CN107353008B - 一种层状金属-陶瓷复合材料零件的制备方法 - Google Patents
一种层状金属-陶瓷复合材料零件的制备方法 Download PDFInfo
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- CN107353008B CN107353008B CN201710471833.XA CN201710471833A CN107353008B CN 107353008 B CN107353008 B CN 107353008B CN 201710471833 A CN201710471833 A CN 201710471833A CN 107353008 B CN107353008 B CN 107353008B
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- 239000000919 ceramic Substances 0.000 title claims abstract description 96
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- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 239000011347 resin Substances 0.000 claims abstract description 58
- 229920005989 resin Polymers 0.000 claims abstract description 58
- 229910052751 metal Inorganic materials 0.000 claims abstract description 37
- 239000002184 metal Substances 0.000 claims abstract description 37
- 238000000034 method Methods 0.000 claims abstract description 22
- 239000002002 slurry Substances 0.000 claims abstract description 18
- 239000000463 material Substances 0.000 claims abstract description 17
- 238000000016 photochemical curing Methods 0.000 claims abstract description 12
- 238000001746 injection moulding Methods 0.000 claims abstract description 11
- 238000005238 degreasing Methods 0.000 claims abstract description 8
- 238000005516 engineering process Methods 0.000 claims abstract description 8
- 238000004108 freeze drying Methods 0.000 claims abstract description 8
- 238000013329 compounding Methods 0.000 claims abstract description 5
- 239000010410 layer Substances 0.000 claims description 52
- 235000015895 biscuits Nutrition 0.000 claims description 26
- 238000001764 infiltration Methods 0.000 claims description 20
- 230000008595 infiltration Effects 0.000 claims description 20
- 239000007788 liquid Substances 0.000 claims description 11
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 8
- 238000001723 curing Methods 0.000 claims description 8
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 6
- 238000005229 chemical vapour deposition Methods 0.000 claims description 6
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 4
- 229910052581 Si3N4 Inorganic materials 0.000 claims description 4
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims description 4
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 4
- 229910045601 alloy Inorganic materials 0.000 claims description 4
- 239000000956 alloy Substances 0.000 claims description 4
- 229910052786 argon Inorganic materials 0.000 claims description 4
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- 238000013461 design Methods 0.000 claims description 4
- 239000007789 gas Substances 0.000 claims description 4
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- AVSXGQJYEFAQNK-UHFFFAOYSA-N prop-2-enamide;hydrate Chemical compound O.NC(=O)C=C AVSXGQJYEFAQNK-UHFFFAOYSA-N 0.000 claims description 4
- 229910010271 silicon carbide Inorganic materials 0.000 claims description 4
- HQVNEWCFYHHQES-UHFFFAOYSA-N silicon nitride Chemical compound N12[Si]34N5[Si]62N3[Si]51N64 HQVNEWCFYHHQES-UHFFFAOYSA-N 0.000 claims description 4
- 229910052726 zirconium Inorganic materials 0.000 claims description 4
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 3
- 238000000151 deposition Methods 0.000 claims description 3
- 239000011229 interlayer Substances 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 238000000465 moulding Methods 0.000 claims description 3
- QYEXBYZXHDUPRC-UHFFFAOYSA-N B#[Ti]#B Chemical compound B#[Ti]#B QYEXBYZXHDUPRC-UHFFFAOYSA-N 0.000 claims description 2
- 229910052580 B4C Inorganic materials 0.000 claims description 2
- 229910052582 BN Inorganic materials 0.000 claims description 2
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 claims description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 2
- 229910052782 aluminium Inorganic materials 0.000 claims description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 2
- INAHAJYZKVIDIZ-UHFFFAOYSA-N boron carbide Chemical compound B12B3B4C32B41 INAHAJYZKVIDIZ-UHFFFAOYSA-N 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 claims description 2
- 229910052802 copper Inorganic materials 0.000 claims description 2
- 239000010949 copper Substances 0.000 claims description 2
- 229910052742 iron Inorganic materials 0.000 claims description 2
- 239000011777 magnesium Substances 0.000 claims description 2
- 229910052749 magnesium Inorganic materials 0.000 claims description 2
- 229910052759 nickel Inorganic materials 0.000 claims description 2
- 238000012545 processing Methods 0.000 claims description 2
- 239000002356 single layer Substances 0.000 claims description 2
- 230000003068 static effect Effects 0.000 claims description 2
- 239000010936 titanium Substances 0.000 claims description 2
- 229910052719 titanium Inorganic materials 0.000 claims description 2
- MTPVUVINMAGMJL-UHFFFAOYSA-N trimethyl(1,1,2,2,2-pentafluoroethyl)silane Chemical compound C[Si](C)(C)C(F)(F)C(F)(F)F MTPVUVINMAGMJL-UHFFFAOYSA-N 0.000 claims description 2
- UONOETXJSWQNOL-UHFFFAOYSA-N tungsten carbide Chemical compound [W+]#[C-] UONOETXJSWQNOL-UHFFFAOYSA-N 0.000 claims description 2
- 239000007787 solid Substances 0.000 claims 1
- 238000005245 sintering Methods 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 4
- 238000005470 impregnation Methods 0.000 abstract description 2
- 238000007740 vapor deposition Methods 0.000 abstract description 2
- 238000005266 casting Methods 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 239000007790 solid phase Substances 0.000 description 5
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- KWYHDKDOAIKMQN-UHFFFAOYSA-N N,N,N',N'-tetramethylethylenediamine Chemical compound CN(C)CCN(C)C KWYHDKDOAIKMQN-UHFFFAOYSA-N 0.000 description 4
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium peroxydisulfate Substances [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 description 4
- VAZSKTXWXKYQJF-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)OOS([O-])=O VAZSKTXWXKYQJF-UHFFFAOYSA-N 0.000 description 4
- 229910001870 ammonium persulfate Inorganic materials 0.000 description 4
- 238000000498 ball milling Methods 0.000 description 4
- 239000003054 catalyst Substances 0.000 description 4
- 238000007710 freezing Methods 0.000 description 4
- 230000008014 freezing Effects 0.000 description 4
- 239000003999 initiator Substances 0.000 description 4
- WGTYBPLFGIVFAS-UHFFFAOYSA-M tetramethylammonium hydroxide Chemical compound [OH-].C[N+](C)(C)C WGTYBPLFGIVFAS-UHFFFAOYSA-M 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 229910010293 ceramic material Inorganic materials 0.000 description 3
- 150000002739 metals Chemical class 0.000 description 3
- 229910018566 Al—Si—Mg Inorganic materials 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 229910052593 corundum Inorganic materials 0.000 description 2
- 239000010431 corundum Substances 0.000 description 2
- 239000008367 deionised water Substances 0.000 description 2
- 229910021641 deionized water Inorganic materials 0.000 description 2
- 239000002270 dispersing agent Substances 0.000 description 2
- 238000003801 milling Methods 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- ZIUHHBKFKCYYJD-UHFFFAOYSA-N n,n'-methylenebisacrylamide Chemical compound C=CC(=O)NCNC(=O)C=C ZIUHHBKFKCYYJD-UHFFFAOYSA-N 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
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- 238000003756 stirring Methods 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- 238000013459 approach Methods 0.000 description 1
- 239000013590 bulk material Substances 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000007731 hot pressing Methods 0.000 description 1
- 238000010030 laminating Methods 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 238000009715 pressure infiltration Methods 0.000 description 1
- 238000001308 synthesis method Methods 0.000 description 1
Images
Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/56—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides
- C04B35/565—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides based on silicon carbide
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D23/00—Casting processes not provided for in groups B22D1/00 - B22D21/00
- B22D23/04—Casting by dipping
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/10—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5093—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with elements other than metals or carbon
- C04B41/5096—Silicon
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- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
- C04B2235/602—Making the green bodies or pre-forms by moulding
- C04B2235/6023—Gel casting
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Laminated Bodies (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
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CN201710471833.XA CN107353008B (zh) | 2017-06-20 | 2017-06-20 | 一种层状金属-陶瓷复合材料零件的制备方法 |
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CN107353008A CN107353008A (zh) | 2017-11-17 |
CN107353008B true CN107353008B (zh) | 2020-03-17 |
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Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108675798B (zh) * | 2018-08-03 | 2021-08-13 | 广东工业大学 | 一种氮化硅陶瓷及其制备方法 |
CN109516809A (zh) * | 2018-11-07 | 2019-03-26 | 三峡大学 | 一种基于i-wp曲面的铜碳化硅复合材料的制备方法 |
CN110041088A (zh) * | 2019-05-09 | 2019-07-23 | 西北工业大学 | 一种层状ZrB2复合陶瓷材料及制备方法 |
CN111112569B (zh) * | 2019-12-30 | 2021-03-30 | 珠海凯利得新材料有限公司 | 一种金属基陶瓷复合材料零件的加工工艺 |
CN112047737B (zh) * | 2020-07-23 | 2021-07-13 | 西安交通大学 | 一种面向带有微结构特征的碳化硅基陶瓷的熔渗方法 |
CN112062589A (zh) * | 2020-08-03 | 2020-12-11 | 西安交通大学 | 一种基于氧化铝-钛-镍实现氧化铝陶瓷的扩散连接方法 |
CN113145830A (zh) * | 2021-03-12 | 2021-07-23 | 昆明理工大学 | 一种金属与陶瓷连接体及其连接方法 |
CN113351827B (zh) * | 2021-05-24 | 2022-08-05 | 西安交通大学 | 一种基于间接增材制造的金属基超材料制备方法 |
CN114367663B (zh) * | 2021-12-20 | 2023-01-10 | 北京科技大学 | 一种全致密复杂形状钛合金薄壁零部件的制备方法 |
Family Cites Families (22)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2004176123A (ja) * | 2002-11-27 | 2004-06-24 | Taiheiyo Cement Corp | 中空構造を有する金属−セラミックス複合材料の製造方法 |
CN101301677A (zh) * | 2008-06-03 | 2008-11-12 | 西安交通大学 | 一种复杂零件快速精密铸造方法 |
CN101306465A (zh) * | 2008-06-27 | 2008-11-19 | 西安交通大学 | 带有异型气膜孔的空心涡轮叶片制造方法 |
CN103031479A (zh) * | 2011-09-29 | 2013-04-10 | 比亚迪股份有限公司 | 一种铝基金属陶瓷复合材料及其制备方法 |
CN102335460B (zh) * | 2011-10-15 | 2014-01-29 | 西安交通大学 | 基于光固化和凝胶注模的镁合金/生物陶瓷骨支架及其成型方法 |
CN102327648B (zh) * | 2011-10-15 | 2013-08-14 | 西安交通大学 | 一种多孔镁合金/生物陶瓷仿生复合支架及其快速成型方法 |
JP2013237597A (ja) * | 2012-05-17 | 2013-11-28 | Hitachi Metals Ltd | プリフォーム、それを用いた金属−セラミックス複合材及びその製造方法 |
KR101409294B1 (ko) * | 2012-09-06 | 2014-06-24 | 한국기계연구원 | 무가압함침법을 이용한 알루미늄 기지 복합재료의 제조방법 |
CN103113112B (zh) * | 2013-02-04 | 2014-06-04 | 西安交通大学 | 一种金属增韧陶瓷基复合材料涡轮叶片的制备方法 |
CN103203448B (zh) * | 2013-02-20 | 2015-02-11 | 邓金刚 | 一种金属基陶瓷复合材料零件的制造方法 |
CN103223689B (zh) * | 2013-04-16 | 2015-04-29 | 西安交通大学 | 一种梯度功能材料型芯型壳一体化陶瓷铸型的制备方法 |
ITTO20130531A1 (it) * | 2013-06-27 | 2013-09-26 | Torino Politecnico | Metodo per la fabbricazione di compositi a matrice di alluminio tramite infiltrazione senza pressione |
CN103895285B (zh) * | 2014-02-28 | 2015-10-28 | 吉林大学 | 高强度层状Al基金属陶瓷复合材料及其制备方法 |
CN104003732B (zh) * | 2014-05-30 | 2015-12-02 | 西安交通大学 | 一种凝胶注模涡轮叶片陶瓷铸型真空脱脂的方法 |
CN104073703B (zh) * | 2014-06-20 | 2016-09-07 | 青岛农业大学 | 一种Al2O3-TiN-Al陶瓷复合材料及其制备方法 |
CN105274380A (zh) * | 2014-07-07 | 2016-01-27 | 陈焕铭 | 一种改善Al2O3多孔预制体与NbAl合金熔体浸润性能的方法 |
CN104529497B (zh) * | 2014-11-28 | 2017-02-01 | 西安交通大学 | 一种采用真空冷冻干燥技术提高陶瓷铸型精度的方法 |
CN104529458B (zh) * | 2014-12-01 | 2016-08-17 | 西安交通大学 | 高性能SiC陶瓷基复合材料航空发动机叶片的制造方法 |
CN104526856B (zh) * | 2014-12-31 | 2016-08-24 | 西安交通大学 | 一种提高整体式陶瓷铸型型芯位置精度的方法 |
CN104674047B (zh) * | 2015-02-10 | 2016-08-17 | 北京交通大学 | 一种双连续相Ti3AlC2/Ni基复合材料及其无压浸渗制备方法 |
CN105349817A (zh) * | 2015-10-29 | 2016-02-24 | 无锡桥阳机械制造有限公司 | 一种复合材料的制备工艺 |
CN106083205B (zh) * | 2016-06-14 | 2018-06-26 | 西安交通大学 | 一种通过化学气相渗透提高整体式氧化铝基陶瓷铸型高温强度的方法 |
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