CN107419577A - A kind of preparation method of high intensity paper twine body paper - Google Patents

A kind of preparation method of high intensity paper twine body paper Download PDF

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Publication number
CN107419577A
CN107419577A CN201710894153.9A CN201710894153A CN107419577A CN 107419577 A CN107419577 A CN 107419577A CN 201710894153 A CN201710894153 A CN 201710894153A CN 107419577 A CN107419577 A CN 107419577A
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parts
paper
weight
preparation
body paper
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CN201710894153.9A
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CN107419577B (en
Inventor
江峰
陈君花
严金英
周兆祥
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Shun Pu Paper Co Ltd
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Shun Pu Paper Co Ltd
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    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21B—FIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
    • D21B1/00—Fibrous raw materials or their mechanical treatment
    • D21B1/04—Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
    • D21B1/12—Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres by wet methods, by the use of steam
    • D21B1/30—Defibrating by other means
    • D21B1/34—Kneading or mixing; Pulpers
    • D21B1/345—Pulpers
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H13/00—Pulp or paper, comprising synthetic cellulose or non-cellulose fibres or web-forming material
    • D21H13/10—Organic non-cellulose fibres
    • D21H13/12—Organic non-cellulose fibres from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D21H13/14—Polyalkenes, e.g. polystyrene polyethylene
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
    • D21H21/18—Reinforcing agents
    • D21H21/20—Wet strength agents

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Mechanical Engineering (AREA)
  • Paper (AREA)

Abstract

The invention provides a kind of preparation method of high intensity paper twine body paper, needlebush wood pulp is placed in pulper, adds dyestuff, beating consistency 3 5%, it is beaten 40 45 ° of SR of beating degree, feeding matches somebody with somebody stock tank, adds color fixing agent, wet strength agent, ionic liquid remover, it is sufficiently mixed, slurry is sent into net cage, PVC chemical fibres dispersion liquid is sent into net cage；Turn into page through dehydration forming, PVC chemical fibres are uniformly attached to page surface, then through press dewatering, are heated 5 15 hours at 90 100 DEG C, obtain paper twine body paper.

Description

A kind of preparation method of high intensity paper twine body paper
Technical field
The present invention relates to establishment paper field, especially a kind of preparation method of high intensity paper twine body paper.
Background technology
Weave paper is a kind of emerging technique textile material.It is with easy to process, handsome in appearance, bright in colour, durable Without fading, the main dry various paper strings of braiding, various sudd caps, paper cloth is made, summer sleeping mat, folds pillow mat, wall cloth and various Art.With ventilated ability of sweat absorption, and good endurance, the change of cold-resistant hot weather, can recycling, no Pollute environment.Traditional establishment paper is these paper to reach required intensity by the mutual winding of fiber and longitudinal arrangement More than 6mm paper slip can only typically be cut into by opening, and can only work out rag paper rope.
Paper yarn body paper is also referred to as paper twine body paper, often using safety and environmental protection, good toughness string as raw material, by specific bar Part is processed into paper paper slip, and paper slip is through twisting with the fingers or winding into paper yarn;Also the paper yarn of sub-thread further can be twisted bifilar or multiply Paper yarn, to meet the requirement of different fabrics.Paper yarn body paper has the characteristics of quantitative low, intensity is high, elongation is larger, can slitting Into narrow serial obbbin.
CN101440588B discloses a kind of base paper of paper yarn for textile and preparation technology, and it is with following percentage by weight Raw material is made：Bleached softwood wood sulfate pulpboard 60-80%, jute pulp or/and bamboo pulp 20-30%, water soluble fiber 3-8%, own Component total 100%.The preparation technology of base paper of paper yarn for textile, profit in its upper cylinder half process before being batched in paper pulp copy paper technique The film given with glue spreader before batching spreads colloid to increase the dry and wet intensity of body paper.Product of the present invention has water suction fast, ventilative Property good, light and comfortable, machine washable, cut twist with the fingers it is functional, be a kind of reproducible environment-friendly products.
CN103741556A discloses a kind of preparation technology of base paper of paper yarn for textile, in described raw material, water soluble fiber, Wood pulp, bleached softwood wood sulfate pulpboard, the proportioning of bacterial fibers are：Water soluble fiber 3%~8%, wood pulp 25%~35%, bleaching pin Leaf wood sulfate pulpboard 50%~85%, bacterial fibers 2.5%~5%, all components total 100%.It is of the invention mainly to use bleaching pin Leaf wood sulfate pulpboard avoids the bleaching of sulfur dioxide, so as to which product is not easy to turn to be yellow, influences outward appearance as main slurries；And The present invention added with non-plant fibre is bacterial fibers, and by the cooperative effect of the auxiliary agent during manufacturing paper with pulp, makes the thing of body paper Reason intensity greatly improves, and while ensure that into the dry strength and wet strength of paper, there is preferable water imbibition and flexibility again.
CN101280532B discloses the preparation technology of base paper of paper yarn for textile, and water-solubility PVA synthetic fibers exist first Soaked in water；Then bacterial cellulose wet-coating is soaked in NaOH solution, then wood pulp cellulose is discongested with Valley beater Cut-out, then it is mixed with the water-solubility PVA synthetic fibers by pretreatment, refining is carried out in PFI fiberizers, is finally added Enter bacterial fibers, PEO, CMC, PAE are well mixed, by approach system, paper is manufactured paper with pulp into using usual manner.The present invention is using non- String is that bacterial fibers, WATER-SOLUBLE PVA FIBER are mixed and manufactured paper with pulp in proportion with wood pulp string.Using methods of beating to each Kind of fiber has carried out different mashing and handled to improve the ru nnability of fiber, adhesion between reinforcing fiber；And by manufacturing paper with pulp During auxiliary agent cooperative effect, greatly improve the physical strength of body paper.
The dry strength and wet strength of the paper yarn body paper produced now are all not up to standard, and the hydrocarbon of auxiliary agent is peeled off currently used as corrugation Oil is incompatible with creping adhesives, it is therefore desirable to Wrinkling stripping-agent is improved, and water imbibition and flexibility be not also up to standard, page is contaminating Xerotripsis during color, wet rubbing, grade is low, and wet strength is low.Therefore the development of some related textile industries is also constrained.
The content of the invention
It is an object of the invention to provide a kind of processing and fabricating is easy, strong operability, paper strength is high, and water-fastness one kind is high The preparation method of intensity paper twine body paper.
There is provided a kind of preparation method of high intensity paper twine body paper, it is characterised in that following steps：
（1）By weight, 100 parts of needlebush wood pulps are placed in pulper, add 0.01-0.5 part dyestuffs, beating consistency 2-10%, 40-45 ° of SR of beating degree is beaten, feeding matches somebody with somebody stock tank, adds 0.1-1 part color fixing agent, 3-10 part wet strength agents, 0.1-0.5 parts Ionic liquid remover, is sufficiently mixed；
（2）By weight, by 100 parts of PVC chemical fibres, 3000-7000 part water, 2-8 hours is stirred, obtain PVC chemical fibre dispersion liquids.
（3）By weight, the slurry of 100 parts of steps 1 is sent into net cage, 100-500 part PVC chemical fibres dispersion liquid is sent into Net cage；Turning into page through dehydration forming, PVC chemical fibres are uniformly attached to page surface, then through press dewatering, in 90-100 DEG C of heating 5-15 hours, obtain paper twine body paper.
The ionic liquid remover preparation method is：By weight：100 parts of ethylene glycol, 0.5-2 parts tall oil acid and Asia more Alkyl polyamine reactant, 0.1-1 part trimethyl hydroxyethylammonium ammonium hexafluorophosphates, 0.01-0.1 part cerium naphthenate salt, 30-60 DEG C mixed 1-5 hours are closed, obtain ionic liquid remover.
The color fixing agent, wet strength agent are auxiliary agent commonly used in the art, are commercially available prod, and the present invention is not limited.
The ethylene glycol, tall oil acid and polyalkylenepolyamines reactant, trimethyl hydroxyethylammonium ammonium hexafluorophosphate, cycloalkanes Sour cerium salt is commercially available prod.
The product of the present invention has the advantages that：
A kind of preparation method of high intensity paper twine body paper of the present invention, remover are changed with creping adhesives compatibility It is kind, while solve page xerotripsis in dyeing course, the problem of wet rubbing, grade is low, and wet strength is low.
Embodiment
Following instance is only to further illustrate the present invention, is not limitation the scope of protection of the invention.
Embodiment 1
Pink paper twine body paper preparation method, it is characterised in that following steps：
（1）By weight, 100 parts of needlebush wood pulps are placed in pulper, add 0.02 part of pink color, mashing is dense Degree 4%, 43 ° of SR of beating degree are beaten, are sent into and match somebody with somebody stock tank, 0.3 part of color fixing agent of addition, 7 parts of wet strength agents, 0.4 part of ionic liquid remover, It is sufficiently mixed；
（2）By weight, by 100 parts of PVC chemical fibres, 5000 parts of water, stir 5 hours, obtain PVC chemical fibre dispersion liquids.
（3）By weight, the slurry of 100 parts of steps 1 is sent into net cage, 250 parts of PVC chemical fibres dispersion liquids is sent into net Case；Turning into page through dehydration forming, PVC chemical fibres are uniformly attached to page surface, then through press dewatering, are heated 8 hours at 94 DEG C, Obtain paper twine body paper.
The ionic liquid remover preparation method is：By weight：100 parts of ethylene glycol, 1 part of tall oil acid and polyalkylene Polyamine reactant, 0.3 part of trimethyl hydroxyethylammonium ammonium hexafluorophosphate, 0.05 portion of cerium naphthenate salt, 40 DEG C mix 3 hours, obtain Ionic liquid remover.
Page is detected, does and resists strong index 101Nm/g, it is wet to resist strong index 46.8Nm/g, wet rubbing：3 grades；Xerotripsis：4 Level.
Embodiment 2
There is provided a kind of preparation method of high intensity paper twine body paper, it is characterised in that following steps：
（1）By weight, 100 parts of needlebush wood pulps are placed in pulper, add 0.01 part of dyestuff, beating consistency 2%, 40 ° of SR of beating degree are beaten, is sent into and matches somebody with somebody stock tank, 0.1 part of color fixing agent of addition, 3 parts of wet strength agents, 0.1 part of ionic liquid remover, fully Mixing；
（2）By weight, by 100 parts of PVC chemical fibres, 3000 parts of water, stir 2 hours, obtain PVC chemical fibre dispersion liquids.
（3）By weight, the slurry of 100 parts of steps 1 is sent into net cage, 100 parts of PVC chemical fibres dispersion liquids is sent into net Case；Turning into page through dehydration forming, PVC chemical fibres are uniformly attached to page surface, then through press dewatering, are heated 5 hours at 90 DEG C, Obtain paper twine body paper.
The ionic liquid remover preparation method is：By weight：100 parts of ethylene glycol, 0.5 part of tall oil acid and more alkylenes Quito amine reactant, 0.1 part of trimethyl hydroxyethylammonium ammonium hexafluorophosphate, 0.01 portion of cerium naphthenate salt, 30 DEG C mix 5 hours, obtain To ionic liquid remover.
Page is detected, does and resists strong index 98Nm/g, it is wet to resist strong index 45.4Nm/g, wet rubbing：3 grades；Xerotripsis：4 grades.
Embodiment 3
（1）By weight, 100 parts of needlebush wood pulps are placed in pulper, add 0.5 part of dyestuff, beating consistency 10%, 45 ° of SR of beating degree are beaten, feeding matches somebody with somebody stock tank, adds 1 part of color fixing agent, 10 parts of wet strength agents, 0.5 part of ionic liquid remover, fully mixes Close；
（2）By weight, by 100 parts of PVC chemical fibres, 7000 parts of water, stir 8 hours, obtain PVC chemical fibre dispersion liquids.
（3）By weight, the slurry of 100 parts of steps 1 is sent into net cage, 500 parts of PVC chemical fibres dispersion liquids is sent into net Case；Turning into page through dehydration forming, PVC chemical fibres are uniformly attached to page surface, then through press dewatering, it is small in 100 DEG C of heating 15 When, obtain paper twine body paper.
The ionic liquid remover preparation method is：By weight：100 parts of ethylene glycol, 2 parts of tall oil acids and polyalkylene Polyamine reactant, 1 part of trimethyl hydroxyethylammonium ammonium hexafluorophosphate, 0.1 portion of cerium naphthenate salt, 60 DEG C of mixing hours, obtain ion Liquid remover.
Page is detected, does and resists strong index 112Nm/g, it is wet to resist strong index 48.5Nm/g, wet rubbing：3 grades；Xerotripsis：4 Level.
Embodiment 4
The preparation method of grey paper twine body paper, it is characterised in that following steps：
（1）By weight, 100 parts of Canadian North Sea needlebush wood pulps are placed in pulper, add 0.3 part of grey dye Material, beating consistency 5%, be beaten 42 ° of SR of beating degree, feeding match somebody with somebody stock tank, 0.2 part of color fixing agent of addition, 7 parts of wet strength agents, 0.15 part from Sub- liquid remover, is sufficiently mixed；
（2）By weight, by 100 parts of PVC chemical fibres, 3000-7000 part water, 2-8 hours is stirred, obtain PVC chemical fibre dispersion liquids.
（3）By weight, the slurry of 100 parts of steps 1 is sent into net cage, 260 parts of PVC chemical fibres dispersion liquids is sent into net Case；Turning into page through dehydration forming, PVC chemical fibres are uniformly attached to page surface, then through press dewatering, are heated 6 hours at 95 DEG C, Obtain paper twine body paper.
The ionic liquid remover preparation method is：100 parts of ethylene glycol, 0.77 part of tall oil acid and polyalkylenepolyamines are anti- Thing is answered, 0.6 part of trimethyl hydroxyethylammonium ammonium hexafluorophosphate, 0.04 portion of cerium naphthenate salt, 50 DEG C mix 3 hours, obtain ionic liquid Remover.
Page is detected, does and resists strong index 103Nm/g, it is wet to resist strong index 44Nm/g, wet rubbing：3 grades；Xerotripsis：4 grades.
Comparative example 1
Tall oil acid and polyalkylenepolyamines reactant are added without, other conditions are the same as embodiment 1.
Page is detected, does and resists strong index 95Nm/g, it is wet to resist strong index 40Nm/g, wet rubbing：3 grades；Xerotripsis：4 grades.
Comparative example 2
Trimethyl hydroxyethylammonium ammonium hexafluorophosphate is added without, other conditions are the same as embodiment 1.
Page is detected, does and resists strong index 93Nm/g, it is wet to resist strong index 41Nm/g, wet rubbing：3 grades；Xerotripsis：4 grades.
Comparative example 3
Cerium naphthenate salt is added without, other conditions are the same as embodiment 1.
Page is detected, does and resists strong index 94Nm/g, it is wet to resist strong index 40Nm/g, wet rubbing：3 grades；Xerotripsis：4 grades.
Comparative example 4
Ionic liquid remover is replaced using ethylene glycol, other conditions are the same as embodiment 1.
Page is detected, does and resists strong index 89Nm/g, it is wet to resist strong index 35Nm/g, wet rubbing：3 grades；Xerotripsis：3 grades.
The specific embodiment of the present invention is these are only, but the technical characteristic of the present invention is not limited thereto.It is any with this hair Based on bright, to solve essentially identical technical problem, essentially identical technique effect is realized, made simple change, etc. With replacement or modification etc., all it is covered by among protection scope of the present invention.

Claims (4)

  1. A kind of 1. preparation method of high intensity paper twine body paper, it is characterised in that following steps：
    Step 1
    By weight, 100 parts of needlebush wood pulps are placed in pulper, add 0.01-0.5 part dyestuffs, beating consistency 2- 10%, be beaten 40-45 ° of SR of beating degree, feeding match somebody with somebody stock tank, addition 0.1-1 part color fixing agent, 3-10 part wet strength agents, 0.1-0.5 parts from Sub- liquid remover, is sufficiently mixed；
    Step 2
    By weight, by 100 parts of PVC chemical fibres, 3000-7000 part water, 2-8 hours is stirred, obtain PVC chemical fibre dispersion liquids；
    Step 3
    By weight, the slurry of 100 parts of steps 1 is sent into net cage, 100-500 part PVC chemical fibres dispersion liquid is sent into net cage；Through Dehydration forming turns into page, and PVC chemical fibres are uniformly attached to page surface, then through press dewatering, it is small to heat 5-15 at 90-100 DEG C When, obtain paper twine body paper.
  2. A kind of 2. preparation method of high intensity paper twine body paper described in claim 1, it is characterised in that：The ionic liquid remover Preparation method is：By weight：100 parts of ethylene glycol, 0.5-2 parts tall oil acid and polyalkylenepolyamines reactant, 0.1-1 parts three Dimethyl hydroxyethyl ammonium hexafluorophosphate, 0.01-0.1 part cerium naphthenate salt, 30-60 DEG C of mixing 1-5 hour, obtain ionic liquid stripping Agent.
  3. A kind of 3. preparation method of high intensity paper twine body paper described in claim 1, it is characterised in that：Also include a kind of grey coloured paper The preparation method of yarn body paper, it is characterised in that following steps：
    Step 1
    By weight, 100 parts of Canadian North Sea needlebush wood pulps are placed in pulper, add 0.3 part of gray dyes, beat Concentration 4% is starched, is beaten 42 ° of SR of beating degree, feeding matches somebody with somebody stock tank, adds 0.2 part of color fixing agent, 7 parts of wet strength agents, 0.15 part of ionic liquid stripping From agent, it is sufficiently mixed；
    Step 2
    By weight, by 100 parts of PVC chemical fibres, 3000-7000 part water, 2-8 hours is stirred, obtain PVC chemical fibre dispersion liquids；
    Step 3
    By weight, the slurry of 100 parts of steps 1 is sent into net cage, 260 parts of PVC chemical fibres dispersion liquids is sent into net cage；Through dehydration Turn into page, PVC chemical fibres are uniformly attached to page surface, then through press dewatering, are heated 6 hours at 95 DEG C, obtain paper twine Body paper.
  4. A kind of 4. preparation method of high intensity paper twine body paper described in claim 1, it is characterised in that：Also include a kind of pink Paper twine body paper preparation method, it is characterised in that following steps：
    Step 1
    By weight, 100 parts of needlebush wood pulps are placed in pulper, add 0.02 part of pink color, beating consistency 4%, 43 ° of SR of beating degree are beaten, feeding matches somebody with somebody stock tank, adds 0.3 part of color fixing agent, 7 parts of wet strength agents, 0.4 part of ionic liquid remover, fills Divide mixing；
    Step 2
    By weight, by 100 parts of PVC chemical fibres, 5000 parts of water, stir 5 hours, obtain PVC chemical fibre dispersion liquids；
    Step 3
    By weight, the slurry of 100 parts of steps 1 is sent into net cage, 250 parts of PVC chemical fibres dispersion liquids is sent into net cage；Through dehydration Turn into page, PVC chemical fibres are uniformly attached to page surface, then through press dewatering, are heated 8 hours at 94 DEG C, obtain paper twine Body paper.
CN201710894153.9A 2017-09-28 2017-09-28 A kind of preparation method of high intensity paper twine body paper Active CN107419577B (en)

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Cited By (6)

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Publication number Priority date Publication date Assignee Title
CN110318282A (en) * 2019-06-12 2019-10-11 浙江舜浦新材料科技有限公司 A kind of preparation method of uvioresistant braiding body paper
WO2020034284A1 (en) * 2018-08-16 2020-02-20 何炽斌 Production method for dyeing pure natural colored paper
CN111021135A (en) * 2019-12-06 2020-04-17 安徽天扬纺织品有限公司 Preparation method of high-strength recyclable paper socks
CN113863055A (en) * 2021-10-13 2021-12-31 浙江舜浦新材料科技有限公司 Preparation method of colored paper yarn base paper
CN115726219A (en) * 2021-08-31 2023-03-03 温岭市丝美达草艺厂 Preparation method of nano paper yarns with good waterproof performance
CN115821629A (en) * 2022-10-20 2023-03-21 浙江舜浦新材料科技有限公司 Method for preparing paper yarn base paper with high color fastness by deeply coloring water-based nano organic pigment

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CN104775326A (en) * 2015-04-10 2015-07-15 浙江舜浦纸业有限公司 Production process for deep-color craft woven paper
CN104818651A (en) * 2015-04-10 2015-08-05 浙江舜浦纸业有限公司 Technology for producing light color technical braiding paper

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CN102251431A (en) * 2011-07-22 2011-11-23 浙江舜浦纸业有限公司 Method for producing colored knitting paper for handicraft articles by using mixed bamboo and wood pulp
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2020034284A1 (en) * 2018-08-16 2020-02-20 何炽斌 Production method for dyeing pure natural colored paper
CN110318282A (en) * 2019-06-12 2019-10-11 浙江舜浦新材料科技有限公司 A kind of preparation method of uvioresistant braiding body paper
CN111021135A (en) * 2019-12-06 2020-04-17 安徽天扬纺织品有限公司 Preparation method of high-strength recyclable paper socks
CN115726219A (en) * 2021-08-31 2023-03-03 温岭市丝美达草艺厂 Preparation method of nano paper yarns with good waterproof performance
CN113863055A (en) * 2021-10-13 2021-12-31 浙江舜浦新材料科技有限公司 Preparation method of colored paper yarn base paper
CN115821629A (en) * 2022-10-20 2023-03-21 浙江舜浦新材料科技有限公司 Method for preparing paper yarn base paper with high color fastness by deeply coloring water-based nano organic pigment
CN115821629B (en) * 2022-10-20 2023-10-17 浙江舜浦新材料科技有限公司 Method for preparing high-color-fastness paper yarn base paper by deep coloring of water-based nano organic pigment

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