CN107362070A - A kind of anti-acne of essential oil containing rabdosia lophanthide repairs the preparation method of facial mask - Google Patents
A kind of anti-acne of essential oil containing rabdosia lophanthide repairs the preparation method of facial mask Download PDFInfo
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- CN107362070A CN107362070A CN201710761827.8A CN201710761827A CN107362070A CN 107362070 A CN107362070 A CN 107362070A CN 201710761827 A CN201710761827 A CN 201710761827A CN 107362070 A CN107362070 A CN 107362070A
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- Prior art keywords
- acne
- rabdosia lophanthide
- facial mask
- preparation
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
Abstract
A kind of anti-acne of essential oil containing rabdosia lophanthide repairs the preparation method of facial mask, belongs to facial mask preparing technical field.The preparation method of the present invention includes：Mask substrate is prepared, rabdosia lophanthide essential oil is prepared, prepares aqueous phase liquid, prepare oil phase liquid, prepare Essence, prepare facial mask.Rabdosia lophanthide has the effect of clearing heat and detoxicating, anti-inflammation.Especially for dry skin, fuel-displaced grade has good action.There is good effect for whelk.OPC is that the main composition of grape pip has the superpower anti-oxidant ability for removing free radical, fundamentally prevents the release of inflammatory factor, so as to remove this inflammation symptom of acne, suppresses allergic phenomena.Grape pip can suppress to produce the enzyme that histamine needs, and prevent from generating histamine, so as to dephlogistication symptom, effectively go acne.Fibroin has the effect of repairing skin tissue's cell.The silk mask good biocompatibility of the present invention, natural component is high, easily absorption, anti-acne effect is good, and preparation method is simple.
Description
Technical field
The present invention relates to facial mask preparing technical field, the anti-acne of more particularly to a kind of essential oil containing rabdosia lophanthide repairs the system of facial mask
Preparation Method.
Background technology
Acne is a kind of chronic inflammatory skin of pilosebaceous unit, teenager is mainly apt to occur in, to teenager
Psychology and social influence it is very big.Clinical manifestation using be apt to occur in the acne of face, papule, warts, the polymorphy skin lesion such as tubercle as
Feature, nickname acne, whelk.The generation of acne mainly blocks with hypersteatosis, pilosebaceous duct, bacterium infection
It is closely related with the factor such as inflammatory reaction.Adolesce the rapid rise of level of androgen particularly testosterone in descendant's body, promotees
Enter sebaceous glands to develop and produce a large amount of sebums.The dyskeratosis of pilosebaceous duct causes catheter blockage, sebum discharge simultaneously
Obstacle, it is micro mist thorn to form horn plug.Multiple-microorganism especially propionibacterium acnes amount reproduction in hair follicle, acne propionic acid bar
Lipase caused by bacterium decomposes sebum generation free fatty, while chemotactic inflammatory cell and medium, finally induces and aggravates inflammation
Reaction.
The method for the treatment of acne has at present：Oral antibiotic/vitamin/glucocorticoid/sex hormone zinc preparation and external application
Drug therapy, the therapy such as injection treatment/laser ultraviolet in skin lesion.Although these methods also have certain effect, have
The drawbacks of certain, such as the side effect such as endo-medicine overlong time, antibiotic/hormone, injection treatment/laser ultraviolet in skin lesion
Compare pain etc. therapy, laser therapy easily forms the charring layer of black, disturbs surgical field of view, patient is not easy observation and grasps treatment
The depth reached.The result of control treatment is difficult to if if over the course for the treatment of, assurance is not in place.
For this phenomenon we in addition to hospital can be gone to use the treatment method such as medicine/laser, contained using some
The facial mask of anti-acne composition also has good therapeutic effect, so as to develop the facial mask of the present invention.
The content of the invention
In order to solve problems of the prior art, the present invention provides a kind of anti-acne of the essential oil containing rabdosia lophanthide and repairs facial mask
Preparation method.
The present invention uses following technical scheme：
A kind of anti-acne of essential oil containing rabdosia lophanthide repairs the preparation method of facial mask, comprises the following steps：
Step 1：Silk cocoon is removed into pupa, it is bath raio 1 in 0.5% aqueous sodium carbonate to insert the mass concentration boiled:
50, silk cocoon surface silk gum is removed, will pull out and wring out into thread silk cocoon, after repeating aforesaid operations once, use deionization
Water is cleaned, and degumming fibroin is obtained after air-drying；
Step 2：By CaCl2It is dissolved under room temperature state in formic acid, stirs 30min, it is 5wt.%'s that concentration, which is made,
CaCl2- FA solution, degumming fibroin is then dissolved in CaCl2In-FA solution, magnetic agitation 3h, it is molten to obtain regenerated silk fibroin
Liquid, drying and forming-film in facial mask mould is poured at room temperature, film is soaked into 3h with deionized water, then be freeze-dried, obtain silk mask
Base material；
Step 3：Rabdosia lophanthide is beaten into powder, crosses 20 mesh sieves, takes 5g rabdosia lophanthide powder, 200mL distilled water is added, obtains sample liquid,
Described sample liquid is through ultrasonication, power 600W, processing time 30min, described sample liquid again through super-pressure at
Reason, pressure 400MPa, dwell time 30min；
Step 4：Sample liquid is transferred in 500mL round-bottomed flask, adds zeolite, carries out steam distillation extraction, is steamed
100 DEG C, distillation time 1.5h of temperature is evaporated, gained extract obtains rabdosia lophanthide essential oil after rotary evaporation in vacuo concentrates；
Step 5：According to the mass fraction, by 4 parts of glycerine, 2 parts of propane diols, 1 part of fibroin, 1 part of essence, 0.4 part of three second
Hydramine is added in 68 parts of deionized waters, and aqueous phase liquid is made until dissolving in 70 DEG C of heating stirrings；
Step 6：According to the mass fraction, by 4 parts of rabdosia lophanthide essential oils, 1.5 parts of grape-kernel oils, 1.5 parts of methyl-silicone oils, 1 part of list
Sweet fat, 1.2 parts of polyoxyethylene sorbitan monolaurates, 0.8 part of compound emulsifying agent AC-402,0.4 part of xanthan gum, 60
Stirred under the conditions of DEG C, oil phase liquid is made；
Step 7：Under conditions of being stirred continuously, oil phase liquid is added slowly in aqueous phase liquid, described oil phase liquid and
The mass ratio of aqueous phase liquid is 1:8,15min is stirred using high speed disperser, cooling discharging, both obtains Essence；
Step 8：After the sterilization irradiation of silk mask base material, load aluminium foil bag and be transported to packaging production line, bottle placer injection
After Essence, sealing machine sealing.
Preferably, the mixing speed of the high speed disperser described in step 7 is 5000r/min.
Preferably, the essence described in step 5 is flavoring rose essence.
The beneficial effects of the present invention are：
1) rabdosia lophanthide has the effect of clearing heat and detoxicating, anti-inflammation.Especially for dry skin, fuel-displaced grade has well
Effect.There is good effect for whelk.
2) OPC (OPC) is that the main composition of grape pip has the superpower anti-oxidant ability for removing free radical,
The harmful substances such as free radical can be removed rapidly, the release of inflammatory factor is fundamentally prevented, so as to remove this inflammation disease of acne
Shape, suppress allergic phenomena.Grape pip can suppress to produce the enzyme that histamine needs, and prevent from generating histamine, so as to dephlogistication symptom, have
Effect goes acne.
3) fibroin has the effect of repairing skin tissue's cell.
4) silk mask good biocompatibility of the invention, natural component is high, easily absorption, anti-acne effect is good, and preparation side
Method is simple.
Embodiment
Below with reference to specific embodiment, the present invention is described further.
Embodiment 1
A kind of anti-acne of essential oil containing rabdosia lophanthide repairs the preparation method of facial mask, comprises the following steps：
Step 1：Silk cocoon is removed into pupa, it is bath raio 1 in 0.5% aqueous sodium carbonate to insert the mass concentration boiled:
50, silk cocoon surface silk gum is removed, will pull out and wring out into thread silk cocoon, after repeating aforesaid operations once, use deionization
Water is cleaned, and degumming fibroin is obtained after air-drying；
Step 2：By CaCl2It is dissolved under room temperature state in formic acid, stirs 30min, it is 5wt.%'s that concentration, which is made,
CaCl2- FA solution, degumming fibroin is then dissolved in CaCl2In-FA solution, magnetic agitation 3h, it is molten to obtain regenerated silk fibroin
Liquid, drying and forming-film in facial mask mould is poured at room temperature, film is soaked into 3h with deionized water, then be freeze-dried, obtain silk mask
Base material；
Step 3：Rabdosia lophanthide is beaten into powder, crosses 20 mesh sieves, takes 5g rabdosia lophanthide powder, 200mL distilled water is added, obtains sample liquid,
Described sample liquid is through ultrasonication, power 600W, processing time 30min, described sample liquid again through super-pressure at
Reason, pressure 400MPa, dwell time 30min；
Step 4：Sample liquid is transferred in 500mL round-bottomed flask, adds zeolite, carries out steam distillation extraction, is steamed
100 DEG C, distillation time 1.5h of temperature is evaporated, gained extract obtains rabdosia lophanthide essential oil after rotary evaporation in vacuo concentrates；
Step 5：According to the mass fraction, by 4 parts of glycerine, 2 parts of propane diols, 1 part of fibroin, 1 part of essence, 0.4 part of three second
Hydramine is added in 68 parts of deionized waters, and aqueous phase liquid is made until dissolving in 70 DEG C of heating stirrings；
Step 6：According to the mass fraction, by 4 parts of rabdosia lophanthide essential oils, 1.5 parts of grape-kernel oils, 1.5 parts of methyl-silicone oils, 1 part of list
Sweet fat, 1.2 parts of polyoxyethylene sorbitan monolaurates, 0.8 part of compound emulsifying agent AC-402,0.4 part of xanthan gum, 60
Stirred under the conditions of DEG C, oil phase liquid is made；
Step 7：Under conditions of being stirred continuously, oil phase liquid is added slowly in aqueous phase liquid, described oil phase liquid and
The mass ratio of aqueous phase liquid is 1:8,15min is stirred using high speed disperser, cooling discharging, both obtains Essence；
Step 8：After the sterilization irradiation of silk mask base material, load aluminium foil bag and be transported to packaging production line, bottle placer injection
After Essence, sealing machine sealing.
The mixing speed of high speed disperser described in step 7 is 5000r/min.
Essence described in step 5 is flavoring rose essence.
The physical and chemical index of embodiment 1 is as follows：The serious people of volunteer 15 of face acnes is chosen, by the face of the gained of embodiment 1
Film is used at volunteer's face acnes symptom, and volunteer is generally comfortable on, and acne lightens, and does not stay acne print.Through a period of time
Continuous use, the situation of acne are obviously improved or even disappeared.
Claims (3)
1. a kind of anti-acne of essential oil containing rabdosia lophanthide repairs the preparation method of facial mask, it is characterised in that comprises the following steps：
Step 1：Silk cocoon is removed into pupa, it is bath raio 1 in 0.5% aqueous sodium carbonate to insert the mass concentration boiled:50, remove
Silk cocoon surface silk gum is removed, will pull out and wring out into thread silk cocoon, after repeating aforesaid operations once, be washed with deionized water
Only, degumming fibroin is obtained after air-drying；
Step 2：By CaCl2It is dissolved under room temperature state in formic acid, stirs 30min, the CaCl that concentration is 5wt.% is made2-
FA solution, degumming fibroin is then dissolved in CaCl2In-FA solution, magnetic agitation 3h, regenerated silk fibroin solution, room are obtained
Drying and forming-film in facial mask mould is poured under temperature, film is soaked into 3h with deionized water, then is freeze-dried, obtains silk mask base material；
Step 3：Rabdosia lophanthide is beaten into powder, crosses 20 mesh sieves, takes 5g rabdosia lophanthide powder, 200mL distilled water is added, obtains sample liquid, it is described
Sample liquid through ultrasonication, power 600W, processing time 30min, described sample liquid is again through ultra high pressure treatment, pressure
Power is 400MPa, dwell time 30min；
Step 4：Sample liquid is transferred in 500mL round-bottomed flask, adds zeolite, carries out steam distillation extraction, distillation temperature
100 DEG C, distillation time 1.5h of degree, gained extract obtain rabdosia lophanthide essential oil after rotary evaporation in vacuo concentrates；
Step 5：According to the mass fraction, by 4 parts of glycerine, 2 parts of propane diols, 1 part of fibroin, 1 part of essence, 0.4 part of triethanolamine
It is added in 68 parts of deionized waters, aqueous phase liquid is made until dissolving in 70 DEG C of heating stirrings；
Step 6：According to the mass fraction, it is 4 parts of rabdosia lophanthide essential oils, 1.5 parts of grape-kernel oils, 1.5 parts of methyl-silicone oils, 1 part of list is sweet
Fat, 1.2 parts of polyoxyethylene sorbitan monolaurates, 0.8 part of compound emulsifying agent AC-402,0.4 part of xanthan gum, at 60 DEG C
Under the conditions of stir, oil phase liquid is made；
Step 7：Under conditions of being stirred continuously, oil phase liquid is added slowly in aqueous phase liquid, described oil phase liquid and aqueous phase
The mass ratio of liquid is 1:8,15min is stirred using high speed disperser, cooling discharging, both obtains Essence；
Step 8：After the sterilization irradiation of silk mask base material, load aluminium foil bag and be transported to packaging production line, bottle placer injection elite
After liquid, sealing machine sealing.
2. a kind of anti-acne of essential oil containing rabdosia lophanthide according to claim 1 repairs the preparation method of facial mask, it is characterised in that：
The mixing speed of high speed disperser described in step 7 is 5000r/min.
3. a kind of anti-acne of essential oil containing rabdosia lophanthide according to claim 1 repairs the preparation method of facial mask, it is characterised in that：
Essence described in step 5 is flavoring rose essence.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710761827.8A CN107362070A (en) | 2017-08-30 | 2017-08-30 | A kind of anti-acne of essential oil containing rabdosia lophanthide repairs the preparation method of facial mask |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710761827.8A CN107362070A (en) | 2017-08-30 | 2017-08-30 | A kind of anti-acne of essential oil containing rabdosia lophanthide repairs the preparation method of facial mask |
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| Publication Number | Publication Date |
|---|---|
| CN107362070A true CN107362070A (en) | 2017-11-21 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710761827.8A Pending CN107362070A (en) | 2017-08-30 | 2017-08-30 | A kind of anti-acne of essential oil containing rabdosia lophanthide repairs the preparation method of facial mask |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103173882A (en) * | 2013-04-11 | 2013-06-26 | 大连海事大学 | Method for preparing graphene/ silk composite fiber |
| CN104233628A (en) * | 2014-09-01 | 2014-12-24 | 浙江金三发非织造布有限公司 | Production process of special non-woven fabric for facial mask |
| CN105596222A (en) * | 2016-01-25 | 2016-05-25 | 广东工业大学 | Preparation method of mask for accurate repair and care |
| CN105616172A (en) * | 2016-01-19 | 2016-06-01 | 广州市美姿贺化妆品有限公司 | Pure mulberry silk facial mask and preparation method thereof |
-
2017
- 2017-08-30 CN CN201710761827.8A patent/CN107362070A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103173882A (en) * | 2013-04-11 | 2013-06-26 | 大连海事大学 | Method for preparing graphene/ silk composite fiber |
| CN104233628A (en) * | 2014-09-01 | 2014-12-24 | 浙江金三发非织造布有限公司 | Production process of special non-woven fabric for facial mask |
| CN105616172A (en) * | 2016-01-19 | 2016-06-01 | 广州市美姿贺化妆品有限公司 | Pure mulberry silk facial mask and preparation method thereof |
| CN105596222A (en) * | 2016-01-25 | 2016-05-25 | 广东工业大学 | Preparation method of mask for accurate repair and care |
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Application publication date: 20171121 |