CN107382223A - A kind of preparation method of cement foaming insulation board - Google Patents
A kind of preparation method of cement foaming insulation board Download PDFInfo
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- CN107382223A CN107382223A CN201710520023.9A CN201710520023A CN107382223A CN 107382223 A CN107382223 A CN 107382223A CN 201710520023 A CN201710520023 A CN 201710520023A CN 107382223 A CN107382223 A CN 107382223A
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- cement
- insulation board
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/06—Aluminous cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B22/00—Use of inorganic materials as active ingredients for mortars, concrete or artificial stone, e.g. accelerators, shrinkage compensating agents
- C04B22/06—Oxides, Hydroxides
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B22/00—Use of inorganic materials as active ingredients for mortars, concrete or artificial stone, e.g. accelerators, shrinkage compensating agents
- C04B22/06—Oxides, Hydroxides
- C04B22/068—Peroxides, e.g. hydrogen peroxide
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
- C04B24/08—Fats; Fatty oils; Ester type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
- C04B24/085—Higher fatty acids
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
- C04B24/12—Nitrogen containing compounds organic derivatives of hydrazine
- C04B24/121—Amines, polyamines
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
- C04B24/40—Compounds containing silicon, titanium or zirconium or other organo-metallic compounds; Organo-clays; Organo-inorganic complexes
- C04B24/42—Organo-silicon compounds
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
- Building Environments (AREA)
Abstract
The invention discloses a kind of preparation method of cement foaming insulation board, belong to building material field.The present invention is to count in parts by weight, carry out taking raw material, then first the cement in raw material, silicone acrylic emulsion, water reducer and catalyst are uniformly mixed, add water stirring, add the composite foamable agent in raw material, after auxiliary agent continues stirring, collect stirring mixture, through stand foaming, at room temperature stand, be stripped and must be stripped thing, demoulding thing is conserved, dried, you can obtains cement foaming insulation board.The beneficial effects of the invention are as follows:Cement foaming insulation board air vent aperture of the present invention is in the same size, is evenly distributed, while has higher compression strength, is worthy to be popularized and uses.
Description
Technical field
The present invention relates to a kind of preparation method of cement foaming insulation board, belong to building material field.
Background technology
Cement foaming insulation board refers to the warming plate manufactured using foam cement technology;Cement foaming insulation board, also known as send out
Steep concrete insulation board, inorganic fireproof heat insulating plate.It is for original with Portland cement, flyash, foaming agent, additive etc.
Material, it is in concrete through lightweight balloon shape heat-insulating material made of technique, its prominent features such as compound, stirring, foaming, cuttings
Portion is formed.
Foam cement can be divided into physical blowing and chemical blowing by mode of production difference.Physical blowing:Foaming agent is passed through
Plant equipment is prepared into foam, then by foam be added to by cement-based gelling material, gather materials, admixture, additive and water are made
Slurry in, heat preservation plate material that blended stirring, moulding by casting, maintenance form(Cement insulation board).Chemical blowing:Will hair
Infusion adds by cement-based gelling material, gathered materials, made of admixture, additive and water in slurry, blended stirring, cast,
It is set to make to produce sealed porosity, the heat preservation plate material through conserving, cutting inside slurry by chemical reaction in a mold.But
Obtained cement foaming insulation board thermal conductivity factor is high, bulk density is big, causes fire resistance to reduce.Chinese Patent Application No.
CN201310703099.7 discloses a kind of superfine cement base foaming insulation board and preparation method thereof, and the warming plate is by superfine cement
It is prepared with additive for raw material, described additive, by the percentages for accounting for superfine cement weight, by following each component group
Into:1%~10% pore structure conditioning agent, 1%~15% adjustable solidification agent, 0.002%~0.5% viscosity-controlling agent, 2%~
8% waterproofing agent, 0.5%~2% cracking resistance component and 0.2%~0.5% composite water-reducing agent.The foaming insulation board has
Stable quality, the cement foaming insulation board being prepared with it have lower a thermal conductivity factor and density, and combustibility is reachable
National A levels standard, but due to air vent aperture cause not of uniform size, skewness, stress concentration phenomenon easily occurs, causes cement to be sent out
Steeping warming plate compression strength reduces.Therefore, the cement foamed insulation that a kind of air vent aperture is in the same size, compression strength is high is researched and developed
Plate, there is necessary meaning, the development of cement foaming insulation board can not only be effectively facilitated, also to widen cement foaming insulation board
Application field lays the foundation.
The content of the invention
The technical problems to be solved by the invention:For current cement foaming insulation board air vent aperture cause not of uniform size, divide
Cloth is uneven, easily occur stress concentration phenomenon, cause its compression strength reduce the drawbacks of, there is provided a kind of cement foaming insulation board
Preparation method.
In order to solve the above technical problems, the present invention is using technical scheme as described below:
(1)Count in parts by weight, take raw material, 95~100 parts of cement, 30~40 parts of water, 8~10 parts of composite foamable agents, 6~
9 parts of silicone acrylic emulsions, 3~5 parts of auxiliary agents, 1~2 part of water reducer and 1.4~1.5 parts of catalyst;
(2)Cement, silicone acrylic emulsion, water reducer and catalyst are uniformly mixed first, add water, is stirred at 50~60 DEG C
After mixing, after addition composite foamable agent, auxiliary agent continue stirring, stirring mixture is collected, is put into mould, mould is placed in 70~80
DEG C stand foaming;
(3)After the completion of foaming, mould is placed in and stood at room temperature, then be stripped, collect demoulding thing, demoulding thing is supported
Shield, dry, you can obtain cement foaming insulation board.
The step(1)Middle cement is Portland cement, sulphate aluminium cement in mass ratio 3~5:1, mixing and
Into.
The step(1)Middle composite foamable agent is that sodium lauroyl sarcosine, N- acyl glutamates and hydrogen peroxide press quality
Than 1:1:5 mix.
The step(1)Middle auxiliary agent is polyglutamic acid, neopelex in mass ratio 4~6:1, mix.
The step(1)Middle water reducer is any one in amino water reducer, polycarboxylate high performance water-reducing agent.
The step(1)Middle catalyst is titanium dioxide, manganese dioxide in mass ratio 1:3 mix.
Compared with other method, advantageous effects are the present invention:
The present invention by adding silicone acrylic emulsion in the feed, in foaming process, the compound sodium lauroyl sarcosine in agent that is soaked,
In the presence of N- acyl glutamates and titanium dioxide, silicone acrylic emulsion is set to carry out microdilatancy, while hydrogen peroxide release oxygen, two
Hydrogen peroxide is increased using oxygen velocity in the presence of manganese oxide, so as to produce substantial amounts of bubble, in the work of silicone acrylic emulsion microdilatancy
Under, the liquid film of bubble appearance to be protected, prevents liquid-sheet disintegration, generation is collapsed film, causes stomata non-uniform phenomenon, while
In the presence of silicone acrylic emulsion, cement foam board can be made to carry out Quick cross-linking, caused stomata is protected, and then make cement
Foaming insulation board air vent aperture is in the same size, is evenly distributed.
Embodiment
The preparation of cement in the present invention:In mass ratio 3~5:1, by Portland cement, sulphate aluminium cement(Two
Cement needs to write manufacturer)It is put into mixer and stirs, you can.
The preparation of composite foamable agent:Sodium lauroyl sarcosine, N- acyl glutamates and 1.6mol/L hydrogen peroxide are pressed into matter
Measure ratio 1:1:5 mix.
The preparation of auxiliary agent:By polyglutamic acid, neopelex in mass ratio 4~6:1 is well mixed, you can.
The selection of water reducer is amino water reducer, polycarboxylate high performance water-reducing agent(Liang Ge manufacturers)In it is any one
Kind.
The preparation of catalyst:By titanium dioxide, manganese dioxide in mass ratio 1:3 mix.
The preparation method of cement foaming insulation board of the present invention, comprises the following steps:
(1)Count in parts by weight, take raw material, 95~100 parts of cement, 30~40 parts of water, 8~10 parts of composite foamable agents, 6~
9 parts of silicone acrylic emulsions, 3~5 parts of auxiliary agents, 1~2 part of water reducer and 1.4~1.5 parts of catalyst;
(2)Cement, silicone acrylic emulsion, water reducer and catalyst are put into mixer first, 30 are stirred with 300r/min~
50min, water is added, after stirring 20~30min at 50~60 DEG C, add composite foamable agent, auxiliary agent continues 1~2h of stirring
Afterwards, stirring mixture is collected, is put into mould, mould is placed in 70~80 DEG C of 3~5h of stand foaming;
(3)After the completion of foaming, mould is placed in 3~6h of standing, then be stripped at room temperature, demoulding thing is collected, to being stripped thing
Conserved, dried, you can obtain cement foaming insulation board.
Example 1
The preparation of cement in the present invention:In mass ratio 3:1, by Portland cement(Manufacturer:Upper byssus rising sun engineering science and technology
Co., Ltd), sulphate aluminium cement(Manufacturer:Hangzhou Yao Wei building materials Science and Technology Ltd.)It is put into mixer and stirs
It is even, you can.
The preparation of composite foamable agent:Sodium lauroyl sarcosine, N- acyl glutamates and 1.6mol/L hydrogen peroxide are pressed into matter
Measure ratio 1:1:5 mix.
The preparation of auxiliary agent:By polyglutamic acid, neopelex in mass ratio 4:1 is well mixed, you can.
The selection of water reducer is amino water reducer(Manufacturer:Shaanxi Qin Fen building materials Co., Ltd).
The preparation of catalyst:By titanium dioxide, manganese dioxide in mass ratio 1:3 mix.
The preparation method of cement foaming insulation board of the present invention, comprises the following steps:
(1)Count in parts by weight, take raw material, 95 parts of cement, 30 parts of water, 8 parts of composite foamable agents, 6 parts of silicone acrylic emulsions, 3 parts
Auxiliary agent, 1 part of water reducer and 1.4 parts of catalyst;
(2)Cement, silicone acrylic emulsion, water reducer and catalyst are put into mixer first, are stirred with 300r/min
30min, water is added, after stirring 20min at 50 DEG C, addition composite foamable agent, auxiliary agent continue after stirring 1h, and it is mixed to collect stirring
Compound, it is put into mould, mould is placed in 70 DEG C of stand foaming 3h;
(3)After the completion of foaming, mould is placed in and stands 3h at room temperature, then be stripped, collect demoulding thing, demoulding thing is carried out
Maintenance, dry, you can obtain cement foaming insulation board.
Example 2
The preparation of cement in the present invention:In mass ratio 4:1, by Portland cement(Manufacturer:Upper byssus rising sun engineering science and technology
Co., Ltd), sulphate aluminium cement(Manufacturer:Hangzhou Yao Wei building materials Science and Technology Ltd.)It is put into mixer and stirs
It is even, you can.
The preparation of composite foamable agent:Sodium lauroyl sarcosine, N- acyl glutamates and 1.6mol/L hydrogen peroxide are pressed into matter
Measure ratio 1:1:5 mix.
The preparation of auxiliary agent:By polyglutamic acid, neopelex in mass ratio 5:1 is well mixed, you can.
The selection of water reducer is polycarboxylate high performance water-reducing agent(Manufacturer:Shaanxi Qin Fen building materials Co., Ltd).
The preparation of catalyst:By titanium dioxide, manganese dioxide in mass ratio 1:3 mix.
The preparation method of cement foaming insulation board of the present invention, comprises the following steps:
(1)Count in parts by weight, take raw material, 98 parts of cement, 35 parts of water, 9 parts of composite foamable agents, 7 parts of silicone acrylic emulsions, 4 parts
Auxiliary agent, 2 parts of water reducers and 1.5 parts of catalyst;
(2)Cement, silicone acrylic emulsion, water reducer and catalyst are put into mixer first, are stirred with 300r/min
40min, water is added, after stirring 25min at 55 DEG C, addition composite foamable agent, auxiliary agent continue after stirring 2h, and it is mixed to collect stirring
Compound, it is put into mould, mould is placed in 75 DEG C of stand foaming 4h;
(3)After the completion of foaming, mould is placed in and stands 5h at room temperature, then be stripped, collect demoulding thing, demoulding thing is carried out
Maintenance, dry, you can obtain cement foaming insulation board.
Example 3
The preparation of cement in the present invention:In mass ratio 5:1, by Portland cement(Manufacturer:Upper byssus rising sun engineering science and technology
Co., Ltd), sulphate aluminium cement(Manufacturer:Hangzhou Yao Wei building materials Science and Technology Ltd.)It is put into mixer and stirs
It is even, you can.
The preparation of composite foamable agent:Sodium lauroyl sarcosine, N- acyl glutamates and 1.6mol/L hydrogen peroxide are pressed into matter
Measure ratio 1:1:5 mix.
The preparation of auxiliary agent:By polyglutamic acid, neopelex in mass ratio 6:1 is well mixed, you can.
The selection of water reducer is amino water reducer(Manufacturer:Shaanxi Qin Fen building materials Co., Ltd).
The preparation of catalyst:By titanium dioxide, manganese dioxide in mass ratio 1:3 mix.
The preparation method of cement foaming insulation board of the present invention, comprises the following steps:
(1)Count in parts by weight, carry out taking raw material, 100 parts of cement, 40 parts of water, 10 parts of composite foamable agents, 9 parts of silicone acrylic emulsions, 5
Part auxiliary agent, 2 parts of water reducers and 1.5 parts of catalyst;
(2)Cement, silicone acrylic emulsion, water reducer and catalyst are put into mixer first, are stirred with 300r/min
50min, water is added, after stirring 30min at 60 DEG C, addition composite foamable agent, auxiliary agent continue after stirring 2h, and it is mixed to collect stirring
Compound, it is put into mould, mould is placed in 80 DEG C of stand foaming 5h;
(3)After the completion of foaming, mould is placed in and stands 6h at room temperature, then be stripped, collect demoulding thing, demoulding thing is carried out
Maintenance, dry, you can obtain cement foaming insulation board.
Reference examples:The cement foaming insulation board of Yangzhou company production.
The cement foaming insulation board of cement foaming insulation board obtained by above-described embodiment and reference examples is detected, specific inspection
Survey as follows:
1st, compression strength:With reference to GB/T11968-2008《Steam-pressing aero-concrete method for testing performance》Tested;
2nd, rupture strength:Tested with reference to GB/T 5486.
As a result as shown in Table 1.
Table one:
Detection project | Example 1 | Example 2 | Example 3 | Reference examples |
Compression strength/MPa | 1.25 | 1.59 | 1.85 | 0.75 |
Rupture strength/MPa | 0.89 | 1.46 | 1.95 | 0.55 |
Aperture/mm | 1.7~1.8 | 1.8~1.9 | 1.7~1.9 | 1.5~2.0 |
As seen from the above table, cement foaming insulation board air vent aperture of the present invention is in the same size, is evenly distributed, while has higher resist
Compressive Strength, it is worthy to be popularized and uses.
Claims (6)
1. a kind of preparation method of cement foaming insulation board, it is characterised in that the preparation method comprises the following steps:
(1)Count in parts by weight, take raw material, 95~100 parts of cement, 30~40 parts of water, 8~10 parts of composite foamable agents, 6~
9 parts of silicone acrylic emulsions, 3~5 parts of auxiliary agents, 1~2 part of water reducer and 1.4~1.5 parts of catalyst;
(2)Cement, silicone acrylic emulsion, water reducer and catalyst are uniformly mixed first, add water, is stirred at 50~60 DEG C
After mixing, after addition composite foamable agent, auxiliary agent continue stirring, stirring mixture is collected, is put into mould, mould is placed in 70~80
DEG C stand foaming;
(3)After the completion of foaming, mould is placed in and stood at room temperature, then be stripped, collect demoulding thing, demoulding thing is supported
Shield, dry, you can obtain cement foaming insulation board.
2. the preparation method of cement foaming insulation board according to claim 1, it is characterised in that the step(1)Reclaimed water
Mud is Portland cement, sulphate aluminium cement in mass ratio 3~5:1, mix.
3. the preparation method of cement foaming insulation board according to claim 1, it is characterised in that the step(1)In it is multiple
Conjunction foaming agent is sodium lauroyl sarcosine, N- acyl glutamates and hydrogen peroxide in mass ratio 1:1:5 mix.
4. the preparation method of cement foaming insulation board according to claim 1, it is characterised in that the step(1)In help
Agent is polyglutamic acid, neopelex in mass ratio 4~6:1, mix.
5. the preparation method of cement foaming insulation board according to claim 1, it is characterised in that the step(1)In subtract
Aqua is any one in amino water reducer, polycarboxylate high performance water-reducing agent.
6. the preparation method of cement foaming insulation board according to claim 1, it is characterised in that the step(1)In urge
Agent is titanium dioxide, manganese dioxide in mass ratio 1:3 mix.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115650659A (en) * | 2022-09-28 | 2023-01-31 | 湖南诚友绿色建材科技有限公司 | Novel heat insulation material for fabricated building and preparation method thereof |
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CN103113064A (en) * | 2013-02-21 | 2013-05-22 | 济宁跃峰建材科技有限公司 | Novel environment-friendly fireproof insulation board and production method thereof |
CN104261865A (en) * | 2014-10-10 | 2015-01-07 | 乔生艮 | Concrete foamed insulating brick and preparation method thereof |
CN106747123A (en) * | 2017-01-24 | 2017-05-31 | 四川省黄氏防腐保温工程有限公司 | A kind of self-heat conserving template cement foaming insulation board and preparation method thereof |
-
2017
- 2017-06-30 CN CN201710520023.9A patent/CN107382223A/en active Pending
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CN103113064A (en) * | 2013-02-21 | 2013-05-22 | 济宁跃峰建材科技有限公司 | Novel environment-friendly fireproof insulation board and production method thereof |
CN104261865A (en) * | 2014-10-10 | 2015-01-07 | 乔生艮 | Concrete foamed insulating brick and preparation method thereof |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115650659A (en) * | 2022-09-28 | 2023-01-31 | 湖南诚友绿色建材科技有限公司 | Novel heat insulation material for fabricated building and preparation method thereof |
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Application publication date: 20171124 |