CN107384742A - The preparation method of setose thistle purple dendrobium health-care vinegar - Google Patents
The preparation method of setose thistle purple dendrobium health-care vinegar Download PDFInfo
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- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12J—VINEGAR; PREPARATION OR PURIFICATION THEREOF
- C12J1/00—Vinegar; Preparation or purification thereof
- C12J1/04—Vinegar; Preparation or purification thereof from alcohol
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
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- A61K36/18—Magnoliophyta (angiosperms)
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- A61K36/46—Eucommiaceae (Eucommia family), e.g. hardy rubber tree
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/70—Polygonaceae (Buckwheat family), e.g. spineflower or dock
- A61K36/704—Polygonum, e.g. knotweed
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- A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
- A61K36/8969—Polygonatum (Solomon's seal)
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/899—Poaceae or Gramineae (Grass family), e.g. bamboo, corn or sugar cane
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
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- A61K36/8994—Coix (Job's tears)
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Abstract
The invention discloses a kind of preparation method of setose thistle purple dendrobium health-care vinegar, belong to health-care vinegar manufacture field.It is characterized in that：Described setose thistle stem of noble dendrobium health-care vinegar, the high stem of noble dendrobium of health value, setose thistle are used as raw material, add the nutritional ingredient of health-care vinegar, after respective pretreatment, by extracting, making the active material brewageed process, raw material can be sufficiently reserved of fermenting grain, filtering, fermentation, ageing, flavouring after-ripening and packaging, the nutritive value of health-care vinegar is improved, make the mouthfeel of health-care vinegar soft pure, also with health-care efficacies such as reinforcing stomach reg fluid, nourishing Yin and clearing heat, hypotensives.
Description
Technical field
The present invention relates to a kind of preparation method of health-care vinegar, more particularly, to a kind of making of setose thistle purple dendrobium health-care vinegar
Method.
Background technology
Setose thistle, Chinese medicine name, it is composite family (Compositae) tubular flower subfamily cynara scolymus race (Cvnareae)
Cirsium (Cirsium Mill.) plant C. japonicum DC. dry aerial parts or root.Perennial herb
, wild in hillside, roadside etc., summer, season in autumn two tap aerial part when the flowers are in blossom, remove impurity, dry.Grass contains alkaloid, waved
Hair oil.Root is containing taraxasterylacetate, stigmasterol, the amyrins of a mono-, B- amyrins, B- sitosterol.Fresh leaf is spent containing Linaria vulgaris
Glucoside 2.1%.Root contains volatile oil, contains 4 kinds of unsaturated hydrocarbons in oil, is aplotaxene, dihydro aplotaxene, tetrahydrochysene list purple
China fir alkene, hexahydroaplotaxene.Function controls haematemesis, bleeding from five sense organs or subcutaneous tissue, hematuria, blood strangury, metrorrhagia, under band, intestines wind, and acute appendicitis, large carbuncle pyogenic infections, malignant boil
Sore.Infusion, the infusion of ethanol one and the alcohol leaching liquid of pharmacology setose thistle, are tested in anesthetized animals such as dog, cat and rabbits, it was demonstrated that have
Hypotensive activity.Field thistle is ibid tested, it was demonstrated that has the more significant and lasting large and small Ji of hypotensive activity function to have heat-clearing
Removing toxic substances, anti-inflammatory, hemostasis and recovery liver function, the effect for promoting liver cell regeneration, it is yellow suitable for the inflammatory bleeding of acute fever
Subcutaneous ulcer, hepatitis, heat gonorrhea, hematuria etc..
Purple dendrobium, it is a kind of orchid family Dendrobium Sw using dendrobium devonianum as representative;Dendrobium devonianum also known as purple skin are blue, are
Orchid dendrobium devonianum, meridian distribution of property and flavor:It is slightly cold;It is sweet;Return stomach, kidney channel.Cure mainly:Traumatic injury is controlled in external application, the injury of the tissues of fracturing;It is for oral administration
Control throat to itch, cough.Reinforcing stomach reg fluid, nourishing Yin and clearing heat.For impairment of yin body fluid deficiency, dry polydipsia, deficiency of food is retched, and abnormal heat, mesh are dark after being ill
It is not clear.Certain antipyretic effect;Gastric secretion can be promoted, it is aid digestion;There is metabolic, the anti-ageing effect of waiting for a long time of enhancing.
At present, setose thistle, purple dendrobium is used to be processed into setose thistle purple dendrobium health-care vinegar for raw material, there are no correlation
Report and launch, a new way is provided for the deep processing of the stem of noble dendrobium and setose thistle.
The content of the invention
It is an object of the invention to provide a kind of preparation method of setose thistle purple dendrobium health-care vinegar, using the big of nutrition and health care
Ji, purple dendrobium are raw material, are processed into setose thistle stem of noble dendrobium health-care vinegar, and a new way is provided for the deep processing of the stem of noble dendrobium and setose thistle.
The technical scheme adopted by the invention to solve the technical problem is that：
A kind of preparation method of setose thistle purple dendrobium health-care vinegar, it is characterised in that：Through pretreatment of raw material, extraction, make fermenting grain,
Filtering, fermentation, ageing, flavouring after-ripening and packaging brewage process, and described processing method uses following steps：
A, setose thistle pre-processes：The setose thistle of dry and high quality is selected, adds appropriate Bark of Eucommia Ulmoides, polygoni cuspidati,radix, after cleaning, low temperature drying, is broken
Wall crushes, and setose thistle fine powder is made；
B, the stem of noble dendrobium pre-processes：High-quality purple dendrobium is selected, a little radix polygonati officinalis, Rui cores is added, after cleaning, is put into baking oven and softens,
It is 55 DEG C to set temperature, and after low temperature bakes 30min, break process is freeze-dried, and broken wall crushes, and stem of noble dendrobium fine powder is made；
C, extract：Setose thistle fine powder, stem of noble dendrobium fine powder are pressed 2:After 3 ratio is well mixed, mixed material is made, using multistage continuous
Countercurrent extraction machine, one end add 35 DEG C of softened waters, and the other end adds mixed material, realize that multiple stage continuous adverse current extracts, just extraction
It is 45 DEG C that stage, which sets temperature, time 10min；It is 50 DEG C that the deep extraction stage, which sets temperature, time 8min；Ooze the stage of washing
Extracting temperature is 55 DEG C, time 3min, filtering, extract solution is made；
D, fermenting grain is made：It is matrix to select high-quality glutinous rice, adds appropriate blood wheat and coix seed, cleans impurity elimination, enters pot and cook
Afterwards, distiller's yeast is added when being cooled to 38 DEG C, the weight ratio of ripe mixed material and distiller's yeast is 50:1, remix infiltration, heat-preservation fermentation 8
My god, every stirring in 10 hours once, fermenting grain is made；
E, filter：Using plate and frame filter press, fermenting grain is filtered, obtains zymocyte liquid and filter residue；
F, ferment：Take the extract solution of 30 parts by weight, the zymocyte liquid of 55 parts by weight, the material residue of 10 parts by weight, the grape of 5 parts by weight
Liquid glucose, it is well mixed, accesses 12% acetic acid bacteria, the fermentation of eddy current type acetic acid deep drainpipe is carried out using Fring types acidifier, 32
Fermented 10 days under conditions of DEG C, until acidity no longer rises, the acidity of adjustment acetic fermentation unstrained spirits is 12g/100ml, fermentation ends；
G, ageing：By the filtered equipment refined filtration of acetic fermentation unstrained spirits, filtrate is made；Filtrate is pumped into wooden barrel, using microwave radiation technology
Cold treatment accelerate filtrate ageing, microwave frequency 220MHz, 2 days cold treatment time, 6 DEG C of temperature, add a little chitosan with
Alum is clarified, and extracts to obtain clarified solution；
H, flavouring after-ripening：Clarified solution is placed under air-proof condition and carries out flavouring after-ripening in 55 DEG C, is terminated after 1 day, setose thistle stone is made
Dry measure used in former times health-care vinegar；
I, pack：Setose thistle stem of noble dendrobium health-care vinegar is subjected to sterile filling with vial, after packing, as finished product.
Beneficial effect：The setose thistle stem of noble dendrobium health-care vinegar that this method makes, uses the high stem of noble dendrobium of health value, setose thistle as raw material,
The nutritional ingredient of health-care vinegar is added, after respective pretreatment, after extracting, making fermenting grain, filtering, fermentation, ageing, flavouring
Ripe and packaging the active material brewageed process, can be sufficiently reserved raw material, improves the nutritive value of health-care vinegar, makes health-care vinegar
Mouthfeel it is soft pure, A sweety scent assails the nostrils, also with health-care efficacies such as reinforcing stomach reg fluid, nourishing Yin and clearing heat, hypotensive, cooling blood and hemostasis.
Embodiment
Embodiment 1：
A kind of preparation method of setose thistle purple dendrobium health-care vinegar, it is characterised in that：Through pretreatment of raw material, extraction, make fermenting grain,
Filtering, fermentation, ageing, flavouring after-ripening and packaging brewage process, using following steps：
A, setose thistle pre-processes：The setose thistle of dry and high quality is selected, adds the appropriate bighead atractylodes rhizome, the fruit-rind of Chinese trichosanthes, after cleaning, low temperature drying, broken wall
Crush, setose thistle fine powder is made；
B, the stem of noble dendrobium pre-processes：High-quality purple dendrobium is selected, adds a little Radix Rhapontici seu Radix Echinopsis root, radix polygonati officinalis, after cleaning, is put into soft in baking oven
Change, it is 55 DEG C to set temperature, and after low temperature bakes 30min, break process is freeze-dried, and broken wall crushes, and stem of noble dendrobium fine powder is made；
C, extract：Setose thistle fine powder, stem of noble dendrobium fine powder are pressed 1:After 1 ratio is well mixed, mixed material is made, using multistage continuous
Countercurrent extraction machine, one end add 35 DEG C of softened waters, and the other end adds mixed material, realize that multiple stage continuous adverse current extracts, just extraction
It is 45 DEG C that stage, which sets temperature, time 10min；It is 50 DEG C that the deep extraction stage, which sets temperature, time 8min；Ooze the stage of washing
Extracting temperature is 55 DEG C, time 3min, filtering, extract solution is made；
D, fermenting grain is made：It is matrix to select high-quality glutinous rice, adds appropriate bitter buckwheat and coix seed, cleans impurity elimination, enters pot and cook
Afterwards, distiller's yeast is added when being cooled to 38 DEG C, the weight ratio of ripe mixed material and distiller's yeast is 50:1, remix infiltration, heat-preservation fermentation 8
My god, every stirring in 10 hours once, fermenting grain is made；
E, filter：Using plate and frame filter press, fermenting grain is filtered, obtains zymocyte liquid and filter residue；
F, ferment：Take the extract solution of 30 parts by weight, the zymocyte liquid of 55 parts by weight, the material residue of 10 parts by weight, the grape of 5 parts by weight
Liquid glucose, it is well mixed, accesses 12% acetic acid bacteria, the fermentation of eddy current type acetic acid deep drainpipe is carried out using Fring types acidifier, 32
Fermented 10 days under conditions of DEG C, until acidity no longer rises, the acidity of adjustment acetic fermentation unstrained spirits is 12g/100ml, fermentation ends；
G, ageing：By the filtered equipment refined filtration of acetic fermentation unstrained spirits, filtrate is made；Filtrate is pumped into wooden barrel, using microwave radiation technology
Cold treatment accelerate filtrate ageing, microwave frequency 220MHz, 2 days cold treatment time, 6 DEG C of temperature, add a little chitosan with
Alum is clarified, and extracts to obtain clarified solution；
H, flavouring after-ripening：Clarified solution is placed under air-proof condition and carries out flavouring after-ripening in 55 DEG C, is terminated after 1 day, setose thistle stone is made
Dry measure used in former times health-care vinegar；
I, pack：Setose thistle stem of noble dendrobium health-care vinegar is subjected to sterile filling with vial, after packing, as finished product.
Embodiment 2：
A kind of preparation method of setose thistle purple dendrobium health-care vinegar, it is characterised in that：Through pretreatment of raw material, extraction, make fermenting grain,
Filtering, fermentation, ageing, flavouring after-ripening and packaging brewage process, using following steps：
A, setose thistle pre-processes：The setose thistle of dry and high quality is selected, adds appropriate radix bardanae, adenophora tetraphylla, after cleaning, low temperature drying, is broken
Wall crushes, and setose thistle fine powder is made；
B, the stem of noble dendrobium pre-processes：High-quality purple dendrobium is selected, adds a little fruit of Cherokee rose, the root bark of white mulberry, after cleaning, is put into soft in baking oven
Change, it is 55 DEG C to set temperature, and after low temperature bakes 30min, break process is freeze-dried, and broken wall crushes, and stem of noble dendrobium fine powder is made；
C, extract：Setose thistle fine powder, stem of noble dendrobium fine powder are pressed 3:After 1 ratio is well mixed, mixed material is made, using multistage continuous
Countercurrent extraction machine, one end add 35 DEG C of softened waters, and the other end adds mixed material, realize that multiple stage continuous adverse current extracts, just extraction
It is 45 DEG C that stage, which sets temperature, time 10min；It is 50 DEG C that the deep extraction stage, which sets temperature, time 8min；Ooze the stage of washing
Extracting temperature is 55 DEG C, time 3min, filtering, extract solution is made；
D, fermenting grain is made：It is matrix to select high-quality glutinous rice, adds appropriate dregs of beans and blood wheat, cleans impurity elimination, is entered after pot cooks,
Add distiller's yeast when being cooled to 38 DEG C, the weight ratio of ripe mixed material and distiller's yeast is 35:1, remix infiltration, heat-preservation fermentation 8 days, often
Every stirring in 10 hours once, fermenting grain is made；
E, filter：Using plate and frame filter press, fermenting grain is filtered, obtains zymocyte liquid and filter residue；
F, ferment：Take the extract solution of 30 parts by weight, the zymocyte liquid of 55 parts by weight, the material residue of 10 parts by weight, the grape of 5 parts by weight
Liquid glucose, it is well mixed, accesses 12% acetic acid bacteria, the fermentation of eddy current type acetic acid deep drainpipe is carried out using Fring types acidifier, 32
Fermented 10 days under conditions of DEG C, until acidity no longer rises, the acidity of adjustment acetic fermentation unstrained spirits is 12g/100ml, fermentation ends；
G, ageing：By the filtered equipment refined filtration of acetic fermentation unstrained spirits, filtrate is made；Filtrate is pumped into wooden barrel, using microwave radiation technology
Cold treatment accelerate filtrate ageing, microwave frequency 220MHz, 2 days cold treatment time, 6 DEG C of temperature, add a little chitosan with
Alum is clarified, and extracts to obtain clarified solution；
H, flavouring after-ripening：Clarified solution is placed under air-proof condition and carries out flavouring after-ripening in 55 DEG C, is terminated after 1 day, setose thistle stone is made
Dry measure used in former times health-care vinegar；
I, pack：Setose thistle stem of noble dendrobium health-care vinegar is subjected to sterile filling with vial, after packing, as finished product.
Part that the present invention does not relate to is same as the prior art or can be realized using prior art.
Claims (1)
1. a kind of preparation method of setose thistle purple dendrobium health-care vinegar, it is characterised in that through pretreatment of raw material, extraction, make and ferment
Unstrained spirits, filtering, fermentation, ageing, flavouring after-ripening and packaging brewage process, and described processing method uses following steps：
A, setose thistle pre-processes：The setose thistle of dry and high quality is selected, adds appropriate Bark of Eucommia Ulmoides, polygoni cuspidati,radix, after cleaning, low temperature drying, is broken
Wall crushes, and setose thistle fine powder is made；
B, the stem of noble dendrobium pre-processes：High-quality purple dendrobium is selected, a little radix polygonati officinalis, Rui cores is added, after cleaning, is put into baking oven and softens,
It is 55 DEG C to set temperature, and after low temperature bakes 30min, break process is freeze-dried, and broken wall crushes, and stem of noble dendrobium fine powder is made；
C, extract：Setose thistle fine powder, stem of noble dendrobium fine powder are pressed 2:After 3 ratio is well mixed, mixed material is made, using multistage continuous
Countercurrent extraction machine, one end add 35 DEG C of softened waters, and the other end adds mixed material, realize that multiple stage continuous adverse current extracts, just extraction
It is 45 DEG C that stage, which sets temperature, time 10min；It is 50 DEG C that the deep extraction stage, which sets temperature, time 8min；Ooze the stage of washing
Extracting temperature is 55 DEG C, time 3min, filtering, extract solution is made；
D, fermenting grain is made：It is matrix to select high-quality glutinous rice, adds appropriate blood wheat and coix seed, cleans impurity elimination, enters pot and cook
Afterwards, distiller's yeast is added when being cooled to 38 DEG C, the weight ratio of ripe mixed material and distiller's yeast is 50:1, remix infiltration, heat-preservation fermentation 8
My god, every stirring in 10 hours once, fermenting grain is made；
E, filter：Using plate and frame filter press, fermenting grain is filtered, obtains zymocyte liquid and filter residue；
F, ferment：Take the extract solution of 30 parts by weight, the zymocyte liquid of 55 parts by weight, the material residue of 10 parts by weight, the grape of 5 parts by weight
Liquid glucose, it is well mixed, accesses 12% acetic acid bacteria, the fermentation of eddy current type acetic acid deep drainpipe is carried out using Fring types acidifier, 32
Fermented 10 days under conditions of DEG C, until acidity no longer rises, the acidity of adjustment acetic fermentation unstrained spirits is 12g/100ml, fermentation ends；
G, ageing：By the filtered equipment refined filtration of acetic fermentation unstrained spirits, filtrate is made；Filtrate is pumped into wooden barrel, using microwave radiation technology
Cold treatment accelerate filtrate ageing, microwave frequency 220MHz, 2 days cold treatment time, 6 DEG C of temperature, add a little chitosan with
Alum is clarified, and extracts to obtain clarified solution；
H, flavouring after-ripening：Clarified solution is placed under air-proof condition and carries out flavouring after-ripening in 55 DEG C, is terminated after 1 day, setose thistle stone is made
Dry measure used in former times health-care vinegar；
I, pack：Setose thistle stem of noble dendrobium health-care vinegar is subjected to sterile filling with vial, packed.
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114773131A (en) * | 2022-05-23 | 2022-07-22 | 郑州昕爵生物技术有限公司 | Special suspended alcohol water-soluble fertilizer for figs and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107058046A (en) * | 2017-05-22 | 2017-08-18 | 芜湖市三山区绿色食品产业协会 | A kind of preparation method of cortex acanthopanacis stem of noble dendrobium health-care vinegar |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107058046A (en) * | 2017-05-22 | 2017-08-18 | 芜湖市三山区绿色食品产业协会 | A kind of preparation method of cortex acanthopanacis stem of noble dendrobium health-care vinegar |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114773131A (en) * | 2022-05-23 | 2022-07-22 | 郑州昕爵生物技术有限公司 | Special suspended alcohol water-soluble fertilizer for figs and preparation method thereof |
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Application publication date: 20171124 |