CN107419511A - The method for bleaching and textile product of textile material - Google Patents
The method for bleaching and textile product of textile material Download PDFInfo
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- CN107419511A CN107419511A CN201710813566.XA CN201710813566A CN107419511A CN 107419511 A CN107419511 A CN 107419511A CN 201710813566 A CN201710813566 A CN 201710813566A CN 107419511 A CN107419511 A CN 107419511A
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- bleaching
- textile material
- agent
- liquid
- refining
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
- D06L4/10—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen
- D06L4/12—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen combined with specific additives
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
- D06L4/10—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen
- D06L4/13—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen using inorganic agents
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Treatment Of Fiber Materials (AREA)
- Detergent Compositions (AREA)
- Coloring (AREA)
Abstract
The present invention relates to a kind of method for bleaching of textile material and textile product, the method for bleaching comprises the following steps:Refining agent, brightening agent and water are mixed to get refining liquid, textile material is immersed in the refining liquid, and in 80~110 DEG C of 10~60min of isothermal holding;The textile material handled through the refining liquid is immersed in bleaching liquid, and in 90~110 DEG C of 60~120min of isothermal holding.The method for bleaching of the present invention can effectively avoid the generation of the irregular phenomenon of fluorescence, in the case of the 0.0001%~0.3% of the quality of the dosage as little as textile material of brightening agent, the process remains able to ensure that brightening agent is uniform in the absorption of textile material surface, so as to reduce the usage amount of brightening agent, the quality of textile product is improved simultaneously, significantly reduces production cost.
Description
Technical field
The present invention relates to textile technology field, more particularly to the method for bleaching and textile product of a kind of textile material.
Background technology
Textile industry is the important economic support industry in China, and bleach be yarn fabric dyeing and finishing processing in one it is highly important
Link, it can improve the presentation quality of yarn fabric, improve wetability, permeability etc., the quality of Bleaching Quality will directly affect
The quality of colour of final products.
At present, with the development of the social economy, people are multifarious to color to require more and more higher, therefore textile industry pair
The requirement of textile product whiteness scope also more and more higher.But it is irregular easily to produce fluorescence in traditional bleaching plus white technique
Phenomenon, so that the textile product whiteness after bleaching is irregular, the quality of colour for ultimately resulting in product is bad.
The content of the invention
Based on this, it is necessary to provide a kind of method for bleaching for avoiding producing the textile material of the irregular phenomenon of fluorescence.
Specific technical scheme is as follows:
A kind of method for bleaching of textile material, comprises the following steps:
Refining agent, brightening agent and water are mixed to get refining liquid, textile material is immersed in the refining liquid, and in 80~
110 DEG C of 10~60min of isothermal holding;
By the textile material handled through the refining liquid immerse bleaching liquid in, and in 90~110 DEG C of isothermal holdings 60~
120min。
In one of the embodiments, in the refining liquid, the concentration of the refining agent is 0.3~1g/L;The increasing
The quality of white agent is the 0.0001%~0.3% of the quality of the textile material.
In one of the embodiments, the bath raio of the textile material and the refining liquid is 1:3~1:30.
In one of the embodiments, refining agent, chelating agent, bleaching agent and sodium hydroxide are included in the bleaching liquid.
In one of the embodiments, the bleaching agent is hydrogen peroxide, and hydrogen peroxide stabilizer is also included in the bleaching liquid.
In one of the embodiments, in the bleaching liquid, the concentration of the refining agent is 0.3~1g/L, the chela
The concentration of mixture is 0.3~1g/L, and the concentration of the hydrogen peroxide is 10~14g/L, and the concentration of the hydrogen peroxide stabilizer is 0.5
~1g/L, the concentration of the sodium hydroxide is 1~4g/L.
In one of the embodiments, the bath raio of the textile material and the bleaching liquid handled through the refining liquid is
1:3~1:30.
In one of the embodiments, it is further comprising the steps of:The textile material handled through the bleaching liquid is immersed into water
In, and in 90~110 DEG C of 2~10min of isothermal holding, it is then immersed in 5~20min of immersion in acid solution.
In one of the embodiments, the acid solution is aqueous acetic acid, and concentration is 0.2~0.5g/L.
Present invention also offers a kind of textile product being prepared according to above-mentioned method for bleaching.
The present invention principle and have the beneficial effect that:
Brightening agent is a kind of organic compound that can improve the whiteness such as fabric and paper, also known as Optical Bleaching Agent, glimmering
Optical brightener, white dye etc., effect are that the sightless ultraviolet radiation that product absorbs is transformed into indigo fluorescence spoke
Penetrate, complementary color turns into white light each other with the radiation of original gold-tinted, improves the whiteness of product in the sunlight.
The present invention is by researching and analysing discovery, and traditional bleaching adds in white technique, due to being directly added into bleaching liquid
Brightening agent, and brightening agent has stronger affinity in the presence of bleaching liquid to textile material, thus will promptly adsorb
In textile material, the brightening agent for easily causing subregion to be adsorbed is more, and the brightening agent of other regions absorption is less so that pole
It is also easy to produce that textile product whiteness is irregular, the bad situation of quality of colour, can only so improves and increase by increasing the dosage of brightening agent
The saturation degree of white agent, to reduce the problem of textile product whiteness is irregular.
The method for bleaching of the present invention is innovative on the basis of rationally control refining stage and bleaching stage technological parameter
Brightening agent is added in the refining stage of textile material first, now because absorption of the textile material to brightening agent is also weaker, because
This brightening agent can progressively reach uniform adsorption in the dynamic process of continuation adsorption-desorption, avoid producing that fluorescence is irregular shows
As, in ensuing bleaching process, adsorb uniform brightening agent and then combined closely with textile material, it is equal so as to obtain whiteness
Even product.In the case of the 0.0001%~0.3% of the quality of the dosage as little as textile material of brightening agent, the process
Remain able to ensure that brightening agent is uniform in the absorption of textile material surface, so as to reduce the usage amount of brightening agent, improve simultaneously
The quality of textile product, significantly reduces production cost.
Embodiment
For the ease of understanding the present invention, the present invention will be described more fully below.But the present invention can be with perhaps
More different form is realized, however it is not limited to embodiment described herein.On the contrary, the purpose for providing these embodiments is to make
Understanding more thorough and comprehensive to the disclosure.
Unless otherwise defined, all of technologies and scientific terms used here by the article is with belonging to technical field of the invention
The implication that technical staff is generally understood that is identical.Term used in the description of the invention herein is intended merely to description tool
The purpose of the embodiment of body, it is not intended that in the limitation present invention.Term as used herein "and/or" includes one or more phases
The arbitrary and all combination of the Listed Items of pass.
The method for bleaching of the textile material of an embodiment of the present invention, comprises the following steps S1~S2:
S1, refining agent, brightening agent and water is mixed to get refining liquid, textile material is immersed in refining liquid, and in 80~
110 DEG C of 10~60min of isothermal holding.
Alternatively, in refining liquid, the concentration of refining agent is 0.3~1g/L, and the quality of brightening agent is the matter of textile material
The 0.0001%~0.3% of amount.
Alternatively, the bath raio of textile material and refining liquid is 1:3~1:30.
Specifically, textile material refers to fiber, yarn, fabric and its compound etc..
S2, the textile material for handling refined liquid are immersed in bleaching liquid, and in 90~110 DEG C of isothermal holdings 60~
120min。
Specifically, refining agent, chelating agent, bleaching agent and sodium hydroxide are included in bleaching liquid.
In one embodiment, bleaching agent is hydrogen peroxide, and hydrogen peroxide stabilizer is also included in bleaching liquid.
Specifically, in bleaching liquid, the concentration of refining agent is 0.3~1g/L, and the concentration of chelating agent is 0.3~1g/L, double
The concentration of oxygen water is 10~14g/L, and the concentration of hydrogen peroxide stabilizer is 0.5~1g/L, and the concentration of sodium hydroxide is 1~4g/L.
Alternatively, the textile material of refined liquid processing and the bath raio of bleaching liquid are 1:3~1:30.
In one embodiment, it is further comprising the steps of:The textile material handled through bleaching liquid is immersed in the water, and in 90
~110 DEG C of 2~10min of isothermal holding, it is then immersed in 5~20min of immersion in acid solution.
Alternatively, acid solution is aqueous acetic acid, and concentration is 0.2~0.5g/L.
It is appreciated that brightening agent in the present invention, refining agent, the specific species of chelating agent and bleaching agent can be entered as needed
Row selection, such as diphenyl ethylene derivatives, Phenylpyrazole quinoline derivant, benzimidizole derivatives, benzene pyrazole derivatives, cumarin
The brightening agent such as derivative and Naphthalamide derivatives, neopelex, SAS and fatty alcohol ether sulphur
The refining agents such as hydrochlorate, inorganic polyphosphate, aminocarboxylic acid type chelating agent, hydroxycarboxylic acid type chelating agent and organic phosphate etc. chelate
The bleaching agent such as agent, hydrogen peroxide, sodium hypochlorite, sodium peroxide and calcium hypochlorite, is not limited herein.
Brightening agent is a kind of organic compound that can improve the whiteness such as fabric and paper, also known as Optical Bleaching Agent, glimmering
Optical brightener, white dye etc., effect are that the sightless ultraviolet radiation that product absorbs is transformed into indigo fluorescence spoke
Penetrate, complementary color turns into white light each other with the radiation of original gold-tinted, improves the whiteness of product in the sunlight.
The present invention is by researching and analysing discovery, and traditional bleaching adds in white technique, due to being directly added into bleaching liquid
Brightening agent, and brightening agent has stronger affinity in the presence of bleaching liquid to textile material, thus will promptly adsorb
In textile material, the brightening agent for easily causing subregion to be adsorbed is more, and the brightening agent of other regions absorption is less so that pole
It is also easy to produce that textile product whiteness is irregular, the bad situation of quality of colour, can only so improves and increase by increasing the dosage of brightening agent
The saturation degree of white agent, to reduce the problem of textile product whiteness is irregular.
The method for bleaching of the present invention is innovative on the basis of rationally control refining stage and bleaching stage technological parameter
Brightening agent is added in the refining stage of textile material first, now because absorption of the textile material to brightening agent is also weaker, because
This brightening agent can progressively reach uniform adsorption in the dynamic process of continuation adsorption-desorption, avoid producing that fluorescence is irregular shows
As, in ensuing bleaching process, adsorb uniform brightening agent and then combined closely with textile material, it is equal so as to obtain whiteness
Even product.In the case of the 0.0001%~0.3% of the quality of the dosage as little as textile material of brightening agent, the process
Remain able to ensure that brightening agent is uniform in the absorption of textile material surface, so as to reduce the usage amount of brightening agent, improve simultaneously
The quality of textile product, significantly reduces production cost.
Present invention also offers a kind of textile product being prepared according to above-mentioned method for bleaching.
It is specific embodiment below.
Embodiment 1
One cylinder 40S pure cotton warp beams of dye, yarn weight 522kg, density 0.47g/ are thrown in a diameter of 1800mm dye vat
Cm3, bath raio 1:7.72, whiteness requirement is 125~130 degree.
After textile material enters cylinder, a certain amount of water is added in master cylinder, then adds refining agent EPD-C and brightening agent
BHT LIQ 115% obtain refining liquid, wherein, refining agent EPD-C concentration is 0.3g/L, brightening agent BHT LIQ's 115%
Quality is the 0.12% of the quality of textile material, and the bath raio of textile material and refining liquid is 1:7.72, it is warming up to 100 DEG C of insulation fortune
Discharged after row 20min.
Add bleaching liquid in master cylinder, refining agent EPD-C concentration is 0.3g/L, chelating agent LEOUEST in bleaching liquid
98-3 concentration is 0.5g/L, and hydrogen peroxide stabilizer PL concentration is 0.8g/L, and the concentration of 50% liquid caustic soda is 3.8g/L, hydrogen peroxide
Concentration be 10g/L, the bath raio of textile material and bleaching liquid is 1:7.72, discharged after being warming up to 100 DEG C of insulation operation 90min.
Hot water is added in master cylinder, be warming up to 100 DEG C insulation operation 5min after discharge, then in master cylinder add hot water and
HAc obtains acetum, and wherein HAc concentration is 0.3g/L, is discharged after running 10min.
It is 128.91 to take 40S purified cotton yarns test whiteness value, and yarn whiteness is uniform, and unstressed configuration is not in follow-up weaving process
Even feedback.
Embodiment 2
One cylinder 40S pure cotton cylinder yarns of dye, yarn weight 213.15kg, bath raio 1 are thrown in a diameter of 1400MM dye vat:
11.59, whiteness requirement is 110~120 degree.
After textile material enters cylinder, a certain amount of water is added in master cylinder, then adds refining agent EPD-C and brightening agent
BHT LIQ 115% obtain refining liquid, wherein, refining agent EPD-C concentration is 0.3g/L, brightening agent BHT LIQ's 115%
Quality is the 0.05% of the quality of textile material, and the bath raio of textile material and refining liquid is 1:11.59, it is warming up to 100 DEG C of insulations
Discharged after operation 20min.
Add bleaching liquid in master cylinder, refining agent EPD-C concentration is 0.3g/L, chelating agent LEOUEST in bleaching liquid
98-3 concentration is 0.5g/L, and hydrogen peroxide stabilizer PL concentration is 0.8g/L, and the concentration of 50% liquid caustic soda is 3.8g/L, hydrogen peroxide
Concentration be 10g/L, the bath raio of textile material and bleaching liquid is 1:11.59, discharged after being warming up to 100 DEG C of insulation operation 90min.
Hot water is added in master cylinder, be warming up to 100 DEG C insulation operation 5min after discharge, then in master cylinder add hot water and
HAc obtains acetum, and wherein HAc concentration is 0.2g/L, is discharged after running 10min.
Take the 40S purified cotton yarns test ectonexine whiteness value, respectively 114.1 and 119.9, yarn ectonexine whiteness is equal
It is even, and the irregular feedback of unstressed configuration in follow-up weaving process.
Embodiment 3
One cylinder 40S pure cotton cylinder yarns of dye, yarn weight 200kg, bath raio 1 are thrown in a diameter of 1400MM dye vat:30, in vain
Degree requires to be 130~140 degree.
After textile material enters cylinder, a certain amount of water is added in master cylinder, then add refining agent SAS and
Brightening agent Phenylpyrazole quinoline derivant obtains refining liquid, wherein, the concentration of refining agent SAS is 0.5g/L, brightening agent
The quality of Phenylpyrazole quinoline derivant is the 0.3% of the quality of textile material, and the bath raio of textile material and refining liquid is 1:30, rise
Temperature is discharged after running 30min to 110 DEG C of insulations.
Add bleaching liquid in master cylinder, the concentration of refining agent SAS is 0.5g/L in bleaching liquid, amino carboxylic acid
The concentration of type chelating agent is 0.3g/L, and hydrogen peroxide stabilizer PL concentration is 0.5g/L, and the concentration of 50% liquid caustic soda is 4g/L, dioxygen
The concentration of water is 12g/L, and the bath raio of textile material and bleaching liquid is 1:30, discharged after being warming up to 110 DEG C of insulation operation 60min.
Hot water is added in master cylinder, be warming up to 110 DEG C insulation operation 2min after discharge, then in master cylinder add hot water and
HAc obtains acetum, and wherein HAc concentration is 0.2g/L, is discharged after running 10min.
Take the 40S purified cotton yarns test ectonexine whiteness value, respectively 140 and 135, yarn ectonexine whiteness is uniform, and
The irregular feedback of unstressed configuration in follow-up weaving process.
Comparative example 1
One cylinder 40S pure cotton warp beams of dye, yarn weight 200kg, bath raio 1 are thrown in a diameter of 1400MM dye vat:12, in vain
Degree requires to be 120~130 degree.
After textile material enters cylinder, a certain amount of water is added in master cylinder, refining agent EPD-C is then added and obtains refining liquid,
Wherein, refining agent EPD-C concentration is 0.3g/L, and the bath raio of textile material and refining liquid is 1:12, it is warming up to 100 DEG C of insulation fortune
Discharged after row 20min.
A certain amount of water is added in master cylinder, then adds refining agent EPD-C, brightening agent BHT LIQ 115%, chelating agent
LEOUEST 98-3, hydrogen peroxide stabilizer PL, 50% liquid caustic soda and hydrogen peroxide, refining agent EPD-C concentration is 0.3g/L in solution,
Brightening agent BHT LIQ 115% quality is the 0.3% of the quality of textile material, and chelating agent LEOUEST 98-3 concentration is
0.5g/L, hydrogen peroxide stabilizer PL concentration are 0.8g/L, and the concentration of 50% liquid caustic soda is 3.8g/L, and the concentration of hydrogen peroxide is 10g/
L, bath raio 1:12, discharged after being warming up to 100 DEG C of insulation operation 100min.
Hot water is added in master cylinder, be warming up to 100 DEG C insulation operation 5min after discharge, then in master cylinder add hot water and
HAc obtains acetum, and wherein HAc concentration is 0.2g/L, is discharged after running 10min.
It is 139.1 to take 40S purified cotton yarns test outer layer whiteness value, the irregular feedback of fluorescence occurs in follow-up weaving process,
Have a strong impact on cloth cover quality of colour.
Comparative example 2
One cylinder 40S pure cotton cylinder yarns of dye, yarn weight 200kg, bath raio 1 are thrown in a diameter of 1400MM dye vat:12, in vain
Degree requires to be 120~130 degree.
After textile material enters cylinder, a certain amount of water is added in master cylinder, then adds refining agent EPD-C and brightening agent
BHT LIQ 115% obtain refining liquid, wherein, refining agent EPD-C concentration is 0.3g/L, brightening agent BHT LIQ's 115%
Quality is the 0.3% of the quality of textile material, and the bath raio of textile material and refining liquid is 1:12, it is warming up to 70 DEG C of insulation operations
Discharged after 5min.
Add bleaching liquid in master cylinder, refining agent EPD-C concentration is 0.3g/L, chelating agent LEOUEST in bleaching liquid
98-3 concentration is 0.5g/L, and hydrogen peroxide stabilizer PL concentration is 0.8g/L, and the concentration of 50% liquid caustic soda is 3.8g/L, hydrogen peroxide
Concentration be 10g/L, the bath raio of textile material and bleaching liquid is 1:12, discharged after being warming up to 80 DEG C of insulation operation 50min.
Hot water is added in master cylinder, be warming up to 100 DEG C insulation operation 5min after discharge, then in master cylinder add hot water and
HAc obtains acetum, and wherein HAc concentration is 0.2g/L, is discharged after running 10min.
The 40S purified cotton yarns are taken to test ectonexine whiteness value, respectively 142 and 128, yarn ectonexine whiteness is uneven, after
Cloth cover quality of colour is had a strong impact on because fluorescence is irregular in continuous weaving process.
By above-described embodiment 1~3 and comparative example 1~2, method for bleaching of the invention passes through the essence in textile material
The refining stage adds brightening agent, and concise and bleaching is carried out under the conditions of certain temperature and time, uniform so as to obtain whiteness
Product, it is possible to prevente effectively from the generation of the irregular phenomenon of fluorescence, in the quality of the dosage as little as textile material of brightening agent
In the case of 0.0001%~0.3%, the process remains able to ensure that brightening agent is uniform in the absorption of textile material surface, from
And the usage amount of brightening agent can be reduced, while the quality of textile product is improved, significantly reduce production cost.
Each technical characteristic of embodiment described above can be combined arbitrarily, to make description succinct, not to above-mentioned reality
Apply all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited
In contradiction, the scope that this specification is recorded all is considered to be.
Embodiment described above only expresses the several embodiments of the present invention, and its description is more specific and detailed, but simultaneously
Can not therefore it be construed as limiting the scope of the patent.It should be pointed out that come for one of ordinary skill in the art
Say, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the protection of the present invention
Scope.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (10)
1. a kind of method for bleaching of textile material, it is characterised in that comprise the following steps:
Refining agent, brightening agent and water are mixed to get refining liquid, textile material is immersed in the refining liquid, and in 80~110
DEG C 10~60min of isothermal holding;
The textile material handled through the refining liquid is immersed in bleaching liquid, and in 90~110 DEG C of 60~120min of isothermal holding.
2. method for bleaching according to claim 1, it is characterised in that in the refining liquid, the concentration of the refining agent
For 0.3~1g/L;The quality of the brightening agent is the 0.0001%~0.3% of the quality of the textile material.
3. method for bleaching according to claim 1, it is characterised in that the bath raio of the textile material and the refining liquid is
1:3~1:30.
4. method for bleaching according to claim 1, it is characterised in that refining agent, chelating agent, drift are included in the bleaching liquid
White agent and sodium hydroxide.
5. method for bleaching according to claim 4, it is characterised in that the bleaching agent is hydrogen peroxide, in the bleaching liquid
Also include hydrogen peroxide stabilizer.
6. method for bleaching according to claim 5, it is characterised in that in the bleaching liquid, the concentration of the refining agent
For 0.3~1g/L, the concentration of the chelating agent is 0.3~1g/L, and the concentration of the hydrogen peroxide is 10~14g/L, the dioxygen
The concentration of water stabilizer is 0.5~1g/L, and the concentration of the sodium hydroxide is 1~4g/L.
7. according to the method for bleaching described in any one of claim 1~6, it is characterised in that through described in refining liquid processing
The bath raio of textile material and the bleaching liquid is 1:3~1:30.
8. according to the method for bleaching described in any one of claim 1~6, it is characterised in that further comprising the steps of:Will be through described
The textile material of bleaching liquid processing is immersed in the water, and in 90~110 DEG C of 2~10min of isothermal holding, is then immersed in acid solution and is soaked
Steep 5~20min.
9. method for bleaching according to claim 8, it is characterised in that the acid solution is aqueous acetic acid, concentration 0.2
~0.5g/L.
10. a kind of textile product, it is characterised in that the method for bleaching according to any one of claim 1~9 is prepared.
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CN108486859A (en) * | 2018-03-29 | 2018-09-04 | 鲁泰纺织股份有限公司 | The colouring method of the lasting purified cotton yarns of whiteness |
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