min under 460-480MPa pressure condition, make super-pressure
Sterilizer reduction of blood pressure in high-speed in 3-5min to zero, produces C agent, C agent is packed；
Tri- doses of A, B, C that method made above is prepared into is packaged into a nutrition bag, for adult female in different physiology weeks
Phase eats respectively.
In the present invention, in the method for the combination product of further instruction, alleviation dysmenorrhoea and beauty, the A agent, B agent
Packed with C agent by the amount for often wrapping 25g.
In the present invention, in the method for the combination product of further instruction, alleviation dysmenorrhoea and beauty, described, B agent and C
Agent is respectively women premenstruum (premenstrua), menstrual period, postmenstruation conditioning use.
In the present invention, in the method for the combination product of further instruction, alleviation dysmenorrhoea and beauty, in the nutrition bag
Contained A agent, B agent are identical with the amount of C agent.
The present invention has the advantage that compared with prior art：
1. product of the present invention designs according to female pathology physilogical characteristics, it is divided into women premenstruum (premenstrua), menstrual period, postmenstruation conditioning use,
Not only there is the effect of alleviating dysmenorrhoea, while with the good effects of beautifying face and moistering lotion.It is added with the raw material of product of the present invention
Palatinose, palatinose are a kind of sweeteners low in calories, can suppress fat accumulation；The FOS added in its raw material,
Beneficial bacterium in FOS energy fast breeding human body intestinal canal, change pH value in enteron aisle, accelerate intestines peristalsis, increase defecation frequency,
So as to reach poison expelling and beautifying function.Added in A agent containing abundant flavone compound and potassium element in celery stalk, it is often edible
Be advantageous to hypertension and hyperlipemia and functions of improving blood circulation and face-beautifying.Through investigating, there is the women of 5-15 dysmenorrhoea histories, after using this product conditioning, big portion
The dysmenorrhoea symptom of people is divided to be eliminated, the face colour of skin is effectively improved.
2. product of the present invention preparation process using ultralow temperature extract and concentrate, avoid flavone compound etc. it is effective into
Divide under high temperature and degrade, lose product efficacy.
Embodiment
The invention provides a kind of combination product for alleviating dysmenorrhoea and beauty and preparation method thereof is provided, to make the present invention's
Purpose, technical scheme and effect are clearer, clear and definite, and the present invention is described in more detail below.It should be appreciated that this place is retouched
The specific embodiment stated only to explain the present invention, is not intended to limit the present invention.
Embodiment 1
A kind of combination product for alleviating dysmenorrhoea and beauty provided by the invention and preparation method thereof is as follows：
A kind of combination product for alleviating dysmenorrhoea and beauty, is mainly made up of the material of following parts by weight：Including A agent, B agent and C agent,
The A agent is mainly made up of the material of following parts by weight：75 70 parts of type FOS concentrates, 5 parts of palatinose and celery stalk 5
Part；The B agent is mainly made up of the material of following parts by weight：11 parts of old ginger, 5 parts of rose, 14 parts of palatinose, FOS
10 parts and 45 parts of brown sugar；The C agent is mainly made up of the material of following parts by weight：It is 10 parts of jujube, 5 parts of matrimony vine, 5 parts of longan, red
15 parts of 50 parts of sugar and palatinose.
A kind of preparation method of combination product for alleviating dysmenorrhoea and beauty described above, comprises the following steps：
The preparation method of A agent is as follows：
（1）Superfreeze crushes：Fresh celery stalk is weighed by weight, and minus 60 DEG C are placed in after being cut into 2-3mm sections after cleaning
Under the conditions of carry out superfreeze crushing, obtain granularity 1-3mm particulate material, it is standby；
（2）Vacuum ultrasonic low temperature extracts：0 DEG C of frozen water is added in the particulate material obtained toward step (1), adjustment makes the matter of particulate material
It is 3% to measure concentration, obtains system, then by systemVacuum ultrasonic low temperature leaching device is sent into, it is negative to keep vacuum
0.05MPaMPa, carries out vacuum and low temperature ultrasonic-leaching, makes system during extractionTemperature maintain 0 DEG C, after extracting 30min, obtain
To system, then make systemBeing risen under normal pressure makes temperature to 20 DEG C, and makes it rapid after maintenance 60min under conditions of 20 DEG C
0 DEG C is cooled to, obtains system, then by systemIt is placed in a centrifuge, centrifugal force rotating speed is adjusted to 6000r/min, made
SystemHigh speed centrifugation 5min is carried out, takes supernatant, then the temperature conditionss at 0 DEG C carry out filtration sterilization to supernatant, obtain
System, 0 DEG C of stored under sterile conditions is placed on, it is standby；
（3）Vacuum ultralow temperature concentrates：The system that step (2) is obtainedIt is put into concentration tank, makes it in sterile leaching liquor temperature
Distillation, which is carried out, under conditions of being negative 0.05MPa for minus 60 DEG C, vacuum is concentrated into the concentrate that solid content is 75%；
（4）Mixing:By weight, 75 type FOSs and palatinose are weighed, 75 type FOSs and palatinose are added
In concentrate obtained by step (3), mixing 15min makes to be well mixed between each material, obtains system；
（5）Ultrahigh-pressure sterilization：The system that step (4) is obtainedIt is placed in ultra-high pressure sterilization device, ultra-high pressure sterilization device is boosted
To 460MPa, make systemAfter carrying out autoclaving 25min under conditions of 460MPa, make ultra-high pressure sterilization device fast in 3min
Prompt drop is pressed onto zero, that is, obtains A agent, then A is packed.
The preparation method of B agent is as follows：
（1）Superfreeze crushes：By weight, old ginger and rose are taken, and is charged with 1 times of old ginger and rose gross weight
The pure water of part is measured, obtains system, by systemBe placed in minus 60 DEG C-it is minus 100 DEG C under the conditions of carry out superfreeze crushing, obtain
It is standby to granularity 1-3mm particulate material；
（2）Vacuum ultrasonic low temperature extracts：Toward step（1）0 DEG C of frozen water is added in obtained particulate material, adjustment makes the matter of particulate material
It is 3% to measure concentration, obtains system, then by systemIt is sent into vacuum ultrasonic low temperature leaching device, it is negative to keep vacuum
0.05MPa, vacuum and low temperature ultrasonic-leaching is carried out, carry out vacuum and low temperature ultrasonic-leaching, make system during extractionTemperature dimension
Hold at 0 DEG C, after extracting 30min, obtain system, then make system20 DEG C are warming up under normal pressure, and makes it at 20 DEG C
Under conditions of maintain 60min after be rapidly cooled to 0 DEG C, obtain system, then by systemIt is placed in a centrifuge, centrifugal force is turned
Velocity modulation makes system to 6000r/minHigh speed centrifugation 5min is carried out, takes supernatant, then in 0 DEG C of temperature conditionss to supernatant
Filtration sterilization is carried out, obtains system, 0 DEG C of stored under sterile conditions is placed on, it is standby；
（3）Mixing:By weight, palatinose, FOS and brown sugar are weighed, palatinose, FOS and brown sugar are added
Enter step（2）Obtained systemIn, being stirred 15min makes to be well mixed between each material, obtains system；
（4）Ultrahigh-pressure sterilization：The system that step (3) is obtainedIt is placed in ultra-high pressure sterilization device, ultra-high pressure sterilization device is boosted
To 460MPa, make system25min is maintained under 460MPa pressure condition, then makes ultra-high pressure sterilization device quick in 3min
Zero is depressured to, produces B agent, B agent is packed.
The preparation method of C agent is as follows：
（1）Superfreeze crushes：Enuleation date, matrimony vine and longan are weighed by weight and is well mixed, and add 1 times of stoning
The pure water of jujube, matrimony vine and longan total weight parts, obtains system, then by systemCarried out under the conditions of being placed in minus 60 DEG C ultralow
Warm Freezing smashing, granularity 1-3mm particulate material is obtained, it is standby；
（2）Vacuum ultrasonic low temperature extracts：0 DEG C of frozen water is added in the particulate material obtained toward step (1), adjusts the quality of particulate material
Concentration is 3%, and this is system, then by systemIt is sent into vacuum ultrasonic low temperature leaching device, it is negative to keep vacuum
0.05MPa, carries out vacuum and low temperature ultrasonic-leaching, makes system during extractionTemperature maintain 0 DEG C, after extraction time 30min,
Obtain system, by system30 DEG C are warming up under normal pressure, and makes it rapid cold after maintenance 60min under conditions of 30 DEG C
But to 0 DEG C of temperature, system is obtained, then by systemIt is placed in a centrifuge, centrifugal force rotating speed is adjusted to 6000r/min, made
SystemHigh speed centrifugation 5min is carried out, takes supernatant, filtration sterilization then is carried out to supernatant under conditions of 0 DEG C, obtains body
System, then by system0 DEG C of stored under sterile conditions is placed in, it is standby；
（3）Mixing:By weight, brown sugar and palatinose are weighed, brown sugar and palatinose are added into step（2）Obtained systemIn, stirring 15mi makes to be well mixed between each material, obtains system；
（4）Ultrahigh-pressure sterilization：By step（3）Obtained systemIt is placed in ultra-high pressure sterilization device, by ultra-high pressure sterilization device
460MPa is boosted to, makes systemAfter maintaining 25min under 460MPa pressure condition, ultra-high pressure sterilization device is set to exist
Reduction of blood pressure in high-speed produces C agent, C agent is packed with every bag 25g amount to zero in 3min.
Tri- doses of A, B, C that method made above is prepared into is packaged into a nutrition bag, contained A in the nutrition bag
Agent, B agent are identical with the amount of C agent, are eaten respectively in different physiological periods for adult female.
Embodiment 2
A kind of combination product for alleviating dysmenorrhoea and beauty provided by the invention and preparation method thereof is as follows：
A kind of combination product for alleviating dysmenorrhoea and beauty, is mainly made up of the material of following parts by weight：Including A agent, B agent and C agent,
The A agent is mainly made up of the material of following parts by weight：75 85 parts of type FOS concentrates, 15 parts of palatinose and celery stalk
15 parts；The B agent is mainly made up of the material of following parts by weight：16 parts of old ginger, 9 parts of rose, 18 parts of palatinose, oligomeric fruit
55 parts of 13 parts of sugar and brown sugar；The C agent is mainly made up of the material of following parts by weight：15 parts of jujube, 10 parts of matrimony vine, longan 10
20 parts of part, 60 parts of brown sugar and palatinose.
A kind of preparation method of combination product for alleviating dysmenorrhoea and beauty described above, comprises the following steps：
The preparation method of A agent is as follows：
（1）Superfreeze crushes：Fresh celery stalk is weighed by weight, and minus 100 DEG C are placed in after being cut into 2-3mm sections after cleaning
Under the conditions of carry out superfreeze crushing, obtain granularity 1-3mm particulate material, it is standby；
（2）Vacuum ultrasonic low temperature extracts：0 DEG C of frozen water is added in the particulate material obtained toward step (1), adjustment makes the matter of particulate material
It is 10% to measure concentration, obtains system, then by systemVacuum ultrasonic low temperature leaching device is sent into, it is negative to keep vacuum
0.08MPa, carries out vacuum and low temperature ultrasonic-leaching, makes system during extractionTemperature maintain 4 DEG C, after extracting 50min, obtain
System, then make systemBeing risen under normal pressure makes temperature to 25 DEG C, and makes it rapid cold after maintenance 90min under conditions of 25 DEG C
But to 4 DEG C, system is obtained, then by systemIt is placed in a centrifuge, centrifugal force rotating speed is adjusted to 15000r/min, makes body
SystemHigh speed centrifugation 15min is carried out, takes supernatant, then the temperature conditionss at 4 DEG C carry out filtration sterilization to supernatant, obtain
System, 4 DEG C of stored under sterile conditions is placed on, it is standby；
（3）Vacuum ultralow temperature concentrates：The system that step (2) is obtainedIt is put into concentration tank, makes it in sterile leaching liquor temperature
Distillation, which is carried out, under conditions of being negative 0.08MPa for minus 90 DEG C, vacuum is concentrated into the concentrate that solid content is 85%；
（4）Mixing:By weight, 75 type FOSs and palatinose are weighed, 75 type FOSs and palatinose are added
In concentrate obtained by step (3), mixing 18min makes to be well mixed between each material, obtains system；
（5）Ultrahigh-pressure sterilization：The system that step (4) is obtainedIt is placed in ultra-high pressure sterilization device, ultra-high pressure sterilization device is boosted
To 480MPa, make systemAfter carrying out autoclaving 28min under conditions of 480MPa, make ultra-high pressure sterilization device fast in 5min
Prompt drop is pressed onto zero, that is, obtains A agent, then A is packed.
The preparation method of B agent is as follows：
（1）Superfreeze crushes：By weight, old ginger and rose are taken, and is charged with 2 times of old gingers and rose gross weight
The pure water of part is measured, obtains system, by systemSuperfreeze crushing is carried out under the conditions of being placed in minus 100 DEG C, obtains granularity
1-3mm particulate material, it is standby；
（2）Vacuum ultrasonic low temperature extracts：Toward step（1）0 DEG C of frozen water is added in obtained particulate material, adjustment makes the matter of particulate material
It is 10% to measure concentration, obtains system, then by systemIt is sent into vacuum ultrasonic low temperature leaching device, holding vacuum is
Negative 0.08MPa, vacuum and low temperature ultrasonic-leaching is carried out, carry out vacuum and low temperature ultrasonic-leaching, make system during extractionTemperature
4 DEG C are maintained, after extracting 50min, obtains system, then make system25 DEG C are warming up under normal pressure, and makes it 25
4 DEG C are rapidly cooled to after maintaining 90min under conditions of DEG C, obtains system, then by systemIt is placed in a centrifuge, by centrifugal force
Rotating speed is adjusted to 15000r/min, makes systemHigh speed centrifugation 15min is carried out, takes supernatant, then in 4 DEG C of temperature conditionss to upper
Clear liquid carries out filtration sterilization, obtains system, 4 DEG C of stored under sterile conditions is placed on, it is standby；
（3）Mixing:By weight, palatinose, FOS and brown sugar are weighed, palatinose, FOS and brown sugar are added
Enter step（2）Obtained systemIn, being stirred 18min makes to be well mixed between each material, obtains system；
（4）Ultrahigh-pressure sterilization：The system that step (3) is obtainedIt is placed in ultra-high pressure sterilization device, ultra-high pressure sterilization device is boosted
To 480MPa, make system28min is maintained under 480MPa pressure condition, then makes ultra-high pressure sterilization device quick in 5min
Zero is depressured to, produces B agent, B agent is packed.
The preparation method of C agent is as follows：
（1）Superfreeze crushes：Enuleation date, matrimony vine and longan are weighed by weight and is well mixed, and add 2 times of stonings
The pure water of jujube, matrimony vine and longan total weight parts, obtains system, then by systemSurpassed under the conditions of being placed in minus 100 DEG C
Cryogenic freezing crushes, and obtains granularity 1-3mm particulate material, standby；
（2）Vacuum ultrasonic low temperature extracts：0 DEG C of frozen water is added in the particulate material obtained toward step (1), adjusts the quality of particulate material
Concentration is 10%, and this is system, then by systemIt is sent into vacuum ultrasonic low temperature leaching device, it is negative to keep vacuum
0.08MPa, carries out vacuum and low temperature ultrasonic-leaching, makes system during extractionTemperature maintain 4 DEG C, after extraction time 50min,
Obtain system, by system40 DEG C are warming up under normal pressure, and makes it rapid cold after maintenance 90min under conditions of 40 DEG C
But to 4 DEG C of temperature, system is obtained, then by systemIt is placed in a centrifuge, centrifugal force rotating speed is adjusted to 15000r/min, made
SystemHigh speed centrifugation 15min is carried out, takes supernatant, filtration sterilization then is carried out to supernatant under conditions of 4 DEG C, obtains body
System, then by system4 DEG C of stored under sterile conditions is placed in, it is standby；
（3）Mixing:By weight, brown sugar and palatinose are weighed, brown sugar and palatinose are added into step（2）Obtained systemIn, stirring 18min makes to be well mixed between each material, obtains system；
（4）Ultrahigh-pressure sterilization：By step（3）Obtained systemIt is placed in ultra-high pressure sterilization device, by ultra-high pressure sterilization device
460-480MPa is boosted to, makes systemAfter maintaining 25-28min under 460-480MPa pressure condition, make super-pressure
Sterilizer reduction of blood pressure in high-speed in 3-5min to zero, produces C agent, C agent is packed with every bag 25g amount.
Tri- doses of A, B, C that method made above is prepared into is packaged into a nutrition bag, contained A in the nutrition bag
Agent, B agent are identical with the amount of C agent, are eaten respectively in different physiological periods for adult female.
Embodiment 3
A kind of combination product for alleviating dysmenorrhoea and beauty provided by the invention and preparation method thereof is as follows：
A kind of combination product for alleviating dysmenorrhoea and beauty, is mainly made up of the material of following parts by weight：Including A agent, B agent and C agent,
The A agent is mainly made up of the material of following parts by weight：75 type FOS concentrates 74,8 parts of palatinose and celery stalk 8
Part；The B agent is mainly made up of the material of following parts by weight：13 parts of old ginger, 6 parts of rose, 15 parts of palatinose, FOS
11 parts and 48 parts of brown sugar；The C agent is mainly made up of the material of following parts by weight：It is 12 parts of jujube, 7 parts of matrimony vine, 7 parts of longan, red
17 parts of 53 parts of sugar and palatinose.
A kind of preparation method of combination product for alleviating dysmenorrhoea and beauty described above, comprises the following steps：
The preparation method of A agent is as follows：
（1）Superfreeze crushes：Fresh celery stalk is weighed by weight, and minus 75 DEG C are placed in after being cut into 2-3mm sections after cleaning
Under the conditions of carry out superfreeze crushing, obtain granularity 1-3mm particulate material, it is standby；
（2）Vacuum ultrasonic low temperature extracts：0 DEG C of frozen water is added in the particulate material obtained toward step (1), adjustment makes the matter of particulate material
It is 5% to measure concentration, obtains system, then by systemVacuum ultrasonic low temperature leaching device is sent into, it is negative to keep vacuum
0.06MPa, carries out vacuum and low temperature ultrasonic-leaching, makes system during extractionTemperature maintain 1 DEG C, after extracting 35min, obtain
System, then make systemBeing risen under normal pressure makes temperature to 22 DEG C, and makes it rapid cold after maintenance 70min under conditions of 22 DEG C
But to 1 DEG C, system is obtained, then by systemIt is placed in a centrifuge, centrifugal force rotating speed is adjusted to 9000r/min, makes body
SystemHigh speed centrifugation 8min is carried out, takes supernatant, then the temperature conditionss at 1 DEG C carry out filtration sterilization to supernatant, obtain body
System, 1 DEG C of stored under sterile conditions is placed on, it is standby；
（3）Vacuum ultralow temperature concentrates：The system that step (2) is obtainedIt is put into concentration tank, makes it in sterile leaching liquor temperature
Distillation, which is carried out, under conditions of being negative 0.06MPa for minus 70 DEG C, vacuum is concentrated into the concentrate that solid content is 78%；
（4）Mixing:By weight, 75 type FOSs and palatinose are weighed, 75 type FOSs and palatinose are added
In concentrate obtained by step (3), mixing 16min makes to be well mixed between each material, obtains system；
（5）Ultrahigh-pressure sterilization：The system that step (4) is obtainedIt is placed in ultra-high pressure sterilization device, ultra-high pressure sterilization device is boosted
To 465MPa, make systemAfter carrying out autoclaving 26min under conditions of 465MPa, make ultra-high pressure sterilization device fast in 4min
Prompt drop is pressed onto zero, that is, obtains A agent, then A is packed.
The preparation method of B agent is as follows：
（1）Superfreeze crushes：By weight, old ginger and rose are taken, and is charged with 1 times of old ginger and rose gross weight
The pure water of part is measured, obtains system, by systemSuperfreeze crushing is carried out under the conditions of being placed in minus 70 DEG C, obtains granularity 1-
3mm particulate material, it is standby；
（2）Vacuum ultrasonic low temperature extracts：Toward step（1）0 DEG C of frozen water is added in obtained particulate material, adjustment makes the matter of particulate material
It is 5% to measure concentration, obtains system, then by systemIt is sent into vacuum ultrasonic low temperature leaching device, it is negative to keep vacuum
0.06MPa, vacuum and low temperature ultrasonic-leaching is carried out, carry out vacuum and low temperature ultrasonic-leaching, make system during extractionTemperature dimension
Hold at 1 DEG C, after extracting 38min, obtain system, then make system22 DEG C are warming up under normal pressure, and makes it at 22 DEG C
Under conditions of maintain 70min after be rapidly cooled to 1 DEG C, obtain system, then by systemIt is placed in a centrifuge, centrifugal force is turned
Velocity modulation makes system to 9000r/minHigh speed centrifugation 8min is carried out, takes supernatant, then in 1 DEG C of temperature conditionss to supernatant
Filtration sterilization is carried out, obtains system, 1 DEG C of stored under sterile conditions is placed on, it is standby；
（3）Mixing:By weight, palatinose, FOS and brown sugar are weighed, palatinose, FOS and brown sugar are added
Enter step（2）Obtained systemIn, being stirred 16min makes to be well mixed between each material, obtains system；
（4）Ultrahigh-pressure sterilization：The system that step (3) is obtainedIt is placed in ultra-high pressure sterilization device, ultra-high pressure sterilization device is boosted
To 468MPa, make system26min is maintained under 468MPa pressure condition, then makes ultra-high pressure sterilization device quick in 4min
Zero is depressured to, produces B agent, B agent is packed.
The preparation method of C agent is as follows：
（1）Superfreeze crushes：Enuleation date, matrimony vine and longan are weighed by weight and is well mixed, and add 2 times of stonings
The pure water of jujube, matrimony vine and longan total weight parts, obtains system, then by systemCarried out under the conditions of being placed in minus 70 DEG C ultralow
Warm Freezing smashing, granularity 1-3mm particulate material is obtained, it is standby；
（2）Vacuum ultrasonic low temperature extracts：0 DEG C of frozen water is added in the particulate material obtained toward step (1), adjusts the quality of particulate material
Concentration is 5%, and this is system, then by systemIt is sent into vacuum ultrasonic low temperature leaching device, it is negative to keep vacuum
0.06MPa, carries out vacuum and low temperature ultrasonic-leaching, makes system during extractionTemperature maintain 1 DEG C, after extraction time 38min,
Obtain system, by system34 DEG C are warming up under normal pressure, and makes it rapid cold after maintenance 70min under conditions of 34 DEG C
But to 1 DEG C of temperature, system is obtained, then by systemIt is placed in a centrifuge, centrifugal force rotating speed is adjusted to 9000r/min, made
SystemHigh speed centrifugation 8min is carried out, takes supernatant, filtration sterilization then is carried out to supernatant under conditions of 1 DEG C, obtains body
System, then by system1 DEG C of stored under sterile conditions is placed in, it is standby；
（3）Mixing:By weight, brown sugar and palatinose are weighed, brown sugar and palatinose are added into step（2）Obtained systemIn, stirring 16mi makes to be well mixed between each material, obtains system；
（4）Ultrahigh-pressure sterilization：By step（3）Obtained systemIt is placed in ultra-high pressure sterilization device, by ultra-high pressure sterilization device
467MPa is boosted to, makes systemAfter maintaining 26min under 467MPa pressure condition, ultra-high pressure sterilization device is set to exist
Reduction of blood pressure in high-speed produces C agent, C agent is packed with every bag 25g amount to zero in 4min.
Tri- doses of A, B, C that method made above is prepared into is packaged into a nutrition bag, contained A in the nutrition bag
Agent, B agent are identical with the amount of C agent, are eaten respectively in different physiological periods for adult female.
Embodiment 4
A kind of combination product for alleviating dysmenorrhoea and beauty provided by the invention and preparation method thereof is as follows：
A kind of combination product for alleviating dysmenorrhoea and beauty, is mainly made up of the material of following parts by weight：Including A agent, B agent and C agent,
The A agent is mainly made up of the material of following parts by weight：75 80 parts of type FOS concentrates, 12 parts of palatinose and celery stalk
10 parts；The B agent is mainly made up of the material of following parts by weight：15 parts of old ginger, 8 parts of rose, 17 parts of palatinose, oligomeric fruit
53 parts of 12 parts of sugar and brown sugar；The C agent is mainly made up of the material of following parts by weight：13 parts of jujube, 9 parts of matrimony vine, 8 parts of longan,
18 parts of 57 parts of brown sugar and palatinose.
A kind of preparation method of combination product for alleviating dysmenorrhoea and beauty described above, comprises the following steps：
The preparation method of A agent is as follows：
（1）Superfreeze crushes：Fresh celery stalk is weighed by weight, and minus 90 DEG C are placed in after being cut into 2-3mm sections after cleaning
Under the conditions of carry out superfreeze crushing, obtain granularity 1-3mm particulate material, it is standby；
（2）Vacuum ultrasonic low temperature extracts：0 DEG C of frozen water is added in the particulate material obtained toward step (1), adjustment makes the matter of particulate material
It is 8% to measure concentration, obtains system, then by systemVacuum ultrasonic low temperature leaching device is sent into, it is negative to keep vacuum
0.07MPa, carries out vacuum and low temperature ultrasonic-leaching, makes system during extractionTemperature maintain 3 DEG C, after extracting 47min, obtain
System, then make systemBeing risen under normal pressure makes temperature to 24 DEG C, and makes it rapid cold after maintenance 80min under conditions of 24 DEG C
But to 3 DEG C, system is obtained, then by systemIt is placed in a centrifuge, centrifugal force rotating speed is adjusted to 13000r/min, makes body
SystemHigh speed centrifugation 12min is carried out, takes supernatant, then the temperature conditionss at 3 DEG C carry out filtration sterilization to supernatant, obtain
System, 3 DEG C of stored under sterile conditions is placed on, it is standby；
（3）Vacuum ultralow temperature concentrates：The system that step (2) is obtainedIt is put into concentration tank, makes it in sterile leaching liquor temperature
Distillation, which is carried out, under conditions of being negative 0.07MPa for minus 80 DEG C, vacuum is concentrated into the concentrate that solid content is 82%；
（4）Mixing:By weight, 75 type FOSs and palatinose are weighed, 75 type FOSs and palatinose are added
In concentrate obtained by step (3), mixing 17min makes to be well mixed between each material, obtains system；
（5）Ultrahigh-pressure sterilization：The system that step (4) is obtainedIt is placed in ultra-high pressure sterilization device, ultra-high pressure sterilization device is boosted
To 470MPa, make systemAfter carrying out autoclaving 27min under conditions of 470MPa, make ultra-high pressure sterilization device fast in 5min
Prompt drop is pressed onto zero, that is, obtains A agent, then A is packed.
The preparation method of B agent is as follows：
（1）Superfreeze crushes：By weight, old ginger and rose are taken, and is charged with 1.5 times of old gingers and rose is total
The pure water of parts by weight, obtains system, by systemSuperfreeze crushing is carried out under the conditions of being placed in minus 90 DEG C, obtains granularity
1-3mm particulate material, it is standby；
（2）Vacuum ultrasonic low temperature extracts：Toward step（1）0 DEG C of frozen water is added in obtained particulate material, adjustment makes the matter of particulate material
It is 8% to measure concentration, obtains system, then by systemIt is sent into vacuum ultrasonic low temperature leaching device, it is negative to keep vacuum
0.07MPa, vacuum and low temperature ultrasonic-leaching is carried out, carry out vacuum and low temperature ultrasonic-leaching, make system during extractionTemperature dimension
Hold at 3 DEG C, after extracting 47min, obtain system, then make system24 DEG C are warming up under normal pressure, and makes it at 24 DEG C
Under conditions of maintain 80min after be rapidly cooled to 3 DEG C, obtain system, then by systemIt is placed in a centrifuge, centrifugal force is turned
Velocity modulation makes system to 13000r/minHigh speed centrifugation 12min is carried out, takes supernatant, then in 3 DEG C of temperature conditionss to supernatant
Liquid carries out filtration sterilization, obtains system, 3 DEG C of stored under sterile conditions is placed on, it is standby；
（3）Mixing:By weight, palatinose, FOS and brown sugar are weighed, palatinose, FOS and brown sugar are added
Enter step（2）Obtained systemIn, being stirred 17min makes to be well mixed between each material, obtains system；
（4）Ultrahigh-pressure sterilization：The system that step (3) is obtainedIt is placed in ultra-high pressure sterilization device, ultra-high pressure sterilization device is boosted
To 470MPa, make system27min is maintained under 470MPa pressure condition, then makes ultra-high pressure sterilization device quick in 5min
Zero is depressured to, produces B agent, B agent is packed.
The preparation method of C agent is as follows：
（1）Superfreeze crushes：Enuleation date, matrimony vine and longan are weighed by weight and is well mixed, and are added 1-2 times and gone
The pure water of core jujube, matrimony vine and longan total weight parts, obtains system, then by systemSurpassed under the conditions of being placed in minus 90 DEG C
Cryogenic freezing crushes, and obtains granularity 1-3mm particulate material, standby；
（2）Vacuum ultrasonic low temperature extracts：0 DEG C of frozen water is added in the particulate material obtained toward step (1), adjusts the quality of particulate material
Concentration is 8%, and this is system, then by systemIt is sent into vacuum ultrasonic low temperature leaching device, it is negative to keep vacuum
0.07MPa, carries out vacuum and low temperature ultrasonic-leaching, makes system during extractionTemperature maintain 3 DEG C, after extraction time 46min,
Obtain system, by system38 DEG C are warming up under normal pressure, and makes it rapid cold after maintenance 80min under conditions of 38 DEG C
But to 3 DEG C of temperature, system is obtained, then by systemIt is placed in a centrifuge, centrifugal force rotating speed is adjusted to 13000r/min, made
SystemHigh speed centrifugation 12min is carried out, takes supernatant, filtration sterilization then is carried out to supernatant under conditions of 3 DEG C, obtains body
System, then by system3 DEG C of stored under sterile conditions is placed in, it is standby；
（3）Mixing:By weight, brown sugar and palatinose are weighed, brown sugar and palatinose are added into step（2）Obtained systemIn, stirring 15-18mi makes to be well mixed between each material, obtains system；
（4）Ultrahigh-pressure sterilization：By step（3）Obtained systemIt is placed in ultra-high pressure sterilization device, by ultra-high pressure sterilization device
470MPa is boosted to, makes systemAfter maintaining 27min under 470MPa pressure condition, ultra-high pressure sterilization device is set to exist
Reduction of blood pressure in high-speed produces C agent, C agent is packed with every bag 25g amount to zero in 5min.
Tri- doses of A, B, C that method made above is prepared into is packaged into a nutrition bag, contained A in the nutrition bag
Agent, B agent are identical with the amount of C agent, are eaten respectively in different physiological periods for adult female.
Compliance test result
Selecting 200 has 5-15 dysmenorrhoeas history, the average age women of 33 years old as target of investication and study, divides 4 groups, every group 50 by them
People, every group respectively the product made of embodiment 1-4 carry out conditioning 4 months.A agent, B agent and C agent, respectively in premenstrual 7 days, warp
Phase, conditioning in 7 days is used after, is wrapped within one day one.Conditioning is evaluated product after 4 months according to the effect of product, is divided into A etc., B
Deng four grades such as, C etc. and D, wherein, the evaluation criterion of each grade is as follows：
A etc. evaluation criterion is：Dysmenorrhoea is eliminated and the face colour of skin is improved
B etc. evaluation criterion is：Dysmenorrhoea also has but must be eased and the face colour of skin improves
B etc. evaluation criterion is：Dysmenorrhoea is not eased, and the face colour of skin improves
D etc. evaluation criterion is：Dysmenorrhoea is not eased, and the face colour of skin does not change
After 4 months, finding is as shown in the table：
| Test example | A etc. | B etc. | C etc. | D etc. |
| Embodiment 1 | 38 | 6 | 4 | 2 |
| Embodiment 2 | 37 | 7 | 6 | 0 |
| Embodiment 3 | 35 | 8 | 6 | 1 |
| Embodiment 4 | 36 | 9 | 5 | 0 |
Data above finds out that the dysmenorrhoea symptom of most people is effectively eliminated, and the face colour of skin is substantially improved, it was demonstrated that this hair
Bright product has the effect of alleviating dysmenorrhoea and functions of improving blood circulation and face-beautifying effect, it was demonstrated that its promotional value.
Described above is the detailed description for the present invention preferably possible embodiments, but embodiment is not limited to this hair
Bright patent claim, the equal change completed or modification change under the technical spirit suggested by all present invention, all should belong to
Cover the scope of the claims in the present invention.
Claims (6)
- A kind of 1. combination product for alleviating dysmenorrhoea and beauty, it is characterised in that：Including A agent, B agent and C agent, the A agent mainly by The material of following parts by weight is made：75 type FOS concentrate 70-85 parts, palatinose 5-15 parts and celery stalk 5-15 parts； The B agent is mainly made up of the material of following parts by weight：It is old ginger 11-16 parts, rose 5-9 parts, palatinose 14-18 parts, low Fructooligosaccharides 10-13 parts and brown sugar 45-55 parts；The C agent is mainly made up of the material of following parts by weight：Jujube 10-15 parts, matrimony vine 5-10 parts, longan 5-10 parts, brown sugar 50-60 parts and palatinose 15-20 parts.
- 2. a kind of combination product for alleviating dysmenorrhoea and beauty according to claim 1, it is characterised in that including A agent, B agent With C agent, the A agent is mainly made up of the material of following parts by weight：75 type FOS concentrate 74-80 parts, palatinose 8- 12 parts and celery stalk 8-10 parts；The B agent is mainly made up of the material of following parts by weight：Old ginger 13-15 parts, rose 6-8 parts, Palatinose 15-17 parts, FOS 11-12 parts and brown sugar 48-53 parts；The C agent is mainly by the material system of following parts by weight Into：Jujube 12-13 parts, matrimony vine 7-9 parts, longan 7-8 parts, brown sugar 53-57 parts and palatinose 17-18 parts.
- 3. a kind of method of alleviation dysmenorrhoea prepared described in claim 1 or 2 and the combination product of beauty, it is characterised in that bag Include following steps：The preparation method of A agent is as follows：（1）Superfreeze crushes：Weigh fresh celery stalk by weight, be cut into after cleaning after 2-3mm sections be placed in minus 60 DEG C-it is negative Superfreeze crushing is carried out under conditions of 100 DEG C, obtains granularity 1-3mm particulate material, it is standby；（2）Vacuum ultrasonic low temperature extracts：0 DEG C of frozen water is added in the particulate material obtained toward step (1), adjustment makes the matter of particulate material Amount concentration is 3-10%, obtains system, then by systemVacuum ultrasonic low temperature leaching device is sent into, it is negative to keep vacuum 0.05MPa- bears 0.08MPa, carries out vacuum and low temperature ultrasonic-leaching, makes system during extractionTemperature maintain 0-4 DEG C, extraction After 30-50min, system is obtained, then make systemBeing risen under normal pressure makes temperature to 20-25 DEG C, and makes its bar at 20-25 DEG C 0-4 DEG C is rapidly cooled to after maintaining 60-90min under part, obtains system, then by systemIt is placed in a centrifuge, will centrifuges Power rotating speed is adjusted to 6000-15000r/min, makes systemHigh speed centrifugation 5-15min is carried out, supernatant is taken, then at 0-4 DEG C Temperature conditionss carry out filtration sterilization to supernatant, obtain system, by system0-4 DEG C of stored under sterile conditions is placed in, it is standby With；（3）Vacuum ultralow temperature concentrates：The system that step (2) is obtainedIt is put into concentration tank, makes it in sterile leaching liquor temperature For minus 60 DEG C-minus 90 DEG C, vacuum be negative 0.05MPa- bear carry out distillation under conditions of 0.08MPa and be concentrated into solid content be 75-85% concentrate；（4）Mixing:By weight, 75 type FOSs and palatinose are weighed, 75 type FOSs and palatinose are added In concentrate obtained by step (3), mixing 15-18min makes to be well mixed between each material, obtains system；（5）Ultrahigh-pressure sterilization：The system that step (4) is obtainedIt is placed in ultra-high pressure sterilization device, ultra-high pressure sterilization device is boosted to 460-480MPa, make systemAfter carrying out autoclaving 25-28min under conditions of 460-480MPa, make ultra-high pressure sterilization device In 3-5min reduction of blood pressure in high-speed obtains A agent, then A is packed to zero；The preparation method of B agent is as follows：（1）Superfreeze crushes：Old ginger and rose are weighed by weight, and are charged with 1-2 times of old ginger and rose The pure water of total weight parts, obtains system, by systemBe placed in minus 60 DEG C-it is minus 100 DEG C under the conditions of carry out ultra-low temperature cold agar It is broken, granularity 1-3mm particulate material is obtained, it is standby；（2）Vacuum ultrasonic low temperature extracts：Toward step（1）0 DEG C of frozen water is added in obtained particulate material, adjustment makes the matter of particulate material Amount concentration is 3-10%, obtains system, then by systemIt is sent into vacuum ultrasonic low temperature leaching device, holding vacuum is Negative 0.05MPa- bears 0.08MPa, carries out vacuum and low temperature ultrasonic-leaching, carries out vacuum and low temperature ultrasonic-leaching, makes body during extraction SystemTemperature maintain 0-4 DEG C, after extracting 30-50min, obtain system, then make system20- is warming up under normal pressure 25 DEG C, and it is rapidly cooled to 0-4 DEG C after maintaining 60-90min under conditions of 20-25 DEG C, obtain system, then by systemIt is placed in a centrifuge, centrifugal force rotating speed is adjusted to 6000-15000r/min, makes systemHigh speed centrifugation 5-15min is carried out, is taken Supernatant, then 0-4 DEG C temperature conditionss to supernatant carry out filtration sterilization, obtain system, by systemIt is placed in 0-4 DEG C Stored under sterile conditions, it is standby；（3）Mixing:By weight, palatinose, FOS and brown sugar are weighed, palatinose, FOS and brown sugar are added Enter step（2）Obtained systemIn, being stirred 15-18min makes to be well mixed between each material, obtains system；（4）Ultrahigh-pressure sterilization：The system that step (3) is obtainedIt is placed in ultra-high pressure sterilization device, ultra-high pressure sterilization device is boosted To 460-480MPa, make system25-28min is maintained under 460-480MPa pressure condition, then makes ultra-high pressure sterilization device Reduction of blood pressure in high-speed produces B agent, B agent is packed to zero in 3-5min；The preparation method of C agent is as follows：（1）Superfreeze crushes：Enuleation date, matrimony vine and longan are weighed by weight and is well mixed, and are added 1-2 times and gone The pure water of core jujube, matrimony vine and longan total weight parts, obtains system, then by systemIt is placed in minus 60 DEG C-minus 100 DEG C of conditions Lower progress superfreeze crushing, obtains granularity 1-3mm particulate material, standby；（2）Vacuum ultrasonic low temperature extracts：0 DEG C of frozen water is added in the particulate material obtained toward step (1), adjusts the quality of particulate material Concentration is 3-10%, and this is system, then by systemIt is sent into vacuum ultrasonic low temperature leaching device, it is negative to keep vacuum 0.05MPa- bears 0.08MPa, carries out vacuum and low temperature ultrasonic-leaching, makes system during extractionTemperature maintain 0-4 DEG C, extraction After time 30-50min, system is obtained, by system30-40 DEG C is warming up under normal pressure, and makes its condition at 30-40 DEG C 0-4 DEG C of temperature is rapidly cooled to after lower maintenance 60-90min, obtains system, then by systemIt is placed in a centrifuge, will be from Mental and physical efforts rotating speed is adjusted to 6000-15000r/min, makes systemHigh speed centrifugation 5-15min is carried out, supernatant is taken, then at 0-4 DEG C Under conditions of to supernatant carry out filtration sterilization, obtain system, then by system0-4 DEG C of stored under sterile conditions is placed in, it is standby With；（3）Mixing:By weight, brown sugar and palatinose are weighed, brown sugar and palatinose are added into step（2）Obtained systemIn, stirring 15-18min makes to be well mixed between each material, obtains system；（4）Ultrahigh-pressure sterilization：By step（3）Obtained systemIt is placed in ultra-high pressure sterilization device, by ultra-high pressure sterilization device460-480MPa is boosted to, makes systemAfter maintaining 25-28min under 460-480MPa pressure condition, make super-pressure Sterilizer reduction of blood pressure in high-speed in 3-5min to zero, produces C agent, C agent is packed；Tri- doses of A, B, C that method made above is prepared into is packaged into a nutrition bag, for adult female in different physiology weeks Phase eats respectively.
- A kind of 4. method for preparing the combination product for alleviating dysmenorrhoea and beauty according to claim 3, it is characterised in that：Institute A agent, B agent and C agent is stated to be packed by every bag 25g amount.
- A kind of 5. method for preparing the combination product for alleviating dysmenorrhoea and beauty according to claim 3, it is characterised in that：Institute It is respectively that women is edible through five days before and after row to state B agent and C agent（Menstrual period do not eat）, A agent is usually conditioning use.
- A kind of 6. method for preparing the combination product for alleviating dysmenorrhoea and beauty according to claim 3, it is characterised in that：Institute A agent, B agent contained by stating in nutrition bag is identical with the amount of C agent.
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| CN102218127A (en) * | 2010-04-13 | 2011-10-19 | 鲁翠涛 | Traditional Chinese medicine composition for treating dysmenorrhea and preparation method thereof |
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| CN104474380A (en) * | 2014-11-04 | 2015-04-01 | 金光 | Traditional Chinese medicine for treating hyperplasia of mammary glands and preparation method of traditional Chinese medicine |
| CN104770685A (en) * | 2015-04-15 | 2015-07-15 | 杨莉 | Uterine warming cream and preparation method thereof |
| CN106036880A (en) * | 2016-07-13 | 2016-10-26 | 广州正广生物科技有限公司 | Composition for relieving dysmenorrhea, application thereof and healthy food prepared from composition |
| CN106072656A (en) * | 2016-07-10 | 2016-11-09 | 吉林农业大学 | A kind of additive-free prevention and alleviate the health food of dysmenorrhea and production method thereof |
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- 2017-08-25 CN CN201710742800.4A patent/CN107510052A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1843446A (en) * | 2005-04-08 | 2006-10-11 | 李砚秋 | Combined matched pharmaceutical for treating irregular menses |
| CN102218127A (en) * | 2010-04-13 | 2011-10-19 | 鲁翠涛 | Traditional Chinese medicine composition for treating dysmenorrhea and preparation method thereof |
| CN102488763A (en) * | 2011-12-28 | 2012-06-13 | 吕慧侠 | Composition with functions of treating dysmenorrhoea and beautifying |
| CN104474380A (en) * | 2014-11-04 | 2015-04-01 | 金光 | Traditional Chinese medicine for treating hyperplasia of mammary glands and preparation method of traditional Chinese medicine |
| CN104770685A (en) * | 2015-04-15 | 2015-07-15 | 杨莉 | Uterine warming cream and preparation method thereof |
| CN106072656A (en) * | 2016-07-10 | 2016-11-09 | 吉林农业大学 | A kind of additive-free prevention and alleviate the health food of dysmenorrhea and production method thereof |
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Application publication date: 20171226 |