CN107412040B - Gardenia facial mask powder and preparation method thereof - Google Patents
Gardenia facial mask powder and preparation method thereof Download PDFInfo
- Publication number
- CN107412040B CN107412040B CN201710320222.5A CN201710320222A CN107412040B CN 107412040 B CN107412040 B CN 107412040B CN 201710320222 A CN201710320222 A CN 201710320222A CN 107412040 B CN107412040 B CN 107412040B
- Authority
- CN
- China
- Prior art keywords
- gardenia
- parts
- powder
- freeze
- extract
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention provides a gardenia facial mask powder and a preparation method thereof, wherein the gardenia facial mask powder comprises the following raw materials of, by weight, 25-35 parts of gardenia iridoid glycoside powder, 5-10 parts of rhododendron extract, 1-5 parts of gardenia extract, 5-15 parts of white tea extract, 20-23 parts of konjac glucomannan, 12-16 parts of seaweed gel and 10-16 parts of collagen. The facial mask contains gardenia iridoid glycoside substances, and the white tea, the konjac glucomannan and the seaweed gel are all pure plant components, have no preservative or additive, have no stimulation or damage to the skin, are accompanied by the peculiar fragrance of the white tea, and have better curative effect on whelk suppuration and cystic acne formation.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to gardenia facial mask powder and a preparation method thereof.
Background
Gardenia is a dry mature fruit of Gardenia jasminoides Ellis (Gardenia jasminoides Ellis) which is a plant of Rubiaceae (Rubiaceae), is widely distributed in China, has complex plant sources and large demand, and is a first-published medicinal and edible dual-purpose variety of the Ministry of health. The iridoid glycoside in fructus Gardeniae has effects in protecting liver, promoting function of gallbladder, clearing away heat and toxic materials, and resisting bacteria and inflammation. The gardenia fruit is used as a medicine and mainly used for treating excessive fire toothache, mouth and tongue sores, conjunctivitis, pyocutaneous disease, pyogenic infections and the like. The great white tea from Fuding is native to Fuding Tailao mountain, and has the characteristics of unique region, natural process, unique efficacy and the like. The white tea leaves keep tea polyphenol, theanine and the like of the tea leaves, contains more flavonoid substances, and the flavonoid has an antioxidant function, the content of the antioxidant component of the white tea leaves is more than 3 times that of the antioxidant component of the green tea leaves, so that the white tea leaves can neutralize free radicals more effectively, are still strongest antioxidant plants in the nature so far, have the antioxidant function which is 200 times higher than that of vitamin E, and can improve the functions of detoxification and defense of human bodies. White tea is used for clearing heat, removing toxicity and eliminating inflammation in the ancient times by common people in the origin, and the white tea extract has a prevention effect on the growth of bacteria causing staphylococcus infection, streptococcus infection, pneumonia and the like.
Acne is usually caused by male and female in adolescence, is commonly called as whelk, has great influence on the psychology and social interaction of teenagers, often brings great pain to patients, can prevent and treat the acne early or can avoid the acne or minimize the harm, and cosmetics containing various chemical additives which are frequently used in the market at present have great damage to the skin and certain danger and toxic and side effects. There are many kinds of facial masks on the market today for removing acne. A plurality of mask products are available in the market, different preservatives and different chemical reagents which have certain skin irritation harm are added into raw materials of the mask products, and non-woven fabrics are used more, so that the mask products are troublesome to operate by consumers and high in cost.
The mask specially aiming at the acne curative effect is less, and the defects of the existing product are overcome. The mask which is cheap, safe, free of side effect, antibacterial and anti-inflammatory and has a good curative effect on acne and has the effects of clearing away heat and toxic materials and resisting bacteria is developed by taking safe and green gardenia, white tea, gardenia and the like as natural raw materials.
The facial mask is a facial mask which is safe and convenient to use, and has the synergistic effect on the curative effect of whelk suppuration and cystic acne formation, does not need to add preservatives for damaging skin, is mild in property, has no stimulation to skin, and is safe and convenient to use.
Compared with the prior art, the mask powder belongs to a pure natural formula, does not contain preservative, has mild action on human skin, no stimulation, no toxic or side effect, safety and reliability; the mask is convenient to use and carry, low-carbon and environment-friendly, and the waste mask can be completely biodegraded; has effects in clearing away heat and toxic materials, resisting bacteria, relieving inflammation, resisting oxidation, improving toxin expelling and defense effects, and treating acne with good therapeutic effect and complicated with special herb of white tea.
The gardenia planting area is large in China, the resource is rich, so that the research on the preparation process of low-cost and high-quality gardenia series products is further developed, and the comprehensive development and utilization of gardenia are realized.
Disclosure of Invention
The invention aims to provide gardenia facial mask powder and a preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
a facial mask powder comprises (by weight parts) iridoid glycoside powder 25-35 parts of fructus Gardeniae, flos Rhododendri Simsii extract 5-10 parts, flos Gardeniae extract 1-5 parts, white tea extract 5-15 parts, konjac glucomannan 20-23 parts, alginate jelly 12-16 parts, and collagen 10-16 parts.
Preferably, the mask powder comprises the following raw materials, by weight, 30 parts of gardenia iridoid glycoside powder, 8 parts of rhododendron extract, 3 parts of gardenia extract, 10 parts of white tea extract, 22 parts of konjac glucomannan, 14 parts of seaweed gel and 13 parts of collagen.
The preparation method of the gardenia iridoid glycoside powder comprises the following steps:
(1) freeze-drying: selecting high-quality gardenia and gardenia, respectively soaking the gardenia and the gardenia in 0.1wt.% of food-grade hydrogen peroxide solution for 4-6 min, washing the gardenia and the gardenia with clear water, draining off water, respectively freeze-drying the pre-treated gardenia and the gardenia in a vacuum freeze-drying machine, and requiring that the water content of the freeze-dried gardenia and the gardenia is below 10%;
(2) shell breaking: breaking the shell of gardenia, and removing the shell of gardenia;
(3) degreasing treatment: pulverizing fructus Gardeniae, sieving with 10-18 mesh sieve, and deoiling in supercritical carbon dioxide extraction kettle with the following parameters: the extraction pressure is 25-30MPa, the temperature of the extraction preheater is set to be 40-45 ℃, the carbon dioxide flow is 600-800L/H, the separation pressure is 10MPa, the separation temperature is 50-55 ℃, the separation time is 2 hours, and the crude fat content of the deoiled gardenia is less than 1.0 percent;
(4) superfine grinding: micronizing the degreased gardenia and the freeze-dried gardenia by carbon dioxide supercritical extraction to 350-mesh and 500-mesh to obtain gardenia powder;
(5) extracting iridoid glycosides: the solid-liquid mass ratio of the gardenia powder to the edible ethanol is 1: (5-8), the microwave power is 500-2000 w, the extraction temperature is 40-50 ℃, and the extraction time is 40-60 min;
(6) clarifying and filtering: centrifuging and filtering the solution extracted by the microwave, taking supernatant, adding 0.06-0.1 wt.% of pectinase, 0.03-0.05 wt.% of chitosan and 1.0-2.0 wt.% of honey into the supernatant, performing composite clarification, treating at 40-50 ℃ for 3 hours, and filtering;
(7) concentration: concentrating the supernatant obtained in the step (6) at a vacuum degree of 100kPa and a temperature of 50-55 ℃ and a density of 1.2-1.4 to obtain iridoid glycoside concentrated paste;
(8) freeze-drying: freeze-drying the iridoid glycoside concentrated paste at-45 deg.C under vacuum pressure of 50-100Pa for 25h until the water content of iridoid glycoside extract is less than 2%, and preparing into iridoid glycoside powder. The extraction rate reaches 75-85%.
The application method of the facial mask comprises the following steps: each packet is typically 1.0 g. When in use, the package is opened, 100ml of hot water with the temperature of 85 ℃ is taken, and the mask powder is slowly and uniformly poured into the hot water while stirring. And then stirring until the product powder is fully dissolved, pouring into a membrane plate, cooling and forming to obtain the facial mask, applying the facial mask on the face, and staying for 20-30 minutes.
The invention has the advantages that:
1. the invention has remarkable curative effect on whelk suppuration and cystic acne, and the components are pure plant components, no preservative and additive, and no stimulation and harm to skin. Iridoid glycoside extract in fructus Gardeniae has antibacterial and anti-inflammatory effects, and can inhibit various bacteria causing acne; the azalea acid in the rhododendron has the effects of regulating lipid secretion, inhibiting seborrheic sebum, removing acne, inhibiting abnormal keratinization process of epidermis and whitening and removing freckles; the seaweed gel has moisture keeping, antibacterial, antiaging, antiinflammatory, lipid secretion improving, melanin synthesis inhibiting, and pigment speckle reducing effects; the catechin in the white tea has the oxidation resistance, can strengthen the skin resistance and can relieve the aging; the polyphenol component in the white tea can improve the toxin expelling and defense effects of human bodies; the collagen has effects of keeping moisture, repairing and brightening skin, improving metabolism of skin cells, and relieving aging. The konjac glucomannan has film forming property, fruit fiber, non-woven fabric and the like are not needed as media, and effective factors of the mask cannot be lost due to mask paper;
3. the product of the invention has good moisturizing effect, is convenient to use, low-carbon and environment-friendly, and the waste facial mask can be completely biodegraded.
4. The facial mask contains gardenia iridoid glycoside substances, and the white tea, the konjac glucomannan and the seaweed gel are all pure plant components, have no preservative, do not stimulate and damage the skin, are accompanied with the unique fragrance of the white tea, and have good curative effect on acne suppuration and cystic acne formation.
Detailed Description
Example 1
A mask powder of fructus Gardeniae comprises (by weight parts) iridoid glycoside powder 30, flos Rhododendri Simsii extract 8, flos Gardeniae extract 3, white tea extract 10, konjac glucomannan 22, alginate jelly 14, and collagen 13.
The preparation method of the gardenia iridoid glycoside powder comprises the following steps:
(1) freeze-drying: selecting high-quality gardenia and gardenia, respectively soaking the gardenia and the gardenia in 0.1wt.% of food-grade hydrogen peroxide solution for 5min, washing the gardenia and the gardenia with clear water, draining off water, respectively freeze-drying the pre-treated gardenia and the gardenia in a vacuum freeze-drying machine, wherein the water content of the freeze-dried gardenia and the gardenia is 8%;
(2) shell breaking: breaking the shell of gardenia, and removing the shell of gardenia;
(3) degreasing treatment: taking the crushed gardenia, sieving the crushed gardenia through a 15-mesh sieve, and then putting the crushed gardenia into a carbon dioxide supercritical extraction kettle for deoiling, wherein the carbon dioxide supercritical extraction parameters are as follows: the extraction pressure is 28MPa, the temperature of an extraction preheater is set to be 43 ℃, the carbon dioxide flow is 700L/H, the separation pressure is 10MPa, the separation temperature is 53 ℃, the separation time is 2 hours, and the crude fat content of the deoiled gardenia is less than 1.0 percent;
(4) superfine grinding: extracting defatted fructus Gardeniae and lyophilized flos Gardeniae by supercritical carbon dioxide extraction, and micronizing to 400 mesh to obtain fructus Gardeniae powder;
(5) extracting iridoid glycosides: the solid-liquid mass ratio of the gardenia powder to the edible ethanol is 1: 7, extracting for 50min at the microwave power of 1000w and the extraction temperature of 45 ℃;
(6) clarifying and filtering: centrifuging and filtering the solution obtained by microwave extraction, taking supernatant, adding pectinase 0.06%, chitosan 0.03% and honey 1.0% to perform composite clarification, treating at 45 deg.C for 3h, and filtering;
(7) concentration: concentrating the supernatant obtained in step (6) at a vacuum degree of 100kPa and a temperature of 52 ℃ to a density of 1.2 to obtain iridoid glycoside concentrated paste;
(8) freeze-drying: freeze-drying the iridoid glycoside concentrated paste at-45 deg.C under vacuum pressure of 80Pa for 25h to obtain iridoid glycoside powder with water content of 1%. The extraction rate reaches 85 percent.
Example 2
A gardenia facial mask comprises the following raw materials, by weight, 25 parts of gardenia iridoid glycoside powder, 5 parts of azalea extract freeze-dried powder, 1 part of gardenia extract, 5 parts of white tea extract, 20 parts of konjac glucomannan, 12 parts of alginate jelly and 10 parts of collagen.
The preparation method of the gardenia iridoid glycoside powder comprises the following steps:
(1) freeze-drying: selecting high-quality gardenia and gardenia, respectively soaking the gardenia and the gardenia in 0.1wt.% of food-grade hydrogen peroxide solution for 4 min, washing the gardenia and the gardenia with clear water, draining off water, respectively freeze-drying the pre-treated gardenia and the gardenia in a vacuum freeze-drying machine, and requiring that the water content of the freeze-dried gardenia and the gardenia is below 10%;
(2) shell breaking: breaking the shell of gardenia, and removing the shell of gardenia;
(3) degreasing treatment: taking the crushed gardenia, sieving the crushed gardenia through a sieve with 10 meshes, and then putting the crushed gardenia into a carbon dioxide supercritical extraction kettle for deoiling, wherein the carbon dioxide supercritical extraction parameters are as follows: the extraction pressure is 25MPa, the temperature of an extraction preheater is set to be 40 ℃, the carbon dioxide flow is 600L/H, the separation pressure is 10MPa, the separation temperature is 50 ℃, the separation time is 2 hours, and the crude fat content of the deoiled gardenia is less than 1.0 percent;
(4) superfine grinding: micronizing fructus Gardeniae degreased by supercritical carbon dioxide extraction and lyophilized fructus Gardeniae flower to 350 mesh to obtain fructus Gardeniae powder;
(5) extracting iridoid glycosides: the solid-liquid mass ratio of the gardenia powder to the edible ethanol is 1: 5, extracting for 40min at the microwave power of 500w and the extraction temperature of 40 ℃;
(6) clarifying and filtering: centrifuging and filtering the solution obtained by microwave extraction, taking supernatant, adding pectinase 0.8%, chitosan 0.04% and honey 1.5% to perform composite clarification, treating at 40 deg.C for 3h, and filtering;
(7) concentration: concentrating the supernatant obtained in step (6) at 50 deg.C under 100kPa to obtain iridoid glycoside concentrated extract with density of 1.3;
(8) freeze-drying: freeze-drying the iridoid glycoside concentrated paste at-45 deg.C under vacuum pressure of 50Pa for 25h to obtain iridoid glycoside powder with water content of 1%. The extraction rate reaches 75 percent.
Example 3
A gardenia facial mask comprises the following raw materials, by weight, 35 parts of gardenia iridoid glycoside powder, 10 parts of azalea extract freeze-dried powder, 5 parts of gardenia extract, 15 parts of white tea extract, 23 parts of konjac glucomannan, 16 parts of alginate jelly and 16 parts of collagen.
The preparation method of the gardenia iridoid glycoside powder comprises the following steps:
(1) freeze-drying: selecting high-quality gardenia and gardenia, respectively soaking the gardenia and the gardenia in 0.1wt.% of food-grade hydrogen peroxide solution for 6min, washing the gardenia and the gardenia with clear water, draining off water, respectively freeze-drying the pre-treated gardenia and the gardenia in a vacuum freeze-drying machine, and requiring that the water content of the freeze-dried gardenia and the gardenia is below 10%;
(2) shell breaking: breaking the shell of gardenia, and removing the shell of gardenia;
(3) degreasing treatment: taking the crushed gardenia, sieving the crushed gardenia through a sieve with 18 meshes, and then putting the crushed gardenia into a carbon dioxide supercritical extraction kettle for deoiling, wherein the carbon dioxide supercritical extraction parameters are as follows: the extraction pressure is 30MPa, the temperature of an extraction preheater is set to be 45 ℃, the carbon dioxide flow is 800L/H, the separation pressure is 10MPa, the separation temperature is 55 ℃, the separation time is 2 hours, and the crude fat content of the deoiled gardenia is less than 1.0 percent;
(4) superfine grinding: micronizing fructus Gardeniae degreased by supercritical carbon dioxide extraction and lyophilized fructus Gardeniae flower to 500 mesh to obtain fructus Gardeniae powder;
(5) extracting iridoid glycosides: the solid-liquid mass ratio of the gardenia powder to the edible ethanol is 1: 8, extracting for 60min at the extraction temperature of 50 ℃ with the microwave power of 2000 w;
(6) clarifying and filtering: centrifuging and filtering the solution obtained by microwave extraction, taking supernatant, adding pectinase 0.1%, chitosan 0.05% and honey 2.0% to perform composite clarification, treating at 50 deg.C for 3h, and filtering;
(7) concentration: concentrating the supernatant obtained in step (6) at vacuum degree of 100kPa and temperature of 55 deg.C to density of 1.5 to obtain iridoid glycoside concentrated paste;
(8) freeze-drying: freeze-drying the iridoid glycoside concentrated paste at-45 deg.C under vacuum pressure of 100Pa for 25h to obtain iridoid glycoside powder with water content of 1%. The extraction rate reaches 80 percent.
Application examples
The test method comprises the following steps: 40 volunteers, who are 16-25 years old, mainly students and office clerks, and 20 men and women, all had acne of different degrees on face, and had acne and inflammation papules of different degrees on face, and the facial mask powder of the invention was used for improving facial skin conditions. The mask powder is coated by 1 bag every night, 100ml of hot water with the temperature of 85 ℃ is taken, and the mask powder is slowly and uniformly poured into the hot water while stirring. And then stirring until the product powder is fully dissolved, pouring into a membrane plate, cooling and forming to obtain the facial mask, applying the facial mask on the face, and staying for 20-30 minutes. The effect judgment standard refers to three standards of effectiveness, effectiveness and ineffectiveness: the effect is obvious that the related symptoms are obviously relieved; effective in relieving the associated symptoms; failure is no change in symptoms.
And (3) test results: after most of the medicines are continuously used for 7 days, the related symptoms are relieved, and after the medicines are continuously used for 15 days, the symptoms are obviously improved. In 40 cases of clinical trials, 30 patients have significant effect, 7 patients have effect, and 3 patients have no effect, and the total effective rate is 92.5%. Therefore, the facial mask powder has certain effect of improving facial skin for facial acne, comedo and inflammatory papule patients
Typical examples of the tests
Wangzhi, male age 19, student, severe acne, more acne and inflammatory papules on face. After the mask powder is used for 10 days, the symptoms of pimple and pustule are obviously improved, and after the mask powder is continuously used for 20 days, the inflammation pimple disappears, and as long as a small amount of acne is generated, the pimple is healed without any side effect.
In a certain year, women are 25 years old, and the civilians are moderate acne, and the face has more comedones and inflammatory papules. After the mask powder is used for 7 days, papules and pustules are obviously improved, and after the mask powder is continuously used for 15 days, inflammatory papules disappear, and only a small amount of acne is needed, the acne is healed without any side effect.
Pool, female 18 years old, student, mild acne, minor acne and inflammatory papules on the face. After the mask powder is used for 5 days, the symptoms of pimple are obviously improved, and after the mask powder is continuously used for 10 days, the inflammation pimple completely disappears and is healed without any side effect.
The above description is only a preferred embodiment of the present invention, and all equivalent changes and modifications made in accordance with the claims of the present invention should be covered by the present invention.
Claims (2)
1. The gardenia facial mask powder is characterized in that: the mask powder comprises the following raw materials, by weight, 25-35 parts of gardenia iridoid glycoside powder, 5-10 parts of rhododendron extract, 1-5 parts of gardenia extract, 5-15 parts of white tea extract, 20-23 parts of konjac glucomannan, 12-16 parts of seaweed gel and 10-16 parts of collagen;
the preparation method of the gardenia iridoid glycoside powder comprises the following steps:
(1) freeze-drying: selecting high-quality gardenia and gardenia, respectively soaking the gardenia and the gardenia in 0.1wt.% of food-grade hydrogen peroxide solution for 4-6 min, washing the gardenia and the gardenia with clear water, draining off water, respectively freeze-drying the pre-treated gardenia and the gardenia in a vacuum freeze-drying machine, and requiring that the water content of the freeze-dried gardenia and the gardenia is below 10%;
(2) shell breaking: breaking the shell of gardenia, and removing the shell of gardenia;
(3) degreasing treatment: pulverizing fructus Gardeniae, sieving with 10-18 mesh sieve, and deoiling in supercritical carbon dioxide extraction kettle with the following parameters: the extraction pressure is 25-30MPa, the temperature of the extraction preheater is set to be 40-45 ℃, the carbon dioxide flow is 600-800L/H, the separation pressure is 10MPa, the separation temperature is 50-55 ℃, the separation time is 2 hours, and the crude fat content of the deoiled gardenia is less than 1.0 percent;
(4) superfine grinding: micronizing the degreased gardenia and the freeze-dried gardenia by carbon dioxide supercritical extraction to 350-mesh and 500-mesh to obtain gardenia powder;
(5) extracting iridoid glycosides: the solid-liquid mass ratio of the gardenia powder to the edible ethanol is 1: (5-8), the microwave power is 500-2000 w, the extraction temperature is 40-50 ℃, and the extraction time is 40-60 min;
(6) clarifying and filtering: centrifuging and filtering the solution extracted by the microwave, taking supernatant, adding 0.06-0.1 wt.% of pectinase, 0.03-0.05 wt.% of chitosan and 1.0-2.0 wt.% of honey into the supernatant, performing composite clarification, treating at 40-50 ℃ for 3 hours, and filtering;
(7) concentration: concentrating the supernatant obtained in the step (6) at a vacuum degree of 100kPa and a temperature of 50-55 ℃ and a density of 1.2-1.4 to obtain iridoid glycoside concentrated paste;
(8) freeze-drying: freeze-drying the iridoid glycoside concentrated paste at-45 deg.C under vacuum pressure of 50-100Pa for 25h until the water content of iridoid glycoside extract is less than 2%, and preparing into iridoid glycoside powder.
2. The gardenia facial mask powder according to claim 1, characterized in that: the facial mask comprises the following raw materials of, by weight, 30 parts of gardenia iridoid glycoside powder, 8 parts of rhododendron extract, 3 parts of gardenia extract, 10 parts of white tea extract, 22 parts of konjac glucomannan, 14 parts of seaweed gel and 13 parts of collagen.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710320222.5A CN107412040B (en) | 2017-05-09 | 2017-05-09 | Gardenia facial mask powder and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710320222.5A CN107412040B (en) | 2017-05-09 | 2017-05-09 | Gardenia facial mask powder and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107412040A CN107412040A (en) | 2017-12-01 |
| CN107412040B true CN107412040B (en) | 2020-06-16 |
Family
ID=60425458
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710320222.5A Active CN107412040B (en) | 2017-05-09 | 2017-05-09 | Gardenia facial mask powder and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107412040B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117797055B (en) * | 2024-02-29 | 2024-06-18 | 江西瑞秀朗科技有限公司 | Compound essential oil for improving skin aging and skin care product composition containing compound essential oil |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104257587A (en) * | 2014-10-08 | 2015-01-07 | 杜翔宇 | Salvia miltiorrhiza and gardenia mask |
| CN104306251A (en) * | 2014-10-08 | 2015-01-28 | 苏州市天灵中药饮片有限公司 | Traditional Chinese medicine facial mask for treating acne and preparation method of traditional Chinese medicine facial mask |
| CN104666511A (en) * | 2014-11-27 | 2015-06-03 | 安徽农业大学 | Technique for preparing gardenia iridoid glycoside compound employing leaves of gardenia plant |
| CN104996579A (en) * | 2015-06-25 | 2015-10-28 | 浙江农林大学 | Plant milk and preparation method thereof |
| CN105030609A (en) * | 2015-08-14 | 2015-11-11 | 武汉狼堡科技有限公司 | Gardenoside soft facial mask and preparation method thereof |
| CN105342952A (en) * | 2015-11-27 | 2016-02-24 | 金建文 | Conditioning cream prepared by Chinese herb medicine extract superfine powder and with functions of acne removing and whitening and preparation method of conditioning cream |
| CN106496292A (en) * | 2015-09-08 | 2017-03-15 | 中国中医科学院中药研究所 | A kind of method for preparing 6 iridoid glycoside constituents from Fructus Gardeniae simultaneously |
-
2017
- 2017-05-09 CN CN201710320222.5A patent/CN107412040B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104257587A (en) * | 2014-10-08 | 2015-01-07 | 杜翔宇 | Salvia miltiorrhiza and gardenia mask |
| CN104306251A (en) * | 2014-10-08 | 2015-01-28 | 苏州市天灵中药饮片有限公司 | Traditional Chinese medicine facial mask for treating acne and preparation method of traditional Chinese medicine facial mask |
| CN104666511A (en) * | 2014-11-27 | 2015-06-03 | 安徽农业大学 | Technique for preparing gardenia iridoid glycoside compound employing leaves of gardenia plant |
| CN104996579A (en) * | 2015-06-25 | 2015-10-28 | 浙江农林大学 | Plant milk and preparation method thereof |
| CN105030609A (en) * | 2015-08-14 | 2015-11-11 | 武汉狼堡科技有限公司 | Gardenoside soft facial mask and preparation method thereof |
| CN106496292A (en) * | 2015-09-08 | 2017-03-15 | 中国中医科学院中药研究所 | A kind of method for preparing 6 iridoid glycoside constituents from Fructus Gardeniae simultaneously |
| CN105342952A (en) * | 2015-11-27 | 2016-02-24 | 金建文 | Conditioning cream prepared by Chinese herb medicine extract superfine powder and with functions of acne removing and whitening and preparation method of conditioning cream |
Also Published As
| Publication number | Publication date |
|---|---|
| CN107412040A (en) | 2017-12-01 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103494747B (en) | Compound peony skin-caring essential oil and preparation method thereof | |
| CN103751058B (en) | Peony skin care product and preparation method thereof | |
| CN104814908A (en) | Mask with effects of resisting wrinkle and tendering skin | |
| CN105213284A (en) | A kind of anti-acne moisturiser and preparation method thereof | |
| CN108392445B (en) | Herbal antipruritic lotion | |
| CN109771348B (en) | Whitening, moisturizing and wrinkle-removing face cream rich in natural product extract components and preparation method thereof | |
| CN105055251A (en) | Anti-aging cosmetic and preparation method thereof | |
| CN104013564A (en) | Oil-tea camellia honey moisturizer | |
| CN111973481A (en) | Blue ketone peptide repair essence and preparation method thereof | |
| CN113018238A (en) | Anti-bacterial, anti-inflammatory, refreshing and skin-benefiting acne-removing gel and preparation method thereof | |
| CN110559229A (en) | Night cream containing cannabidiol CBD nano-emulsion and preparation method thereof | |
| CN107157835A (en) | A kind of compound essential oil for preventing or repairing striae of pregnancy and preparation method thereof | |
| CN105326733A (en) | Pore-fining liquid facial cleanser and preparation method thereof | |
| CN105193693A (en) | Pore refining cream containing deep-sea essence and preparation method of cream | |
| CN105434195A (en) | Composition with functions of removing acne and inhibiting pockmark generation and application thereof | |
| CN113797143A (en) | Bromelain acne-removing essence and preparation method thereof | |
| CN103772525A (en) | Method for extracting dragon fruit flower polysaccharide | |
| KR101168796B1 (en) | Skin care cosmetic composition | |
| CN107412040B (en) | Gardenia facial mask powder and preparation method thereof | |
| CN101869542A (en) | Toner comprising pawpaw extract and lotus leaf extract and preparation method thereof | |
| CN105168104A (en) | Infant body lotion containing sea fennel extract and preparation method thereof | |
| CN111973544A (en) | Carnosine firming lifting mask and preparation method thereof | |
| CN105213285A (en) | A kind of anti-acne facial cleanser and preparation method thereof | |
| KR101163069B1 (en) | Cosmetic composition for anti-blemish and anti-wrinkle and method for manufacturing thereof | |
| KR20150109031A (en) | Cosmetic composition and a method of manufacturing |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |