CN107485978A - Sulfur hexafluoride and nitrogen mixed gas recovery separating-purifying device and method - Google Patents

Sulfur hexafluoride and nitrogen mixed gas recovery separating-purifying device and method Download PDF

Info

Publication number
CN107485978A
CN107485978A CN201710561349.6A CN201710561349A CN107485978A CN 107485978 A CN107485978 A CN 107485978A CN 201710561349 A CN201710561349 A CN 201710561349A CN 107485978 A CN107485978 A CN 107485978A
Authority
CN
China
Prior art keywords
gas
valve
sulfur hexafluoride
mixed gas
vacuum
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710561349.6A
Other languages
Chinese (zh)
Inventor
汪献忠
***
申红志
李�浩
朱会
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henan Relations Co Ltd
Original Assignee
Henan Relations Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henan Relations Co Ltd filed Critical Henan Relations Co Ltd
Priority to CN201710561349.6A priority Critical patent/CN107485978A/en
Publication of CN107485978A publication Critical patent/CN107485978A/en
Pending legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/22Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by diffusion
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/45Compounds containing sulfur and halogen, with or without oxygen
    • C01B17/4507Compounds containing sulfur and halogen, with or without oxygen containing sulfur and halogen only
    • C01B17/4515Compounds containing sulfur and halogen, with or without oxygen containing sulfur and halogen only containing sulfur and fluorine only
    • C01B17/453Sulfur hexafluoride
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00Nitrogen; Compounds thereof
    • C01B21/04Purification or separation of nitrogen
    • C01B21/0405Purification or separation processes
    • C01B21/0433Physical processing only
    • C01B21/0438Physical processing only by making use of membranes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/151Reduction of greenhouse gas [GHG] emissions, e.g. CO2

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Gas-Insulated Switchgears (AREA)
  • Treating Waste Gases (AREA)

Abstract

Sulfur hexafluoride and nitrogen mixed gas recovery separating-purifying device, including pass sequentially through mixed gas air inlet, first pressure table, the first valve, unstrpped gas input power system, the first check valve, gas pretreatment system, the second valve, second pressure gauge, separation system of mixed gas, the 3rd pressure gauge, the 3rd valve, product gas recovery system, the 4th valve, the 4th pressure gauge and the sulfur hexafluoride gas gas outlet of gas withdrawal line connection;Mixed gas circulation line is also associated between gas separation system and gas pretreatment system, gas separation system is connected with exhaust emission tube road.The invention also discloses a kind of sulfur hexafluoride and the recovery process for separation and purification of nitrogen mixed gas recovery separating-purifying device.The present invention realizes SF6/N2The separating-purifying of mixed gas, contributes to SF6/N2Mix insulation gas replaces pure SF6The popularization of gas, reduce SF6Gas usage amount, there are great economy and environmental benefit, also energetically promoted the construction of national green power network.

Description

Sulfur hexafluoride and nitrogen mixed gas recovery separating-purifying device and method
Technical field
The invention belongs to sulfur hexafluoride gas purification technique field, more particularly to a kind of sulfur hexafluoride and nitrogen mixing Gas reclaims separating-purifying device and method.
Background technology
Sulfur hexafluoride(SF6)Gas is a kind of sufficiently stable gas of chemical property, as a kind of excellent insulation and is gone out Arc medium, it is widely used in various electrical equipments.But SF6Gas also has its weak point in the application:(1)To electric field Uniformity coefficient is more sensitive, and its advantage only can be just shown in uniform or slightly uneven electric field;(2)SF6Gas be by It is included in《The Kyoto Protocol》With《Bali's route map》In greenhouse gases, its greenhouse effects is equivalent CO2Gas 23900 times, and SF6Gas can be stabilized up to 3200 in an atmosphere;(3)SF6The price of gas is higher etc..Thus Its application is limited, and is finding SF at present6Before gas substitute, SF is utilized6Mixed gas replaces pure SF6Gas is More effective method.To solve the greenhouse effects of SF6 gases and becoming increasingly conspicuous for the easy Liquefaction of low temperature, SF6/N2, SF6/ The mix insulation gas such as CF4 is considered as substitute medium most promising at present
By being considered to environment and economic aspect, due to N2Non-hazardous and the reason such as cheap, use SF6/N2Gaseous mixture Body replaces high-purity SF6Gas is as the trend that dielectric is green electric power supply development.Research papers show, in N2Middle note After entering 20%~30% SF6 gases, SF6/N2Mixed gas insulation performance indications can reach pure SF680% or so of gas;Again It is reported that SF6(30%)With N2(70%) hybrid gas insulation switchgear has been included in State Grid Corporation of China and south electric network is public Take charge of in the project of SF6 mixed gas high voltage electric equipment projects.
SF6/N2Mixed gas electrical equipment unavoidably needs to carry out repair and maintenance work in the process of running, and is examining SF during repairing6、N2The work such as the recovery storage of mixed gas and isolation of purified is also to carry out.
With the trend of China SF6/N2 mix insulation outlet openings equipment developments, the separating-purifying of SF6/N2 mixed gas Technology is also put on using schedule.SF6/N2 mixed gas separation method mainly has cryogenic rectification method, PSA methods at present(Pressure-variable adsorption Method)And membrane separating method.Cryogenic rectification method is applied to the SF6 gases or mixed gas of processing high concentration, handles low mixing ratio Because the process conditions such as required temperature, pressure are higher during SF6/N2 mixed gas, equipment build is larger, is not suitable for SF6/N2 Gas quick separating recovery process during mix insulation gas site examining and repairing, and the recovery of its mixed gas separates with mixed gas Flow is performs stage by stage, and gas recovery can not be carried out simultaneously with separation phase, and gas on-site treatment effeciency is relatively low, so unsuitable Using;PSA methods have been commercially used for separating oxygen from air, and Technical comparing is ripe, but handle SF6 gas contents and compare During low SF6/N2 mixed gas, when recovery it is resulting SF6 gas concentrations it is not high, storage can not be compressed and liquefied;Second, PSA Need to regenerate after its pressure-swing absorption apparatus saturation during method in-situ processing, so also not recommending onsite application.And utilize membrane technology point From SF6/N2 mixed gas, it can be very good solve the problem.
The content of the invention
For the present invention in order to solve weak point of the prior art, the present invention provides a kind of sulfur hexafluoride and nitrogen mixture Body reclaims separating-purifying device and method, and it can be by the SF after separation6Concentration is improved to 90%(Volume ratio)More than, and separate The N emitted2Middle SF6Content is less than 1000ppm;High concentration SF after separating-purifying6Gas be easy to compress and liquefy storage and For SF6The purification of gas, which recycles, provides facility.
In order to solve the above technical problems, the present invention adopts the following technical scheme that:Sulfur hexafluoride and nitrogen mixed gas recovery Separating-purifying device, including pass sequentially through the mixed gas air inlet, first pressure table, the first valve of gas withdrawal line connection Door, unstrpped gas input power system, the first check valve, gas pretreatment system, the second valve, second pressure gauge, gaseous mixture Body piece-rate system, the 3rd pressure gauge, the 3rd valve, product gas recovery system, the 4th valve, the 4th pressure gauge and sulfur hexafluoride Gas outlet;
The 5th pressure gauge and thermometer are connected with gas pretreatment system;
Mixed gas circulation line, gas separation system connection are also associated between gas separation system and gas pretreatment system There is exhaust emission tube road.
On mixed gas circulation line the 5th is disposed with by the direction of gas separation system to gas pretreatment system Valve, recyclegas dynamical system and the second check valve.
Also including pumped vacuum systems, pumped vacuum systems includes vavuum pump, the first vacuum-pumping pipeline and the second vacuum-pumping pipeline, The bleeding point of first vacuum-pumping pipeline is connected with product gas recovery system, and the bleeding point of the second vacuum-pumping pipeline is connected to the 4th On gas withdrawal line between valve and the 4th pressure gauge, the 6th valve is provided with the first vacuum-pumping pipeline, second takes out very The 7th valve is provided with blank pipe road, the bleeding point of the gas outlet and vacuum of the first vacuum-pumping pipeline and the second vacuum-pumping pipeline connects Connect, the bleeding point of vavuum pump is provided with the 6th pressure gauge.
Exhaust emission tube curb airflow direction is disposed with the 8th valve, exhaust treatment system and exhaust port.
The recovery process for separation and purification of sulfur hexafluoride and nitrogen mixed gas recovery separating-purifying device, including following step Suddenly,
(1), mixed gas air inlet is connected with the exhaust outlet of sulfur hexafluoride and nitrogen mix insulation outlet openings equipment, by six Sulfur fluoride gas outlet is connected with the air inlet of sulfur hexafluoride external container or sulfur hexafluoride external pipeline;
(2), open the 6th valve and the 7th valve, start vavuum pump at least 30 minutes, by the first vacuum-pumping pipeline to product Vacuumized inside gas recovery system, by the second vacuum-pumping pipeline to sulfur hexafluoride external container or sulfur hexafluoride extension tube attached Road vacuumizes;
(3), close vavuum pump, the 6th valve and the 7th valve, open the first valve, the second valve, the 3rd valve, the 4th valve Door, the 5th valve and the 8th valve, start unstrpped gas input power system, gas pretreatment system, mixed gas segregative line System and recyclegas dynamical system, sulfur hexafluoride and nitrogen mixed gas enter gas recovery pipe by mixed gas air inlet Road, first by the first valve regulated charge flow rate, then by unstrpped gas input power system, through check valve, to determine Pressure enter gas pretreatment system, dust floccule, SF6 catabolites in gas pretreatment system processing mixed gas And moisture, dust processing accuracy can reach 0.01 μm, and unstrpped gas is heated up to specified temperature 45 C, then adjust again Two valves, gas separation system is entered with stable pressure, flow;
Gas separation system uses gaseous jet simulation principle, passes through unstrpped gas input power system, gas pretreatment system, One valve and the second valve cause feedstock gas pressures, temperature, flow to reach the requirement of gas separation system process conditions;
Sulfur hexafluoride and nitrogen mixed gas are entered with specified pressure, temperature, flow by gas separation system raw material gas inlet, After gas separation system separates, mixed gas is divided into three road gases:Tail gas, product gas and recyclegas, tail gas it is main into It is divided into nitrogen, contains micro sulfur hexafluoride gas;The principal component of recyclegas is nitrogen and sulfur hexafluoride gas, sulfur hexafluoride Gas accounting is more than 50%;The principal component of product gas is sulfur hexafluoride gas, concentration >=90% of sulfur hexafluoride gas;
Recyclegas is exported by the circulating air of gas separation system, through the 5th valve, recyclegas dynamical system, second unidirectional Valve enters gas pretreatment system, rejoins mixed gas separation process;
Tail gas is entered in exhaust treatment system, through exhaust treatment system by gas separation system offgas outlet through the 8th valve Processing it is up to standard after discharged by exhaust port, its discharge gas in sulfur hexafluoride content be less than 1000ppm;
Product gas is by the product gas outlet of gas separation system, through the 3rd valve, product gas recovery system, the 4th valve Afterwards, the high concentration sulfur hexafluoride product gas after mixed gas is separated is reclaimed and stored into external hexafluorated sulphur vessel;
(4), after the registration of first pressure table is less than 5000Pa, represent sulfur hexafluoride and nitrogen mix insulation outlet openings equipment Middle mixed gas is pumped, and is closed and is opened the first valve, the second valve, the 3rd valve, the 4th valve, the 5th valve and the 8th valve Door, close unstrpped gas input power system, gas pretreatment system, separation system of mixed gas and recyclegas dynamical system System, reclaim the separating-purifying end of job.
Using above-mentioned technical proposal, the present invention can handle SF6Volume ratio is 0-60% SF6/N2Mixed gas, To cause SF6Product gas concentration reaches 90%(Volume ratio)More than, and N2 floss holes SF6Content is less than 1000ppm.The present invention realizes SF6/N2The separating-purifying of mixed gas, working condition requirement is high when overcoming cryogenic rectification method separation, SF when PSA methods separate6Purity The problems such as not high enough.So that SF6/N2Mixed gas solves the problem of live quick recovery separation and recovery in application process. Contribute to SF6/N2Mix insulation gas replaces pure SF6The popularization of gas, reduce SF6Gas usage amount, there are great economy and ring Border benefit, the construction of national green power network is also energetically promoted.
Brief description of the drawings
Fig. 1 is the structural representation of the present invention.
Embodiment
As shown in figure 1, sulfur hexafluoride and nitrogen mixed gas the recovery separating-purifying device of the present invention, including pass sequentially through The mixed gas air inlet 1 of gas withdrawal line connection, first pressure table 2, the first valve 3, unstrpped gas input power system 4th, the first check valve 5, gas pretreatment system 6, the second valve 7, second pressure gauge 8, separation system of mixed gas the 9, the 3rd are pressed Power table 27, the 3rd valve 10, product gas recovery system 11, the 4th valve 12, the 4th pressure gauge 13 and sulfur hexafluoride gas go out Gas port 14;
The 5th pressure gauge 15 and thermometer 16 are connected with gas pretreatment system 6;
Mixed gas circulation line is also associated between gas separation system and gas pretreatment system 6, gas separation system connects It is connected to exhaust emission tube road.
On mixed gas circulation line the 5th is disposed with by the direction of gas separation system to gas pretreatment system 6 Valve 17, the check valve 19 of recyclegas dynamical system 18 and second.
Present invention additionally comprises pumped vacuum systems, pumped vacuum systems includes vavuum pump 20, the first vacuum-pumping pipeline and second is taken out Vacuum line, the bleeding point of the first vacuum-pumping pipeline are connected with product gas recovery system 11, the pumping of the second vacuum-pumping pipeline Mouthful it is connected on the gas withdrawal line between the 4th valve 12 and the 4th pressure gauge 13, the is provided with the first vacuum-pumping pipeline Six valves 21, are provided with the 7th valve 22 in the second vacuum-pumping pipeline, and the first vacuum-pumping pipeline and the second vacuum-pumping pipeline go out Gas port and the bleeding point of vacuum connect, and the bleeding point of vavuum pump 20 is provided with the 6th pressure gauge 23.
Exhaust emission tube curb airflow direction is disposed with the 8th valve 24, exhaust treatment system 25 and exhaust port 26;
The recovery process for separation and purification of sulfur hexafluoride and nitrogen mixed gas recovery separating-purifying device, comprises the following steps,
(1), mixed gas air inlet 1 is connected with the exhaust outlet of sulfur hexafluoride and nitrogen mix insulation outlet openings equipment, will Sulfur hexafluoride gas gas outlet 14 is connected with the air inlet of sulfur hexafluoride external container or sulfur hexafluoride external pipeline;
(2), open the 6th valve 21 and the 7th valve 22, start vavuum pump 20 at least 30 minutes, pass through the first vacuum-pumping pipeline To being vacuumized inside product gas recovery system, by the second vacuum-pumping pipeline to sulfur hexafluoride external container or sulfur hexafluoride External pipeline vacuumizes;
(3), close vavuum pump 20, the 6th valve 21 and the 7th valve 22, open the first valve 3, the second valve 7, the 3rd valve 10th, the 4th valve 12, the 5th valve 17 and the 8th valve 24, unstrpped gas input power system 4, gas pretreatment system are started 6th, separation system of mixed gas 9 and recyclegas dynamical system 18, sulfur hexafluoride and nitrogen mixed gas are by mixed gas air inlet Mouth 1 enters gas withdrawal line, adjusts charge flow rate by the first valve 3 first, then passes through unstrpped gas input power System 4, through check valve, gas pretreatment system 6 is entered with the pressure of determination, gas pretreatment system 6 is handled in mixed gas Dust floccule, SF6 catabolites and moisture, dust processing accuracy can reach 0.01 μm, and unstrpped gas is heated up into volume Fixed temperature 45 C, the second valve 7 is then adjusted again, gas separation system is entered with stable pressure, flow;
Gas separation system uses gaseous jet simulation principle, by unstrpped gas input power system 4, gas pretreatment system 6, First valve 3 and the second valve 7 cause feedstock gas pressures, temperature, flow to reach the requirement of gas separation system process conditions;
Sulfur hexafluoride and nitrogen mixed gas are entered with specified pressure, temperature, flow by gas separation system raw material gas inlet, After gas separation system separates, mixed gas is divided into three road gases:Tail gas, product gas and recyclegas, tail gas it is main into It is divided into nitrogen, contains micro sulfur hexafluoride gas;The principal component of recyclegas is nitrogen and sulfur hexafluoride gas, sulfur hexafluoride Gas accounting is more than 50%;The principal component of product gas is sulfur hexafluoride gas, concentration >=90% of sulfur hexafluoride gas;
Recyclegas is exported by the circulating air of gas separation system, through the 5th valve 17, recyclegas dynamical system 18, second Check valve 19 enters gas pretreatment system 6, rejoins mixed gas separation process;
Tail gas is entered in exhaust treatment system 25, through vent gas treatment by gas separation system offgas outlet through the 8th valve 24 Discharged after the processing of system 25 is up to standard by exhaust port 26, it discharges sulfur hexafluoride content in gas and is less than 1000ppm;
Product gas is by the product gas outlet of gas separation system, through the 3rd valve 10, product gas recovery system the 11, the 4th After valve 12, the high concentration sulfur hexafluoride product gas after mixed gas is separated is reclaimed and stored to external hexafluorated sulphur vessel In;
(4), after the registration of first pressure table 2 is less than 5000Pa, represent that sulfur hexafluoride and nitrogen mix insulation outlet openings are set Standby middle mixed gas is pumped, and is closed and is opened the first valve 3, the second valve 7, the 3rd valve 10, the 4th valve 12, the 5th valve 17 and the 8th valve 24, close unstrpped gas input power system 4, gas pretreatment system 6, the and of separation system of mixed gas 9 Recyclegas dynamical system 18, reclaim the separating-purifying end of job.

Claims (5)

1. sulfur hexafluoride and nitrogen mixed gas recovery separating-purifying device, it is characterised in that:Including passing sequentially through gas recovery Pipeline connection mixed gas air inlet, first pressure table, the first valve, unstrpped gas input power system, the first check valve, Gas pretreatment system, the second valve, second pressure gauge, separation system of mixed gas, the 3rd pressure gauge, the 3rd valve, product Gas recovery system, the 4th valve, the 4th pressure gauge and sulfur hexafluoride gas gas outlet;
The 5th pressure gauge and thermometer are connected with gas pretreatment system;
Mixed gas circulation line, gas separation system connection are also associated between gas separation system and gas pretreatment system There is exhaust emission tube road.
2. sulfur hexafluoride according to claim 1 and nitrogen mixed gas recovery separating-purifying device, it is characterised in that:It is mixed Close and the 5th valve, circulating air are disposed with by the direction of gas separation system to gas pretreatment system on gas circulation line Body dynamical system and the second check valve.
3. sulfur hexafluoride according to claim 2 and nitrogen mixed gas recovery separating-purifying device, it is characterised in that:Also Including pumped vacuum systems, pumped vacuum systems includes vavuum pump, the first vacuum-pumping pipeline and the second vacuum-pumping pipeline, and first vacuumizes The bleeding point of pipeline is connected with product gas recovery system, and the bleeding point of the second vacuum-pumping pipeline is connected to the 4th valve and the 4th On gas withdrawal line between pressure gauge, the 6th valve is provided with the first vacuum-pumping pipeline, is set in the second vacuum-pumping pipeline It is equipped with the 7th valve, the bleeding point connection of the gas outlet and vacuum of the first vacuum-pumping pipeline and the second vacuum-pumping pipeline, vavuum pump Bleeding point be provided with the 6th pressure gauge.
4. sulfur hexafluoride and nitrogen mixed gas recovery separating-purifying device according to right wants 3, it is characterised in that:Tail gas Discharge line is disposed with the 8th valve, exhaust treatment system and exhaust port along airflow direction.
5. the recovery separation using sulfur hexafluoride as claimed in claim 4 and nitrogen mixed gas recovery separating-purifying device carries Pure method, it is characterised in that:Comprise the following steps,
(1), mixed gas air inlet is connected with the exhaust outlet of sulfur hexafluoride and nitrogen mix insulation outlet openings equipment, by six Sulfur fluoride gas outlet is connected with the air inlet of sulfur hexafluoride external container or sulfur hexafluoride external pipeline;
(2), open the 6th valve and the 7th valve, start vavuum pump at least 30 minutes, by the first vacuum-pumping pipeline to product Vacuumized inside gas recovery system, by the second vacuum-pumping pipeline to sulfur hexafluoride external container or sulfur hexafluoride extension tube attached Road vacuumizes;
(3), close vavuum pump, the 6th valve and the 7th valve, open the first valve, the second valve, the 3rd valve, the 4th valve Door, the 5th valve and the 8th valve, start unstrpped gas input power system, gas pretreatment system, mixed gas segregative line System and recyclegas dynamical system, sulfur hexafluoride and nitrogen mixed gas enter gas recovery pipe by mixed gas air inlet Road, first by the first valve regulated charge flow rate, then by unstrpped gas input power system, through check valve, to determine Pressure enter gas pretreatment system, dust floccule, SF6 catabolites in gas pretreatment system processing mixed gas And moisture, dust processing accuracy can reach 0.01 μm, and unstrpped gas is heated up to specified temperature 45 C, then adjust again Two valves, gas separation system is entered with stable pressure, flow;
Gas separation system uses gaseous jet simulation principle, passes through unstrpped gas input power system, gas pretreatment system, One valve and the second valve cause feedstock gas pressures, temperature, flow to reach the requirement of gas separation system process conditions;
Sulfur hexafluoride and nitrogen mixed gas are entered with specified pressure, temperature, flow by gas separation system raw material gas inlet, After gas separation system separates, mixed gas is divided into three road gases:Tail gas, product gas and recyclegas, tail gas it is main into It is divided into nitrogen, contains micro sulfur hexafluoride gas;The principal component of recyclegas is nitrogen and sulfur hexafluoride gas, sulfur hexafluoride Gas accounting is more than 50%;The principal component of product gas is sulfur hexafluoride gas, concentration >=90% of sulfur hexafluoride gas;
Recyclegas is exported by the circulating air of gas separation system, through the 5th valve, recyclegas dynamical system, second unidirectional Valve enters gas pretreatment system, rejoins mixed gas separation process;
Tail gas is entered in exhaust treatment system, through exhaust treatment system by gas separation system offgas outlet through the 8th valve Processing it is up to standard after discharged by exhaust port, its discharge gas in sulfur hexafluoride content be less than 1000ppm;
Product gas is by the product gas outlet of gas separation system, through the 3rd valve, product gas recovery system, the 4th valve Afterwards, the high concentration sulfur hexafluoride product gas after mixed gas is separated is reclaimed and stored into external hexafluorated sulphur vessel;
(4), after the registration of first pressure table is less than 5000Pa, represent sulfur hexafluoride and nitrogen mix insulation outlet openings equipment Middle mixed gas is pumped, and is closed and is opened the first valve, the second valve, the 3rd valve, the 4th valve, the 5th valve and the 8th valve Door, close unstrpped gas input power system, gas pretreatment system, separation system of mixed gas and recyclegas dynamical system System, reclaim the separating-purifying end of job.
CN201710561349.6A 2017-07-11 2017-07-11 Sulfur hexafluoride and nitrogen mixed gas recovery separating-purifying device and method Pending CN107485978A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710561349.6A CN107485978A (en) 2017-07-11 2017-07-11 Sulfur hexafluoride and nitrogen mixed gas recovery separating-purifying device and method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710561349.6A CN107485978A (en) 2017-07-11 2017-07-11 Sulfur hexafluoride and nitrogen mixed gas recovery separating-purifying device and method

Publications (1)

Publication Number Publication Date
CN107485978A true CN107485978A (en) 2017-12-19

Family

ID=60644437

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710561349.6A Pending CN107485978A (en) 2017-07-11 2017-07-11 Sulfur hexafluoride and nitrogen mixed gas recovery separating-purifying device and method

Country Status (1)

Country Link
CN (1) CN107485978A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108101006A (en) * 2017-12-20 2018-06-01 国网河北省电力有限公司电力科学研究院 A kind of SF6And N2The quick recycling and processing device of mixed gas and method
CN108355461A (en) * 2018-04-16 2018-08-03 西安交通大学 Sulfur hexafluoride and nitrogen mixed gas purification separation purifying plant and its reclaiming clean purify sulfur hexafluoride method
CN109516441A (en) * 2018-11-06 2019-03-26 国网浙江省电力有限公司检修分公司 A kind of recycling of sulfur hexafluoride, low temperature fluid injection bulking system and its working method
CN111547685A (en) * 2020-04-10 2020-08-18 国网河北省电力有限公司电力科学研究院 Low concentration SF in enclosed space6Gas recovery processing device and method
CN113499662A (en) * 2021-07-27 2021-10-15 中国南方电网有限责任公司超高压输电公司昆明局 Sulfur hexafluoride gas recovery processing device and gas recovery system under full positive pressure condition

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108101006A (en) * 2017-12-20 2018-06-01 国网河北省电力有限公司电力科学研究院 A kind of SF6And N2The quick recycling and processing device of mixed gas and method
CN108101006B (en) * 2017-12-20 2020-01-24 国网河北省电力有限公司电力科学研究院 SF (sulfur hexafluoride)6And N2Device and method for rapidly recovering and treating mixed gas
CN108355461A (en) * 2018-04-16 2018-08-03 西安交通大学 Sulfur hexafluoride and nitrogen mixed gas purification separation purifying plant and its reclaiming clean purify sulfur hexafluoride method
CN108355461B (en) * 2018-04-16 2024-05-24 西安交通大学 Sulfur hexafluoride and nitrogen mixed gas purifying and separating device and sulfur hexafluoride recovering and purifying method
CN109516441A (en) * 2018-11-06 2019-03-26 国网浙江省电力有限公司检修分公司 A kind of recycling of sulfur hexafluoride, low temperature fluid injection bulking system and its working method
CN109516441B (en) * 2018-11-06 2024-05-10 国网浙江省电力有限公司检修分公司 Sulfur hexafluoride recovery and low-temperature liquid injection filling system and working method thereof
CN111547685A (en) * 2020-04-10 2020-08-18 国网河北省电力有限公司电力科学研究院 Low concentration SF in enclosed space6Gas recovery processing device and method
CN111547685B (en) * 2020-04-10 2022-01-25 国网河北省电力有限公司电力科学研究院 Low-concentration SF6 gas recovery processing device and method in closed space
CN113499662A (en) * 2021-07-27 2021-10-15 中国南方电网有限责任公司超高压输电公司昆明局 Sulfur hexafluoride gas recovery processing device and gas recovery system under full positive pressure condition
CN113499662B (en) * 2021-07-27 2022-08-30 中国南方电网有限责任公司超高压输电公司昆明局 Sulfur hexafluoride gas recovery processing device and gas recovery system under full positive pressure condition

Similar Documents

Publication Publication Date Title
CN107485978A (en) Sulfur hexafluoride and nitrogen mixed gas recovery separating-purifying device and method
CN105864632B (en) Mobile sulfur hexafluoride and carbon tetrafluoride mixed gas quickly recycle making-up air device
CN102921266B (en) Tail gas recovery device of sulfur hexafluoride gas test instrument
CN108355461B (en) Sulfur hexafluoride and nitrogen mixed gas purifying and separating device and sulfur hexafluoride recovering and purifying method
CN208406522U (en) Sulfur hexafluoride and nitrogen mixed gas purification separation purifying plant
CN107433111A (en) A kind of quick recovery system of mix insulation gas and method
CN207012771U (en) Sulfur hexafluoride and nitrogen mixed gas recovery separating-purifying device
CN112516746A (en) C4F7N/CO2Mixed gas recovery and purification device
CN205773343U (en) Portable sulfur hexafluoride and carbon tetrafluoride mixed gas Rapid recovery device
CN106040527A (en) Nitrogen filling vacuum pressure impregnation equipment and method
CN207153420U (en) A kind of quick recovery system of mix insulation gas
CN101732947A (en) Method for safe adsorption and enrichment of gas with low concentration
CN202823087U (en) Tail gas recovery device of sulfur hexafluoride gas test instrument
CN102976291A (en) Variable pressure adsorption nitrogen production equipment and method thereof
CN102495175A (en) Zero discharge device and working method for detecting sulfur hexafluoride gas
SA00210147B1 (en) Separation of sulfur hexafluoride SF6 from gases isolated from gas-insulated lines
CN218774566U (en) C4F7N/CO2 mixed gas purification treatment system for on-site recovery
CN105084325A (en) Sulfur hexafluoride recovery device and sulfur hexafluoride recovery vehicle
CN203703604U (en) SF6 gas recovery device with gas component analysis function
CN102921301B (en) Method for preparing medical oxygen from mixed gases containing oxygen air components through multi-cycle membrane separation
CN205709851U (en) efficient molecular sieve oxygenerator
CN113893642B (en) Ring main unit C 4 F 7 N/CO 2 Mixed gas on-site recovery device and method
JP3385053B2 (en) Rare gas high yield recovery and purification method and rare gas high yield recovery and purification device
CN214051036U (en) Emergent recovery unit of electrical equipment leakage gas
CN214051037U (en) Emergent recovery unit of electrical equipment leakage gas

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination