CN107328231A - A kind of Muffle furnace apparatus of environmental protection - Google Patents

A kind of Muffle furnace apparatus of environmental protection Download PDF

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Publication number
CN107328231A
CN107328231A CN201710786782.XA CN201710786782A CN107328231A CN 107328231 A CN107328231 A CN 107328231A CN 201710786782 A CN201710786782 A CN 201710786782A CN 107328231 A CN107328231 A CN 107328231A
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CN
China
Prior art keywords
muffle furnace
environmental protection
absorbent charcoal
heater
charcoal adsorber
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710786782.XA
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Chinese (zh)
Inventor
王伟建
闭莉河
范勐
郝媛媛
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Qinzhou University
Original Assignee
Qinzhou University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Qinzhou University filed Critical Qinzhou University
Priority to CN201710786782.XA priority Critical patent/CN107328231A/en
Publication of CN107328231A publication Critical patent/CN107328231A/en
Pending legal-status Critical Current

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Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B5/00Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B5/00Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated
    • F27B5/06Details, accessories, or equipment peculiar to furnaces of these types
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D17/00Arrangements for using waste heat; Arrangements for using, or disposing of, waste gases
    • F27D17/008Arrangements for using waste heat; Arrangements for using, or disposing of, waste gases cleaning gases

Abstract

The invention discloses a kind of Muffle furnace apparatus of environmental protection, including Muffle furnace main body, the Muffle furnace main body includes offering steam vent, in addition to exhaust gas processing device at the top of heater and the heating furnace above heater, heating furnace.The exhaust gas processing device includes vertically-mounted heat sink and absorbent charcoal adsorber, the lower end of heat sink is connected by appendix with steam vent, its top is connected by the top of pipe fitting and absorbent charcoal adsorber, and the lower end of absorbent charcoal adsorber is connected with blast pipe;One control valve is installed on appendix.The present invention is improved in the Muffle furnace apparatus of existing structure, pass through the exhaust gas processing device of setting, purified treatment is carried out to pernicious gases such as the SO2 and NOx that are produced in high-temperature calcination process, environment is purified, pernicious gas is reduced to environment luxuriantly, simple in construction, environmental protection, is beneficial to promote.

Description

A kind of Muffle furnace apparatus of environmental protection
Technical field
The present invention relates to a kind of experimental instrument and equipment, and in particular to a kind of Muffle furnace apparatus of environmental protection.
Background technology
Muffle furnace is English Muffle furnace translated next, is a kind of general firing equipment, according to outward appearance shape Shape can be divided into batch-type furnace, tube furnace, crucible furnace.Muffle furnace is as a kind of general firing equipment in industry, medicine, chemical analysis All it is widely applied to Deng field.For example when preparing catalyst in laboratory, typically catalyst is calcined using Muffle furnace. In catalyst roasting process, due to containing a large amount of inorganic salts and water in catalyst activity component, and inorganic salts are in roasting process meeting Discharge the pernicious gases such as S02, NOx.The Muffle furnace of traditional structure, particularly applies the Muffle furnace on laboratory due to no phase The vent gas treatment structure answered.Steam vent usually is set at the top of Muffle furnace or other positions, directly roasting process is discharged The noxious gas emissions such as S02, the NOx gone out are into environment.On the one hand the air in laboratory can be polluted, when people be chronically at it is this When carrying out scientific experiment under environment, it will threaten user's healthy;On the other hand environment is polluted.
The need for production and application, the Muffle furnace of various structures, such as Application No. are occurred in that in the market 200920299535.8 Chinese invention patent discloses the Muffle furnace that a kind of laboratory is used, including Muffle furnace body, Muffle The top of furnace body is provided with fume extractor;Described fume extractor is made up of enclosure and smoke discharging pipe, smoke discharging pipe one end It is connected with enclosure, the other end stretches out outdoor, and enclosure is suspended on the upper end of Muffle furnace body fire door.The Muffle of this kind of structure Stove, organic matter heat can be decomposed to produce after substantial amounts of smog is collected by enclosure and quickly discharged by smoke discharging pipe again, have Beneficial to improve laboratory in environment, while it also avoid because it is full of smoke made a mistake in the laboratory of closing alarm and in The situation of disconnected experiment.But this kind of Muffle furnace, which is only the smog for producing organic matter, extracts laboratory out, not to containing Some pernicious gases are handled, and are cured the symptoms, not the disease, therefore can still pollute atmospheric environment containing pernicious gases such as S02, NOx, no Beneficial to environmental protection.
The content of the invention
For above-mentioned deficiency, the technical problems to be solved by the invention are to provide a kind of environmental protection simple in construction Muffle furnace apparatus, it can handle the pernicious gases such as S02, NOx that inanimate matter roasting process in Muffle furnace is discharged.
To achieve the above object, the present invention is achieved through the following technical solutions:
A kind of Muffle furnace apparatus of environmental protection, including Muffle furnace main body, the Muffle furnace main body include heater and Guidance panel, the heating furnace are installed on the heating furnace above heater, the housing of the heater Top offer steam vent and key switch door, in addition to exhaust gas processing device, institute be installed in the sidepiece of heating furnace Exhaust gas processing device is stated including vertically-mounted heat sink and absorbent charcoal adsorber, the lower end of the heat sink passes through defeated Tracheae is connected with steam vent, its top is connected by the top of pipe fitting and absorbent charcoal adsorber, under absorbent charcoal adsorber End is connected with blast pipe;One control valve is installed on appendix.
In such scheme, for further filtering noxious gas, it can be provided with the lower end of absorbent charcoal adsorber with holes Sieve plate.
It is the structure of predigested running device and cost-effective in such scheme, the absorbent charcoal adsorber includes two The hollow housing of end opening, the inside of the hollow housing is provided with activated carbon adsorption bed, and is connected in the side of hollow housing There is the device for being filled with ammonia.
In such scheme, the heat sink is specifically as follows the internal casing that the aqueous solution is housed.
In such scheme, to be further ensured that security that Muffle furnace is used, it can pacify on the housing of the heater Equipped with a leakage switch;While the heat insulation effect in order to improve Muffle furnace, the heating furnace is excellent from milk high temperature, heat insulation effect Good light aluminum oxide ceramic fibre burner hearth.
The present invention beneficial aspects be:
The present invention is improved in the Muffle furnace apparatus of existing structure, and by the exhaust gas processing device of setting, high temperature is roasted The pernicious gases such as the SO2 and NOx that are produced during burning carry out purified treatment, have purified environment, have reduced pernicious gas to environment Luxuriantly, simple in construction, environmental protection, is beneficial to promote.
Brief description of the drawings
Fig. 1 is a kind of structural representation of this Muffle furnace apparatus.
In figure marked as:1st, steam vent, 2, key switch door, 3, guidance panel, 4, leakage switch, 5, heater, 6th, appendix, 7, control valve, 8, heat sink, 9, absorbent charcoal adsorber, 10, slotted plate, 11, blast pipe, 12, heating furnace Thorax.
Embodiment
As shown in figure 1, a kind of Muffle furnace apparatus of environmental protection, including Muffle furnace main body, the Muffle furnace main body includes Heater 5 and the heating furnace 12 installed in the top of heater 5.Operating surface is installed on the housing of the heater 5 Plate 3, the top of the heating furnace 12 offers steam vent 1 and is provided with key switch door 2 in the sidepiece of heating furnace 12. The Muffle furnace apparatus also includes exhaust gas processing device, and the exhaust gas processing device is including vertically-mounted heat sink 8 and lives Property charcoal adsorbent equipment 9.In the present embodiment, a leakage switch 4, and the heating are installed on the housing of the heater 5 Burner hearth 12 selects light aluminum oxide ceramic fibre burner hearth.
In the present embodiment, the heat sink 8 is specially the internal casing that the aqueous solution is housed.The lower end of heat sink 8 leads to Cross that appendix 6 is connected with steam vent 1, its top is connected by pipe fitting with the top of absorbent charcoal adsorber 9.The activated carbon is inhaled The lower end of adsorption device 9 is connected with blast pipe 11, for further filtration, purification pernicious gas, under absorbent charcoal adsorber 9 End is provided with slotted plate 10.In order to control gas to enter the flow of heat sink 8, a control valve is installed on appendix 6 7。
In the present embodiment, the absorbent charcoal adsorber 9 includes the hollow housing of both ends open, the hollow housing it is interior Portion is provided with activated carbon adsorption bed, and is connected with the device for being filled with ammonia in the side of hollow housing.
In the use of the present invention, first, switching on power, the temperature control on inspection operation panel 3 after earth leakage circuit-breaker is opened Display is then shut off earth leakage circuit-breaker whether in the range of 25-30 DEG C of room temperature;Then key switch door 2, inspection are opened Look into whether heating furnace 12 has the sample not taken out or catalyst roasting debris, steam vent 1, and and gas transmission are opened in inspection after finishing Pipe 6 is connected, and opens control valve 7, and be filled with into activated carbon adsorption bed ammonia, you can added into heating furnace 12 it is to be heated/ The material of burning, Muffle furnace main body is started working.The tail gas that the substance release of heating/roasting goes out in Muffle furnace main body is described The process of exhaust gas processing device is as follows:
1) tail gas out enters heat sink 8 from steam vent 1 and carried out after cooling processing, subsequently enters activated carbon adsorption bed In, the SO2 wherein in tail gas is first by the physisorption of activated carbon, and in the presence of O2 and H2O, SO2 further by Catalysis, occurs to generate H2O4 and NH4SHSO4 after oxidation reaction, and be stored in the micropore of activated carbon;And NOx is in NH3 condition Under, after the catalytic action of activated carbon surface, occur redox reaction generation N2.That is the change of the generation of activated carbon adsorption bed Learn reaction as follows:
SO2+2H2O+O2 → H2SO4,
H2SO4+NH3 → NH4HSO4,
4NO+4NH3+O2→4N2+6H2O。
2) tail gas after exhaust gas processing device, SO2 and NOx gases clearance can reach 95% and 90% respectively;And And after activated carbon adsorption bed is reaching saturation absorption, be sent in regenerating unit and carry out heating desorption, activated carbon is not failing On the premise of it is reusable.
SO2 and NOx content are relatively low in the tail gas gone out due to Muffle furnace body bleeder, and the floor height of activated carbon adsorption bed can be set Put between 92-100mm, to avoid the replacement repeatedly of activated carbon, activated carbon adsorption bed is except by SO2 in tail gas and NOx and entering Row purification is outer, the noxious material such as volatile organic matter in tail gas can also be removed, while accessory substance H2SO4 and NH4HSO4 are entered Row is recycled.
Explanation embodiments of the present invention are these are only, are not intended to limit the invention, for those skilled in the art For, within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc. should be included in this hair Within bright protection domain.

Claims (5)

1. a kind of Muffle furnace apparatus of environmental protection, including Muffle furnace main body, the Muffle furnace main body include heater (5) and Guidance panel (3) is installed on heating furnace (12) above heater (5), the housing of the heater (5), Steam vent (1) is offered at the top of the heating furnace (12) and key switch door is installed in the sidepiece of heating furnace (12) (2), it is characterised in that:Also include exhaust gas processing device, the exhaust gas processing device include vertically-mounted heat sink (8) and Absorbent charcoal adsorber (9), the lower end of the heat sink (8) is connected by appendix (6) with steam vent (1), its top leads to The top that pipe fitting is crossed with absorbent charcoal adsorber (9) is connected, and the lower end of absorbent charcoal adsorber (9) is connected with blast pipe (11); One control valve (7) is installed on appendix (6).
2. the Muffle furnace apparatus of environmental protection according to claim 1, it is characterised in that:In absorbent charcoal adsorber (9) Lower end slotted plate (10) is installed.
3. the Muffle furnace apparatus of environmental protection according to claim 1 or 2, it is characterised in that:The charcoal absorption dress Putting (9) includes the hollow housing of both ends open, and the inside of the hollow housing is provided with activated carbon adsorption bed, and in hollow housing Side be connected with device for being filled with ammonia.
4. the Muffle furnace apparatus of environmental protection according to claim 3, it is characterised in that:The heat sink (8) is interior Portion is equipped with the casing of the aqueous solution.
5. the Muffle furnace apparatus of environmental protection according to claim 1, it is characterised in that:The shell of the heater (5) One leakage switch (4) is installed, the heating furnace (12) is light aluminum oxide ceramic fibre burner hearth on body.
CN201710786782.XA 2017-09-04 2017-09-04 A kind of Muffle furnace apparatus of environmental protection Pending CN107328231A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710786782.XA CN107328231A (en) 2017-09-04 2017-09-04 A kind of Muffle furnace apparatus of environmental protection

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710786782.XA CN107328231A (en) 2017-09-04 2017-09-04 A kind of Muffle furnace apparatus of environmental protection

Publications (1)

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CN107328231A true CN107328231A (en) 2017-11-07

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111298644A (en) * 2020-03-11 2020-06-19 安徽艾可蓝环保股份有限公司 DPF high-temperature regeneration furnace and DPF high-temperature regeneration furnace exhaust purification method
CN114539038A (en) * 2022-03-17 2022-05-27 南京嘉言新材料科技有限公司 Preparation method of propylene glycol monobutyl ether

Citations (14)

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RU2129692C1 (en) * 1996-05-16 1999-04-27 Открытое акционерное общество "Боровичский комбинат огнеупоров" Rotary muffle furnace
CN201561635U (en) * 2009-12-22 2010-08-25 上海悦胜芜湖药业有限公司 Muffle furnace
CN102580455A (en) * 2011-12-29 2012-07-18 山西太钢不锈钢股份有限公司 Sintering smoke treatment system and sintering smoke treatment method
CN203043829U (en) * 2013-02-25 2013-07-10 王荣成 Flue gas desulfurization-denitration tower based on active carbon
CN103861439A (en) * 2014-03-25 2014-06-18 云南亚太环境工程设计研究有限公司 Method for simultaneously desulfurizing, denitrating and purifying flue gas
CN103868078A (en) * 2014-02-14 2014-06-18 国家电网公司 Waste liquor treatment device and waste liquor treatment process
CN203797670U (en) * 2014-02-14 2014-08-27 国家电网公司 Liquid waste treatment device
CN204043376U (en) * 2014-06-26 2014-12-24 北京盛昌百年石油科技有限公司 A kind of Muffle furnace
CN105126617A (en) * 2015-09-24 2015-12-09 常州市长宇实用气体有限公司 Detachable flue gas denitrification device
CN105688622A (en) * 2014-11-28 2016-06-22 中冶长天国际工程有限责任公司 A flue gas desulphurization denitration method adopting two adsorption columns in series connection and a device therefor
CN205482315U (en) * 2016-01-20 2016-08-17 广西大学 Muffle furnace
CN206240258U (en) * 2016-06-30 2017-06-13 中冶长天国际工程有限责任公司 Prevent the flue gas desulfurization and denitrification device of corrosion
CN206266666U (en) * 2016-12-26 2017-06-20 深圳市超卓实业有限公司 A kind of automobile die stress tempering treatment Muffle furnace
CN207299897U (en) * 2017-09-04 2018-05-01 钦州学院 A kind of environmentally protective Muffle furnace apparatus

Patent Citations (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2129692C1 (en) * 1996-05-16 1999-04-27 Открытое акционерное общество "Боровичский комбинат огнеупоров" Rotary muffle furnace
CN201561635U (en) * 2009-12-22 2010-08-25 上海悦胜芜湖药业有限公司 Muffle furnace
CN102580455A (en) * 2011-12-29 2012-07-18 山西太钢不锈钢股份有限公司 Sintering smoke treatment system and sintering smoke treatment method
CN203043829U (en) * 2013-02-25 2013-07-10 王荣成 Flue gas desulfurization-denitration tower based on active carbon
CN203797670U (en) * 2014-02-14 2014-08-27 国家电网公司 Liquid waste treatment device
CN103868078A (en) * 2014-02-14 2014-06-18 国家电网公司 Waste liquor treatment device and waste liquor treatment process
CN103861439A (en) * 2014-03-25 2014-06-18 云南亚太环境工程设计研究有限公司 Method for simultaneously desulfurizing, denitrating and purifying flue gas
CN204043376U (en) * 2014-06-26 2014-12-24 北京盛昌百年石油科技有限公司 A kind of Muffle furnace
CN105688622A (en) * 2014-11-28 2016-06-22 中冶长天国际工程有限责任公司 A flue gas desulphurization denitration method adopting two adsorption columns in series connection and a device therefor
CN105126617A (en) * 2015-09-24 2015-12-09 常州市长宇实用气体有限公司 Detachable flue gas denitrification device
CN205482315U (en) * 2016-01-20 2016-08-17 广西大学 Muffle furnace
CN206240258U (en) * 2016-06-30 2017-06-13 中冶长天国际工程有限责任公司 Prevent the flue gas desulfurization and denitrification device of corrosion
CN206266666U (en) * 2016-12-26 2017-06-20 深圳市超卓实业有限公司 A kind of automobile die stress tempering treatment Muffle furnace
CN207299897U (en) * 2017-09-04 2018-05-01 钦州学院 A kind of environmentally protective Muffle furnace apparatus

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111298644A (en) * 2020-03-11 2020-06-19 安徽艾可蓝环保股份有限公司 DPF high-temperature regeneration furnace and DPF high-temperature regeneration furnace exhaust purification method
CN114539038A (en) * 2022-03-17 2022-05-27 南京嘉言新材料科技有限公司 Preparation method of propylene glycol monobutyl ether

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Application publication date: 20171107

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