CN107382294B - Magnificent jade porcelain and preparation method thereof - Google Patents
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- 229910052573 porcelain Inorganic materials 0.000 title claims abstract description 40
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 239000010977 jade Substances 0.000 title description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 11
- 210000000988 bone and bone Anatomy 0.000 claims abstract description 10
- 239000000203 mixture Substances 0.000 claims abstract description 7
- 239000000126 substance Substances 0.000 claims abstract description 7
- 229910001634 calcium fluoride Inorganic materials 0.000 claims abstract description 6
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titanium dioxide Inorganic materials O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 4
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 3
- 229910052681 coesite Inorganic materials 0.000 claims abstract description 3
- 229910052593 corundum Inorganic materials 0.000 claims abstract description 3
- 229910052906 cristobalite Inorganic materials 0.000 claims abstract description 3
- 239000012535 impurity Substances 0.000 claims abstract description 3
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims abstract description 3
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 3
- 229910052682 stishovite Inorganic materials 0.000 claims abstract description 3
- 229910052905 tridymite Inorganic materials 0.000 claims abstract description 3
- 229910001845 yogo sapphire Inorganic materials 0.000 claims abstract description 3
- 239000002994 raw material Substances 0.000 claims description 19
- 239000002689 soil Substances 0.000 claims description 19
- 238000000498 ball milling Methods 0.000 claims description 12
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 10
- 239000010453 quartz Substances 0.000 claims description 8
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 claims description 7
- 239000004927 clay Substances 0.000 claims description 6
- 239000010433 feldspar Substances 0.000 claims description 6
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical compound [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 claims description 5
- 239000012065 filter cake Substances 0.000 claims description 5
- 238000010304 firing Methods 0.000 claims description 5
- 229910052742 iron Inorganic materials 0.000 claims description 5
- 238000003825 pressing Methods 0.000 claims description 5
- 238000007873 sieving Methods 0.000 claims description 5
- 239000011265 semifinished product Substances 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 2
- 239000000463 material Substances 0.000 claims 1
- 239000000919 ceramic Substances 0.000 abstract description 9
- 230000000694 effects Effects 0.000 abstract description 4
- 238000005516 engineering process Methods 0.000 abstract description 3
- 238000005286 illumination Methods 0.000 abstract description 3
- 239000000047 product Substances 0.000 description 9
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000010436 fluorite Substances 0.000 description 4
- 235000015895 biscuits Nutrition 0.000 description 3
- 229910052761 rare earth metal Inorganic materials 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 241001122767 Theaceae Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052793 cadmium Inorganic materials 0.000 description 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- -1 rare earth ion Chemical class 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000006104 solid solution Substances 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 238000002834 transmittance Methods 0.000 description 1
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/14—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silica
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- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/04—Clay; Kaolin
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- C04B33/00—Clay-wares
- C04B33/24—Manufacture of porcelain or white ware
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/447—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on phosphates, e.g. hydroxyapatite
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
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- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
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- C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
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- Compositions Of Oxide Ceramics (AREA)
Abstract
The present invention relates to beautiful porcelain of a kind of China and preparation method thereof, belong to ceramic technology field.The beautiful porcelain of China of the present invention, green body chemical composition weight percent are as follows: SiO239~43%, Al2O310~15%, CaO 21~26%, P2O517~23%, KNaO 2~5%, Fe2O30.2~0.5%, TiO20.05~0.2%, CaF21.2-2%, Pr2O30.02~0.08%, surplus is impurity.The beautiful porcelain of China of the present invention, formula is simple, and the transparency with Bone China, glaze is smooth, glow under light illumination it is faint yellow, also with the bandwagon effect of artistic porcelain；Invention also provides a kind of simple and easy preparation methods.
Description
Technical field
The present invention relates to beautiful porcelain of a kind of China and preparation method thereof, belong to ceramic technology field.
Background technique
With the raising of living standards of the people and appreciation level, the appearance and dicoration of domestic ceramics increasingly cause people
Concern, emerged many new porcelain kinds, such as steatite ceramic, Shandong jade porcelain, quartz enriched porcelain and Bone China, made domestic ceramic product
The development trend of windy lattice, multiscale is presented, the color of porcelain is gradually enriched also with the development of ceramics.
Traditional ceramic whiteware color is single, ornamental value is poor, has had many Ceramics Enterprises to improve the formula of porcelain, but
The product developed is only applicable to masses, does not all create exclusively for women a especially soft, brief luxurious without losing
Product.
Summary of the invention
The purpose of the present invention is to provide a kind of beautiful porcelain of China, and formula is simple, the transparency with Bone China, glaze light
Profit, glow under light illumination it is faint yellow, also with artistic porcelain bandwagon effect；Invention also provides a kind of simple and easy systems
Preparation Method.
The beautiful porcelain of China of the present invention, green body chemical composition weight percent are as follows: SiO239~43%, Al2O310~
15%, CaO 21~26%, P2O517~23%, KNaO 2~5%, Fe2O30.2~0.5%, TiO20.05~0.2%,
CaF21.2-2%, Pr2O30.02~0.08%, surplus is impurity.
The beautiful porcelain of the China, is made of the raw material of following weight percentage: synthos 38~46%, feldspar 8~
13%, quartz 8~14%, Datong District's soil 13~18%, elutriation Longyan clay 6~15%, Guangdong black mud 2~8%, Laiyang soil 1~5%
With lane soil 1~5%；It is 100% metering, additional CaF with the total weight of the above raw material22-3%, Pr2O30.05~0.1%.
Preferably, the beautiful porcelain of the China, is made of the raw material of following weight percentage: synthos 38~43%, length
Stone 8~12%, Datong District's soil 13~15%, eluriates Longyan clay 6~9%, Guangdong black mud 2~6%, Laiyang soil 1 at quartz 8~11%
~4% and lane soil 1~4%；It is 100% metering, additional CaF with the total weight of the above raw material22-3%, Pr2O30.05~
0.1%.
The preparation method of the beautiful porcelain of the China, comprising the following steps:
(1) after mixing raw material, ball milling is carried out, then removes iron, sieving, filters pressing, pugging, compacting；
(2) step (1) pressed semi-finished product are subjected to biscuiting at 1250-1280 DEG C；
(3) to the green body glazing after step (2) biscuiting；
(4) semi-finished product after step (3) glazing are subjected at 1150-1180 DEG C secondary glaze firing, obtain the Hua Yu
Porcelain.
In step (1), Ball-milling Time is 60-70 hours, ball milling fineness >=87%.
In step (1), when pugging, filter cake is practiced to the mud item for being 20-25% at moisture.
In step (3), when glazing, glaze used was Bone China high gloss leadless glaze.
The present invention is using raw materials such as the various clays such as synthos and feldspar, quartz, Datong District's soil as basic raw material, in high temperature
Physical reaction is carried out during biscuiting forms solid solution.Then it is generated according to rare earth element Pr is exclusive since its wavelength is long
Chromophoric mechanism, by all unique textures of rare earth ion itself and property, under high temperature action enter fluorite lattice, not
Under the premise of destroying fluorite octahedron lattice, the calcium in fluorite is substituted by Pr and yellow is wrapped up to the octahedra monocrystalline into fluorite
Inside lattice (it uses inorganic coating structure), the package for foring stable color development is yellow, has no effect on the light transmittance of porcelain；And it ties
Optical principle is closed, the refraction principle of light is made full use of, further promotes the purity and grade of raw material, adjustment and optimization body recipe
In potassium, sodium content, the beautiful porcelain of China developed issues light milk yellow, and translucence with higher, glaze smoothness is bright,
Entire body is more glittering and translucent, gentle as beautiful, it is soft in show Huang, brief luxurious without losing, appearance is high-end, generous, is traditional potter
Skill combines later perfect product with modern science and technology, can make as the first choice of porcelain for women.
Compared with the prior art, the present invention has the following beneficial effects:
(1) formula is simple, scientific and reasonable, and the beautiful ceramic glaze surface brightness of the China of preparation is high, thermal stability is good, glows under light illumination
Faint yellow, Lead and cadmium rate is zero；
(2) the beautiful porcelain of the China of preparation increases the color kind of Bone China, further improves the class of Bone China, has wide
General applicability is particularly suitable for doing gift tea set, vase etc., the bandwagon effect with artistic porcelain；
(3) preparation method of the beautiful porcelain of China described in uses oxidizing flame calcining system, and controlling of production process difficulty is small, easily grasps
Make, is conducive to large-scale production.
Specific embodiment
Below with reference to embodiment, the present invention is further illustrated, but it is not intended to limit implementation of the invention.
Embodiment 1
A kind of beautiful porcelain of China, is made of the raw material of following weight percentage: synthos 38%, feldspar 12%, Datong District's soil
17%, quartz 12%, elutriation Longyan clay 10%, Guangdong black mud 6%, Laiyang soil 4% and lane soil 1%, additional CaF22%,
Pr2O30.05%.
Ball mill is added after above-mentioned raw materials are prepared according to above-mentioned formula, Ball-milling Time is 60 hours, and ball milling fineness is
87%, then remove iron, sieving, filters pressing, then with vacuum deairing machine filter cake practiced at moisture be 21% mud item, suppressed with roller press
At 8 cun of square positions, in 1265 ± 15 DEG C of at a temperature of biscuiting, the beautiful porcelain biscuit of faint yellow China is obtained, then glazing (Bone China when glazing
With high gloss leadless glaze), make color through glaze by high-temperature chemical reaction in 1165 ± 15 DEG C of at a temperature of secondary glaze firing
Layer is refracted to product surface, and it is flat to obtain the smooth beautiful porcelain 8 of faint yellow China as beautiful.
Embodiment 2
A kind of beautiful porcelain of China, is made of the raw material of following weight percentage: synthos 42%, feldspar 11%, Datong District's soil
16%, quartz 12%, elutriation Longyan clay 8%, Guangdong black mud 6%, Laiyang soil 4% and lane soil 1%, additional CaF23%,
Pr2O30.08%.
Ball mill is added after above-mentioned raw materials are prepared according to above-mentioned formula, Ball-milling Time is 65 hours, and ball milling fineness is
90%, then remove iron, sieving, filters pressing, then with vacuum deairing machine filter cake practiced at moisture be 22% mud item, suppressed with roller press
At 6 cun of square positions, in 1265 ± 15 DEG C of at a temperature of biscuiting, the beautiful porcelain biscuit of faint yellow China is obtained, then glazing (Bone China when glazing
With high gloss leadless glaze), make color through glaze by high-temperature chemical reaction in 1165 ± 15 DEG C of at a temperature of secondary glaze firing
Layer is refracted to product surface, and it is flat to obtain the smooth beautiful porcelain 6 of faint yellow China as beautiful.
Embodiment 3
A kind of beautiful porcelain of China, is made of the raw material of following weight percentage: synthos 46%, feldspar 10%, Datong District's soil
15%, quartz 12%, elutriation Longyan clay 8%, Guangdong black mud 5%, Laiyang soil 3% and lane soil 1%, additional CaF22.5%,
Pr2O30.1%.
Ball mill is added after above-mentioned raw materials are prepared according to above-mentioned formula, Ball-milling Time is 70 hours, and ball milling fineness is
88%, then remove iron, sieving, filters pressing, then with vacuum deairing machine filter cake practiced at moisture be 25% mud item, suppressed with roller press
The beautiful porcelain biscuit of faint yellow China is obtained, then glazing (is used when glazing with Bone China in 1265 ± 15 DEG C of at a temperature of biscuiting at 5 cun of bowls
High gloss leadless glaze), make color through glaze layer by high-temperature chemical reaction in 1165 ± 15 DEG C of at a temperature of secondary glaze firing
It is refracted to product surface, is obtained smooth such as the beautiful flat bowl of the faint yellow beautiful porcelain 5 of China.
Raw materials used chemical weight percentage composition, is shown in Table 1.
The raw materials used chemical weight percentage composition of table 1
The chemical weight percentage composition of the product of embodiment 1-3 preparation, is shown in Table 2.
The chemical weight percentage composition of the product of 2 embodiment 1-3 of table preparation
Claims (6)
1. a kind of beautiful porcelain of China, it is characterised in that: green body chemical composition weight percent are as follows: SiO239~43%, Al2O310~
15%, CaO 21~26%, P2O517~23%, KNaO 2~5%, Fe2O3 0.2~0.5%, TiO2 0.05~0.2%, CaF2
1.2-2%、Pr2O3 0.02~0.08%, surplus is impurity.
2. the beautiful porcelain of China according to claim 1, it is characterised in that be made of the raw material of following weight percentage: calcium phosphate
Salt 38~46%, feldspar 8~13%, quartz 8~14%, Datong District's soil 13~18%, eluriate Longyan clay 6~15%, Guangdong black mud 2~8%,
Laiyang soil 1~5% and lane soil 1~5%；It is 100% metering, additional CaF with the total weight of the above raw material2 2-3%、Pr2O3 0.05
~0.1%.
3. a kind of preparation method of the beautiful porcelain of China of any of claims 1 or 2, it is characterised in that the following steps are included:
(1) after mixing raw material, ball milling is carried out, then removes iron, sieving, filters pressing, pugging, compacting；
(2) step (1) pressed semi-finished product are subjected to biscuiting at 1250-1280 DEG C；
(3) to the green body glazing after step (2) biscuiting；
(4) semi-finished product after step (3) glazing are subjected at 1150-1180 DEG C secondary glaze firing, obtain the beautiful porcelain of the China.
4. the preparation method of the beautiful porcelain of China according to claim 3, it is characterised in that: in step (1), Ball-milling Time 60-
70 hours, ball milling fineness >=87%.
5. the preparation method of the beautiful porcelain of China according to claim 3, it is characterised in that: in step (1), when pugging, by filter cake
Practice the mud item for being 20-25% at moisture.
6. the preparation method of the beautiful porcelain of China according to claim 3, it is characterised in that: in step (3), when glazing glaze used
Material is Bone China high gloss leadless glaze.
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| CN112794707B (en) * | 2021-04-14 | 2021-07-20 | 佛山市东鹏陶瓷有限公司 | High-whiteness and high-strength light-transmitting ceramic tile and preparation method thereof |
| CN114262207B (en) * | 2021-12-31 | 2022-08-12 | 四川美术学院 | Composite material health-care ceramic tea set and preparation method thereof |
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| CN1935738A (en) * | 2006-10-12 | 2007-03-28 | 淄博华光瓷业有限公司 | Bone-green porcelain |
| CN101913843A (en) * | 2010-07-23 | 2010-12-15 | 华南理工大学 | Preparation method of emerald ceramic |
| CN102515704A (en) * | 2011-12-27 | 2012-06-27 | 淄博华光陶瓷科技文化有限公司 | Hua celadon and preparation method thereof |
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2017
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1935738A (en) * | 2006-10-12 | 2007-03-28 | 淄博华光瓷业有限公司 | Bone-green porcelain |
| CN101913843A (en) * | 2010-07-23 | 2010-12-15 | 华南理工大学 | Preparation method of emerald ceramic |
| CN102515704A (en) * | 2011-12-27 | 2012-06-27 | 淄博华光陶瓷科技文化有限公司 | Hua celadon and preparation method thereof |
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