CN107377661A - A kind of preparation method of spectacle frame titanium alloy wire materials - Google Patents
A kind of preparation method of spectacle frame titanium alloy wire materials Download PDFInfo
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- CN107377661A CN107377661A CN201710866069.6A CN201710866069A CN107377661A CN 107377661 A CN107377661 A CN 107377661A CN 201710866069 A CN201710866069 A CN 201710866069A CN 107377661 A CN107377661 A CN 107377661A
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- titanium alloy
- alloy wire
- wire materials
- spectacle frame
- cold drawn
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21C—MANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
- B21C37/00—Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape
- B21C37/04—Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape of bars or wire
- B21C37/045—Manufacture of wire or bars with particular section or properties
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- Mechanical Engineering (AREA)
- Eyeglasses (AREA)
- Metal Extraction Processes (AREA)
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Abstract
The invention discloses a kind of preparation method of spectacle frame titanium alloy wire materials, following steps are specifically included：Titanium, vanadium, aluminum metal raw material are carried out after uniformly mixing, melting is passed sequentially through, forges, strip off the skin, reconditioning, place into and cold drawn processing is carried out on roller die wire drawing machine, it is heat-treated when working modulus is 60%~70% after over cleaning, it is 3mm~4mm to continue to be cold drawn to diameter Ф afterwards, that is, obtains spectacle frame titanium alloy wire materials；Titanium alloy wire materials quality prepared by this method is higher, elastic good and processing characteristics is excellent, is highly suitable for the requirement of spectacle frame titanium alloy wire materials, meanwhile, production efficiency is high and production cost is low, available for large-scale production.
Description
Technical field
The invention belongs to technical field of metal material preparation, is related to a kind of preparation method of spectacle frame titanium alloy wire materials.
Background technology
Titanium alloy has the advantages that light weight, specific strength height and good corrosion resistance, thus is widely used in space flight, navigation
In the field such as automobile.In recent years, with the application and development to titanium alloy material, start to prepare glasses with titanium material both at home and abroad
Frame, the spectacle frame of the type have high good degree, anti-fatigue performance and environmental corrosion resisting performance, shape-plastic preferable.So
And when preparing spectacle frame using titanium material, its preparation technology is complicated, production cost is high and the titanium alloy wire materials of preparation are of poor quality,
Therefore, in spectacle frame preparation field, design a kind of preparation method of spectacle frame titanium alloy wire materials and have great importance.
The content of the invention
It is an object of the invention to provide a kind of preparation method of spectacle frame titanium alloy wire materials, plasticity is preferable, very suitable
Close manufacturing spectacle.
The technical solution adopted in the present invention is a kind of preparation method of spectacle frame titanium alloy wire materials, specifically include with
Lower step：
Step 1, weigh respectively by weight percentage as follows：Titanium 67%~70%, vanadium 25%~27%, aluminium 5%~6%,
The percentage by weight summation of above each component is 100%；
Step 2, after the raw material metal in step 1 is mixed, by melting, forge, strip off the skin, most removed afterwards through reconditioning
Surface scale is removed, obtains titanium alloy wire materials；
Step 3, the titanium alloy wire materials obtained in step 2 are carried out on roller die wire drawing machine it is cold drawn, working modulus be 60%
The titanium alloy wire materials after cold drawn are cleaned with cleaning fluid when~70%, dried；
Step 4, the titanium alloy wire materials obtained after step 3 are put into tube furnace and be heat-treated；
Step 5, the titanium alloy wire materials after step 4 is heat-treated are cooled down, then will be carried out on roller die wire drawing machine it is cold drawn,
Finally it is polished on polishing machine, removes surface defect and improve surface gloss, that is, obtain spectacle frame titanium alloy wire materials.
The features of the present invention also resides in,
In step 3, cold drawn diameter Ф is 6mm~8mm.
In step 3, the mass ratio of cleaning agent and water is 0.03~0.05 in cleaning fluid:1.
In step 4, process of thermal treatment condition is：Vacuum in tube furnace is 1 × 10-2Pa~3 × 10-2Pa, heating
Temperature is 400 DEG C~700 DEG C, and the heat time is 30min~60min.
In step 5, cold drawn diameter Ф is 3mm~4mm.
The invention has the advantages that
1. the preparation method of spectacle frame titanium alloy wire materials of the present invention, the titanium alloy wire materials quality prepared is higher, elastic
Good and processing characteristics is excellent, is highly suitable for the requirement of spectacle frame titanium alloy wire materials, meanwhile, the spectacle frame of preparation has quality
Gently, the characteristics of corrosion-resistant, antifatigue and wearing is comfortable；
2. the preparation method of spectacle frame titanium alloy wire materials of the present invention has, processing step is simple, production efficiency is high and produces
Cost is low, available for large-scale production.
Embodiment
With reference to embodiment, the present invention is described in detail.
A kind of preparation method of spectacle frame titanium alloy wire materials, specifically includes following steps：
Step 1, the following raw material is weighed respectively by weight percentage：Titanium 67%~70%, vanadium 25%~27%, aluminium 3%~
8%, the percentage by weight summation of above each component is 100%；
Step 2, after the raw material metal weighed in step 1 is mixed, then melting is passed sequentially through, forges, strip off the skin, most
Surface scale is removed by reconditioning, obtains titanium alloy wire materials；
Step 3, the titanium alloy wire materials obtained in step 2 are subjected to cold drawn processing, cold drawn diameter Ф on roller die wire drawing machine
For 6mm~8mm, dried after being cleaned when working modulus is 60%~70% with cleaning fluid to the titanium alloy wire materials after cold drawn,
Wherein, it is 0.03~0.05 in mass ratio by cleaning agent and water that cleaning fluid, which is,:1 well mixed composition, cleaning agent are
Water solubility scour；
Step 4, the titanium alloy wire materials obtained after step 3 are put into tube furnace and be heat-treated；
Process of thermal treatment condition is：Vacuum in tube furnace is 1 × 10-2Pa~3 × 10-2Pa, heating-up temperature are
400 DEG C~700 DEG C, the heat time is 30min~60min；
Step 5, the titanium alloy wire materials after step 4 is heat-treated are cooled down, then will be carried out on roller die wire drawing machine it is cold drawn,
Cold drawn diameter Ф is 3mm~4mm, is finally polished on polishing machine, removes surface defect and improves surface gloss, produces
To spectacle frame titanium alloy wire materials.
Embodiment 1
A kind of preparation method of spectacle frame titanium alloy wire materials, specifically includes following steps：
Step 1, the following raw material is weighed respectively by weight percentage：Titanium 70%, vanadium 27%, aluminium 3%, the weight of above each component
It is 100% to measure percentage summation；
Step 2, after the raw material metal weighed in step 1 is mixed, then melting is passed sequentially through, forges, strip off the skin, most
Surface scale is removed by reconditioning, obtains titanium alloy wire materials；
Step 3, the titanium alloy wire materials obtained in step 2 are subjected to cold drawn processing, cold drawn diameter Ф on roller die wire drawing machine
For 6mm, the titanium alloy wire materials after cold drawn are cleaned with cleaning fluid when working modulus is 60%, dried, wherein, cleaning fluid is
It is 0.03 in mass ratio by cleaning agent and water:1 well mixed composition；
Step 4, the titanium alloy wire materials obtained after step 3 are put into tube furnace and be heat-treated；Process of thermal treatment
Condition is：Vacuum in tube furnace is 1 × 10-2Pa, heating-up temperature are 400 DEG C, heat time 30min；
Step 5, the titanium alloy wire materials after step 4 is heat-treated are cooled down, then will be carried out on roller die wire drawing machine it is cold drawn,
Cold drawn diameter Ф is 3mm, is finally polished on polishing machine, removes surface defect and improves surface gloss, that is, obtains eye
Mirror holder titanium alloy wire materials.
Embodiment 2
A kind of preparation method of spectacle frame titanium alloy wire materials, specifically includes following steps：
Step 1, the following raw material is weighed respectively by weight percentage：Titanium 68%, vanadium 26%, aluminium 6%, the weight of above each component
It is 100% to measure percentage summation；
Step 2, after the raw material metal weighed in step 1 is mixed, then melting is passed sequentially through, forges, strip off the skin, most
Surface scale is removed by reconditioning, obtains titanium alloy wire materials；
Step 3, the titanium alloy wire materials obtained in step 2 are subjected to cold drawn processing, cold drawn diameter Ф on roller die wire drawing machine
For 6.3mm, the titanium alloy wire materials after cold drawn are cleaned with cleaning fluid when working modulus is 62%, dried, wherein, cleaning fluid
It is 0.032 in mass ratio by cleaning agent and water to be:1 well mixed composition；
Step 4, the titanium alloy wire materials obtained after step 3 are put into tube furnace and be heat-treated；Process of thermal treatment
Condition is：Vacuum in tube furnace is 1.5 × 10-2Pa, heating-up temperature are 450 DEG C, heat time 35min；
Step 5, the titanium alloy wire materials after step 4 is heat-treated are cooled down, then will be carried out on roller die wire drawing machine it is cold drawn,
Cold drawn diameter Ф is 3.2mm, is finally polished on polishing machine, removes surface defect and improves surface gloss, that is, obtains
Spectacle frame titanium alloy wire materials.
Embodiment 3
A kind of preparation method of spectacle frame titanium alloy wire materials, specifically includes following steps：
Step 1, the following raw material is weighed respectively by weight percentage：Titanium 68.5%, vanadium 26.5%, aluminium 5%, above each component
Percentage by weight summation be 100%；
Step 2, after the raw material metal weighed in step 1 is mixed, then melting is passed sequentially through, forges, strip off the skin, most
Surface scale is removed by reconditioning, obtains titanium alloy wire materials；
Step 3, the titanium alloy wire materials obtained in step 2 are subjected to cold drawn processing, cold drawn diameter Ф on roller die wire drawing machine
For 6.5mm, the titanium alloy wire materials after cold drawn are cleaned with cleaning fluid when working modulus is 64%, dried, wherein, cleaning fluid
It is 0.035 in mass ratio by cleaning agent and water to be:1 well mixed composition；
Step 4, the titanium alloy wire materials obtained after step 3 are put into tube furnace and be heat-treated；Process of thermal treatment
Condition is：Vacuum in tube furnace is 2 × 10-2Pa, heating-up temperature are 500 DEG C, heat time 40min；
Step 5, the titanium alloy wire materials after step 4 is heat-treated are cooled down, then will be carried out on roller die wire drawing machine it is cold drawn,
Cold drawn diameter Ф is 3.4mm, is finally polished on polishing machine, removes surface defect and improves surface gloss, that is, obtains
Spectacle frame titanium alloy wire materials.
Embodiment 4
A kind of preparation method of spectacle frame titanium alloy wire materials, specifically includes following steps：
Step 1, the following raw material is weighed respectively by weight percentage：Titanium 69%, vanadium 27%, aluminium 4%, the weight of above each component
It is 100% to measure percentage summation；
Step 2, after the raw material metal weighed in step 1 is mixed, then melting is passed sequentially through, forges, strip off the skin, most
Surface scale is removed by reconditioning, obtains titanium alloy wire materials；
Step 3, the titanium alloy wire materials obtained in step 2 are subjected to cold drawn processing, cold drawn diameter Ф on roller die wire drawing machine
For 7mm, the titanium alloy wire materials after cold drawn are cleaned with cleaning fluid when working modulus is 65%, dried, wherein, cleaning fluid is
It is 0.04 in mass ratio by cleaning agent and water:1 well mixed composition；
Step 4, the titanium alloy wire materials obtained after step 3 are put into tube furnace and be heat-treated；Process of thermal treatment
Condition is：Vacuum in tube furnace is 2.5 × 10-2Pa, heating-up temperature are 600 DEG C, heat time 50min；
Step 5, the titanium alloy wire materials after step 4 is heat-treated are cooled down, then will be carried out on roller die wire drawing machine it is cold drawn,
Cold drawn diameter Ф is 3.8mm, is finally polished on polishing machine, removes surface defect and improves surface gloss, that is, obtains
Spectacle frame titanium alloy wire materials.
Embodiment 5
A kind of preparation method of spectacle frame titanium alloy wire materials, specifically includes following steps：
Step 1, the following raw material is weighed respectively by weight percentage：Titanium 67%, vanadium 25%, aluminium 8%, the weight of above each component
It is 100% to measure percentage summation；
Step 2, after the raw material metal weighed in step 1 is mixed, then melting is passed sequentially through, forges, strip off the skin, most
Surface scale is removed by reconditioning, obtains titanium alloy wire materials；
Step 3, the titanium alloy wire materials obtained in step 2 are subjected to cold drawn processing, cold drawn diameter Ф on roller die wire drawing machine
For 8mm, the titanium alloy wire materials after cold drawn are cleaned with cleaning fluid when working modulus is 70%, dried, wherein, cleaning fluid is
It is 0.05 in mass ratio by cleaning agent and water:1 well mixed composition；
Step 4, the titanium alloy wire materials obtained after step 3 are put into tube furnace and be heat-treated；Process of thermal treatment
Condition is：Vacuum in tube furnace is 3 × 10-2Pa, heating-up temperature are 700 DEG C, heat time 60min；
Step 5, the titanium alloy wire materials after step 4 is heat-treated are cooled down, then will be carried out on roller die wire drawing machine it is cold drawn,
Cold drawn diameter Ф is 4mm, is finally polished on polishing machine, removes surface defect and improves surface gloss, that is, obtains eye
Mirror holder titanium alloy wire materials.
Titanium alloy wire materials quality prepared by the present invention is higher, elastic good and processing characteristics is excellent, is highly suitable for spectacle frame
With the requirement of titanium alloy wire materials, meanwhile, the processing step is simple, production efficiency is high and production cost is low, available for scale metaplasia
Production.
Claims (5)
1. a kind of preparation method of spectacle frame titanium alloy wire materials, it is characterised in that specifically include following steps：
Step 1, the following raw material is weighed respectively by weight percentage：Titanium 67%~70%, vanadium 25%~27%, aluminium 5%~6%,
The percentage by weight summation of above each component is 100%；
Step 2, after the raw material metal weighed in step 1 is mixed, then melting is passed sequentially through, forges, strip off the skin, most passed through afterwards
Reconditioning removes surface scale, obtains titanium alloy wire materials；
Step 3, the titanium alloy wire materials obtained in step 2 are subjected to cold drawn processing on roller die wire drawing machine, are 60% in working modulus
The titanium alloy wire materials after cold drawn are cleaned with cleaning fluid when~70%, dried；
Step 4, the titanium alloy wire materials obtained after step 3 are put into tube furnace and be heat-treated；
Step 5, the titanium alloy wire materials after step 4 is heat-treated are cooled down, then will be carried out on roller die wire drawing machine it is cold drawn, finally
It is polished on polishing machine, removes surface defect and improve surface gloss, that is, obtain spectacle frame titanium alloy wire materials.
A kind of 2. preparation method of spectacle frame titanium alloy wire materials according to claim 1, it is characterised in that the step
In 3, cold drawn diameter Ф is 6mm~8mm.
A kind of 3. preparation method of spectacle frame titanium alloy wire materials according to claim 1, it is characterised in that the step
In 3, the mass ratio of cleaning agent and water is 0.03~0.05 in cleaning fluid:1.
A kind of 4. preparation method of spectacle frame titanium alloy wire materials according to claim 1, it is characterised in that the step
In 4, process of thermal treatment condition is：Vacuum in tube furnace is 1 × 10-2Pa~3 × 10-2Pa, heating-up temperature are 400 DEG C
~700 DEG C, the heat time is 30min~60min.
A kind of 5. preparation method of spectacle frame titanium alloy wire materials according to claim 1, it is characterised in that the step
In 5, cold drawn diameter Ф is 3mm~4mm.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710866069.6A CN107377661A (en) | 2017-09-22 | 2017-09-22 | A kind of preparation method of spectacle frame titanium alloy wire materials |
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| CN201710866069.6A CN107377661A (en) | 2017-09-22 | 2017-09-22 | A kind of preparation method of spectacle frame titanium alloy wire materials |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108421840A (en) * | 2018-02-11 | 2018-08-21 | 陕西兴盛金属有限公司 | A kind of TA16 titanium alloy wire materials processing technology |
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| EP1070558A2 (en) * | 1999-07-13 | 2001-01-24 | Bridgestone Corporation | Method of manufacturing titanium fiber or titanium alloy fiber |
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| CN101716715A (en) * | 2009-11-20 | 2010-06-02 | 宝鸡市三鑫金属有限责任公司 | Processing method of titanium and titanium alloy wires |
| CN102477521A (en) * | 2010-11-30 | 2012-05-30 | 西安赛特金属材料开发有限公司 | Online non-oxidation heat treatment method for beta titanium alloy wire |
| CN103203390A (en) * | 2013-03-22 | 2013-07-17 | 西安思维金属材料有限公司 | Processing method for beta titanium alloy wires used for glass frames |
| CN103480685A (en) * | 2013-09-13 | 2014-01-01 | 贵州顶效经济开发区沈兴实业有限责任公司 | Processing method of TC18 titanium alloy wires |
| CN106269972A (en) * | 2016-08-16 | 2017-01-04 | 宝鸡核新金属有限公司 | The preparation for processing of big substance high-performance titanium or titanium alloy light parcel |
| CN107142402A (en) * | 2017-05-22 | 2017-09-08 | 温州市佳宏眼镜厂 | A kind of alloy in lightweight spectacle frame and preparation method thereof |
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2017
- 2017-09-22 CN CN201710866069.6A patent/CN107377661A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1070558A2 (en) * | 1999-07-13 | 2001-01-24 | Bridgestone Corporation | Method of manufacturing titanium fiber or titanium alloy fiber |
| CN1749424A (en) * | 2004-09-13 | 2006-03-22 | 西安赛特金属材料开发有限公司 | Multipurpose new type beta type titanium alloy |
| CN101716715A (en) * | 2009-11-20 | 2010-06-02 | 宝鸡市三鑫金属有限责任公司 | Processing method of titanium and titanium alloy wires |
| CN102477521A (en) * | 2010-11-30 | 2012-05-30 | 西安赛特金属材料开发有限公司 | Online non-oxidation heat treatment method for beta titanium alloy wire |
| CN103203390A (en) * | 2013-03-22 | 2013-07-17 | 西安思维金属材料有限公司 | Processing method for beta titanium alloy wires used for glass frames |
| CN103480685A (en) * | 2013-09-13 | 2014-01-01 | 贵州顶效经济开发区沈兴实业有限责任公司 | Processing method of TC18 titanium alloy wires |
| CN106269972A (en) * | 2016-08-16 | 2017-01-04 | 宝鸡核新金属有限公司 | The preparation for processing of big substance high-performance titanium or titanium alloy light parcel |
| CN107142402A (en) * | 2017-05-22 | 2017-09-08 | 温州市佳宏眼镜厂 | A kind of alloy in lightweight spectacle frame and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108421840A (en) * | 2018-02-11 | 2018-08-21 | 陕西兴盛金属有限公司 | A kind of TA16 titanium alloy wire materials processing technology |
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Application publication date: 20171124 |
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