CN107496286A - One kind desalination microgroove moisturizing moist type water and milk and preparation method thereof - Google Patents
One kind desalination microgroove moisturizing moist type water and milk and preparation method thereof Download PDFInfo
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Abstract
The invention provides one kind desalination microgroove moisturizing moist type water and milk and preparation method thereof, contain following material：Shea butter, jojoba oil, olive oil, Rice oil, laurate APEO 4, olive emulsifying agent, distilled water, heartsease extract solution, oriental cherry extract solution, root of kudzu vine extract, radix polygonati officinalis extract solution, camellia extract solution, glycerine, sodium alginate, sodium carboxymethylcellulose, anion guar gum, saualane, silicone oil, ethylparaben, 75% ethanol solution and essence.Compared with prior art, water and milk property prepared by the present invention is gentle, it is safe, using the active material in natural plants, improve percutaneous permeability, reach the effect of gentle moisturizing, nutrition, the moisture of skin needs can be supplemented, skin water shortage is prevented, reaches the effect of moist moisturizing, can antibacterial, anti-aging, anti-oxidant, make that skin exquisiteness is glossy, increase elasticity of skin.
Description
Technical field
The present invention relates to face beautifying medicine field, and in particular to one kind desalination microgroove moisturizing moist type water and milk and its preparation side
Method.
Background technology
In this allegro epoch, people by computer due to being radiated for a long time, koniology etc. is influenceed, along with work
Work, life stress are big, and work and rest is irregular, and a series of problem just occurs in stress etc., fragile skin at this moment.Skin
Water shortage is most common and the problem of most merits attention, and the state that healthy skin shows is fine and smooth ruddy glossy, is given
What others brought be water profit and flexible visual experience, and skin water shortage will cause dry skin decortication, pore it is thick,
The problems such as dark yellow, dry line microgroove also can be following.If there are the one or more in problem above in skin, bring just not only
Only be influence in appearance, more can be subtle influence our quality of life, brought very big puzzlement.
Moisturizing water and milk in the market with the addition of various chemical reagent or additive mostly, and skin tape may be come
In short term, long-term or even permanent injury.And natural plant kind cosmetics are current and domestic and international cosmetics research and development from now on are most main
The trend and direction wanted, so the moisturizing water and milk using plant extraction liquid as main adding ingredient be able to will be selected preferably as people
Select.
The content of the invention
It is an object of the invention to provide one kind to desalinate microgroove moisturizing moist type water and milk, is used as and added using day drug extract
Add thing, moisten moisturizing, do not stimulate naturally.
Present invention also offers the preparation method of desalination microgroove moisturizing moist type water and milk.
A kind of desalination microgroove moisturizing moist type water and milk provided by the invention, the raw material components containing following proportionings：
The heartsease extract solution is prepared by the following method：
It is appropriate to weigh heartsease petal, heating and refluxing extraction is three times：For the first time plus 20-22 times is measured water, extracts 1.5-2.5h；
For the second time plus 18-20 times is measured water, extracts 1.0-1.5h；Third time adds 14-18 times to measure water, extracts 0.5-1.0h；Filter every time
Filtrate, merging filtrate, by 3-6 times of g/mL of the volume concentration of filtrate to heartsease weight, filter and produce.
The oriental cherry extract solution is prepared by the following method：
It is appropriate to weigh oriental cherry petal, heating and refluxing extraction is three times：For the first time plus 14-18 times is measured 75% ethanol, extracts 1.0-
1.5h；For the second time plus 12-14 times is measured 75% ethanol, extracts 1.0-1.5h；Third time adds 8-12 times to measure 75% ethanol, extracts 0.5-
1.0h；Filtrate is filtered to obtain every time, merging filtrate, by 2-8 times of g/mL of the volume concentration of filtrate to oriental cherry weight, filters and produces.
The root of kudzu vine extract is prepared by the following method：
It is appropriate to weigh root of kudzu vine coarse powder, soaks 0.2-0.6h, heating and refluxing extraction is three times：For the first time plus 22-26 times is measured water, is carried
Take 1.0-1.5h；For the second time plus 20-22 times is measured water, extracts 1.0-1.5h；Third time adds 16-18 times to measure water, extracts 0.5-1.0h；
Filtrate is filtered to obtain every time, merging filtrate, by 2-6 times of g/mL of the volume concentration of filtrate to root of kudzu vine weight, filters and produces.
The radix polygonati officinalis extract solution is prepared by the following method：
It is appropriate to weigh radix polygonati officinalis coarse powder, soaks 0.3-0.8h, heating and refluxing extraction is three times：For the first time plus 18-22 times is measured water, is carried
Take 1.5-2.0h；For the second time plus 12-16 times is measured water, extracts 1.5-2.0h；Third time adds 10-12 times to measure water, extracts 0.5-1.0h；
Filtrate is filtered to obtain every time, merging filtrate, by 4-6 times of g/mL of the volume concentration of filtrate to radix polygonati officinalis weight, filters and produces.
The camellia extract solution is prepared by the following method：
It is appropriate to weigh camellia, heating and refluxing extraction is three times：For the first time plus 14-16 times is measured 65% ethanol, extracts 1.0-2.0h；
For the second time plus 12-14 times is measured 65% ethanol, extracts 1.0-2.0h；Third time adds 8-10 times to measure 65% ethanol, extracts 0.5-1.0h；
Filtrate is filtered to obtain every time, merging filtrate, by 3-5 times of g/mL of the volume concentration of filtrate to camellia weight, filters and produces.
The essence is flavoring rose essence, milk flavour, cream jasmin france, green cucumber essence, lily essence, peach flavor or Huang
One or more in melon essence.
A kind of preparation method for desalinating microgroove moisturizing moist type water and milk provided by the invention comprises the following steps：
A) sodium alginate 0.5-1.5g is weighed, is added in 10.0-50.0mL distilled water, 30-60 DEG C of heating water bath, side
Heat side stirring, it is to be mixed uniformly after, stand overnight, it is fully swelled, dissolved, obtain sodium alginate gel liquid, it is stand-by；
B) cation guar gum 0.2-0.8g is weighed, is added in 20.0-80.0mL distilled water, 30-60 DEG C of water-bath adds
Heat, heat while stirring, it is to be mixed uniformly after, stand overnight, it is fully swelled, dissolved, obtain cation guar gum coagulant liquid,
It is stand-by；
C) sodium carboxymethylcellulose 0.2-0.8g is weighed, is added in 20.0-80.0mL distilled water, 30-60 DEG C of water-bath
Heating, heat while stirring, it is to be mixed uniformly after, stand overnight, it is fully swelled, dissolved, obtain sodium carboxymethylcellulose and coagulate
Glue, it is stand-by；
D) olive oil 0.3-0.8g, shea butter 0.3-0.8g, jojoba oil 0.3-0.8g, Rice oil 0.3- are weighed respectively
0.8g, saualane 0.3-0.8g, the 0.8-2.0g of laurate APEO -4 and olive emulsifying agent 0.8-2.5g mixing, are placed in
Heating and melting in 70-90 DEG C of thermostat water bath, it is well mixed, as oil phase；
E) weigh glycerine 0.3-0.8g to mix with distilled water 5.0-15.0mL, be placed in 70-90 DEG C of thermostat water bath and heat,
As aqueous phase；When oil phase reaches mutually synthermal with aqueous phase, aqueous phase is added in oil phase into thread shape, stirred while adding, directly
To the emulsion bases for forming uniform and smooth；
F) oriental cherry extract solution 0.5-1.5mL, heartsease extract solution 0.5-1.5mL, camellia extract solution 0.5- are measured respectively
1.5mL, root of kudzu vine extract 0.5-1.5mL and radix polygonati officinalis extract solution 0.5-1.5mL mixing, stir, obtain mixed liquor 1；
G) 0.08-0.15g ethylparabens are weighed to be dissolved in 0.5-1.5mL75% ethanol, obtain antiseptic solution；
H) the sodium alginate gel liquid, cation guar gum coagulant liquid, carboxymethyl of preparation are separately added into emulsion bases
Sodium cellulosate coagulant liquid, mixed liquor 1, antiseptic solution, silicone oil 0.3-0.8g and essence 0.05-0.2mL, stir, you can
Microgroove moisturizing moist type water and milk must be desalinated.
Various composition in the present invention is as follows：
Shea butter contains pure natural vegetable fat, has superpower oxidation resistant effect and gentle non-stimulated, such a oil
Very close with human secretory grease index, can prevent dry skin, cracking with deep layer Glycerin, have to the top layer of skin
Long-term moistening effect.It can also form diaphragm in skin surface, and moist, moisturizing, moisturizing effect are extremely obvious, long-term use of
The elasticity of skin can be kept afterwards.Shea butter also contains substantial amounts of unsaponifiable lipid, can be provided for skin abundant Alphalin,
D, E, F etc., enough nutritional ingredients are supplemented to skin, more can effectively help cytothesis and promote microcirculation, moreover it is possible to
The problems such as effectively preventing skin ageing, drying, explosion.
The main component of jojoba oil is unsaturated higher alcohol and aliphatic acid, has good stability, easily melts with skin
Close, there is superpower inoxidizability.In addition, jojoba oil has the effect of nourishing softening skin also containing abundant vitamin.
Jojoba oil is the most strong base oil of permeability, is easily absorbed by the skin, and salubrious moist, non-greasy, can recover skin pH balances,
Wrinkle is removed, is effectively improved Oily, nurses one's health smegma function, pore refining, while is also optimal skin moisture-keeping oil.
The oil film that it is formed is different from mineral oil, can pass through evaporation moisture, can also control the loss of moisture, can firm skin, and
Exclude the toxin in skin.
Olive oil is rich in the squalene and essential fatty acid splendid with skin affinity, absorbs rapid, effectively holding
Skin elasticity and moist, abundant monounsaturated fatty acids and vitamin E, K, A, D etc. and phenols polyphenoils contained therein,
Facial wrinkles can be eliminated, prevent skin aging, ultraviolet prevention cutaneum carcinoma can be resisted by smearing skin with olive oil in addition.In olive
In oily numerous compositions, carrotene and chlorophyll assign olive oil yellow green, can accelerate the metabolism of human body skin, promote
Cell growth, keep the moist of skin.
The vitamin E contained in Rice oil can effectively antagonize free radical, suppress lipid peroxide and generate, eliminating chloasma,
Suppress the activity of tyrosinase, so as to reduce melanin generation, moreover it is possible to which elimination is caused by extraneous factors such as ultraviolet, air pollutions
Excessive oxygen radical, play delaying aging, prevention sunburn and suppress sunburn generation etc. effect.
Silicone oil is usually used in the making of the cosmetics such as light cream, emulsion, mildy wash, toner, color make-up, there is moist, lock
The effect of water, moisturizing, it can also make component different in prescription that there is higher compatibility, reduce the sticky sense of product, because
It is gentle non-stimulated, therefore is often added in the making prescription of cosmetics or skin care item, increases the sense of the uniform and smooth of product.
Laurate APEO -4 has good emulsification, wetting, solubilising, scattered, plasticising performance, have property it is gentle,
Non-stimulated characteristic, make emulsifying agent in cosmetics, dispersiveness of the different material in same system in prescription can be increased, it is especially right
There is significant effect in the system of oil-in-water type, therefore be usually used in the making of cosmetics and skin care item, be mainly used in improving
Wetability, dispersiveness in the aqueous solution.
Olive emulsifier ability is superpower, for the salubrious water of user's skin sense can be allowed to moisten in skin care item, there is good benefit
Water moisture-keeping efficacy, cream, water miscible olive oil derivative, water and milk etc. particularly suitable for top grade, are good emollients
And emulsifying agent.
Heartsease plays the role of stronger sterilization, sterilizing, the growth for suppressing bacterium, can eliminate one existing for skin surface
Harmful microorganism a bit, keep the cleaning of skin surface and shallow-layer skin, because its bactericidal effect is notable, for treat whelk,
The skin problems such as acne, allergy.
Oriental cherry has the effect of good pore refining and Sage Extract, but also containing abundant natural vitamin A, B,
E, wherein vitamin E and ascorbic content are very high, and both vitamins can directly act on Skin Cell, to U.S.
It is particularly evident to hold skin effect.In addition, the oriental cherry ferment in oriental cherry can play a part of tender skin, anti-acne, lightening skin color.Oriental cherry should
Can be with beautifying face and moistering lotion, reinforcing mucous membrane, promotion sugar metabolism in skin care item, antioxygen essence therein can be effectively anti-oxidant,
It may be employed to the flower of youth for keeping skin young.
The Puerarin contained in the root of kudzu vine has promoting blood circulation beauty treatment and sterilization acne-removing, energy anti-aging, can mutually be equal to ginseng
It is beautiful.Root of kudzu vine extract can penetrate into skin, deep layer cleaning, red and swollen and suppuration phenomenon caused by easing whelk, while also have suppression
Fat secretion processed, the regeneration of prevention small pox, avoid bacteria breed, regulation skin resistivity, repair damage skin, desalination red seal and
The function of pigment.Root of kudzu vine extract makes an addition in cosmetics the decline that can improve face's chloasma, regression whelk, enhancing skin
Fine and smooth glossy, increase elasticity of skin is thick with improving pore.
The characteristic that radix polygonati officinalis has matter soft and moistened, its rhizome extract have the effect of beauty and skin care.Radix polygonati officinalis is rich in retinoid
Material and mucilaginous substance, vitamin A can effectively improve skin it is dry and cracked, coarse the problems such as, lubricate skin emolliency, so as to play grow
Moisten the effect of skin, beauty and skin care.Contain steroid saponin, flavones and its glucosides, trace element, amino acid, vitamin A in radix polygonati officinalis
Sample material etc., have and suppress TYR enzyme activity, suppress melanin generation, anti-oxidant and other effects.
The pure white petal of camellia contains abundant vitamin and lot of trace mineral matter, can play convergence, rouse oneself flesh
The effect of skin.And the camellia seed essential oil therefrom extracted can more promote internal layer cytothesis, nourish sebaceous cell.Camellia may be used also
With the tender skin of cunning, color spot is removed, and as a kind of natural flowers, its nontoxic nutritive value for being but rich in flowers, to skin
It is a kind of gentle maintenance and care.
Saualane be closest to human sebaceous a kind of lipid, affinity is strong, can melt with the sebum film of mankind itself for
One, one layer of natural barrier is formed in skin surface, maintenance epidermis can be strengthened, is effectively formed natural diaphragm, helps flesh
Balance between skin and sebum.Saualane can also suppress the peroxidating of skin lipid, can effectively infiltrate through skin, and promote skin base
The propagation of floor cells, to delay skin aging, improving and eliminating chloasma has obvious physiologic effect.In addition, saualane is also
Skin pore can be opened, promote blood microcirculation, promote the metabolism of cell, damaged cell is repaired in help.
Glycerine has very strong hygroscopicity, and pure glycerine can absorb more moisture, so putting on the skin can form on skin
Thin film, play the role of to completely cut off air and prevent moisture evaporation, moreover it is possible to the moisture in absorption air, skin can be made to keep soft
Soft, high resilience, do not damaged by dust, weather etc. the problem of dry, play a part of preventing chapped skin decortication.
Sodium carboxymethylcellulose has the effects such as bonding, thickening, and the hydrosol is used as in cosmetics, is used as increasing in emulsion
Thick dose.
Anion guar gum is a kind of good thickener, and the cationic guar solution of small concentration is as clear as crystal, flowing
Property it is good, the fusion degree of each composition in systems can be increased, each material is had preferable dispersiveness in prescription, made every
A kind of both effectiveness composition all plays their maximum effects and effect.
Sodium alginate hydrophily is strong, can be dissolved in cold water and warm water, forms fine and smooth uniform solution, formation it is water-soluble
Liquid also there are other analogs to be difficult to the flexibility, homogeneity and other good characteristics obtained.Additionally have simultaneously very strong
The effect of protecting colloid, it is strong to the emulsifying ability of grease.Because of its action temperature and, it is small to skin irritation, be usually used in the increasing of skin care item
Thick dose.
Substantial amounts of extracted form natural plant composition is with the addition of in this water and milk prescription.On the one hand by pore refining Sage Extract come
Keep the cleaning of skin.Such as the good firm skin of composition energy and control water and oil balance in oriental cherry, it contains flavones with beautiful
Hold beauty treatment, strengthen mucous membrane, promote the effect of sugar metabolism；Root of kudzu vine extract can penetrate into skin, deep layer cleaning, have oil-control
Secrete, avoid bacteria breed, the ability of regulation skin resistance environmental stimuli.On the other hand further through anti-oxidant, skin of moistening
Play a part of moisturizing.As radix polygonati officinalis is rich in retinoid material and mucilaginous substance, vitamin A has and improves chapped skin problem of rough
Effect, be allowed to soft lubrication；Steroid saponin, flavones and its glucosides that radix polygonati officinalis contains, trace element, amino acid, vitamin A sample
Material etc., have and suppress TYR enzyme activity, suppress melanin generation, anti-oxidant and other effects.
Compared with prior art, water and milk provided by the invention can conditioning skin water and oil balance, promote pore convergence, improve
Pore is thick, the fine and smooth sense of lifting skin, can also promote internal layer cytothesis, nourish sebaceous cell, firmly pin skin moisture, subtract
Few water loss, suppresses melanin bright color, makes skin gloss flexible, reaches the effect of cleaning skin care.
Embodiment
With reference to embodiment, the present invention will be further described.
Embodiment 1
One kind desalination microgroove moisturizing moist type water and milk, the raw material components containing following proportionings：
The preparation of 1.1 heartsease extract solutions
Heartsease petal 30g is weighed, heating and refluxing extraction is three times：For the first time plus 20 times are measured water, extract 1.5h；Add for the second time
18 times of amount water, extract 1.0h；Third time plus 14 times of amount water, extract 0.5h；Filter to obtain filtrate, merging filtrate, by filtrate every time
Volume concentration is filtered and produced to 3 times of g/mL of heartsease weight.
The preparation of 1.2 oriental cherry extract solutions
Oriental cherry petal 40g is weighed, heating and refluxing extraction is three times：For the first time plus 14 times are measured 75% ethanol, extract 1.0h；Second
Secondary plus 12 times of 75% ethanol of amount, extract 1.0h；Third time plus 8 times of 75% ethanol of amount, extract 0.5h；Filtrate is filtered to obtain every time, is closed
And filtrate, by 2 times of g/mL of the volume concentration of filtrate to oriental cherry weight, filter and produce.
The preparation of 1.3 root of kudzu vine extract
Root of kudzu vine coarse powder 30g is weighed, soaks 0.2h, heating and refluxing extraction is three times：For the first time plus 22 times are measured water, extract 1.0h；
Second plus 20 times of amount water, extract 1.0h；Third time plus 16 times of amount water, extract 0.5h；Filter to obtain filtrate every time, merging filtrate,
By 2 times of g/mL of the volume concentration of filtrate to root of kudzu vine weight, filter and produce.
The preparation of 1.4 radix polygonati officinalis extract solutions
Radix polygonati officinalis coarse powder 50g is weighed, soaks 0.3h, heating and refluxing extraction is three times：For the first time plus 18 times are measured water, extract 1.5h；
Second plus 12 times of amount water, extract 1.5h；Third time plus 10 times of amount water, extract 0.5h；Filter to obtain filtrate every time, merging filtrate,
By 4 times of g/mL of the volume concentration of filtrate to radix polygonati officinalis weight, filter and produce.
The preparation of 1.5 camellia extract solutions
Camellia 30g is weighed, heating and refluxing extraction is three times：For the first time plus 14 times are measured 65% ethanol, extract 1.0h；Add for the second time
12 times of 65% ethanol of amount, extract 1.0h；Third time plus 8 times of 65% ethanol of amount, extract 0.5h；Filtrate is filtered to obtain every time, merges filter
Liquid, by 3 times of g/mL of the volume concentration of filtrate to camellia weight, filter and produce.
The preparation method of 1.6 desalination microgroove moisturizing moist type water and milk
A) sodium alginate 0.5g is weighed, is added in 30.0mL distilled water, 50 DEG C of heating water baths, is heated while stirring,
It is to be mixed uniformly after, stand overnight, it is fully swelled, dissolved, obtain sodium alginate gel liquid, it is stand-by；
B) cation guar gum 0.2g is weighed, is added in 50.0mL distilled water, 30-60 DEG C of heating water bath, side heating
Side stir, it is to be mixed uniformly after, stand overnight, it is fully swelled, dissolved, obtain cation guar gum coagulant liquid, it is stand-by；
C) sodium carboxymethylcellulose 0.2g is weighed, is added in 50.0mL distilled water, 50 DEG C of heating water baths, in heating
Stirring, it is to be mixed uniformly after, stand overnight, it is fully swelled, dissolved, obtain sodium carboxymethylcellulose coagulant liquid, it is stand-by；
D) weigh respectively olive oil 0.3g, shea butter 0.3g, jojoba oil 0.4g, Rice oil 0.3g, saualane 0.5g,
The 0.8g of laurate APEO -4 and olive emulsifying agent 0.8g are placed in 70 DEG C of thermostat water baths to heat and melted in beaker 1
Change, be well mixed, as oil phase；
E) glycerine 0.3g is weighed in beaker 2, then measures distilled water 5.0mL and is added thereto, and is placed in 70 DEG C of thermostat water baths
Middle heating, as aqueous phase；When oil phase reaches mutually synthermal with aqueous phase, aqueous phase is added in oil phase into thread shape, when adding
Stirring, until forming the emulsion bases of uniform and smooth；
F) oriental cherry extract solution 0.5mL, heartsease extract solution 0.5mL, camellia extract solution 0.5mL, root of kudzu vine extraction are measured respectively
Liquid 0.5mL and radix polygonati officinalis extract solution 1.0mL are placed in beaker, are stirred, are obtained mixed liquor 1；
G) 0.08g ethylparabens are weighed to be dissolved in 0.5mL75% ethanol, obtain antiseptic solution；
H) sodium alginate gel liquid, cation guar gum coagulant liquid, carboxymethyl cellulose are separately added into emulsion bases
Sodium gel liquid, mixed liquor 1, antiseptic solution, silicone oil 0.3g and cucumber essence 0.05mL, stir, you can must desalinate microgroove
Moisturizing moist type water and milk.
Embodiment 2
One kind desalination microgroove moisturizing moist type water and milk, the raw material components containing following proportionings：
The preparation of 2.1 heartsease extract solutions
Heartsease petal 50g is weighed, heating and refluxing extraction is three times：For the first time plus 20 times are measured water, extract 2.0h；Add for the second time
18 times of amount water, extract 1.0h；Third time plus 18 times of amount water, extract 1.0h；Filter to obtain filtrate, merging filtrate, by filtrate every time
Volume concentration is filtered and produced to 4 times of g/mL of heartsease weight.
The preparation of 2.2 oriental cherry extract solutions
Oriental cherry petal 30g is weighed, heating and refluxing extraction is three times：For the first time plus 16 times are measured 75% ethanol, extract 1.5h；Second
Secondary plus 13 times of 75% ethanol of amount, extract 1.0h；Third time plus 10 times of 75% ethanol of amount, extract 1.0h；Filtrate is filtered to obtain every time, is closed
And filtrate, by 5 times of g/mL of the volume concentration of filtrate to oriental cherry weight, filter and produce.
The preparation of 2.3 root of kudzu vine extract
Root of kudzu vine coarse powder 50g is weighed, soaks 0.5h, heating and refluxing extraction is three times：For the first time plus 24 times are measured water, extract 1.5h；
Second plus 20 times of amount water, extract 1.5h；Third time plus 18 times of amount water, extract 1.0h；Filter to obtain filtrate every time, merging filtrate,
By 3 times of g/mL of the volume concentration of filtrate to root of kudzu vine weight, filter and produce.
The preparation of 2.4 radix polygonati officinalis extract solutions
Radix polygonati officinalis coarse powder 40g is weighed, soaks 0.6h, heating and refluxing extraction is three times：For the first time plus 20 times are measured water, extract 2.0h；
Second plus 14 times of amount water, extract 1.5h；Third time plus 12 times of amount water, extract 1.0h；Filter to obtain filtrate every time, merging filtrate,
By 5 times of g/mL of the volume concentration of filtrate to radix polygonati officinalis weight, filter and produce.
The preparation of 2.5 camellia extract solutions
Camellia 50g is weighed, heating and refluxing extraction is three times：For the first time plus 15 times are measured 65% ethanol, extract 1.5h；Add for the second time
12 times of 65% ethanol of amount, extract 1.5h；Third time plus 10 times of 65% ethanol of amount, extract 1.0h；Filtrate is filtered to obtain every time, merges filter
Liquid, by 4 times of g/mL of the volume concentration of filtrate to camellia weight, filter and produce.
The preparation method of 2.6 desalination microgroove moisturizing moist type water and milk
A) sodium alginate 1.0g is weighed, is added in 40.0mL distilled water, 50 DEG C of heating water baths, is heated while stirring,
It is to be mixed uniformly after, stand overnight, it is fully swelled, dissolved, obtain sodium alginate gel liquid, it is stand-by；
B) cation guar gum 0.6g is weighed, is added in 60.0mL distilled water, 50 DEG C of heating water baths, is stirred in heating
Mix, it is to be mixed uniformly after, stand overnight, it is fully swelled, dissolved, obtain cation guar gum coagulant liquid, it is stand-by；
C) sodium carboxymethylcellulose 0.5g is weighed, is added in 80.0mL distilled water, 50 DEG C of heating water baths, in heating
Stirring, it is to be mixed uniformly after, stand overnight, it is fully swelled, dissolved, obtain sodium carboxymethylcellulose coagulant liquid, it is stand-by；
D) weigh respectively olive oil 0.5g, shea butter 0.4g, jojoba oil 0.3g, Rice oil 0.5g, saualane 0.5g,
The 1.0g of laurate APEO -4 and olive emulsifying agent 1.5g are placed in 80 DEG C of thermostat water baths to heat and melted in beaker 1
Change, be well mixed, as oil phase；
E) glycerine 0.5g is weighed in beaker 2, then measures distilled water 10.0mL and is added thereto, and is placed in 80 DEG C of thermostat water baths
Middle heating, as aqueous phase；When oil phase reaches mutually synthermal with aqueous phase, aqueous phase is added in oil phase into thread shape, when adding
Stirring, until forming the emulsion bases of uniform and smooth；
F) oriental cherry extract solution 1.0mL, heartsease extract solution 1.2mL, camellia extract solution 1.0mL, root of kudzu vine extraction are measured respectively
Liquid 0.8mL and radix polygonati officinalis extract solution 1.0mL are placed in beaker, are stirred, are obtained mixed liquor 1；
G) 0.1g ethylparabens are weighed to be dissolved in 1.2mL75% ethanol, obtain antiseptic solution；
H) sodium alginate gel liquid, cation guar gum coagulant liquid, carboxymethyl cellulose are separately added into emulsion bases
Sodium gel liquid, mixed liquor 1, antiseptic solution, silicone oil 0.5g and green cucumber essence 0.08mL, stir, you can must desalinate microgroove
Moisturizing moist type water and milk.
Embodiment 3
One kind desalination microgroove moisturizing moist type water and milk, the raw material components containing following proportionings：
The preparation of 3.1 heartsease extract solutions
Heartsease petal 40g is weighed, heating and refluxing extraction is three times：For the first time plus 22 times are measured water, extract 2.5h；Add for the second time
20 times of amount water, extract 1.5h；Third time plus 18 times of amount water, extract 1.0h；Filter to obtain filtrate, merging filtrate, by filtrate every time
Volume concentration is filtered and produced to 6 times of g/mL of heartsease weight.
The preparation of 3.2 oriental cherry extract solutions
Oriental cherry petal 50g is weighed, heating and refluxing extraction is three times：For the first time plus 18 times are measured 75% ethanol, extract 1.5h；Second
Secondary plus 14 times of 75% ethanol of amount, extract 1.5h；Third time plus 12 times of 75% ethanol of amount, extract 1.0h；Filtrate is filtered to obtain every time, is closed
And filtrate, by 8 times of g/mL of the volume concentration of filtrate to oriental cherry weight, filter and produce.
The preparation of 3.3 root of kudzu vine extract
It is appropriate to weigh root of kudzu vine coarse powder, soaks 0.6h, heating and refluxing extraction is three times：For the first time plus 26 times are measured water, extract 1.5h；
Second plus 22 times of amount water, extract 1.5h；Third time plus 18 times of amount water, extract 1.0h；Filter to obtain filtrate every time, merging filtrate,
By 6 times of g/mL of the volume concentration of filtrate to root of kudzu vine weight, filter and produce.
The preparation of 3.4 radix polygonati officinalis extract solutions
Radix polygonati officinalis coarse powder 40g is weighed, soaks 0.8h, heating and refluxing extraction is three times：For the first time plus 22 times are measured water, extract 2.0h；
Second plus 16 times of amount water, extract 2.0h；Third time plus 12 times of amount water, extract 1.0h；Filter to obtain filtrate every time, merging filtrate,
By 6 times of g/mL of the volume concentration of filtrate to radix polygonati officinalis weight, filter and produce.
The preparation of 3.5 camellia extract solutions
Camellia 50g is weighed, heating and refluxing extraction is three times：For the first time plus 16 times are measured 65% ethanol, extract 2.0h；Add for the second time
14 times of 65% ethanol of amount, extract 2.0h；Third time plus 10 times of 65% ethanol of amount, extract 1.0h；Filtrate is filtered to obtain every time, merges filter
Liquid, by 5 times of g/mL of the volume concentration of filtrate to camellia weight, filter and produce.
The preparation method of 3.6 desalination microgroove moisturizing moist type water and milk
A) sodium alginate 1.5g is weighed, is added in 50.0mL distilled water, 60 DEG C of heating water baths, is heated while stirring,
It is to be mixed uniformly after, stand overnight, it is fully swelled, dissolved, obtain sodium alginate gel liquid, it is stand-by；
B) cation guar gum 0.8g is weighed, is added in 80.0mL distilled water, 60 DEG C of heating water baths, is stirred in heating
Mix, it is to be mixed uniformly after, stand overnight, it is fully swelled, dissolved, obtain cation guar gum coagulant liquid, it is stand-by；
C) sodium carboxymethylcellulose 0.8g is weighed, is added in 80.0mL distilled water, 60 DEG C of heating water baths, in heating
Stirring, it is to be mixed uniformly after, stand overnight, it is fully swelled, dissolved, obtain sodium carboxymethylcellulose coagulant liquid, it is stand-by；
D) weigh respectively olive oil 0.8g, shea butter 0.6g, jojoba oil 0.8g, Rice oil 0.5g, saualane 0.6g,
The 2.0g of laurate APEO -4 and olive emulsifying agent 1.5g are placed in 90 DEG C of thermostat water baths to heat and melted in beaker 1
Change, be well mixed, as oil phase；
E) glycerine 0.8g is weighed in beaker 2, then measures distilled water 15.0mL and is added thereto, and is placed in 90 DEG C of thermostat water baths
Middle heating, as aqueous phase；When oil phase reaches mutually synthermal with aqueous phase, aqueous phase is added in oil phase into thread shape, when adding
Stirring, until forming the emulsion bases of uniform and smooth；
F) oriental cherry extract solution 1.5mL, heartsease extract solution 1.5mL, camellia extract solution 1.2mL, root of kudzu vine extraction are measured respectively
Liquid 1.5mL and radix polygonati officinalis extract solution 1.0mL are placed in beaker, are stirred, are obtained mixed liquor 1；
G) 0.1g ethylparabens are weighed to be dissolved in 1.5mL75% ethanol, obtain antiseptic solution；
H) sodium alginate gel liquid, cation guar gum coagulant liquid, carboxymethyl cellulose are separately added into emulsion bases
Sodium gel liquid, mixed liquor 1, antiseptic solution, silicone oil 0.8g and milk flavour 0.1mL, stir, you can must desalinate microgroove benefit
Moistening water type water and milk.
Embodiment 4
The physical and chemical index of embodiment 1,2,3 is as follows：
4.1 character
This product is that viscosity is suitable, fine and smooth uniform, the good milky water and milk of absorbability.
4.2pH values check
A small amount of water and milk, pH 6-7 are dipped with the pH test paper of wetting.
4.3 caloric test
Water and milk is packaged in transparency emulsion bottle, in 4 DEG C of refrigerator cold-storage observations in one week or so without lamination.In 55 DEG C
Insulating box in 24h, it is no layering emulsification it is spoiled phenomena such as.
4.4 centrifugal test
Water and milk is packaged in 3000r/min in tool plug test tube and centrifuges 20min, no lamination.
4.5 irritation tests, anaphylaxis experiment
Small white mouse back cuts off hair, smears respectively by water and milk prepared by embodiment 1,2,3 in cutting plucked position, and do not apply
Position is compared, as a result without excitant and allergic reaction.
1 gram of Example is applied in volunteer (15-65 year, 180 people) gesture and facial expression, is observed after spending 30 minutes, is not sent out
It is red, dermexanthesis, foaming phenomena.
4.6 room temperatures place experiment
1,2,3 made water and milk of embodiment is placed in lotion pump, is stored at room temperature investigation 6 months, no lamination, after
Feel unchanged, smell is unchanged.
4.7 moisturizing effects
Volunteer's (15-65 year, 180 people) is chosen, obtained water and milk is used for volunteer, volunteers generally feel water
Moisten moisturizing, texture is preferable, and absorbability is good, either dry skin or health, moistening effect is all preferable, after without allergy,
Red and swollen phenomenon, quality is frivolous, energy Sage Extract, skin will not be made to feel vexed, and skin substantially becomes water profit after a use in month
Light, it is moist.
Embodiment 5
Resultant effect is investigated
Following with probation the effect of feeling to evaluate water and milk that embodiment 1,2,3 produces.Scored using opinion poll
Method, the women of 90 25-50 year age brackets is chosen as object on probation, three groups is arbitrarily divided into, is made respectively with embodiment 1,2,3
Standby water and milk.Daily using twice, usage time is two months.Every using effect total score is 5 points：5 points are best result, are represented
Very well, it is very satisfied；4 points are preferable；3 points are to receive；Less than 3 points are bad, it is impossible to are received.It is averaged below to be every
Point.It the results are shown in Table 1：
The resultant effect of table 1 is investigated
In summary, the made water and milk water profit moisturizing of the present invention, has good moisture retention, moistness, absorbability, uses
When feel it is frivolous uniformly, it is good with rear skin elasticity, have moisturizing, water lock, it is moist, anti-oxidant, desalinate microgroove, the effect of whitening.
Claims (8)
1. one kind desalination microgroove moisturizing moist type water and milk, it is characterised in that under the desalination microgroove moisturizing moist type water and milk contains
State the raw material components of proportioning：
2. desalinate microgroove moisturizing moist type water and milk according to claim 1, it is characterised in that the heartsease extract solution passes through
It is prepared by following methods：
It is appropriate to weigh heartsease petal, heating and refluxing extraction is three times：For the first time plus 20-22 times is measured water, extracts 1.5-2.5h；Second
It is secondary to add 18-20 times to measure water, extract 1.0-1.5h；Third time adds 14-18 times to measure water, extracts 0.5-1.0h；Filtrate is filtered to obtain every time,
Merging filtrate, by 3-6 times of g/mL of the volume concentration of filtrate to heartsease weight, filter and produce.
3. desalination microgroove moisturizing moist type water and milk according to claim 1 or claim 2, it is characterised in that the oriental cherry extract solution leads to
Cross following methods preparation：
It is appropriate to weigh oriental cherry petal, heating and refluxing extraction is three times：For the first time plus 14-18 times is measured 75% ethanol, extracts 1.0-1.5h；
For the second time plus 12-14 times is measured 75% ethanol, extracts 1.0-1.5h；Third time adds 8-12 times to measure 75% ethanol, extracts 0.5-1.0h；
Filtrate is filtered to obtain every time, merging filtrate, by 2-8 times of g/mL of the volume concentration of filtrate to oriental cherry weight, filters and produces.
4. according to any one of the claim 1-3 desalination microgroove moisturizing moist type water and milk, it is characterised in that the root of kudzu vine extraction
Liquid is prepared by the following method：
It is appropriate to weigh root of kudzu vine coarse powder, soaks 0.2-0.6h, heating and refluxing extraction is three times：For the first time plus 22-26 times is measured water, is extracted
1.0-1.5h；For the second time plus 20-22 times is measured water, extracts 1.0-1.5h；Third time adds 16-18 times to measure water, extracts 0.5-1.0h；Often
It is secondary to filter to obtain filtrate, merging filtrate, by 2-6 times of g/mL of the volume concentration of filtrate to root of kudzu vine weight, filter and produce.
5. according to any one of the claim 1-4 desalination microgroove moisturizing moist type water and milk, it is characterised in that the radix polygonati officinalis extraction
Liquid is prepared by the following method：
It is appropriate to weigh radix polygonati officinalis coarse powder, soaks 0.3-0.8h, heating and refluxing extraction is three times：For the first time plus 18-22 times is measured water, is extracted
1.5-2.0h；For the second time plus 12-16 times is measured water, extracts 1.5-2.0h；Third time adds 10-12 times to measure water, extracts 0.5-1.0h；Often
It is secondary to filter to obtain filtrate, merging filtrate, by 4-6 times of g/mL of the volume concentration of filtrate to radix polygonati officinalis weight, filter and produce.
6. according to any one of the claim 1-5 desalination microgroove moisturizing moist type water and milk, it is characterised in that the camellia extraction
Liquid is prepared by the following method：
It is appropriate to weigh camellia, heating and refluxing extraction is three times：For the first time plus 14-16 times is measured 65% ethanol, extracts 1.0-2.0h；Second
It is secondary to add 12-14 times to measure 65% ethanol, extract 1.0-2.0h；Third time adds 8-10 times to measure 65% ethanol, extracts 0.5-1.0h；Every time
Filtrate is filtered to obtain, merging filtrate, by 3-5 times of g/mL of the volume concentration of filtrate to camellia weight, filters and produces.
7. according to any one of the claim 1-6 desalination microgroove moisturizing moist type water and milk, it is characterised in that the essence is rose
Rare essence, milk flavour, cream jasmin france, green cucumber essence, lily essence, peach flavor or one kind or more in cucumber essence
Kind.
A kind of 8. preparation method of any one of claim 1-7 desalination microgroove moisturizing moist type water and milk, it is characterised in that institute
Preparation method is stated to comprise the following steps：
A) sodium alginate 0.5-1.5g is weighed, is added in 10.0-50.0mL distilled water, 30-60 DEG C of heating water bath, side heating
Side stir, it is to be mixed uniformly after, stand overnight, it is fully swelled, dissolved, obtain sodium alginate gel liquid, it is stand-by；
B) cation guar gum 0.2-0.8g is weighed, is added in 20.0-80.0mL distilled water, 30-60 DEG C of heating water bath, side
Heat side stirring, it is to be mixed uniformly after, stand overnight, it is fully swelled, dissolved, obtain cation guar gum coagulant liquid, it is stand-by；
C) sodium carboxymethylcellulose 0.2-0.8g is weighed, is added in 20.0-80.0mL distilled water, 30-60 DEG C of heating water bath,
Heat while stirring, it is to be mixed uniformly after, stand overnight, it is fully swelled, dissolved, obtain sodium carboxymethylcellulose coagulant liquid,
It is stand-by；
D) olive oil 0.3-0.8g, shea butter 0.3-0.8g, jojoba oil 0.3-0.8g, Rice oil 0.3- are weighed respectively
0.8g, saualane 0.3-0.8g, the 0.8-2.0g of laurate APEO -4 and olive emulsifying agent 0.8-2.5g mixing, are placed in
Heating and melting in 70-90 DEG C of thermostat water bath, it is well mixed, as oil phase；
E) weigh glycerine 0.3-0.8g to mix with distilled water 5.0-15.0mL, be placed in 70-90 DEG C of thermostat water bath and heat, as
Aqueous phase；When oil phase reaches mutually synthermal with aqueous phase, aqueous phase is added in oil phase into thread shape, stirred while adding, until shape
Into the emulsion bases of uniform and smooth；
F) measure respectively oriental cherry extract solution 0.5-1.5mL, heartsease extract solution 0.5-1.5mL, camellia extract solution 0.5-1.5mL,
Root of kudzu vine extract 0.5-1.5mL and radix polygonati officinalis extract solution 0.5-1.5mL mixing, stirs, obtains mixed liquor 1；
G) 0.08-0.15g ethylparabens are weighed to be dissolved in 0.5-1.5mL75% ethanol, obtain antiseptic solution；
H) the sodium alginate gel liquid, cation guar gum coagulant liquid, carboxymethyl cellulose of preparation are separately added into emulsion bases
Plain sodium gel liquid, mixed liquor 1, antiseptic solution, silicone oil 0.3-0.8g and essence 0.05-0.2mL, stir, you can obtain light
Change microgroove moisturizing moist type water and milk.
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| CN113633582A (en) * | 2021-09-06 | 2021-11-12 | 广州安若希医药科技有限公司 | Bioactive small-molecule penetration-skin-bottom stock solution and skin care method thereof |
| CN113925819A (en) * | 2021-11-17 | 2022-01-14 | 陈勇 | Polypeptide factor cosmetic and preparation method thereof |
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| CN103599063A (en) * | 2013-11-28 | 2014-02-26 | 杭州贞尔生物科技有限公司 | Anti-aging face cream |
| CN105078868A (en) * | 2015-09-18 | 2015-11-25 | 皖南医学院 | Whitening and moisturizing freckle removal lotion and preparation method thereof |
| CN105853300A (en) * | 2016-05-26 | 2016-08-17 | 皖南医学院 | Degreasing, dandruff removing, itching relieving and moistening cream shampoo and preparation method thereof |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103599063A (en) * | 2013-11-28 | 2014-02-26 | 杭州贞尔生物科技有限公司 | Anti-aging face cream |
| CN105078868A (en) * | 2015-09-18 | 2015-11-25 | 皖南医学院 | Whitening and moisturizing freckle removal lotion and preparation method thereof |
| CN105853300A (en) * | 2016-05-26 | 2016-08-17 | 皖南医学院 | Degreasing, dandruff removing, itching relieving and moistening cream shampoo and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113633582A (en) * | 2021-09-06 | 2021-11-12 | 广州安若希医药科技有限公司 | Bioactive small-molecule penetration-skin-bottom stock solution and skin care method thereof |
| CN113925819A (en) * | 2021-11-17 | 2022-01-14 | 陈勇 | Polypeptide factor cosmetic and preparation method thereof |
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