CN107467296A - A kind of spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking and preparation method thereof - Google Patents
A kind of spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking, its every 1000 parts by weight beverage is made up of the raw material of following parts by weight:10~15 parts of cassia seeds, 5~10 parts of semen astragali complanatis, 5~10 portions of raspberries, 5~10 portions of fruit of glossy privets, 10~15 portions of fruits of Chinese wolfberry, 15~20 portions of selfheals, 10~15 portions of dandelions, 4~8 parts of chrysanthemums, 4~6 parts of sophoras flower, 3~5 parts of spices, surplus is water.It is main to use raw material crushing enzymolysis, the extraction of ultrasound adverse current, allotment, homogeneous, filtering, micro-pore-film filtration to be made up of key step the invention also discloses the preparation method of spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking.Herbal raw material source of the present invention is wide, and cheap, scientific formulation is reasonable, and preparation technology is simple, and extraction Chinese herbal medicine functional components are high, product safety environmental protection, spirit refreshing and eye-brightening significant effect without any side effects to human body.
Description
Technical field
The invention discloses a kind of health drink, more particularly to a kind of spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking and its
Preparation method, belong to technical field of beverage processing.
Background technology
Beverage is the important composition of modern people's personal consumption.China's beverage market is with soda, fruit drink at present
And based on functional beverage, consumer demand is met to a certain extent, but with expanding economy and people's lives water
Flat raising, the increase of quickening and life stress in particular with rhythm of life, beverage market structure become there occurs obvious
Change, enjoyed the soda of high praise gradually to bring down a fever originally, selection of the people to beverage starts to be particular about from nutrition and taste to it
Healthcare function and auxiliary therapeutic action propose higher requirement.Therefore, health drink emerges rapidly, turns into the new main force in market
Army.But current health drink has that product category is single, and function active ingredient is low, and health-care effect is not notable, product can not meet
The problems such as demand of different Consumer groups.Therefore, pure natural health-care beverage of the exploitation with healthcare function good mouthfeel is one
Item significantly works.
Chinese herbal medicine is the rarity of Chinese traditional culture, proves that a variety of Chinese herbal medicines have in practice and enhances metabolism, changes
Kind blood circulation, spirit refreshing and eye-brightening, tonifies the liver and kidney, nourishing heart arrest sweating, promotes the production of body fluid to quench thirst, strong liver of reinforcing the kidney, strengthening the spleen and stomach, and the work(such as relax bowel
Effect.Therefore, Chinese herbal medicine is applied to health drink for improving national life quality, it is highly important ensures that living safety has
Meaning, but at present there is spirit refreshing and eye-brightening Chinese herbal medicine beverage not yet to realize scale and industrialization, subject matter is Chinese herbal medicine compatibility
It is unreasonable, the drawback such as functional component recovery rate is low, be difficult to industrialized production, effect is poor, taste bad, therefore develop and new refresh oneself
Eyesight-improving health drink has important practical significance.
The content of the invention
It is an object of the invention to the above mentioned problem according to existing for existing spirit refreshing and eye-brightening health-care beverage product and technology of preparing,
Prepared using nontoxic pure ecological medicinal material and raw-food material, develop a kind of spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking, the guarantor
Strong beverage is nutritious, and health value is high, without any side effects, contains a large amount of flavones, polysaccharide, alkaloid, glucoside, volatilization
The function factors such as oil, vitamin, organic acid, trace element, amino acid, there is spirit refreshing and eye-brightening, tonify the liver and kidney, nourishing heart arrest sweating is raw
Tianjin is quenched the thirst, strong liver of reinforcing the kidney, strengthening the spleen and stomach, relax bowel and other effects, dizzy suitable for the blurring of image, yctalopia etc..Chinese holly in formula
Matrimony vine contains abundant carrotene, vitamin, the nutriment such as calcium and iron, has tonifying kidneys and nourishing brain improving eyesight;Cassia seed has heat-clearing,
Improving eyesight, cerebrum tonifying marrow, town irritability, the effect of beneficial muscles and bones, mulberry leaf, the refrigerant improving eyesight of chrysanthemum.
To achieve these goals, the present invention uses following technical scheme:
A kind of spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking, its every 1000 parts by weight beverage by following parts by weight raw material system
Into:10~15 parts of cassia seeds, 5~10 parts of semen astragali complanatis, 5~10 portions of raspberries, 5~10 portions of fruit of glossy privets, 10~15 portions of fruits of Chinese wolfberry, 15
~20 portions of selfheals, 10~15 portions of dandelions, 4~8 parts of chrysanthemums, 4~6 parts of sophoras flower, 3~5 parts of spices, surplus is water.
Preferably, the weight/mass percentage composition of described spice each component is:10~15% stevias, 10~15% is low
Fructooligosaccharides, 5~10% sorbierites, 5~10% Sucraloses, 5~10% citric acids, 10~15% calcium lactates, 4~8% taurines are remaining
Measure as honey.Spice can improve the mouthfeel of Chinese herbal health-caring beverage, and a variety of spices are complementary, can meet different crowd
Demand.
A kind of preparation method of spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking of the present invention, comprises the following steps:
(1)Stock:The impurity in herbal raw material is rejected, goes mouldy with after infested raw material, is stocked up according to aforementioned proportion;
(2)Feedstock treating:Herbal raw material is cleaned up, at 60~80 DEG C, after air blast drying, pulverizer crushes, and crosses 40
~60 mesh sieves, mix, obtain composite Chinese herbal raw material;
(3)Enzymolysis:By step(2)Gained composite Chinese herbal raw material adds water to solid-to-liquid ratio 1:4~6, by 3.0~4.0 g/L, 2.0
~3.0 g/L, 1.5~2.5 g/L ratios add cellulase, α~amylase, zytase in 300 ~ 500 W ultrasounds respectively
Under ripple booster action, the min of coordinated enzymatic hydrolysis 90~120 under the conditions of 40~50 DEG C;
(4)Separation of solid and liquid:After enzymolysis terminates, enzymolysis liquid is heated to 85~95 DEG C, the min of enzyme deactivation 5~10, is cooled to 50~60
DEG C, cross 100 ~ 150 mesh filter clothes and obtain filter residue and Enzymolysis liquid;
(5)Ultrasonic adverse current is extracted:By step(4)The filter residue being filtrated to get after enzymolysis, 4~6 times of 50~60% ethanol are added, are put
Enter in ultrasonic Continuous Countercurrent Extraction machine, under the effect of 400 ~ 600 W ultrasonic assistants, after adverse current extracts 60 ~ 90 min, excessively 100 ~
150 mesh filter clothes obtain alcohol extract.Filter residue adds 2 ~ 4 times of 50~60% ethanol, carries out ultrasonic continuous countercurrent in the same way and carries
Take, it is ethanol extract to merge extract solution twice;
(6)It is concentrated under reduced pressure:By step(5)The ethanol extract of gained is at 50~65 DEG C of temperature, vacuum -0.06~-0.08
It is evaporated under reduced pressure under MPa, reclaims the ethanol in extracts of Chinese herbal medicine to without alcohol taste, obtain removing ethanol extracts of Chinese herbal medicine;
(7)Allotment:By the spice described in formula with after 50 DEG C of hot water dissolvings, with step(4)Gained Enzymolysis liquid and step
Suddenly(6)Gained, which removes ethanol extracts of Chinese herbal medicine and merged, to be stirred and evenly mixed, then with 50 ~ 60 DEG C of pure water constant volumes, through 200 ~ 250
Mesh filter-cloth filtering removes impurity and insoluble matter therein;
(8)Homogeneous:Deployed beverage is placed in homogenizer, at the MPa of homogenization pressure 20 ~ 30,50~60 DEG C of temperature
Homogeneous, various nutritional ingredients are homogenized, prevents product from layering and precipitating occur, product stability is further ensured;
(9)Refined filtration:By step(8)Beverage after homogeneous first filters through 250 ~ 300 mesh duplex strainers, then through diatom filter essence
Filter to remove impurity and insoluble matter therein;
(10)Micro-pore-film filtration:Spirit refreshing and eye-brightening compound Cassia is produced with the leaching liquor for the micro-pore-film filtration refined filtration that aperture is 1.5 μm
Sub- Chinese herbal medicine tea-drinking;
(11)Sterile filling seals:The filling and sealing in sterile filling production line.
The present invention provides a kind of spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking, and the characteristic of each Chinese herbal medicine, is used in combined formulation
Chinese medical discrimination theory is developed, and scientific formulation is reasonable, is acted synergistically between each component, and product has the distinctive delicate fragrance of Chinese herbal medicine
Taste, mellow in taste, sense of taste is soft, and juice is limpid bright, free from admixture free from extraneous odour.The g/L of soluble solid in product >=60, always
Arsenic (in terms of As)≤0.3 mg/L, lead (in terms of Pb)≤0.3 mg/L, the cfu/mL of total plate count≤80, coliform≤35
MPN/L, the cfu/mL of mould≤10, the cfu/mL of yeast≤10, no pathogenic bacteria detection, other indices meet national related rule
Provisioning request.Make acute oral toxicity test, genetoxic examination to product of the present invention according to national food safety standard pertinent regulations
Test, chronic toxicity test, toxicology test and the safety evaluatio such as Reproductive and developmental toxicity experiment and tertogenicity test, result of the test table
Bright product of the present invention meets national food safety standard, it is thus determined that product of the present invention belongs to nontoxic based food, can be with safe and secure
It is edible.This product contains a large amount of flavones, polysaccharide, alkaloid, glucoside, volatile oil, vitamin, organic acid, trace element, amino acid
Deng function factor, prove that the present invention has spirit refreshing and eye-brightening, tonifies the liver and kidney by long-term use, nourishing heart arrest sweating promotes the production of body fluid to quench thirst, and reinforces the kidney strong
Liver, strengthening the spleen and stomach, relax bowel and other effects, it is the healthy beverage that a kind of health-care effect is notable, green.
Advantage of the invention is that:(1)The nontoxic pure ecological medicinal material and food using Chinese medical discrimination theory compatible use
Raw material is prepared, product safety environmental protection, without any side effects to human body;(2)Compared with Chinese herbal medicine simply immersing extracts, the present invention adopts
Countercurrently extracted with enzymolysis and ultrasound is crushed by raw material, improve Chinese herbal medicine functional components, spirit refreshing and eye-brightening effect is notable;(3)Production
Product with the addition of a variety of spices, and improvement product palatability is good, be substituted from stevia, FOS, sorbierite, Sucralose
Traditional sweetener, more conducively health;(4)Raw material sources are wide in the present invention, cheap, and production and processing technology is simple,
It is adapted to large-scale production.
Embodiment
Below by embodiment, the present invention will be further described.In the present invention, if not refering in particular to, Suo Youbai
Point ratio is unit of weight, and all devices and raw material are commercially available or the industry is commonly used, in following embodiments
Method, it is this area conventional method unless otherwise instructed.
Embodiment 1
A kind of spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking, by cassia seed, semen astragali complanati, raspberry, the fruit of glossy privet, the fruit of Chinese wolfberry, summer
Withered grass, dandelion, chrysanthemum, sophora flower and spice are made.The specific proportioning of each component is as shown in table 1 in Chinese herbal medicine tea-drinking, medium-height grass
The specific formula of spice is as shown in table 2 in medicinal herb tea drink.
A kind of preparation method of spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking of the present invention, comprises the following steps:
(1)Stock:The impurity in herbal raw material is rejected, goes mouldy with after infested raw material, is stocked up according to aforementioned proportion;
(2)Feedstock treating:Herbal raw material is cleaned up, at 75 DEG C, after air blast drying, pulverizer crushes, and crosses 50 mesh
Sieve, mix, obtain composite Chinese herbal raw material;
(3)Enzymolysis:By step(2)Gained composite Chinese herbal raw material adds water to solid-to-liquid ratio 1:4, by 3.0 g/L, 3.0 g/L, 2.0
G/L ratios add cellulase, α~amylase, zytase under the effect of 350 W ultrasonic assistants respectively, in 42 DEG C of conditions
The lower min of coordinated enzymatic hydrolysis 115;
(4)Separation of solid and liquid:After enzymolysis terminates, enzymolysis liquid is heated to 85 DEG C, the min of enzyme deactivation 8, is cooled to 55 DEG C, crosses the filter of 100 mesh
Cloth obtains filter residue and Enzymolysis liquid;
(5)Ultrasonic adverse current is extracted:By step(4)The filter residue being filtrated to get after enzymolysis, 5 times of 55% ethanol is added, be put into ultrasound even
In continuous countercurrent extraction machine, under the effect of 450 W ultrasonic assistants, after adverse current extracts 80 min, cross 100 mesh filter clothes and obtain alcohol steep
Liquid.Filter residue adds 3 times of 50% ethanol, carries out ultrasonic continuous countercurrent extraction in the same way, and it is that ethanol carries to merge extract solution twice
Take liquid;
(6)It is concentrated under reduced pressure:By step(5)The ethanol extract of gained is carried out at 62 DEG C of temperature under the MPa of vacuum -0.08
It is evaporated under reduced pressure, reclaims the ethanol in extracts of Chinese herbal medicine to without alcohol taste, obtain removing ethanol extracts of Chinese herbal medicine;
(7)Allotment:By the spice described in formula with after 50 DEG C of hot water dissolvings, with step(4)Gained Enzymolysis liquid and step
Suddenly(6)Gained, which removes ethanol extracts of Chinese herbal medicine and merged, to be stirred and evenly mixed, then with 52 DEG C of pure water constant volumes, through 200 mesh filter cloth mistakes
Filter out impurity and insoluble matter therein;
(8)Homogeneous:Deployed beverage is placed in homogenizer, the homogeneous at the MPa of homogenization pressure 30,50 DEG C of temperature, made
Various nutritional ingredient homogenization, prevent product from layering and precipitating occur, product stability is further ensured;
(9)Refined filtration:By step(8)Beverage after homogeneous first filters through 250 mesh duplex strainers, then through diatom filter refined filtration with
Remove impurity and insoluble matter therein;
(10)Micro-pore-film filtration:Spirit refreshing and eye-brightening compound Cassia is produced with the leaching liquor for the micro-pore-film filtration refined filtration that aperture is 1.5 μm
Sub- Chinese herbal medicine tea-drinking;
(11)Sterile filling seals:The filling and sealing in sterile filling production line.
Embodiment 2
A kind of spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking, by cassia seed, semen astragali complanati, raspberry, the fruit of glossy privet, the fruit of Chinese wolfberry, summer
Withered grass, dandelion, chrysanthemum, sophora flower and spice are made.The specific proportioning of each component is as shown in table 1 in Chinese herbal medicine tea-drinking, medium-height grass
The specific formula of spice is as shown in table 2 in medicinal herb tea drink.
A kind of preparation method of spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking of the present invention, comprises the following steps:
(1)Stock:The impurity in herbal raw material is rejected, goes mouldy with after infested raw material, is stocked up according to aforementioned proportion;
(2)Feedstock treating:Herbal raw material is cleaned up, at 65 DEG C, after air blast drying, pulverizer crushes, and crosses 40 mesh
Sieve, mix, obtain composite Chinese herbal raw material;
(3)Enzymolysis:By step(2)Gained composite Chinese herbal raw material adds water to solid-to-liquid ratio 1:5, by 3.5 g/L, 2.5 g/L, 1.5
G/L ratios add cellulase, α~amylase, zytase under the effect of 450 W ultrasonic assistants respectively, in 45 DEG C of conditions
The lower min of coordinated enzymatic hydrolysis 95;
(4)Separation of solid and liquid:After enzymolysis terminates, enzymolysis liquid is heated to 95 DEG C, the min of enzyme deactivation 6, is cooled to 52 DEG C, crosses 100 mesh filter clothes
Obtain filter residue and Enzymolysis liquid;
(5)Ultrasonic adverse current is extracted:By step(4)The filter residue being filtrated to get after enzymolysis, 4 times of 60% ethanol is added, be put into ultrasound even
In continuous countercurrent extraction machine, under the effect of 500 W ultrasonic assistants, after adverse current extracts 85 min, cross 150 mesh filter clothes and obtain alcohol steep
Liquid.Filter residue adds 2 times of 55% ethanol, carries out ultrasonic continuous countercurrent extraction in the same way, and it is that ethanol carries to merge extract solution twice
Take liquid;
(6)It is concentrated under reduced pressure:By step(5)The ethanol extract of gained is carried out at 57 DEG C of temperature under the MPa of vacuum -0.07
It is evaporated under reduced pressure, reclaims the ethanol in extracts of Chinese herbal medicine to without alcohol taste, obtain removing ethanol extracts of Chinese herbal medicine;
(7)Allotment:By the spice described in formula with after 50 DEG C of hot water dissolvings, with step(4)Gained Enzymolysis liquid and step
Suddenly(6)Gained, which removes ethanol extracts of Chinese herbal medicine and merged, to be stirred and evenly mixed, then with 55 DEG C of pure water constant volumes, through 250 mesh filter cloth mistakes
Filter out impurity and insoluble matter therein;
(8)Homogeneous:Deployed beverage is placed in homogenizer, the homogeneous at the MPa of homogenization pressure 20,60 DEG C of temperature, made
Various nutritional ingredient homogenization, prevent product from layering and precipitating occur, product stability is further ensured;
(9)Refined filtration:By step(8)Beverage after homogeneous first filters through 300 mesh duplex strainers, then through diatom filter refined filtration with
Remove impurity and insoluble matter therein;
(10)Micro-pore-film filtration:Spirit refreshing and eye-brightening compound Cassia is produced with the leaching liquor for the micro-pore-film filtration refined filtration that aperture is 1.5 μm
Sub- Chinese herbal medicine tea-drinking;
(11)Sterile filling seals:The filling and sealing in sterile filling production line.
Embodiment 3
A kind of spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking, by cassia seed, semen astragali complanati, raspberry, the fruit of glossy privet, the fruit of Chinese wolfberry, summer
Withered grass, dandelion, chrysanthemum, sophora flower and spice are made.The specific proportioning of each component is as shown in table 1 in Chinese herbal medicine tea-drinking, medium-height grass
The specific formula of spice is as shown in table 2 in medicinal herb tea drink.
A kind of preparation method of spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking of the present invention, comprises the following steps:
(1)Stock:The impurity in herbal raw material is rejected, goes mouldy with after infested raw material, is stocked up according to aforementioned proportion;
(2)Feedstock treating:Herbal raw material is cleaned up, at 70 DEG C, after air blast drying, pulverizer crushes, and crosses 60 mesh
Sieve, mix, obtain composite Chinese herbal raw material;
(3)Enzymolysis:By step(2)Gained composite Chinese herbal raw material adds water to solid-to-liquid ratio 1:6, by 4.0 g/L, 2.0 g/L, 2.5
G/L ratios add cellulase, α~amylase, zytase under the effect of 400 W ultrasonic assistants respectively, in 48 DEG C of conditions
The lower min of coordinated enzymatic hydrolysis 105;
(4)Separation of solid and liquid:After enzymolysis terminates, enzymolysis liquid is heated to 90 DEG C, the min of enzyme deactivation 7, is cooled to 58 DEG C, crosses the filter of 100 mesh
Cloth obtains filter residue and Enzymolysis liquid;
(5)Ultrasonic adverse current is extracted:By step(4)The filter residue being filtrated to get after enzymolysis, 6 times of 50% ethanol is added, be put into ultrasound even
In continuous countercurrent extraction machine, under the effect of 550 W ultrasonic assistants, after adverse current extracts 75 min, cross 120 mesh filter clothes and obtain alcohol steep
Liquid.Filter residue adds 4 times of 60% ethanol, carries out ultrasonic continuous countercurrent extraction in the same way, and it is that ethanol carries to merge extract solution twice
Take liquid;
(6)It is concentrated under reduced pressure:By step(5)The ethanol extract of gained is carried out at 52 DEG C of temperature under the MPa of vacuum -0.06
It is evaporated under reduced pressure, reclaims the ethanol in extracts of Chinese herbal medicine to without alcohol taste, obtain removing ethanol extracts of Chinese herbal medicine;
(7)Allotment:By the spice described in formula with after 50 DEG C of hot water dissolvings, with step(4)Gained Enzymolysis liquid and step
Suddenly(6)Gained, which removes ethanol extracts of Chinese herbal medicine and merged, to be stirred and evenly mixed, then with 58 DEG C of pure water constant volumes, through 200 mesh filter cloth mistakes
Filter out impurity and insoluble matter therein;
(8)Homogeneous:Deployed beverage is placed in homogenizer, the homogeneous at the MPa of homogenization pressure 25,55 DEG C of temperature, made
Various nutritional ingredient homogenization, prevent product from layering and precipitating occur, product stability is further ensured;
(9)Refined filtration:By step(8)Beverage after homogeneous first filters through 250 mesh duplex strainers, then through diatom filter refined filtration with
Remove impurity and insoluble matter therein;
(10)Micro-pore-film filtration:Spirit refreshing and eye-brightening compound Cassia is produced with the leaching liquor for the micro-pore-film filtration refined filtration that aperture is 1.5 μm
Sub- Chinese herbal medicine tea-drinking;
(11)Sterile filling seals:The filling and sealing in sterile filling production line.
The specific proportioning of each component in each embodiment Chinese herbal health-caring beverage of table 1
Sequence number | Component | Embodiment 1 | Embodiment 2 | Embodiment 3 |
1 | Cassia seed(Part) | 13 | 11 | 14 |
2 | Semen astragali complanati(Part) | 9 | 8 | 7 |
3 | Raspberry(Part) | 6 | 9 | 7 |
4 | The fruit of glossy privet(Part) | 8 | 7 | 6 |
5 | The fruit of Chinese wolfberry(Part) | 11 | 14 | 13 |
6 | Selfheal(Part) | 17 | 14 | 18 |
7 | Dandelion(Part) | 13 | 12 | 11 |
8 | Chrysanthemum(Part) | 5 | 6 | 7 |
9 | Sophora flower(Part) | 6 | 5 | 4 |
10 | Spice(Part) | 4 | 5 | 3 |
11 | Summation(Part) | 92 | 91 | 90 |
The specific formula of spice in each embodiment Chinese herbal health-caring beverage of table 2
Sequence number | Component | Embodiment 1 | Embodiment 2 | Embodiment 3 |
1 | Stevia (%) | 13 | 14 | 12 |
2 | FOS (%) | 13 | 11 | 14 |
3 | Sorbierite (%) | 7 | 6 | 8 |
4 | Sucralose (%) | 8 | 6 | 7 |
5 | Citric acid (%) | 6 | 7 | 8 |
6 | Calcium lactate (%) | 14 | 13 | 11 |
7 | Taurine (%) | 7 | 5 | 6 |
8 | Honey (%) | 32 | 38 | 34 |
9 | Summation (%) | 100 | 100 | 100 |
Although to reach illustration purpose, described above is the preferred embodiments of the present invention, is not intended to limit the invention, to the greatest extent
The present invention is described in detail with reference to the foregoing embodiments for pipe, and for those skilled in the art, it still can be with
The technical scheme recorded to foregoing embodiments is modified, or carries out equivalent substitution to which part technical characteristic.It is all
Within the spirit and principles in the present invention, any modification, equivalent substitution and improvements made etc., the protection of the present invention should be included in
Within the scope of.
Claims (3)
1. a kind of spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking, it is characterised in that every 1000 parts by weight beverage is by following weight
The raw material of part is made:10~15 parts of cassia seeds, 5~10 parts of semen astragali complanatis, 5~10 portions of raspberries, 5~10 portions of fruit of glossy privets, 10~15
Part fruit of Chinese wolfberry, 15~20 portions of selfheals, 10~15 portions of dandelions, 4~8 parts of chrysanthemums, 4~6 parts of sophoras flower, 3~5 parts of spices are remaining
Measure as water.
A kind of 2. spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking according to claim 1, it is characterised in that described tune
The weight/mass percentage composition of dispensing each component is:10~15% stevias, 10~15% FOSs, 5~10% sorbierites, 5~
10% Sucralose, 5~10% citric acids, 10~15% calcium lactates, 4~8% taurines, surplus are honey.
A kind of 3. preparation method of spirit refreshing and eye-brightening compound cassia seed Chinese herbal medicine tea-drinking as claimed in claim 1, it is characterised in that
Comprise the following steps:
(1)Stock:The impurity in herbal raw material is rejected, goes mouldy with after infested raw material, is stocked up according to aforementioned proportion;
(2)Feedstock treating:Herbal raw material is cleaned up, at 60~80 DEG C, after air blast drying, pulverizer crushes, and crosses 40
~60 mesh sieves, mix, obtain composite Chinese herbal raw material;
(3)Enzymolysis:By step(2)Gained composite Chinese herbal raw material adds water to solid-to-liquid ratio 1:4~6, by 3.0~4.0 g/L, 2.0
~3.0 g/L, 1.5~2.5 g/L ratios add cellulase, α~amylase, zytase in 300 ~ 500 W ultrasounds respectively
Under ripple booster action, the min of coordinated enzymatic hydrolysis 90~120 under the conditions of 40~50 DEG C;
(4)Separation of solid and liquid:After enzymolysis terminates, enzymolysis liquid is heated to 85~95 DEG C, the min of enzyme deactivation 5~10, is cooled to 50~60
DEG C, cross 100 ~ 150 mesh filter clothes and obtain filter residue and Enzymolysis liquid;
(5)Ultrasonic adverse current is extracted:By step(4)The filter residue being filtrated to get after enzymolysis, 4~6 times of 50~60% ethanol are added, are put
Enter in ultrasonic Continuous Countercurrent Extraction machine, under the effect of 400 ~ 600 W ultrasonic assistants, after adverse current extracts 60 ~ 90 min, excessively 100 ~
150 mesh filter clothes obtain alcohol extract, and filter residue adds 2 ~ 4 times of 50~60% ethanol, carry out ultrasonic continuous countercurrent in the same way and carry
Take, it is ethanol extract to merge extract solution twice;
(6)It is concentrated under reduced pressure:By step(5)The ethanol extract of gained is at 50~65 DEG C of temperature, vacuum -0.06~-0.08
It is evaporated under reduced pressure under MPa, reclaims the ethanol in extracts of Chinese herbal medicine to without alcohol taste, obtain removing ethanol extracts of Chinese herbal medicine;
(7)Allotment:By the spice described in formula with after 50 DEG C of hot water dissolvings, with step(4)Gained Enzymolysis liquid and step
Suddenly(6)Gained, which removes ethanol extracts of Chinese herbal medicine and merged, to be stirred and evenly mixed, then with 50 ~ 60 DEG C of pure water constant volumes, through 200 ~ 250
Mesh filter-cloth filtering removes impurity and insoluble matter therein;
(8)Homogeneous:Deployed beverage is placed in homogenizer, at the MPa of homogenization pressure 20 ~ 30,50~60 DEG C of temperature
Homogeneous, various nutritional ingredients are homogenized, prevents product from layering and precipitating occur, product stability is further ensured;
(9)Refined filtration:By step(8)Beverage after homogeneous first filters through 250 ~ 300 mesh duplex strainers, then through diatom filter essence
Filter to remove impurity and insoluble matter therein;
(10)Micro-pore-film filtration:Spirit refreshing and eye-brightening compound Cassia is produced with the leaching liquor for the micro-pore-film filtration refined filtration that aperture is 1.5 μm
Sub- Chinese herbal medicine tea-drinking;
(11)Sterile filling seals:The filling and sealing in sterile filling production line.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN111388645A (en) * | 2020-05-10 | 2020-07-10 | 临清先锋农产品专业合作社 | Phellinus igniarius granule electuary and preparation method thereof |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH04248971A (en) * | 1991-01-31 | 1992-09-04 | Tube Ekisupaatsu:Kk | Fermented drink containing herb ingredient and production thereof |
CN104904965A (en) * | 2015-07-08 | 2015-09-16 | 青岛嘉瑞生物技术有限公司 | Bran health herbal tea with weight losing function |
CN104920736A (en) * | 2015-07-06 | 2015-09-23 | 青岛嘉瑞生物技术有限公司 | Chinese herbal medicine health care cool tea capable of relieving asthenopia |
-
2017
- 2017-08-23 CN CN201710727671.1A patent/CN107467296A/en not_active Withdrawn
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH04248971A (en) * | 1991-01-31 | 1992-09-04 | Tube Ekisupaatsu:Kk | Fermented drink containing herb ingredient and production thereof |
CN104920736A (en) * | 2015-07-06 | 2015-09-23 | 青岛嘉瑞生物技术有限公司 | Chinese herbal medicine health care cool tea capable of relieving asthenopia |
CN104904965A (en) * | 2015-07-08 | 2015-09-16 | 青岛嘉瑞生物技术有限公司 | Bran health herbal tea with weight losing function |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111388645A (en) * | 2020-05-10 | 2020-07-10 | 临清先锋农产品专业合作社 | Phellinus igniarius granule electuary and preparation method thereof |
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Application publication date: 20171215 |